Acta Crystallographica Section C

Crystal Structure Communications

Volume 52, Part 9 (September 1996)


Cover illustration

inorganic compounds



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Acta Cryst. (1996). C52, 2121-2123    [doi:10.1107/S0108270196003927]

The Hydrogen-Bonding System in Deuterated Copper Fluorosilicate Tetrahydrate: a Neutron Diffraction Study

G. Chevrier and A. Goukassov

Synopsis: In CuSiF6.4D2O, chains of SiF6 and Cu(D2O)4F2 octahedra are linked by hydrogen bonds to form a three-dimensional structure.

Formula: CuSiF6.4D2O



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Acta Cryst. (1996). C52, 2123-2125    [doi:10.1107/S010827019501506X]

La3(Si2O7)Cl3

J.-T. Chen, G.-C. Guo, J.-S. Huang and Q.-E. Zhang

Synopsis: The structure of La3(Si2O7)Cl3 is built up from [La2Cl2Si2O6] sheets stacked along the b direction with [LaClO] units accommodated between adjacent sheets.

Formula: La3(Si2O7)Cl3



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Acta Cryst. (1996). C52, 2125-2127    [doi:10.1107/S0108270195015058]

Nd4V5Si4O22

J.-T. Chen, G.-C. Guo, H.-H. Zhuang, J.-S. Huang and Q.-E. Zhang

Synopsis: Nd4V5Si4O22 has a quasi-two-dimensional chevkinite-type structure, consisting of rutile-like vanadium-oxygen layers with V-V distances of 2.794(2)Å.

Formula: Nd4V5Si4O22



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Acta Cryst. (1996). C52, 2127-2129    [doi:10.1107/S0108270196004969]

The Binary Hafnium Phosphide Hf3P2

H. Kleinke and H. F. Franzen

Synopsis: Hf3P2 has an anti-Sb2S3-type structure in which singly capped and bicapped trigonal Hf6P prisms are interconnected via common edges and faces to form a three-dimensional network.

Formula: Hf3P2



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Acta Cryst. (1996). C52, 2129-2132    [doi:10.1107/S0108270196003198]

Tricaesium Ditellurium Tetravanadium Chloride Tetradecaoxide

J. Marrot and J.-M. Savariault

Synopsis: The structure of (CsCl)Cs2(TeV2O7)2 consists of stacks of [V2TeO7] sheets alternately separated by layers of Cs atoms and layers of Cs and Cl atoms.

Formula: (CsCl)Cs2(TeV2O7)2



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Acta Cryst. (1996). C52, 2132-2139    [doi:10.1107/S0108270196003162]

Rietveld Refinement of the Orthorhombic Pbca Structures of Rb2CdSi5O12, Cs2MnSi5O12, Cs2CoSi5O12 , and Cs2NiSi5O12 Leucites by Synchrotron X-ray Powder Diffraction

A. M. T. Bell and C. M. B. Henderson

Synopsis: The Pbca structures of four leucite analogues have been refined by the Rietveld method using high-resolution synchrotron X-ray powder diffraction patterns collected on stations 2.3 and 9.1 of the Daresbury Synchrotron Radiation Source.

Formula: Rb2CdSi5O12, Cs2MnSi5O12, Cs2CoSi5O12 and Cs2NiSi5O12


metal-organic compounds



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Acta Cryst. (1996). C52, 2140-2141    [doi:10.1107/S0108270195009322]

Sodium Dinitritobis(pyrazine-2-carboxylato-N,O)cobaltate(III)

R. P. Sharma, K. K. Bhasin and E. R. T. Tiekink

Formula: Na[Co(C5H3N2O2)2(NO2)2]



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Acta Cryst. (1996). C52, 2141-2143    [doi:10.1107/S0108270195009334]

Benzyltrichloro(1,10-phenanthroline-N,N')tin(IV) Benzene Solvate (1/1)

V. J. Hall and E. R. T. Tiekink

Formula: [SnCl3(C7H7)(C12H8N2)].C6H6



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Acta Cryst. (1996). C52, 2143-2145    [doi:10.1107/S0108270195009346]

Bis(diethylammonium) Tetrachlorodivinylstannate(IV)

V. J. Hall and E. R. T. Tiekink

Formula: (C4H12N)2[SnCl4(C2H3)2]



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Acta Cryst. (1996). C52, 2145-2148    [doi:10.1107/S0108270196006257]

A 3:1 Disordered Solid Solution of Di-[bold mu]-methoxo-O:O-bis[trimethoxooxomolybdenum(VI)] and Di-[bold mu]-methoxo-O:O-bis[chlorodimethoxooxomolybdenum(VI)]

W. Clegg, M. R. J. Elsegood, R. J. Errington and R. Bakri

Formula: [Mo2(CH3O)8(O)2]0.75.[Mo2Cl2(CH3O)6(O)2]0.25



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Acta Cryst. (1996). C52, 2148-2150    [doi:10.1107/S010827019600563X]

The AsF6- Salt of a 1,2-Dithia-4-azolylium Cation with Sterically Demanding Substituents

W. Clegg, M. R. J. Elsegood, A. J. Banister and T. G. Hibbert

Formula: C16H14NS2+.AsF6-



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Acta Cryst. (1996). C52, 2150-2153    [doi:10.1107/S010827019600385X]

Bis[methyl N[beta]-(4-dimethylaminophenylmethylene)dithiocarbazato]nickel(II)

Y.-P. Tian, C.-Y. Duan, Z.-L. Lu, X.-Z. You, H.-K. Fun and K. Sivakumar

Formula: [Ni(C11H14N3S2)2]



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Acta Cryst. (1996). C52, 2153-2155    [doi:10.1107/S0108270196003757]

1,4-Dimethylpyridinium Bis(6,7-dihydro-5H-1,4-dithiepine-2,3-dithiolato-S,S')cuprate(III)

H.-K. Fun, K. Sivakumar, J.-L. Zuo, F. You and X.-Z. You

Formula: (C7H10N)[Cu(C5H6S4)2]



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Acta Cryst. (1996). C52, 2155-2157    [doi:10.1107/S0108270196005628]

trans-Dichlorotetrakis(pyridine-N)molybdenum(III) Tribromide

R. Rotar, I. Leban and J. V. Brencic

Formula: [MoCl2(C5H5N)4]Br3



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Acta Cryst. (1996). C52, 2157-2159    [doi:10.1107/S010827019600707X]

Tris(N,N-diethyldithiocarbamato-S,S')(thionitrosyl-N)molybdenum(III), [Mo([bold eta]2-S2CNEt2)3(NS)]

T. A. Coffey, G. D. Forster and G. Hogarth

Formula: [Mo(C5H10NS2)3(NS)]



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Acta Cryst. (1996). C52, 2159-2161    [doi:10.1107/S0108270196005896]

(4-Chlorobenzenethiolato-S)([bold eta]5-cyclopentadienyl)(triphenylphosphine-P)nickel(II)

J. Darkwa and W. Milius

Formula: [Ni(C6H4ClS)(C5H5)(C18H15P)]



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Acta Cryst. (1996). C52, 2161-2164    [doi:10.1107/S0108270196004076]

An Mo2(CO)4 (Mo[triple bond]Mo) Fragment Stabilized by a Tripod Ligand

R. Herbst-Irmer and E. Egert

Formula: [Mo(CO)2{Co(C5H5)(C2H6O3P)3}]2



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Acta Cryst. (1996). C52, 2164-2166    [doi:10.1107/S0108270195008882]

trans-Diazidobis[1,2-bis(diethylphosphino)ethane-P,P']iron(II)

L. D. Field, A. V. George, S. R. Pike, I. E. Buys and T. W. Hambley

Formula: [Fe(N3)2(C10H24P2)2]



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Acta Cryst. (1996). C52, 2166-2168    [doi:10.1107/S0108270196002600]

Copper(II) and Nickel(II) Complexes with 3,14-Dimethyl-2,6,13,17-tetraazatricyclo[16.4.0.07,12]docosane, [M(C20H40N4)]Cl2.2H2O (M = CuII and NiII)

K.-Y. Choi, J. C. Kim, W. P. Jensen, I.-H. Suh and S.-S. Choi

Formula: [Cu(C20H40N4)]Cl2.2H2O and [Ni(C20H40N4)]Cl2.2H2O



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Acta Cryst. (1996). C52, 2168-2170    [doi:10.1107/S0108270196006221]

Diiodobis([bold eta]5-trimethylsilylcyclopentadienyl)titanium(IV)

M. G. B. Drew, E. Delgado, E. Hernandez, P. K. Baker and N. Mansilla

Formula: [TiI2(C8H13Si)2]



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Acta Cryst. (1996). C52, 2170-2173    [doi:10.1107/S0108270196006038]

Tetrakis(2,3,5,6-tetramethylpyrazinium) Tetra-[bold mu]3-iodo-hexa-[bold mu]-iodo-dodecaiodohexaantimonate(4-) Tetrahydrate

M. V. Smyth, R. D. Bailey and W. T. Pennington

Formula: (C8H13N2)4[Sb6I22].4H2O



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Acta Cryst. (1996). C52, 2173-2176    [doi:10.1107/S0108270196005811]

A Condensed Dialkoxide Complex of Copper(II), [(CH3)2NCH2CH2N(CH3)2]Cu[{OC(CF3)2}2O]

R. C. Hynes, C. J. Willis and N. C. Payne

Formula: [Cu(C6F12O3)(C6H16N2)]



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Acta Cryst. (1996). C52, 2176-2178    [doi:10.1107/S0108270196006087]

catena-Poly[{di-[bold mu]-nitrato-1:2[bold kappa]4O-bis[(triphenylphosphine-P)copper(I)]}-[bold mu]-4,4'-bipyridyl-N:N'] Tetrahydrofuran Solvate

P.-J. Prest and J. S. Moore

Formula: [Cu2(NO3)2(C18H15P)2(C10H8N2)].2C4H8O



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Acta Cryst. (1996). C52, 2178-2180    [doi:10.1107/S0108270196006130]

(Cyclohexylamine-N){2-[(2-thiophenyl)iminomethyl]phenolato-O,N,S}nickel(II)

M. N. Tahir, D. Ülkü, O. Atakol and A. Kenar

Formula: [Ni(C13H9NOS)(C6H13N)]



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Acta Cryst. (1996). C52, 2180-2183    [doi:10.1107/S0108270196006002]

[N-(2-Amino-[bold kappa]N-ethyl)piperaziniumyl-N1]tetrachloroindium(III)

A. M. Chippindale, S. J. Brech, A. R. Cowley and A. N. Chernega

Formula: [InCl4(C6H16N3)]



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Acta Cryst. (1996). C52, 2183-2185    [doi:10.1107/S0108270196003721]

Bis(p-aminobenzoic acid-N)dichlorocadmium(II)

Y. Le Fur and R. Masse

Formula: [CdCl2(C7H7NO2)2]



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Acta Cryst. (1996). C52, 2185-2188    [doi:10.1107/S0108270196007342]

Caesium 2-(2-Hydroxy-5,5-dimethyl-1,3-dioxo-2-cyclohexyl)-5,5-dimethyl-1,3-cyclohexanedionato(1-) Monohydrate

J. C. Barnes

Formula: Cs+.C16H21O5-.H2O



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Acta Cryst. (1996). C52, 2188-2191    [doi:10.1107/S010827019600604X]

Bis[bis(2-pyridyl-N) sulfide]palladium(II) Bis(tetrafluoroborate)

F. Nicolò, G. Bruno and G. Tresoldi

Formula: [Pd(C10H8N2S)2](BF4)2



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Acta Cryst. (1996). C52, 2191-2193    [doi:10.1107/S0108270196005008]

Bis(nitrato-O,O')bis{2-[2-(2-thienyl)ethynyl]pyridine-N}cobalt(II)

H. Kooijman, A. L. Spek, T. X. Neenan and W. L. Driessen

Formula: [Co(NO3)2(C11H7NS)2]



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Acta Cryst. (1996). C52, 2193-2196    [doi:10.1107/S0108270196006208]

Bis[1,2-bis(diphenylphosphino)ethane-P,P']chloroosmium(II) Hexafluorophosphate Dichloromethane Solvate

A. J. Lough, R. H. Morris and M. Schlaf

Formula: [OsCl(C26H24P2)2]PF6.1.5CH2Cl2



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Acta Cryst. (1996). C52, 2196-2198    [doi:10.1107/S0108270196004118]

1-(R)-{2-[1-(R)-(N,N-Dimethylamino)ethyl]-1,1'-(S,S)-biferrocen-2'-yl}ethyl-N,N-dimethylammonium Trichloro(dimethyl sulfoxide-S)platinate(II)

B. H. Robinson, J. Simpson and D. J. Wilson

Formula: [Fe2(C5H5)2(C18H27N2)][PtCl3(C2H6OS)]



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Acta Cryst. (1996). C52, 2198-2201    [doi:10.1107/S0108270196006105]

Monosodium 4-Amino-1-hydroxy-1,1-butanediyldiphosphonate Trihydrate (Alendronate)

D. Vega, R. Baggio and M. T. Garland

Formula: Na+.C4H12NO7P2-.3H2O



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Acta Cryst. (1996). C52, 2201-2204    [doi:10.1107/S0108270196005732]

Bis(acetato-O)bis(pyridine-N)palladium(II) Monohydrate and Bis(acetato-O)bis(diethylamine-N)palladium(II)

S. V. Kravtsova, I. P. Romm, A. I. Stash and V. K. Belsky

Formula: [Pd(C2H3O2)2(C5H5N)2].H2O and [Pd(C2H3O2)2(C4H11N)2]



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Acta Cryst. (1996). C52, 2204-2206    [doi:10.1107/S0108270196009134]

Aqua[bis(salicylidene)ethylenediaminato](isobutyl)cobalt(III)

H. Chen, D. Han, H. Yan, W. Tang, Y. Yang and W. Yang

Formula: [Co(C4H9)(C16H14N2O2)(H2O)]


organic compounds



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Acta Cryst. (1996). C52, 2207-2212    [doi:10.1107/S0108270196003551]

Dibutyl 2,6-Dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate, Diisobutyl 2,6-Dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate and Di-tert-butyl 2,6-Dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

K. R. Rowan and E. M. Holt

Formula: Three isomers of C23H30N2O6



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Acta Cryst. (1996). C52, 2212-2215    [doi:10.1107/S0108270196003563]

(E)-6-Chloro-3-[2-(4-chlorophenylsulfonyl)ethenyl]-4-chromanone, (E)-6-Bromo-3-[2-(4-bromophenylsulfonyl)ethenyl]-4-chromanone and (E)-3-[2-(4-Chlorophenylsulfonyl)ethenyl]-6-methoxy-4-chromanone

K. V. N. Raju, M. Krishnaiah, Y.-S. Chen, S. N. Rao and E. M. Holt

Formula: C17H10Cl2O4S, C17H10Br2O4S and C18H13ClO5S



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Acta Cryst. (1996). C52, 2216-2218    [doi:10.1107/S0108270196002855]

Trimethyl[2-(2-methyl-2-propenoyloxy)ethyl]ammonium Iodide (Methacryloylcholine Iodide)

O. Angelova, J. Macícek, K. Kossev and N. Koseva

Formula: C9H18NO2+.I-



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Acta Cryst. (1996). C52, 2218-2220    [doi:10.1107/S0108270196006452]

Crystalline Complexes Involving Amino Acids. II. (R)-(-)-1-Phenylglycinium Hydrogen Squarate Monohydrate

O. Angelova, R. Petrova, V. Radomirska and T. Kolev

Formula: C8H10NO2+.C4HO4-.H2O



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Acta Cryst. (1996). C52, 2221-2222    [doi:10.1107/S0108270196002107]

Redetermination of 1,7-Diphenyl-1,7-dicarba-closo-dodecaborane(12)

G. M. Rosair, A. J. Welch and A. S. Weller

Formula: C14H20B10



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Acta Cryst. (1996). C52, 2223-2225    [doi:10.1107/S0108270196004349]

1-Diisopropylphosphino-2-phenyl-1,2-dicarba-closo-dodecaborane(12)

R. Sillanpää, R. Kivekäs, F. Teixidor, C. Viñas and R. Nuñez

Formula: C14H29B10P



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Acta Cryst. (1996). C52, 2225-2229    [doi:10.1107/S0108270196004180]

cis-2-sec-Butyl-4-{4-[4-(4-{[2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl]methoxy}phenyl)-1-piperazinyl]phenyl}-2,4-dihydro-3H-1,2,4-triazol-3-one (Itraconazole)

O. M. Peeters, N. M. Blaton and C. J. De Ranter

Formula: C35H38Cl2N8O4



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Acta Cryst. (1996). C52, 2229-2231    [doi:10.1107/S0108270196004829]

Lupulin D

H. Chen, R. Tan, Z. Liu, J. Liu and M. Chen

Formula: C25H38O8



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Acta Cryst. (1996). C52, 2231-2236    [doi:10.1107/S010827019600371X]

Substituted Imidazonaphthyridine Derivatives. I. C19H14F3N3, C18H10F5N3, C18H11ClF3N3 and C18H11BrF3N3

H.-K. Fun, K. Sivakumar, S.-O. Chua, M.-F. Ooi, M. A. S. Anwair, E.-K. Gan and W. R. Jackson

Formula: C19H14F3N3, C18H10F5N3, C18H11ClF3N3 and C18H11BrF3N3



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Acta Cryst. (1996). C52, 2236-2239    [doi:10.1107/S0108270196003708]

Substituted Imidazonaphthyridine Derivatives. II. C19H17N3O and C24H19N3O

K. Sivakumar, H.-K. Fun, S.-O. Chua, M.-F. Ooi, M. A. S. Anwair, E.-K. Gan and W. R. Jackson

Formula: C19H17N3O and C24H19N3O



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Acta Cryst. (1996). C52, 2239-2243    [doi:10.1107/S0108270196003745]

Substituted Imidazonaphthyridine Derivatives. III. C24H28N4, C24H28N4O and C23H25BrN4

K. Sivakumar, H.-K. Fun, S.-O. Chua, M.-F. Ooi, M. A. S. Anwair, E.-K. Gan and W. R. Jackson

Formula: C24H28N4, C24H28N4O and C23H25BrN4



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Acta Cryst. (1996). C52, 2243-2245    [doi:10.1107/S0108270196004337]

Tris(4-chlorophenyl)phosphine and Tris(4-fluorophenyl)phosphine

O. bin Shawkataly, J. Singh, H.-K. Fun and Sivakumar K.

Formula: C18H12Cl3P and C18H12F3P



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Acta Cryst. (1996). C52, 2246-2248    [doi:10.1107/S0108270196003356]

N,N,N',N'-Tetramethylethylenediammonium Dihydrogendiphosphate Dihydrate

A. Gharbi, M. Charfi and A. Jouini

Formula: C6H18N22+.H2P2O72-.2H2O



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Acta Cryst. (1996). C52, 2248-2250    [doi:10.1107/S0108270196002922]

Tris(1,4-butanediyldiammonium) Bis(cyclotriphosphate) Tetrahydrate

H. Thabet and A. Jouini

Formula: 3C4H14N22+.2P3O93-.4H2O



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Acta Cryst. (1996). C52, 2250-2253    [doi:10.1107/S0108270196003344]

1,6-Hexanediammonium cyclo-Hexaphosphate Hexahydrate

M. Charfi and A. Jouini

Formula: 3C6H18N22+.P6O186-.6H2O



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Acta Cryst. (1996). C52, 2253-2254    [doi:10.1107/S0108270196003873]

A Dihydrooxazinone

H. Beck and E. Egert

Formula: C16H25NO4



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Acta Cryst. (1996). C52, 2254-2256    [doi:10.1107/S0108270196003885]

A Fully Cyclo-Substituted Cyclohexane

N. Schormann and E. Egert

Formula: C18H24O3



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Acta Cryst. (1996). C52, 2256-2258    [doi:10.1107/S0108270196004167]

2-(6-Methoxy-7-methyl-1,2,3,4-tetrahydro-1-naphthyl)ethyl 4,7,7-trimethyl-3-oxo-2-oxabicyclo[2.2.1]heptane-1-carboxylate

M. Noltemeyer, T. Raschke and L. F. Tietze

Formula: C24H32O5



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Acta Cryst. (1996). C52, 2258-2259    [doi:10.1107/S0108270196003897]

A Fluorinated D-Homoestrone Derivative

M. Noltemeyer, L. F. Tietze, J. Wölfling, É. Frank and G. Schneider

Formula: C26H31FN2O3



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Acta Cryst. (1996). C52, 2260-2261    [doi:10.1107/S0108270196005045]

Anticancer and Antifertility Agents. II. N,N'-Hexamethylenebis(3-pyridinecarboxamide)

Q. Liu, S.-W. Zhang, Y. G. Wei and M.-C. Shao

Formula: C18H22N4O2



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Acta Cryst. (1996). C52, 2261-2263    [doi:10.1107/S0108270196002417]

17[alpha]-Ethynyl-19-nor-3-oxo-4-androsten-17[beta]-yl Acetate (Norethindrone Acetate)

Th. Steiner

Formula: C22H28O3



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Acta Cryst. (1996). C52, 2263-2266    [doi:10.1107/S0108270196004490]

Triphenylpropargylphosphonium Bromide

Th. Steiner

Formula: C21H18P+.Br-



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Acta Cryst. (1996). C52, 2266-2269    [doi:10.1107/S0108270196004556]

Glycyl-L-histidinium Chloride Dihydrate: an Unusual Histidine Conformation

Th. Steiner

Formula: C8H13N4O3+.Cl-.2H2O



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Acta Cryst. (1996). C52, 2269-2271    [doi:10.1107/S0108270196003435]

Half-Chair Conformation of trans-1,4-Dimethyl-7,7-diphenylbicyclo[4.1.0]hepta-2,5-dione

H. Moriwaki, T. Kawamoto and T. Oshima

Formula: C21H20O2



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Acta Cryst. (1996). C52, 2271-2272    [doi:10.1107/S0108270196004453]

(1E,3Z,5E)-2,5-Diaza-1,6-bis(dimethylamino)-1,3,5-hexatriene-3,4-dicarbonitrile

H. Küçükbay, E. Çetinkaya, D. Ülkü and M. N. Tahir

Formula: C10H14N6



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Acta Cryst. (1996). C52, 2272-2274    [doi:10.1107/S0108270196004209]

Coumurrayin

Rajnikant, V. K. Gupta, A. Singh, M. Lal and B. Varghese

Formula: C16H18O4



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Acta Cryst. (1996). C52, 2274-2277    [doi:10.1107/S0108270196002375]

The Charge-Transfer Complex 4-(2-Hydroxyethyl)carbazole-2,3-Dichloro-5,6-dicyano-1,4-benzoquinone (1/1) (HEK-DDQ)

F. Qi, W.-T. Yu, L. Hong, X.-Y. Lin and Z.-P. Yu

Formula: C14H13NO.C8Cl2N2O2



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Acta Cryst. (1996). C52, 2277-2281    [doi:10.1107/S0108270196002156]

[beta]-Cyclodextrin Nonanoic Acid 1:1 Complex

A. Rontoyianni and I. M. Mavridis

Formula: 2C42H70O35.1.6C9H18O2.23.9H2O



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Acta Cryst. (1996). C52, 2281-2282    [doi:10.1107/S0108270196004003]

1-(4-Chlorophenyl)-3a-methyl-5-phenyl-3a,4-dihydro-1,2,4-oxadiazolo[4,5-a][1,5]benzodiazepine

A. Baouid, A. Hasnaoui, A. Benharref, M. Giorgi and M. Pierrot

Formula: C23H18ClN3O



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Acta Cryst. (1996). C52, 2283-2285    [doi:10.1107/S0108270196004684]

2,4,6-Tri-O-benzyl-myo-inositol

V. Graingeot, C. Brigando and D. Benlian

Formula: C27H30O6



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Acta Cryst. (1996). C52, 2285-2287    [doi:10.1107/S0108270196003411]

Methyl 6-O-[(R)-1-Carboxyethyl]-[alpha]-D-galactopyranoside

L. Eriksson, Å. Pilotti, R. Stenutz and G. Widmalm

Formula: C10H18O8



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Acta Cryst. (1996). C52, 2288-2290    [doi:10.1107/S0108270196002533]

21-Acetoxy-16[alpha]-propionoxy-11[beta],17[alpha]-dihydroxypregna-1,4-diene-3,20-dione Monohydrate

B. Pniewska, R. Anulewicz and T. Uszycka-Horawa

Formula: C26H34O8.H2O



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Acta Cryst. (1996). C52, 2290-2292    [doi:10.1107/S0108270196005744]

(RS)-4-p-Toluenesulfinylcyclohexa-1,4-dienecarboxylic Acid Ethyl Ester

R. Retoux, J. Molenkamp, E. Bonfand, P. Gosselin and C. Maignan

Formula: C16H18O3S



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Acta Cryst. (1996). C52, 2292-2294    [doi:10.1107/S0108270196004696]

A New Conformationally Restricted Aspartic Acid Analogue with a Bicyclo[2.2.2]octane Skeleton

E. Buñuel, C. Cativiela, M. D. Díaz-de-Villegas and J. A. Gálvez

Formula: C18H21NO5



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Acta Cryst. (1996). C52, 2294-2296    [doi:10.1107/S010827019600491X]

[3-(4-Methylphenyl)-5-isoxazolyl]acetonitrile

N. Kumar, S. Mukherjee, V. S. Parmar and W. Errington

Formula: C12H10N2O



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Acta Cryst. (1996). C52, 2296-2298    [doi:10.1107/S0108270196004088]

Bis[5,5-bis(4-methoxyphenyl)-3,3-dimethyl-2-tetrahydrofuranyl] Ether

J. C. Barnes, W. M. Horspool, G. Hynd, D. Armesto and A. Ramos

Formula: C40H46O7



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Acta Cryst. (1996). C52, 2298-2301    [doi:10.1107/S0108270196004908]

2,10-Dichloro-6-(2,4-dimethylphenoxy)dibenzo[d,g][1,3,6,2]dioxathiaphosphocine 6-Sulfide

M. Krishnaiah, N. J. Kumar, T. V. Narasaiah, B. S. Reddy and C. D. Reddy

Formula: C20H15Cl2O3PS2



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Acta Cryst. (1996). C52, 2301-2303    [doi:10.1107/S0108270196004039]

4-(5-Methyl-1,3,4-oxadiazol-2-yl)-1,3-phenylene Diacetate

I. Vencato, H. Gallardo and E. Meyer

Formula: C13H12N2O5



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Acta Cryst. (1996). C52, 2303-2305    [doi:10.1107/S0108270196002016]

4,4'-Bis(2,4,6-trimethylbenzenesulfonamido)diphenylmethane

M. Feigel, Th. Strassner, J. Manero and E. Weckert

Formula: C31H32N2O4S2



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Acta Cryst. (1996). C52, 2305-2307    [doi:10.1107/S0108270196003903]

Diethyl 5-Bis(diphenylphosphinoyl)methyl-2-hydroxy-3-tert-butylphenylphosphonate Hydrate at 173K

M. Ramm and B. Costisella

Formula: C39H43O6P3.H2O



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Acta Cryst. (1996). C52, 2307-2309    [doi:10.1107/S0108270196002843]

Isopropylamidinium Chloride

J. Barker and H. R. Powell

Formula: C4H11N2+.Cl-



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Acta Cryst. (1996). C52, 2309-2311    [doi:10.1107/S010827019600354X]

Diisopropylammonium Bromide

G. Kociok-Köhn, B. Lungwitz and A. C. Filippou

Formula: C6H16N+.Br-



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Acta Cryst. (1996). C52, 2311-2313    [doi:10.1107/S0108270196003861]

A Substituted cis,trans,cis,cis-[4.5.5.5]Fenestrene

J. Wang, M. Thommen and R. Keese

Formula: C14H18O2



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Acta Cryst. (1996). C52, 2313-2315    [doi:10.1107/S0108270196007950]

3a,7a-Dibromo-2-butyl-4,7-methano-1,3,3a,4,7,7a-hexahydro-2H-isoindole-1,3-dione from the Reaction of 3,4-Dibromo-1-butylmaleimide with Cyclopentadiene

R. L. Beddoes, Y. Zhao and J. A. Joule

Formula: C13H15Br2NO2



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Acta Cryst. (1996). C52, 2315-2317    [doi:10.1107/S0108270196004271]

5,15-Diaza-6,16-dihydroxytetrabenzo[b,e,k,n]perylene

J. Mizuguchi

Formula: C34H18N2O2



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Acta Cryst. (1996). C52, 2318-2320    [doi:10.1107/S0108270196003204]

4-(4-Chlorophenyl)-2,6-diphenyl-(4H)-pyran-3,5-dicarbaldehyde

R. Murugesan, S. Selladurai, K. Subramaniam, D. Velmurugan, J. R. Hamilton, Y.-S. Chen, P. J. Schapiro and S. N. Rao

Formula: C25H17ClO3



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Acta Cryst. (1996). C52, 2320-2323    [doi:10.1107/S0108270196003514]

Biphenyl-3-carboxylic Acid at 296 and 203K

A. C. Blackburn, A. J. Dobson and R. E. Gerkin

Formula: C13H10O2



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Acta Cryst. (1996). C52, 2323-2326    [doi:10.1107/S0108270196003769]

N-Saccharinperacetic Acid Monohydrate and N-Saccharinpentanoic Acid Monohydrate

N. Feeder and W. Jones

Formula: C9H7NO6S.H2O and C12H13NO5S.H2O



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Acta Cryst. (1996). C52, 2326-2332    [doi:10.1107/S0108270196002624]

Ammonium Salts of Phosphoglycolic Acid (H3PG): NH4. H2PG, 3NH4. H2PG. HPG, 2NH4. HPG and 3NH4.PG.H2O at 150K

T. Lis

Formula: NH4+.C2H4O6P-, 3NH4+.C2H3O6P2-.C2H4O6P-, 2NH4+.C2H3O6P2- and 3NH4+.C2H2O6P3-.H2O



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Acta Cryst. (1996). C52, 2332-2334    [doi:10.1107/S0108270196002582]

4-Amino-1-(2-deoxy-[beta]-D-ribofuranosyl)-6,7-dihydro-1H,5H-cyclopentapyrimidine-2-one

S. Neidle, D. C. Capaldi, C. B. Reese and P. D. Roselt

Formula: C12H17N3O4



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Acta Cryst. (1996). C52, 2334-2337    [doi:10.1107/S0108270196001576]

(E)-2,2,5,5-Tetramethyl-3,4-bis[4-(tribromomethyl)phenyl]hex-3-ene

J. E. Gano, K. Kirschbaum and P. Sekher

Formula: C24H26Br6



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Acta Cryst. (1996). C52, 2337-2340    [doi:10.1107/S010827019600621X]

Racemic [alpha],[alpha]'-o-Xylylene-1,1'-bis[(3,5-dimethyl-5,6-dihydro-1,3,5-triazine-6-spiro-9'-fluorene)-2,4(1H,3H)-dione]

P. D. Robinson, Y. Gong and M. J. Bausch

Formula: C42H36N6O4



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Acta Cryst. (1996). C52, 2340-2343    [doi:10.1107/S0108270196002272]

Packing of Four Independent Molecules: 1-Methyl-N,N'-bis(salicylidene)-2,4-phenylenediamine

N. W. Alcock, H. J. Clase, G. R. Willey and L. T. Daly

Formula: C21H18N2O2



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Acta Cryst. (1996). C52, 2343-2345    [doi:10.1107/S0108270196003332]

O-Acetyl-N-(o-hydroxybenzyl)-N-isopropylhydroxylamine

M. S. Hussain and M. Ul-Haque

Formula: C12H17NO3



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Acta Cryst. (1996). C52, 2345-2347    [doi:10.1107/S0108270196003368]

3-Hydroxyanthranilic Acid Hydrochloride

N. Okabe, A. Shimosaki and J. Miura

Formula: C7H8NO3+.Cl-



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Acta Cryst. (1996). C52, 2347-2349    [doi:10.1107/S0108270196006245]

9,10,12,14-Tetrahydro-12,12,14,14-tetraphenyl-9,10[3',4']-furanoanthracene

T. Y. Fu, G. Olovsson, J. R. Scheffer and J. Trotter

Formula: C42H30O



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Acta Cryst. (1996). C52, 2349-2351    [doi:10.1107/S0108270196004441]

C20H10F8, a Divinyl Acetylene

D. C. Swenson, P. A. Morken and D. J. Burton

Formula: C20H10F8



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Acta Cryst. (1996). C52, 2351-2353    [doi:10.1107/S0108270196004465]

1,3,5-Tri-tert-butyl-5-(1,3,5-tri-tert-butyl-4-oxo-2,5-cyclohexadienyl)methylbicyclo[4.1.0]hept-3-en-2-one, a Highly Hindered Propane

A. Rieker, M. Neumayer and W. Hiller

Formula: C38H62O2



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Acta Cryst. (1996). C52, 2354-2356    [doi:10.1107/S0108270196004210]

Structures of the Diels-Alder Reaction Products of Thymoquinone and 1-Vinylcyclohexene. III. 5-Isopropyl-2-methyltricyclo[8.4.0.02,7]tetradeca-4,9-diene-3,6-dione, C18H24O2

J. Zukerman-Schpector, I. Caracelli, F. Silva Jnr and T. J. Brocksom

Formula: C18H24O2



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Acta Cryst. (1996). C52, 2356-2359    [doi:10.1107/S0108270196004611]

Methyl 2,7,7-Trimethyl-4-(3-nitrophenyl)-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate and 3-Acetyl-2,7,7-trimethyl-4-phenyl-1,4,5,6,7,8-hexahydro-5-quinolone

A. D. Morales, S. García-Granda, M. S. Navarro, A. M. Diviú and R. E. Pérez-Barquero

Formula: C20H22N2O5 and C20H23NO2



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Acta Cryst. (1996). C52, 2359-2363    [doi:10.1107/S0108270196004866]

The Anhydrous Racemate of the Carcinostatic Agent Cyclophosphamide and the Bicyclic Degradation Product 1-(2-Chloroethyl)tetrahydro-1H,5H-1,3,2-diazaphospholo[2,1-b][1,3,2]oxazaphosphorine 9-Oxide

P. G. Jones, H. Thönnessen, A. Fischer, I. Neda, R. Schmutzler, J. Engel, B. Kutscher and U. Niemeyer

Formula: C7H15Cl2N2O2P and C7H14ClN2O2P



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Acta Cryst. (1996). C52, 2363-2365    [doi:10.1107/S0108270196004362]

Coumarin 338

T. Honda, I. Fujii, N. Hirayama, N. Aoyama and A. Miike

Formula: C20H23NO4



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Acta Cryst. (1996). C52, 2365-2367    [doi:10.1107/S0108270196004350]

Structural Studies of Mitomycins. VIII. Mitomycin D Hydrate, C15H18N4O5.1.5H2O

N. Hirayama, H. Arai and M. Kasai

Formula: C15H18N4O5.1.5H2O



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Acta Cryst. (1996). C52, 2367-2370    [doi:10.1107/S0108270196004428]

Acetone 4,4-Dimethyl-5-oxo-2-pyrazolin-3-ylhydrazone

C. Y. Meyers, H. G. Lutfi, V. M. Kolb, Y. Hou and P. D. Robinson

Formula: C8H14N4O



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Acta Cryst. (1996). C52, 2370-2372    [doi:10.1107/S0108270196004891]

Racemic 3,6-Dimethyl-3,6-bis(tert-butyldimethylsilyloxy)-1,7-cyclododecadiyne

C. Boss, R. Keese and M. Förtsch

Formula: C26H48O2Si2



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Acta Cryst. (1996). C52, 2372-2376    [doi:10.1107/S0108270196004933]

2-Carboxy- and 2,7-Dicarboxy-4,5-benzotropone: Hydrogen-Bonding Patterns of a [beta]-Keto Acid and a Related [beta]-Keto 1,5-Diacid

H. W. Thompson, R. A. Lalancette and M. L. Coté

Formula: C12H8O3 and C13H8O5



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Acta Cryst. (1996). C52, 2377-2379    [doi:10.1107/S0108270195011000]

Biological Activity of 4-(4-Bromophenyl)thiosemicarbazide

S. Seth, A. Biswas, A. Banerjee, S. K. Chattopadhyay and S. Ghosh

Formula: C7H8BrN3S


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Acta Cryst. (1996). C52, 2380    [doi:10.1107/S0108270196099738]

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