Acta Crystallographica Section C

Crystal Structure Communications

Volume 52, Part 2 (February 1996)

Cover illustration: A 5,18:9,14-Di-o-benzeno-6,17:7,16:8,15-trimethanobenzo\[1'',2'':3,4;4'',5'':3',4'\]dicyclobuta\[1,2-b:1',2'-b'\]dianthracene Derivative, see Parvez pages 444-447. Displacement ellipsoids are plotted at the 50% probability level.

• inorganic compounds
• metal-organic compounds
• organic compounds
• addenda and errata

inorganic compounds

Acta Cryst. (1996). C52, 279-281    [ doi:10.1107/S0108270195011723 ]

Dirubidium Tetrachlorodioxouranium(VI)-Water (1:2)

C. E. Anson, O. Al-Jowder, U. A. Jayasooriya and A. K. Powell

Synopsis: Rb₂[UO₂Cl₄].2H₂O crystallizes in space group P1; the anion approximates to D_4h (4/mmm) symmetry, with a U-O distance of 1.751(9)Å and U-Cl distances of 2.644(3) and 2.650(4)Å. The compound is confirmed to be the dihydrate; the degree of hydration had been controversial.

Formula: Rb₂[UO₂Cl₄].2H₂O

Acta Cryst. (1996). C52, 281-283    [ doi:10.1107/S0108270195013205 ]

Hexachlorotetra-₃-chloro-tetra-₃-telluro-octohexarhenium(III)

Y. V. Mironov, J. A. Cody and J. A. Ibers

Synopsis: The structure of Re₆Te₄Cl₁₀ contains two independent Re₆ octahedral clusters, each with a crystallographic center of symmetry. The Re atoms are coordinated by four ₃-Te atoms and four ₃-Cl atoms that are equally distributed over the faces of the metal polyhedron; the remaining six Cl atoms are terminal ligands coordinated to the apices of the Re₆ octahedron.

Formula: Re₆Te₄Cl₁₀

Acta Cryst. (1996). C52, 283-284    [ doi:10.1107/S0108270195012509 ]

K₂Mn(VO₃)₄, a New Three-Dimensional Potassium Manganese(II) Polyvanadate

J.-H. Liao, C. Sigala, D. Guyomard and Y. Piffard

Synopsis: The structure of K₂Mn(VO₃)₄ is composed of MnO₆ octahedra and VO₄ tetrahedra. Parallel zigzag polyvanadate (VO₃)_n^n- chains of corner-sharing VO₄ tetrahedra are cross-linked by seperate MnO₆ octahedra to form a three-dimensional framework, the cavities of which are occupied by K⁺ ions.

Formula: K₂Mn(VO₃)₄

Acta Cryst. (1996). C52, 284-286    [ doi:10.1107/S0108270195010559 ]

K₂Mn₃(OH)₂(VO₄)₂, a New Two-Dimensional Potassium Manganese(II) Hydroxyvanadate

J.-H. Liao, D. Guyomard, Y. Piffard and M. Tournoux

Synopsis: The structure of K₂Mn₃(OH)₂(VO₄)₂ consists of [Mn₃(OH)₂(VO₄)₂]_n^2n- layers built up from CdI₂-like planes of MnO₄-(OH)₂ octahedra with 1/4 Mn vacancies, to which VO₄ tetrahedra are linked on both sides via three vertices; the fourth vertex points into the interlayer space where the K⁺ ions are situated.

Formula: K₂Mn₃(OH)₂(VO₄)₂

Acta Cryst. (1996). C52, 286-288    [ doi:10.1107/S0108270195012625 ]

Tin(II) Oxyhydroxide by X-ray Powder Diffraction

I. Abrahams, S. M. Grimes, S. R. Johnston and J. C. Knowles

Synopsis: The Sn₆O₄(OH)₄ clusters which form the structure pack in a pseudo-body-centered fashion. The Sn atoms have distorted tetragonal pyramidal coordination geometry; each Sn atom is coordinated to two bridging O atoms and two bridging hydroxy O atoms.

Formula: Sn₆O₄(OH)₄

Acta Cryst. (1996). C52, 288-290    [ doi:10.1107/S0108270195012042 ]

Sodium Hexanitroruthenate(II) Monohydrate

S. A. Gromilov, V. I. Alekseev, V. A. Emelyanov and I. A. Baidina

Synopsis: The structure of sodium hexanitroruthenate(II) monohydrate is composed of [Ru(NO₂)₆]^4- complex anions, Na⁺ cations and water molecules. The Ru atoms have nearly ideal octahedral coordination geometry.

Formula: Na₄[Ru(NO₂)₆].H₂O

Acta Cryst. (1996). C52, 290-291    [ doi:10.1107/S0108270195012510 ]

Diphosphorus Tetraiodide at 120K

Z. Zák and M. Cerník

Synopsis: The structure of P₂I₄ was determined at 120K. It is composed of isolated P₂I₄ molecules, each of which lies on a crystallographic symmetry centre. There are no apparent intermolecular contacts between the molecules.

Formula: P₂I₄

metal-organic compounds

Acta Cryst. (1996). C52, 292-294    [ doi:10.1107/S0108270195001454 ]

[PPN]₂[Cr₂(CO)₁₀], a Salt of the Dimeric Cr^1- Carbonyl Complex Without a Coordinating Counterion

I. Lee, S. J. Geib and N. J. Cooper

Formula: [(C₁₈H₁₅P)₂N]₂[Cr₂(CO)₁₀]

Acta Cryst. (1996). C52, 295-297    [ doi:10.1107/S0108270195007852 ]

The PF₆^-/BF₄^- Mixed Salt of the Cluster Cation [Pt₃(₃-AuPPh₃)(-dppm)₃]⁺, dppm = Ph₂PCH₂PPh₂

K. W. Muir, L. Manojlovic-Muir and J. Fullard

Formula: [AuPt₃(C₂₅H₂₂P₂)₃(C₁₈H₁₅P)](BF₄)_0.25(PF₆)_0.75

Acta Cryst. (1996). C52, 297-300    [ doi:10.1107/S0108270195009243 ]

Dichloro(ethylenediaminetetraacetic acid-N,N')platinum(II)-Water (1/6)

J. T. Whalen, S.-C. Chang and R. E. Norman

Formula: [PtCl₂(C₁₀H₁₆N₂O₈)].6H₂O

Acta Cryst. (1996). C52, 300-302    [ doi:10.1107/S0108270195003507 ]

Chlorohydrido[2(1H)-pyridonato-N,O]bis[tris(1-methylethyl)phosphine]iridium(III)

D. B. Grotjahn, H. C. Lo and T. L. Groy

Formula: [IrCl(H)(C₅H₄NO)(C₉H₂₁P)₂]

Acta Cryst. (1996). C52, 302-305    [ doi:10.1107/S0108270195006068 ]

Bis(methanol-O)(2,3,7,8,12,13,17,18-octaethylporphyrinato-N,N',N'',N''')iron(III) Perchlorate Bis(methanol) Solvate, [Fe^III(oep)(HOCH₃)₂](ClO₄).2CH₃OH

M. O. Senge

Formula: [Fe(C₃₆H₄₄N₄)(CH₄O)₂](ClO₄).2CH₄O

Acta Cryst. (1996). C52, 305-307    [ doi:10.1107/S0108270195008183 ]

Bis(1,3,5-triaza-7-phosphaadamantane-P)gold(I) Chloride

Z. Assefa, R. J. Staples and J. P. Fackler Jnr

Formula: [Au(C₆H₁₂N₃P)₂]Cl

Acta Cryst. (1996). C52, 307-309    [ doi:10.1107/S0108270195008304 ]

cis-Dipyridine Complex of Bis(-nitroacetophenonato)manganese(II)

S. Hicke, T. E. Mueller and L. R. Falvello

Formula: [Mn(C₈H₆NO₃)₂(C₅H₅N)₂]

Acta Cryst. (1996). C52, 309-312    [ doi:10.1107/S0108270195008870 ]

[Cr{tren(impy)₃}](ClO₄)₃, where tren(impy)₃ = N[CH₂CH₂N= C(H)(py)]₃

G. A. McLachlan, G. D. Fallon and L. Spiccia

Formula: [Cr(C₂₄H₂₇N₇)](ClO₄)₃

Acta Cryst. (1996). C52, 312-315    [ doi:10.1107/S0108270195010754 ]

A 2:1 Mixture of Tetrabutylammonium Bis(4,5-dimercapto-1,3-dithiole-2-thionato)nickelate(II) and its 2-Selenone Analogue

H.-K. Fun, K. Sivakumar, J.-L. Zuo, T.-M. Yao and X.-Z. You

Formula: (C₁₆H₃₆N)₂[Ni(C₃S_4.67Se_0.33)₂]

Acta Cryst. (1996). C52, 315-317    [ doi:10.1107/S0108270195007475 ]

Bis(dimethylglyoximato-N,N')(isopropyl)(triphenylphosphine)rhodium(III)

M. Dunaj-Jurco, D. Miklos, I. Potocnák, M. Ludwig and D. Steinborn

Formula: [Rh(C₄H₇N₂O₂)₂(C₃H₇)(C₁₈H₁₅P)]

Acta Cryst. (1996). C52, 317-319    [ doi:10.1107/S0108270195009437 ]

Tetraethylammonium Bis(isothiocyanato)triphenylstannate

P. J. Cox and J. L. Wardell

Formula: (C₈H₂₀N)[Sn(C₆H₅)₃(NCS)₂]

Acta Cryst. (1996). C52, 319-321    [ doi:10.1107/S0108270195010067 ]

Chloro(ethylenediamine)(6-phenylimidazo[2,1-b]thiazole-N⁷)platinum(II) Nitrate

G. M. Arvanitis, A. E. Griffitts, S. P. Baffic and D. M. Ho

Formula: [PtCl(C₂H₈N₂)(C₁₁H₈N₂S)]NO₃

Acta Cryst. (1996). C52, 321-325    [ doi:10.1107/S0108270195010717 ]

Dipyridiniomethane cis- and trans-Difluorotetrachloroosmate(IV), cis- and trans-[(C₅H₅N)₂CH₂][OsCl₄F₂]

C. Bruhn and W. Preetz

Formula: Two isomers of (C₁₁H₁₂N₂)[OsCl₄F₂]

Acta Cryst. (1996). C52, 325-328    [ doi:10.1107/S0108270195009152 ]

Sodium 3,7,12-Trihydroxy-5-cholan-24-oate Ethanolate (Sodium Cholate Ethanolate)

M. C. Wahle, J. G. Stowell and S. R. Byrn

Formula: Na⁺.C₂₄H₃₉O₅^-.C₂H₆O

Acta Cryst. (1996). C52, 328-330    [ doi:10.1107/S0108270195011061 ]

trans-Dichlorobis[tris(pentafluorophenyl)phosphane]palladium(II)

B. Bertsch-Frank and W. Frank

Formula: [PdCl₂(C₁₈F₁₅P)₂]

Acta Cryst. (1996). C52, 330-333    [ doi:10.1107/S0108270195011073 ]

Tetraphenylphosphonium Pentachlorostannat, PPh₄[SnCl₅], und Tetraphenylphosphonium Pentachlorostannat Monohydrat, PPh₄[SnCl₅.H₂O]

U. Müller und J. Frenzen Siekmann

Formula: (C₂₄H₂₀P)[SnCl₅] und (C₂₄H₂₀P)[SnCl₅.H₂O]

Acta Cryst. (1996). C52, 333-336    [ doi:10.1107/S010827019500922X ]

(±)-cis-Dichloro[P-(isopropylamino)dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepine](triethylphosphine)platinum(II) Dichloromethane Solvate

M. Parvez, R. P. K. Babu and S. S. Krishnamurthy

Formula: [PtCl₂(C₂₃H₂₀NO₂P)(C₆H₁₅P)].CH₂Cl₂

Acta Cryst. (1996). C52, 336-338    [ doi:10.1107/S0108270195008729 ]

(⁴-Cycloocta-1,5-diene)(2-pyridinethiolato N-oxide-O,S)iridium(I)

M. Theron, W. Purcell and S. S. Basson

Formula: [Ir(C₅H₄NOS)(C₈H₁₂)]

Acta Cryst. (1996). C52, 338-340    [ doi:10.1107/S0108270195010419 ]

Tetrasodium P¹,P⁴-Bis(5'-adenosyl)tetraphosphate Dodecahydrate

D. Watanabe, M. Ishikawa, M. Yamasaki, M. Ozaki, T. Katayama and H. Nakajima

Formula: 4Na⁺.C₂₀H₂₄N₁₀O₁₉P₄^-.12H₂O

Acta Cryst. (1996). C52, 340-342    [ doi:10.1107/S0108270195009668 ]

Trimethylammonium Trichlorostannate(II)

J. Halfpenny

Formula: [NH(CH₃)₃][SnCl₃]

Acta Cryst. (1996). C52, 342-347    [ doi:10.1107/S0108270195003246 ]

The Role of C-HO Bonds in Stabilizing 3-Furancarboxylic Acid and its Complexes with Calcium and Strontium

B. Paluchowska, J. K. Maurin and J. Leciejewicz

Formula: C₅H₄O₃, [Ca(C₅H₃O₃)(H₂O)₃](C₅H₃O₃)and [Sr(C₅H₃O₃)(H₂O)₃](C₅H₃O₃)

Acta Cryst. (1996). C52, 347-351    [ doi:10.1107/S0108270195009553 ]

Carboxylate and Furan-Ring Oxygen Bonded to Calcium in Polymeric Calcium Furoate

B. Paluchowska, J. K. Maurin and J. Leciejewicz

Formula: Ca²⁺.2C₅H₃O₃^-

Acta Cryst. (1996). C52, 351-354    [ doi:10.1107/S0108270195007785 ]

Tetrakis(o-benzoylbenzoato-O,O')lead(IV) Dichloromethane Solvate

K. Prout, D. Vaughan-Lee, M. G. Moloney and S. C. Prottey

Formula: [Pb(C₁₄H₉O₃)₄].CH₂Cl₂

Acta Cryst. (1996). C52, 354-356    [ doi:10.1107/S0108270195009498 ]

A 1:1 Adduct of Aquachlorotriphenyltin with 3,4,7,8-Tetramethyl-1,10-phenanthroline

S. W. Ng

Formula: [SnCl(C₆H₅)₃(H₂O)].C₁₆H₁₆N₂

Acta Cryst. (1996). C52, 356-358    [ doi:10.1107/S0108270195009577 ]

Hexacarbonyl(^5:1-2-cyclopentadienediylethyl)(-^1:3-1-ethoxy-2-propenylidene)molybdenumtungsten

W. Frank, C. G. Kreiter and G. J. Reiß

Formula: [MoW(C₇H₈)(C₅H₈O)(CO)₆]

Acta Cryst. (1996). C52, 358-360    [ doi:10.1107/S0108270195008195 ]

Bis(N¹-isopropyl-2-methylpropane-1,2-diamine)diisothiocyanatocadmium(II)

C. Pariya, N. R. Chaudhuri, S. Seth and A. Das

Formula: [Cd(NCS)₂(C₇H₁₈N₂)₂]

Acta Cryst. (1996). C52, 361-363    [ doi:10.1107/S0108270195009371 ]

Chloro(5,10,15,20-tetraphenylporphyrinato)manganese(III) with 4/m Symmetry

B. Cheng and W. R. Scheidt

Formula: [Mn(C₄₄H₂₈N₄)Cl]

organic compounds

Acta Cryst. (1996). C52, 364-365    [ doi:10.1107/S0108270195010845 ]

Coumarin 106, C₁₈H₁₉NO₂

T. Honda, I. Fujii, N. Hirayama, N. Aoyama and A. Miike

Formula: C₁₈H₁₉NO₂

Acta Cryst. (1996). C52, 366-368    [ doi:10.1107/S0108270195011589 ]

4-Aza-9(10H)-acridone

G. R. Clark and C. J. Squire

Formula: C₁₂H₈N₂O

Acta Cryst. (1996). C52, 368-369    [ doi:10.1107/S0108270195010882 ]

4a-Phenylperhydro-1,4-dioxacyclopropa[cd]pentalene

M. G. Banwell, D. C. R. Hockless and J. M. Walter

Formula: C₁₂H₁₂O₂

Acta Cryst. (1996). C52, 370-372    [ doi:10.1107/S0108270195010869 ]

An ABC-ring Analogue of Paclitaxel (Taxol^TM)

M. G. Banwell, D. C. R. Hockless and S. C. Peters

Formula: C₂₀H₂₂BrNO₅

Acta Cryst. (1996). C52, 372-375    [ doi:10.1107/S0108270195013035 ]

5-Amino-8-methyl-1,2-dihydrothieno(and furo)[2,3-h][1,6]naphthyridines

R. Kingsford-Adaboh, S. Kashino, K. Sasaki, A. S. S. Rouf and T. Hirota

Formula: C₁₁H₁₁N₃S and C₁₁H₁₁N₃O

Acta Cryst. (1996). C52, 375-377    [ doi:10.1107/S0108270195010390 ]

2-Bromoacetoxybenzoic Acid, a Brominated Aspirin Analog

P. J. Loll, R. M. Garavito, C. J. Carrell and H. L. Carrell

Formula: C₉H₇BrO₄

Acta Cryst. (1996). C52, 377-378    [ doi:10.1107/S0108270195010456 ]

Tetraphenylphosphonium Triiodide

M. Parvez, M. Wang and P. M. Boorman

Formula: C₂₄H₂₀P⁺.I₃^-

Acta Cryst. (1996). C52, 379-381    [ doi:10.1107/S0108270195012327 ]

2,3,10,11-Tetraphenyl-1,4,9,12-tetraoxadispiro[4.2.4.2]tetradeca-6,13-diene

D. E. Hibbs, M. B. Hursthouse, K. M. A. Malik, R. S. Ward, A. Pelter and L. Aalberg

Formula: C₃₄H₂₈O₄

Acta Cryst. (1996). C52, 381-383    [ doi:10.1107/S0108270195013618 ]

2,3,4,5-Tetra-O-acetyl-1,6-di-O-(triphenylmethyl)-D-mannitol

M. A. Shalaby, F. R. Fronczek, R. J. Voll, S. F. Watkins and E. S. Younathan

Formula: C₅₂H₅₀O₁₀

Acta Cryst. (1996). C52, 383-387    [ doi:10.1107/S0108270195012248 ]

Cyclo(L-alanyl-L-seryl).H₂O and Cyclo(glycyl-L-seryl)

D. C. Swenson, S. M. Habermann and K. P. Murphy

Formula: C₆H₁₀N₂O₃.H₂O and C₅H₈N₂O₃

Acta Cryst. (1996). C52, 387-390    [ doi:10.1107/S0108270195012236 ]

The Ribonucleotide Reductase R1 Inhibitor N-Acetyl-N,O-di(propylcarbamoyl)hydroxylamine, an Analogue of Caracemide

B. B. Nielsen, K. Frydenvang and I. K. Larsen

Formula: C₁₀H₁₉N₃O₄

Acta Cryst. (1996). C52, 391-393    [ doi:10.1107/S0108270195011942 ]

8-Chloro-5-(4-methylpiperazin-1-yl)-11H-pyrido[2,3-b][1,5]benzodiazepine

L. Dupont, J.-F. Liégeois, F. Rogister and J. Delarge

Formula: C₁₇H₁₈ClN₅

Acta Cryst. (1996). C52, 393-395    [ doi:10.1107/S0108270195011954 ]

Absolute Configuration of (R)-1-Phenylethylammonium (S)-2-(6-Methoxy-2-naphthyl)propionate

L. Dupont, B. Pirotte, P. De Tullio and J. Delarge

Formula: C₈H₁₂N⁺.C₁₄H₁₃O₃^-

Acta Cryst. (1996). C52, 395-397    [ doi:10.1107/S010827019501239X ]

An Orange Form of Coumarin 314

T. Honda, I. Fujii, N. Hirayama, N. Aoyama and A. Miike

Formula: C₁₈H₁₉NO₄

Acta Cryst. (1996). C52, 397-400    [ doi:10.1107/S0108270195011929 ]

1,1'-Diphenyl-1,1'-bicyclopropyl and 1,1'-Diphenyl-1,1'-bicyclobutyl

Y.-L. Lam, L.-L. Koh and H.-H. Huang

Formula: C₁₈H₁₈ and C₂₀H₂₂

Acta Cryst. (1996). C52, 400-403    [ doi:10.1107/S0108270195012832 ]

Bis(methylthio)ethylenedithiotetrathiafulvalene

B. Zhang, Y.-L. Li, H.-X. Han, J.-K. Yang, D.-B. Zhu and Y.-S. Maruyama

Formula: C₁₀H₁₀S₈

Acta Cryst. (1996). C52, 403-405    [ doi:10.1107/S0108270195011966 ]

A Key Intermediate in the Synthesis of Pentamidine: 4,4'-[1,5-Pentanediylbis(oxy)]bisbenzonitrile

K. Ravikumar, K. C. Mohan, S. Roy and A. K. Singh

Formula: C₁₉H₁₈N₂O₂

Acta Cryst. (1996). C52, 405-407    [ doi:10.1107/S0108270195011334 ]

7-Hydroxy-7-(3-propargyl)-3-methylspiro[5.5]undec-2-en-1-one

S. Lakshmi, K. Subramanian, G. Koellner, Th. Steiner and K. Rajagopalan

Formula: C₁₅H₂₀O₂

Acta Cryst. (1996). C52, 407-409    [ doi:10.1107/S0108270195013060 ]

The -Pyridyl Nucleoside Analogue 2-Bromo-5-(2-deoxy--D-ribofuranosyl)pyridine

S. Neidle, D. C. Capaldi, J. V. Bernadette and C. B. Reese

Formula: C₁₀H₁₂BrNO₃

Acta Cryst. (1996). C52, 409-411    [ doi:10.1107/S0108270195013217 ]

2-Phenylquinoline-4-carboxylic Acid

A. C. Blackburn, A. J. Dobson and R. E. Gerkin

Formula: C₁₆H₁₁NO₂

Acta Cryst. (1996). C52, 411-414    [ doi:10.1107/S0108270195010778 ]

Unsymmetrically Substituted Thioureas. 1,1-Dimethyl-3-o-tolylthiourea and 1,1-Diethyl-3-o-tolylthiourea

A. Ramnathan, K. Sivakumar, N. Janarthanan, D. Meerarani, K. Ramadas and H.-K. Fun

Formula: C₁₀H₁₄N₂S and C₁₂H₁₈N₂S

Acta Cryst. (1996). C52, 414-416    [ doi:10.1107/S0108270195012054 ]

-3,4-Dimethyl-2,5-bis(3,4,5-trimethoxyphenyl)tetrahydrofuran

H.-K. Fun, K. Sivakumar, B.-C. Yip, A. H. Othman and I. M. Said

Formula: C₂₄H₃₂O₇

Acta Cryst. (1996). C52, 416-418    [ doi:10.1107/S0108270195012339 ]

Methyl 3-O-Benzoyl-4,6-O-benzylidene-2-O-trifluoromethylsulfonyl--D-mannopyranoside

J. C. Barnes, J. S. Brimacombe and A. K. M. S. Kabir

Formula: C₂₂H₂₁F₃O₉S

Acta Cryst. (1996). C52, 418-420    [ doi:10.1107/S010827019501448X ]

6-Amino-4-methoxy-2-methylthiopyrimidine

J. N. Low, G. Ferguson, M. L. Godino, J. Cobo, R. Lopez, M. Melguizo, M. Nogueras and A. Sanchez

Formula: C₆H₉N₃OS

Acta Cryst. (1996). C52, 420-423    [ doi:10.1107/S0108270195013990 ]

Tris(4-methoxyphenyl)methanol

G. Ferguson, C. Glidewell and I. L. J. Patterson

Formula: C₂₂H₂₂O₄

Acta Cryst. (1996). C52, 424-429    [ doi:10.1107/S0108270195004902 ]

Bis(diethyldithiocarbamato)(iodo)(4-methoxyphenyl)tellurium(IV), p-MeOC₆H₄Te(Et₂NCS₂)₂I, and its Isomorphous Partially Bromine-Replaced Analogue, p-MeOC₆H₄Te(Et₂NCS₂)₂Br_0.41I_0.59

S. Husebye, S. Kudis and S. V. Lindeman

Formula: C₁₇H₂₇IN₂OS₄Te and C₁₇H₂₇Br_0.41I_0.59N₂OS₄Te

Acta Cryst. (1996). C52, 429-432    [ doi:10.1107/S0108270195004914 ]

Bromobis(dimethyldithiocarbamato)(4-methoxyphenyl)tellurium(IV) Dichloromethane Hemisolvate, p-MeOC₆H₄Te(Me₂NCS₂)₂Br.0.5CH₂Cl₂

S. Husebye, S. Kudis and S. V. Lindeman

Formula: C₁₃H₁₉BrN₂OS₄Te.0.45(CH₂Cl₂)

Acta Cryst. (1996). C52, 432-433    [ doi:10.1107/S010827019500309X ]

Bis(o-phénylènediammonium) cyclo-Tétraphosphate Dihydrate

E. H. Soumhi et T. Jouini

Formula: 2C₆H₁₀N₂²⁺.P₄O₁₂^4-.2H₂O

Acta Cryst. (1996). C52, 434-436    [ doi:10.1107/S0108270195011528 ]

Hexa(para-phénolammonium) cyclo-Hexaphosphate Octahydrate

E. H. Soumhi et T. Jouini

Formula: 6C₆H₈NO⁺.P₆O₁₈^6-.8H₂O

Acta Cryst. (1996). C52, 436-438    [ doi:10.1107/S0108270195012066 ]

Dimethyl 2,2,6,6-Tetramethyl-3,5-dioxo-4-oxaheptanedioate

J. E. Graham, R. A. Bunce and E. M. Holt

Formula: C₁₂H₁₈O₇

Acta Cryst. (1996). C52, 438-441    [ doi:10.1107/S0108270195012078 ]

N-(4-Bromophenyl)-5,6-dichloronicotinamide and 6-Chloro-5-fluoro-N-(3-pyridyl)nicotinamide

J. M. Jethmalani, A. G. Camp, N. G. Soman, J. W. Hawley, F. L. Setliff and E. M. Holt

Formula: C₁₂H₇BrCl₂N₂O and C₁₁H₇ClFN₃O

Acta Cryst. (1996). C52, 441-444    [ doi:10.1107/S0108270195008584 ]

A Chiral Mesogenic Compound

I. Zareba, H. Allouchi, M. Cotrait, C. Destrade and H. T. Nguyen

Formula: C₃₇H₄₄O₅

Acta Cryst. (1996). C52, 444-447    [ doi:10.1107/S0108270195009607 ]

A 5,18:9,14-Di-o-benzeno-6,17:7,16:8,15-trimethanobenzo[1'',2'':3,4;4'',5'':3',4']dicyclobuta[1,2-b:1',2'-b']dianthracene Derivative

M. Parvez

Formula: C₆₃H₅₅Cl₃O₄S.0.5H₂O

Acta Cryst. (1996). C52, 447-449    [ doi:10.1107/S0108270195009206 ]

5-(p-Anisidino)-4-cyano-2,3-dihydro-3-pyrazolone Hemihydrate, C₁₁H₁₀N₄O₂.0.5H₂O

M. V. Capparelli, J. E. Charris and J. N. Domínguez

Formula: C₁₁H₁₀N₄O₂.0.5H₂O

Acta Cryst. (1996). C52, 449-451    [ doi:10.1107/S0108270195009942 ]

4,5-Dicyano-4',5'-ethylenedithiotetrathiafulvalene (CNET): a New Unsymmetrical TTF Derivative

Z. J. Zhong, X.-Z. You and K. Yu

Formula: C₁₀H₄N₂S₆

Acta Cryst. (1996). C52, 451-453    [ doi:10.1107/S0108270195010080 ]

4-Chloro-7-(iodoacetyl)amino-3-methoxyisocoumarin

J. E. Kerrigan, J. C. Powers and D. VanDerveer

Formula: C₁₂H₉ClINO₄

Acta Cryst. (1996). C52, 453-455    [ doi:10.1107/S0108270195012340 ]

Dipyridiniomethane 1-Iodo-closo-decaborate, [(C₅H₅N)₂CH₂][1-IB₁₀H₉]

C. Nachtigal and W. Preetz

Formula: C₁₁H₁₂N₂²⁺.B₁₀H₉I^2-

Acta Cryst. (1996). C52, 455-457    [ doi:10.1107/S0108270195010468 ]

1-(4-Iodobenzoyl)-5-methoxy-2-methyl-3-indoleacetic Acid, an Iodinated Indomethacin Analog

P. J. Loll, R. M. Garavito, C. J. Carrell and H. L. Carrell

Formula: C₁₉H₁₆INO₄

Acta Cryst. (1996). C52, 458-460    [ doi:10.1107/S0108270195011863 ]

trans-(3aR)-1,2,3,3a-Tetrahydro-3a-(methoxymethyl)-5-methyl-7-nitropyrrolo[1,2-a]quinoline-4,4(5H)-dicarbonitrile: Four Independent Molecules in the Unit Cell

E. Kelderman, W. Verboom, J. F. J. Engbersen, D. N. Reinhoudt and S. Harkema

Formula: C₁₇H₁₈N₄O₃

Acta Cryst. (1996). C52, 460-462    [ doi:10.1107/S0108270195010146 ]

Dimethyl(2-{[2,3-di(p-tolyl)-5-methyl-1-indenylidene](p-tolyl)methyl}-5-methoxyphenylmethyl)amine

J. M. Fernández-G, K. Solorzano-Maldonado, K. Panneerselvam, A. Rodríguez-Romero and M. Soriano-García

Formula: C₄₂H₄₁NO

Acta Cryst. (1996). C52, 463-466    [ doi:10.1107/S0108270195011346 ]

Conformational Analysis of (S,S)-Dimethyldiketopyridino-18-crown-6

Z. Böcskei, G. M. Keserü, D. Menyhárd, P. Huszthy, J. S. Bradshaw and R. M. Izatt

Formula: C₁₇H₂₃NO₇

Acta Cryst. (1996). C52, 466-468    [ doi:10.1107/S0108270195011127 ]

1:1 Adduct of Tris(4-hydroxy-3,5-dimethylbenzyl)amine and Hexamethylenetetramine

P. J. de Bruyn, R. W. Gable, A. C. Potter and D. H. Solomon

Formula: C₂₇H₃₃NO₃.C₆H₁₂N₄

Acta Cryst. (1996). C52, 469-470    [ doi:10.1107/S0108270195011796 ]

syn-1,5-Dimethylbicyclo[3.2.1]oct-8-yl N-Phenylcarbamate

S. Pietz, G. Haufe, R. Fröhlich and M. Grehl

Formula: C₁₇H₂₃NO₂

Acta Cryst. (1996). C52, 470-472    [ doi:10.1107/S0108270195010900 ]

A 1:1 Molecular Complex of 1,5-Diphenylbiuret and Phenyl Carbamidonitrile

Q.-C. Yang, D.-M. Huang, H.-Y. Chen and Y.-Q. Tang

Formula: C₁₄H₁₃N₃O₂.C₈H₇N₃O

Acta Cryst. (1996). C52, 472-474    [ doi:10.1107/S0108270195013011 ]

N-[2-(1-3H-Indenyl)ethyl]-p-toluenesulfonamide

G. J. Gainsford and C. Lensink

Formula: C₁₈H₁₉NO₂S

Acta Cryst. (1996). C52, 474-477    [ doi:10.1107/S0108270195008286 ]

Dupeyredioxyl (1,3,5,7-Tetramethyl-2,6-diazaadamantane-N,N'-dioxyl)

Y. Dromzee, R. Chiarelli, S. Gambarelli and A. Rassat

Formula: Two isomers of C₁₂H₂₀N₂O₂

Acta Cryst. (1996). C52, 477-481    [ doi:10.1107/S0108270195011668 ]

A Second Triclinic Polymorph of Coumarin 153

B.-C. Yip, F.-M. Moo, K.-S. Lok, H.-K. Fun and K. Sivakumar

Formula: C₁₆H₁₄F₃NO₂

Acta Cryst. (1996). C52, 481-483    [ doi:10.1107/S0108270195010171 ]

3,3,6,6-Tetramethyl-10-(4-methylphenyl)-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

J. Sivaraman, K. Subramanian, D. Velmurugan, E. Subramanian and P. S. Shanmugasundram

Formula: C₂₄H₂₉NO₂

Acta Cryst. (1996). C52, 484-485    [ doi:10.1107/S0108270195010560 ]

2-(2-Fluorobenzoylamino)benzoic Acid

W. H. Ojala, J. E. Clemons and C. R. Ojala

Formula: C₁₄H₁₀FNO₃

Acta Cryst. (1996). C52, 486-489    [ doi:10.1107/S0108270195013692 ]

Two Isoxazolidines

S. Niwayama, Y. You, K. N. Houk and S. I. Khan

Formula: C₁₉H₁₉NO₃ and C₁₈H₁₇NO₃: Rb₂ZnSi₅O₁₂

addenda and errata

Acta Cryst. (1996). C52, 490    [ doi:10.1107/S0108270196099775 ]

Rietveld refinement of dry-synthesized Rb₂ZnSi₅O₁₂ leucite by synchrotron X-ray powder diffraction. Erratum

A. M. T. Bell and C. M. B. Henderson

Synopsis: Erratum to Acta Cryst. (1994), C50, 984-986.

Copyright © International Union of Crystallography
IUCr Webmaster