# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_s9418 _shelx_title ' S9418 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 492.44 _exptl_crystal_F_000 2580.00 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 78168.88 87865.69 788.07 o 3 0 0 14823.42 13175.21 435.02 o 4 0 0 134812.06 137827.80 1407.54 o 5 0 0 60952.40 65224.61 1064.36 o 6 0 0 26138.14 26191.17 733.96 o 7 0 0 17355.92 18184.61 637.12 o 8 0 0 8191.54 8432.66 431.41 o 9 0 0 5102.37 5394.70 296.49 o 10 0 0 1614.06 1687.27 211.73 o 11 0 0 25570.92 25623.78 622.40 o 12 0 0 3890.82 4276.11 296.42 o 13 0 0 2982.02 3214.56 280.73 o 14 0 0 1623.28 1563.49 319.28 o 1 1 0 94870.95 90573.22 638.18 o 2 1 0 2171.99 2071.41 80.59 o 3 1 0 34505.82 36745.46 679.19 o 4 1 0 2979.69 3215.53 150.97 o 5 1 0 55511.20 57523.18 998.03 o 6 1 0 30037.39 33025.59 792.67 o 7 1 0 7008.35 7144.01 291.05 o 8 1 0 3336.26 3548.18 187.33 o 9 1 0 2611.40 2500.20 205.46 o 10 1 0 9077.87 9670.43 473.30 o 11 1 0 11690.00 11183.73 477.65 o 12 1 0 19205.57 18801.50 498.20 o 13 1 0 1511.15 1748.25 260.12 o 14 1 0 6508.05 6333.69 354.33 o 0 2 0 134194.44 141929.73 891.21 o 1 2 0 2149.23 1576.05 95.35 o 2 2 0 29176.11 27296.17 534.73 o 3 2 0 245.40 510.52 85.64 o 4 2 0 1558.77 1751.38 119.49 o 5 2 0 87.20 250.87 104.67 o 6 2 0 1965.38 1482.06 136.29 o 7 2 0 988.55 1027.00 153.36 o 8 2 0 1940.61 1881.52 174.56 o 9 2 0 2731.03 2967.54 203.55 o 10 2 0 3971.10 4082.22 240.00 o 11 2 0 9912.07 10607.63 460.59 o 12 2 0 1153.67 1593.16 262.94 o 13 2 0 2354.04 1946.04 288.03 o 14 2 0 803.47 1164.41 294.59 o 1 3 0 16439.03 17143.17 442.77 o 2 3 0 12796.77 13557.34 453.89 o 3 3 0 55.30 19.42 87.67 o 4 3 0 11053.10 11059.98 508.75 o 5 3 0 2528.87 2879.31 132.04 o 6 3 0 2495.17 3076.56 193.49 o 7 3 0 742.91 1089.29 154.98 o 8 3 0 188.02 99.32 164.43 o 9 3 0 1002.10 935.06 200.41 o 10 3 0 1135.86 1624.56 221.33 o 11 3 0 789.73 682.49 246.22 o 12 3 0 3578.96 3390.86 289.55 o 13 3 0 314.65 314.95 269.81 o 14 3 0 1698.53 1278.41 321.28 o 0 4 0 80135.88 79760.41 970.71 o 1 4 0 12898.97 15316.58 506.68 o 2 4 0 2188.22 2031.71 98.18 o 3 4 0 13.64 154.16 90.16 o 4 4 0 449.79 492.48 107.28 o 5 4 0 323.19 198.77 121.04 o 6 4 0 10618.46 11723.19 552.65 o 7 4 0 3488.34 3191.09 193.50 o 8 4 0 3292.92 2989.50 200.44 o 9 4 0 126.72 -31.21 189.98 o 10 4 0 21.91 74.41 219.44 o 11 4 0 1009.83 1215.46 251.59 o 12 4 0 5042.31 5071.46 311.96 o 13 4 0 228.16 10.96 273.50 o 14 4 0 92.34 -89.54 300.34 o 1 5 0 18094.07 18034.48 572.46 o 2 5 0 203.91 275.23 91.18 o 3 5 0 25394.59 25763.01 679.61 o 4 5 0 6646.31 6220.06 294.81 o 5 5 0 10964.47 11068.61 545.10 o 6 5 0 5537.34 5321.15 277.94 o 7 5 0 6517.31 6500.35 280.27 o 8 5 0 378.45 690.69 181.18 o 9 5 0 2671.58 2608.16 221.44 o 10 5 0 8443.17 8840.34 401.22 o 11 5 0 1360.01 1355.11 257.76 o 12 5 0 850.15 1212.58 264.77 o 13 5 0 2923.87 2446.64 308.55 o 14 5 0 5885.37 6282.69 371.93 o 0 6 0 72761.37 71628.75 1088.99 o 1 6 0 1989.38 1742.22 109.94 o 2 6 0 25680.32 26727.55 698.99 o 3 6 0 3849.08 4041.23 205.83 o 4 6 0 19131.46 19697.92 650.02 o 5 6 0 4591.14 4322.87 250.57 o 6 6 0 17507.11 16888.66 613.76 o 8 6 0 9225.76 9340.92 405.79 o 9 6 0 9758.42 9913.46 463.07 o 10 6 0 3657.32 3546.28 250.08 o 11 6 0 7306.46 7981.83 337.01 o 12 6 0 2855.87 3111.17 275.59 o 13 6 0 6087.51 6556.15 346.49 o 14 6 0 2355.03 2161.51 326.72 o 1 7 0 54314.59 51958.41 966.00 o 2 7 0 3070.58 3188.25 196.01 o 3 7 0 101820.96 102406.94 1349.18 o 4 7 0 47161.47 45601.88 930.99 o 5 7 0 7411.23 6774.41 318.53 o 6 7 0 17942.85 17747.89 597.98 o 7 7 0 7655.74 8044.52 376.86 o 8 7 0 18610.62 19050.31 597.57 o 9 7 0 1431.95 1292.94 217.56 o 10 7 0 8282.35 8407.83 372.51 o 11 7 0 671.56 616.57 233.33 o 12 7 0 4170.54 4443.77 301.10 o 13 7 0 1228.27 1469.50 286.03 o 0 8 0 43334.26 42021.50 920.52 o 1 8 0 72.19 -37.17 125.59 o 2 8 0 93507.66 93334.81 1321.37 o 3 8 0 18848.90 19513.26 666.88 o 4 8 0 21950.99 21005.46 677.62 o 5 8 0 2222.62 2421.31 174.68 o 6 8 0 11878.55 11784.43 533.98 o 7 8 0 3306.13 2923.83 211.46 o 8 8 0 7683.84 7691.23 394.98 o 9 8 0 9195.78 9149.55 438.73 o 10 8 0 1379.87 1063.41 241.44 o 11 8 0 4200.59 4606.67 284.97 o 12 8 0 486.46 -271.31 283.17 o 13 8 0 8692.57 9221.99 385.85 o 1 9 0 21203.01 20588.90 684.69 o 2 9 0 225.44 269.87 146.64 o 3 9 0 41451.01 40895.54 877.50 o 4 9 0 1712.41 1345.92 170.93 o 5 9 0 15349.66 14830.25 589.61 o 6 9 0 1239.40 1386.13 188.12 o 7 9 0 10672.12 11106.33 491.84 o 8 9 0 1932.01 1696.65 221.96 o 9 9 0 1418.79 1153.70 239.58 o 10 9 0 2518.16 2550.53 270.05 o 11 9 0 1698.94 1945.66 254.50 o 12 9 0 5112.88 4684.98 334.32 o 13 9 0 1929.32 1822.56 321.57 o 0 10 0 9252.41 8852.44 489.20 o 1 10 0 1866.79 1778.20 168.37 o 2 10 0 5410.51 5940.69 282.04 o 3 10 0 15.37 172.14 158.34 o 4 10 0 107.39 334.60 173.34 o 5 10 0 1246.24 1537.16 188.12 o 6 10 0 8337.69 8442.18 430.18 o 7 10 0 478.91 621.76 213.52 o 8 10 0 4196.16 4531.51 267.72 o 9 10 0 688.04 415.03 242.37 o 10 10 0 234.29 206.65 253.61 o 11 10 0 2185.33 2343.63 292.31 o 12 10 0 1550.92 1654.55 308.84 o 1 11 0 299.90 180.78 166.88 o 2 11 0 3086.32 3165.61 197.65 o 3 11 0 301.87 222.13 183.73 o 4 11 0 2851.81 2901.10 204.93 o 5 11 0 1792.30 1516.78 207.40 o 6 11 0 53.10 321.58 194.66 o 7 11 0 25.65 -122.18 224.09 o 8 11 0 275.58 249.57 236.88 o 9 11 0 3116.51 2834.98 287.26 o 10 11 0 149.45 391.81 266.21 o 11 11 0 966.94 886.11 292.99 o 12 11 0 282.51 303.68 299.17 o 0 12 0 7865.63 8938.64 449.33 o 1 12 0 1430.08 1469.39 189.48 o 2 12 0 1104.98 1285.63 198.46 o 3 12 0 13.53 202.55 184.04 o 4 12 0 7224.07 7108.45 371.05 o 5 12 0 213.44 -308.89 212.19 o 6 12 0 4907.21 4286.88 260.74 o 7 12 0 8223.45 8577.58 383.90 o 8 12 0 2650.67 2383.37 278.67 o 9 12 0 91.66 92.75 249.23 o 10 12 0 6243.95 6138.29 345.37 o 11 12 0 855.92 778.03 304.05 o 1 13 0 12750.98 11766.40 517.70 o 2 13 0 3373.71 3194.88 232.71 o 3 13 0 6964.26 6824.12 358.51 o 4 13 0 1602.45 1436.49 237.54 o 5 13 0 8951.43 9306.91 419.48 o 6 13 0 5102.02 4445.80 286.28 o 7 13 0 7246.20 7429.80 362.35 o 8 13 0 2982.39 3348.61 287.26 o 9 13 0 2617.20 2840.51 296.35 o 10 13 0 2421.95 2009.01 325.47 o 11 13 0 2274.49 2589.35 326.17 o 0 14 0 32325.02 31405.05 672.97 o 1 14 0 7.51 43.95 209.96 o 2 14 0 11883.86 12477.93 467.45 o 3 14 0 5091.85 5247.99 269.51 o 4 14 0 15354.40 14099.35 476.28 o 5 14 0 9327.60 8419.36 396.33 o 6 14 0 4805.02 4908.89 292.75 o 7 14 0 7350.51 7229.34 342.48 o 8 14 0 2354.05 2589.18 273.89 o 9 14 0 3273.55 4083.96 315.39 o 10 14 0 734.47 1066.04 287.78 o 1 15 0 21732.95 21691.96 546.30 o 2 15 0 266.14 310.61 234.41 o 3 15 0 12404.85 12480.65 424.82 o 4 15 0 5076.31 4886.03 292.58 o 5 15 0 10584.56 10012.63 383.16 o 6 15 0 3760.15 3490.89 288.49 o 7 15 0 6432.12 6691.25 334.02 o 8 15 0 2110.79 2581.08 303.24 o 9 15 0 1195.70 1309.25 298.74 o 0 16 0 14254.34 14497.71 441.17 o 1 16 0 2.32 98.61 247.58 o 2 16 0 6342.79 6520.85 328.52 o 3 16 0 523.63 608.60 247.84 o 4 16 0 5129.29 5366.93 300.59 o 5 16 0 3448.80 3471.45 298.30 o 6 16 0 5747.29 5510.08 345.41 o 7 16 0 1515.83 1704.07 299.20 o 8 16 0 1001.49 806.23 297.64 o 1 17 0 3387.48 3110.34 310.20 o 2 17 0 268.81 369.49 257.76 o 3 17 0 1393.04 1595.24 278.78 o 4 17 0 223.01 381.93 265.55 o 5 17 0 932.81 601.96 301.23 o 6 17 0 84.17 -43.91 293.21 o 7 17 0 2704.20 3070.37 324.04 o 1 18 0 23.49 92.30 284.62 o 2 18 0 421.20 81.48 291.10 o 3 18 0 339.56 44.31 279.10 o 4 18 0 46.02 -105.74 294.95 o 5 18 0 252.47 -39.67 300.33 o 1 19 0 362.38 508.78 301.62 o 2 19 0 5.80 -597.41 294.92 o -14 1 1 34.12 -70.35 277.75 o -13 1 1 132.00 79.13 244.83 o -12 1 1 122.74 68.49 253.46 o -11 1 1 3284.20 3291.34 261.95 o -10 1 1 1733.05 1691.66 219.72 o -9 1 1 269.76 392.90 172.35 o -8 1 1 3165.81 3273.34 197.56 o -7 1 1 9874.10 10105.27 495.89 o -6 1 1 3769.37 3909.01 242.33 o -5 1 1 34672.88 34231.74 795.21 o -4 1 1 38363.75 36320.30 774.58 o -3 1 1 60094.49 64157.29 872.14 o -2 1 1 5778.63 4470.61 225.81 o -1 1 1 45308.73 40832.85 444.97 o 1 1 1 29748.98 32889.73 413.01 o 2 1 1 15652.50 13237.61 373.81 o 3 1 1 77752.68 76326.33 944.44 o 4 1 1 5616.70 5687.73 267.84 o 5 1 1 1967.69 1867.81 121.93 o 6 1 1 18280.58 19246.26 644.36 o 7 1 1 473.08 599.15 140.59 o 8 1 1 3255.69 3426.15 189.94 o 9 1 1 26.66 262.34 173.61 o 10 1 1 2086.93 2126.51 226.77 o 11 1 1 272.07 323.61 246.22 o 12 1 1 1681.38 2066.09 276.95 o 13 1 1 186.85 30.65 269.54 o 14 1 1 613.78 601.65 295.63 o -14 2 1 3213.05 2873.97 335.00 o -13 2 1 82.73 483.90 243.80 o -12 2 1 7982.95 7638.63 362.18 o -11 2 1 3071.98 3244.97 257.40 o -10 2 1 8869.98 8359.71 446.75 o -9 2 1 2596.53 3105.93 208.65 o -8 2 1 20457.88 22244.84 674.15 o -7 2 1 1897.44 2109.37 160.15 o -6 2 1 39476.30 39506.40 876.67 o -5 2 1 5519.05 6174.45 299.46 o -4 2 1 60231.67 61072.56 988.97 o -3 2 1 10402.88 10774.48 457.03 o -2 2 1 17681.29 18665.54 471.22 o -1 2 1 55281.62 58970.71 644.37 o 0 2 1 104811.73 98825.61 653.76 o 1 2 1 2839.74 2543.26 149.00 o 2 2 1 22739.12 21946.15 494.00 o 3 2 1 17160.27 18584.19 531.38 o 4 2 1 1856.43 1731.35 104.97 o 5 2 1 31505.94 31987.11 781.35 o 6 2 1 688.59 723.46 124.70 o 7 2 1 19855.36 20508.49 660.55 o 8 2 1 5847.99 5448.81 319.96 o 9 2 1 3151.78 2985.77 216.63 o 10 2 1 43.21 .00 201.30 o 11 2 1 10875.74 11075.45 465.19 o 12 2 1 759.51 381.11 263.15 o 13 2 1 3020.79 2745.35 299.43 o 14 2 1 8.06 200.06 283.30 o -14 3 1 3238.59 3495.00 326.44 o -13 3 1 5453.88 5570.29 328.37 o -12 3 1 822.59 642.57 260.02 o -11 3 1 25259.73 24738.52 600.76 o -10 3 1 2501.67 2609.04 234.49 o -9 3 1 28007.90 27959.35 705.25 o -8 3 1 1466.88 1475.93 182.20 o -7 3 1 43866.87 44699.36 924.76 o -6 3 1 416.10 143.75 131.45 o -5 3 1 38796.68 39918.16 868.75 o -4 3 1 7603.90 7342.87 359.99 o -3 3 1 37999.43 36835.83 755.84 o -2 3 1 5033.36 4094.90 225.96 o -1 3 1 1132.29 1807.91 96.81 o 0 3 1 23979.79 20542.21 327.69 o 1 3 1 14639.99 12744.17 403.40 o 2 3 1 6962.44 8591.33 373.64 o 3 3 1 18132.76 18962.76 577.20 o 4 3 1 44952.25 45009.02 874.30 o 5 3 1 9523.69 9252.37 468.12 o 6 3 1 35037.78 34005.62 812.11 o 7 3 1 9499.07 9525.58 489.03 o 8 3 1 17396.65 18156.41 638.16 o 9 3 1 3742.30 3842.69 222.76 o 10 3 1 19747.33 20145.26 600.06 o 11 3 1 2220.28 2776.40 258.66 o 12 3 1 12955.52 12862.96 429.97 o 13 3 1 41.43 -233.54 275.96 o 14 3 1 10446.49 10680.07 418.96 o -14 4 1 4448.86 4590.34 347.98 o -13 4 1 2709.98 3216.27 304.51 o -12 4 1 8652.74 8661.87 385.38 o -11 4 1 1199.34 1232.30 244.51 o -10 4 1 22819.31 22850.77 620.05 o -9 4 1 2955.34 3436.15 215.27 o -8 4 1 31878.34 32978.41 794.22 o -7 4 1 3802.37 3639.24 187.14 o -6 4 1 22781.29 21186.29 686.50 o -5 4 1 2570.98 2851.16 144.10 o -4 4 1 57007.14 56697.13 993.53 o -3 4 1 75.29 -36.11 94.23 o -2 4 1 36275.20 36098.03 735.60 o -1 4 1 6275.24 6666.32 351.04 o 0 4 1 74448.55 75791.07 2751.19 o 1 4 1 95516.80 91323.21 1063.30 o 2 4 1 19301.33 18360.20 554.49 o 3 4 1 45725.64 46896.26 876.42 o 4 4 1 7116.09 7675.59 402.96 o 5 4 1 47949.25 48721.96 957.07 o 6 4 1 6633.11 5595.06 305.70 o 7 4 1 32236.38 31336.65 791.56 o 8 4 1 7400.76 6906.37 377.03 o 9 4 1 16367.06 16745.80 580.99 o 10 4 1 5141.81 5102.46 269.23 o 11 4 1 16959.35 15434.39 502.25 o 12 4 1 150.49 215.24 255.43 o 13 4 1 11697.26 11822.57 396.76 o 14 4 1 404.30 -78.67 308.04 o -14 5 1 2074.53 2383.21 320.61 o -13 5 1 936.90 748.02 286.95 o -12 5 1 2333.18 2118.53 275.66 o -11 5 1 12241.40 12166.19 449.91 o -10 5 1 103.08 55.41 214.58 o -9 5 1 13870.17 12719.21 539.09 o -8 5 1 4344.68 4218.75 235.91 o -7 5 1 28293.31 29567.42 756.24 o -6 5 1 7013.11 7013.65 380.12 o -5 5 1 31297.35 31106.16 772.65 o -4 5 1 7008.41 7089.05 397.02 o -3 5 1 38138.11 39492.82 845.46 o -2 5 1 5158.06 4855.54 229.57 o -1 5 1 22284.18 20883.82 615.77 o 0 5 1 10258.42 10893.30 448.73 o 1 5 1 2552.44 2403.82 137.28 o 2 5 1 48429.62 45197.21 869.45 o 3 5 1 41441.20 41076.54 854.39 o 4 5 1 27833.55 27699.22 727.09 o 5 5 1 10804.88 11384.05 529.73 o 6 5 1 32456.73 30949.14 780.02 o 7 5 1 4078.24 4176.69 223.00 o 8 5 1 26936.40 27212.14 712.69 o 9 5 1 3320.29 2955.76 234.92 o 10 5 1 5922.17 6584.16 324.04 o 11 5 1 3858.50 3794.01 278.08 o 12 5 1 7008.78 7136.67 353.86 o 13 5 1 346.59 755.88 278.86 o 14 5 1 6180.91 5518.93 375.41 o -14 6 1 1482.43 1590.13 315.10 o -13 6 1 728.53 346.77 282.78 o -12 6 1 148.50 72.00 251.20 o -11 6 1 125.01 40.02 232.62 o -10 6 1 6469.77 6208.82 314.42 o -9 6 1 3245.49 2850.80 233.02 o -8 6 1 8274.23 8613.34 459.38 o -7 6 1 8893.24 8509.30 465.72 o -6 6 1 8059.90 7647.74 386.37 o -5 6 1 7787.49 8891.31 380.89 o -4 6 1 34872.12 34495.88 814.57 o -3 6 1 8047.95 9494.25 438.10 o -2 6 1 23559.80 23369.38 681.27 o -1 6 1 11776.00 13777.22 552.97 o 0 6 1 14946.16 14949.41 551.42 o 1 6 1 34162.64 33540.09 769.86 o 2 6 1 1318.36 1385.02 109.85 o 3 6 1 11976.32 10176.23 483.40 o 4 6 1 1060.14 913.24 123.86 o 5 6 1 9015.01 9272.95 484.17 o 6 6 1 900.82 928.78 156.26 o 7 6 1 17126.71 17858.44 608.65 o 8 6 1 1854.60 1764.84 206.07 o 9 6 1 3080.82 3141.80 230.63 o 10 6 1 2529.10 2133.26 250.60 o 11 6 1 716.60 762.07 246.79 o 12 6 1 241.46 397.01 248.65 o 13 6 1 1020.01 457.19 301.54 o -13 7 1 263.69 -123.36 287.17 o -12 7 1 1.11 234.17 244.60 o -11 7 1 392.72 746.97 228.33 o -10 7 1 377.47 327.40 221.66 o -9 7 1 1029.58 949.42 215.38 o -8 7 1 242.15 313.08 189.38 o -7 7 1 26.55 -201.24 180.84 o -6 7 1 237.66 275.69 151.44 o -5 7 1 3515.21 3667.39 203.55 o -4 7 1 4303.64 4464.20 181.06 o -3 7 1 727.57 732.71 126.82 o -2 7 1 445.26 452.84 118.03 o -1 7 1 880.78 1254.86 122.56 o 0 7 1 1812.17 2299.42 133.47 o 1 7 1 1996.30 2414.06 123.67 o 2 7 1 40.44 141.46 112.72 o 3 7 1 4794.88 4713.51 250.77 o 4 7 1 3774.71 3623.24 217.20 o 5 7 1 8180.88 8137.01 374.05 o 6 7 1 7837.40 8666.70 365.71 o 7 7 1 628.17 568.77 173.08 o 8 7 1 955.78 1157.09 197.54 o 9 7 1 2791.52 2724.77 233.15 o 11 7 1 275.36 -18.41 236.72 o 12 7 1 86.34 402.40 256.17 o 13 7 1 427.28 190.62 300.20 o -13 8 1 713.04 807.24 302.90 o -12 8 1 31.65 -322.71 269.96 o -11 8 1 296.78 433.62 247.04 o -10 8 1 80.21 363.89 225.36 o -9 8 1 1599.25 1652.18 230.64 o -8 8 1 206.60 71.27 205.64 o -7 8 1 2575.37 2882.18 205.63 o -6 8 1 1977.33 2032.29 185.50 o -5 8 1 1545.14 1849.64 169.41 o -4 8 1 6039.48 6090.32 325.13 o -3 8 1 1040.73 1119.61 151.19 o -2 8 1 8716.10 9403.89 431.31 o -1 8 1 15727.99 17149.30 640.89 o 0 8 1 5667.15 5727.27 189.68 o 1 8 1 501.15 301.77 125.93 o 2 8 1 9019.70 8351.05 396.53 o 3 8 1 14805.56 15292.44 610.95 o 4 8 1 2021.97 2290.65 162.41 o 5 8 1 1071.26 1344.46 165.67 o 6 8 1 8.93 -174.24 170.96 o 7 8 1 2189.52 2454.94 206.38 o 8 8 1 282.53 157.70 202.90 o 9 8 1 713.07 315.51 231.69 o 10 8 1 768.55 661.73 241.54 o 11 8 1 300.29 699.59 242.25 o 12 8 1 490.77 804.50 265.42 o 13 8 1 1990.14 1987.54 328.99 o -13 9 1 953.35 756.90 325.18 o -12 9 1 74.55 212.67 271.09 o -11 9 1 115.27 -91.70 246.45 o -10 9 1 2456.52 2402.25 263.16 o -9 9 1 4285.41 4170.55 270.59 o -8 9 1 4943.58 5302.95 248.48 o -7 9 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