Acta Crystallographica Section C

Crystal Structure Communications

Volume 52, Part 11 (November 1996)


Cover illustrationCover illustration: Reinvestigation of Crystalline Sulfuric Acid and Oxonium Hydrogensulfate, see Kemmitz, Werner & Trojanov, pages 2665-2668. Displacement ellipsoids are shown at the 50% probability level.

inorganic compounds



Acta Cryst. (1996). C52, 2645-2647    [ doi:10.1107/S0108270196006907 ]

Triammonium Trimetaphosphimate Monohydrate

N. Stock and W. Schnick

Synopsis: (NH4)3(PO2NH)3.H2O contains trimetaphosphimate anions, ammonium cations and water molecules linked by N-H...O and O-H...O hydrogen bonds.

Formula: (NH4)3(PO2NH)3.H2O



Acta Cryst. (1996). C52, 2647-2650    [ doi:10.1107/S0108270196007056 ]

Refinement of the Superstructure of C-Type Chromium(III) Tris(metaphosphate), Cr(PO3)3

M. Gruss and R. Glaum

Synopsis: The superstructure of C-type Cr(PO3)3 has been refined from single-crystal data. The CrO6 octahedra are only slightly distorted and the PO4 tetrahedra show typical geometry for metaphosphate chains.

Formula: Cr(PO3)3



Acta Cryst. (1996). C52, 2650-2652    [ doi:10.1107/S0108270196004398 ]

Tetracarbonyl(tetraphosphorus hexaoxide)iron

M. Jansen and J. Clade

Synopsis: The Fe atom in [Fe(CO)4(P4O6)] has trigonal-bipyramidal coordination geometry and the axial P4O6 unit shows distortions similar to those observed within the series P4O6X (X = O, S, Se).

Formula: [Fe(CO)4(P4O6)]



Acta Cryst. (1996). C52, 2652-2655    [ doi:10.1107/S010827019600724X ]

A New Quaternary Borocarbide, GdRh2B2C

J. Ye, T. Shishido, T. Kimura, T. Matsumoto and T. Fukuda

Synopsis: The structure of GdRh2B2C consists of tetrahedrally coordinated Rh2B2 layers and GdC NaCl-type layers which stack alternately along [001] via short B-C bonds.

Formula: GdRh2B2C



Acta Cryst. (1996). C52, 2655-2660    [ doi:10.1107/S0108270196007366 ]

Na8H18[{Er3O(OH)3(H2O)3}2Al2-(Nb6O19)5].40.5H2O

H. Naruke and T. Yamase

Synopsis: The structure of the [{Er3O(OH)3(H2O)3}2Al2(Nb6O19)5]26- anion is compared with that within the isomorphous Eu complex. The smaller ionic radius of Er3+ induces a contraction of the central [{Ln3O(OH)3(H2O)3}2]8+ cluster with a resultant attraction of the five [Nb6O19]8- groups towards the anion centre.

Formula: Na8H18[{Er3O(OH)3(H2O)3}2Al2(Nb6O19)5].40.5H2O



Acta Cryst. (1996). C52, 2660-2662    [ doi:10.1107/S0108270196006762 ]

The First Beryllium Periodate: Be(H4IO6)2.4H2O

Z. Zhang, H. D. Lutz, M. Georgiev and M. Maneva

Synopsis: The crystal structure of Be(H4IO6)2.4H2O has been established by single-crystal X-ray methods. Two of the H atoms within the [H4IO6]- anion are disordered over split positions.

Formula: Be(H4IO6)2.4H2O



Acta Cryst. (1996). C52, 2662-2664    [ doi:10.1107/S0108270196007378 ]

K2Be2Si3O9, a Potassium Beryllium Silicate Framework Built from Edge-Sharing Be-O Tetrahedra and Three-Ring Silicate Tetrahedra

X. Bu, T. E. Gier and G. D. Stucky

Synopsis: This new potassium beryllium silicate resulted from a high temperature and high pressure synthesis. It has a framework structure built from trimers of silicate tetrahedra and edge-sharing Be-O tetrahedra, and possesses one-dimensional channels along the b axis.

Formula: K2Be2Si3O9



Acta Cryst. (1996). C52, 2665-2668    [ doi:10.1107/S0108270196006749 ]

Reinvestigation of Crystalline Sulfuric Acid and Oxonium Hydrogensulfate

E. Kemnitz, C. Werner and S. Trojanov

Synopsis: The structure of H2SO4 consists of H2SO4 molecules connected by hydrogen bonds to form 44 nets. In (H3O)(HSO4), hydrogen bonding results in the formation of double layers consisting of (HSO4)n chains linked by (H3O) ions.

Formula: H2SO4 and (H3O)(HSO4)



Acta Cryst. (1996). C52, 2668-2670    [ doi:10.1107/S0108270196007883 ]

(NH4)2(VO)(VP)O7, a Layered Structure Comprising Tetrahedral VPO7 Groups

S. Boudin, A. Grandin, P. Labbé and B. Raveau

Synopsis: (NH4)2(VO)(VP)O7 contains [(VO)(VP)O7][infinity] layers consisting of divanadophosphate VPO7 groups and VO5 square pyramids, and layers of NH4+ ions.

Formula: (NH4)2(VO)(VP)O7


metal-organic compounds



Acta Cryst. (1996). C52, 2671-2674    [ doi:10.1107/S010827019600666X ]

Bis(tetraethylammonium) Tetrachlorometallates, [(C2H5)4N]2[MCl4], where M = Hg, Cd, Zn

A. Mahoui, J. Lapasset, J. Moret and P. Saint Grégoire

Formula: (C8H20N)2[HgCl4], (C8H20N)2[CdCl4] and (C8H20N)2[ZnCl4]



Acta Cryst. (1996). C52, 2674-2676    [ doi:10.1107/S0108270196009031 ]

Tetraethylammonium Tetramethylammonium Tetrachlorocuprate(II), [(C2H5)4N][(CH3)4N][CuCl4]

A. Mahoui, J. Lapasset, J. Moret and P. Saint Grégoire

Formula: (C8H20N)(C4H12N)[CuCl4]



Acta Cryst. (1996). C52, 2676-2678    [ doi:10.1107/S0108270196008529 ]

Bis[4-(5-chloro-2-hydroxyphenylimino-N,O:O)-2-penten-2-olato(2-)-O]dicopper(II)

M. N. Tahir, D. Ülkü, O. Atakol and A. Akay

Formula: [Cu2(C11H10ClNO2)2]



Acta Cryst. (1996). C52, 2678-2680    [ doi:10.1107/S0108270196009298 ]

Poly[bis(3,5-dinitrobenzoato-O1:O2)disilver(I)-O2:Ag;Ag':O2']

D. Ülkü, M. N. Tahir and E. M. Movsumov

Formula: [Ag2(C7H3N2O6)2]



Acta Cryst. (1996). C52, 2680-2682    [ doi:10.1107/S0108270196009407 ]

Bis[N-(2,6-dimethylphenyl)aminoglyoximato-N,N']nickel(II)

D. Ülkü, F. Ercan, M. Macit and A. Gülce

Formula: [Ni(C10H12N3O2)2]



Acta Cryst. (1996). C52, 2682-2684    [ doi:10.1107/S010827019600964X ]

(Diethylamine-N){4-methyl-2-[(2-oxidobenzylidene)amino]phenolato(2-)-O,N,O'}nickel(II)

F. Ercan, M. Sari, R. Yagbasan, M. Tastekin and L. Aksu

Formula: [Ni(C14H11NO2)(C4H11N)]



Acta Cryst. (1996). C52, 2684-2687    [ doi:10.1107/S0108270196008724 ]

trans-(5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene-N,N',N'',N''')di(isothiocyanato-N)cobalt(III) Thiocyanate

T.-H. Lu, T. H. Tahirov, B.-H. Chen, C.-Y. Lai and C.-S. Chung

Formula: [Co(NCS)2(C16H32N4)](SCN)



Acta Cryst. (1996). C52, 2687-2689    [ doi:10.1107/S0108270196007925 ]

Aqua(1,5,8,12-tetramethyl-1,4,8,11-tetraazacyclotetradecane-N,N',N'',N''')copper(II) Diperchlorate

T. H. Tahirov, T.-H. Lu, F.-L. Liao, S.-L. Wang, B.-H. Chen, T.-Y. Chi and C.-S. Chung

Formula: [Cu(C14H32N4)(H2O)](ClO4)2



Acta Cryst. (1996). C52, 2689-2691    [ doi:10.1107/S0108270196008505 ]

catena-Poly[[(diethylenetriamine-N,N',N'')copper(II)]-[bold mu]-succinato-O,O':O'']

A. Pajunen, S. Pajunen, J. Kivikoski and J. Valkonen

Formula: [Cu(C4H4O4)(C4H13N3)]



Acta Cryst. (1996). C52, 2691-2693    [ doi:10.1107/S0108270196008670 ]

[1,3-Bis(diphenylphosphino)propane-P,P'](1,3-propanedithiolato-S,S')palladium(II) Acetonitrile Solvate, [Pd{Ph2P(CH2)3PPh2}(SC3H6S)].CH3CN

W. Su, M. Hong, Z. Zhou, F. Xue, H. Liu and T. C. W. Mak

Formula: [Pd(C3H6S2)(C27H26P2)].CH3CN



Acta Cryst. (1996). C52, 2693-2695    [ doi:10.1107/S0108270196007937 ]

Hexaaquacobalt(II) Bis[(2-Hydroxy-1,3-propanediamine-N,N,N',N'-tetraacetato)cobalt(III)]

X.-M. Chen, H.-A. Chen, B.-M. Wu and T. C. W. Mak

Formula: [Co(H2O)6][Co(C11H14N2O9)]2



Acta Cryst. (1996). C52, 2696-2698    [ doi:10.1107/S0108270196009778 ]

[N,N'-Bis(2-thiobenzylidene)-1,2-dimethyl-4,5-phenylenediaminato]nickel(II), Ni(tsaldimph)

R. K. Henderson, E. Bouwman, J. Reedijk and A. K. Powell

Formula: [Ni(C22H18N2S2)]



Acta Cryst. (1996). C52, 2698-2701    [ doi:10.1107/S010827019600981X ]

A Dinuclear Nickel(II) Compound: [bold mu]-{N,N,N',N'-Tetrakis[2-(3,5-dimethyl-1-pyrazolyl)ethyl]-1,2-ethylenediamine}-bis[aqua(nitrato-O,O')nickel(II)] Dinitrate Dimethanol Solvate

N. Veldman, A. L. Spek, G. Tabbì, W. L. Driessen and J. Reedijk

Formula: [Ni2(NO3)2(C30H48N10)(H2O)2](NO3)2.2CH4O



Acta Cryst. (1996). C52, 2701-2703    [ doi:10.1107/S0108270196008165 ]

Photochemical Reactions of Transition Metal Organyl Complexes with Olefins. 15. Tricarbonyl([bold eta]4-1,3-butadiene)-[bold mu]-hydrido-([bold mu]-[bold eta]1:5-indene-1,1-diyl)([bold eta]5-indenyl)-dimolybdenum(Mo-Mo)

C. G. Kreiter, R. Meuser, W. Frank and S. Müller-Becker

Formula: [Mo2(H)(C9H6)(C9H7)(C4H6)(CO)3]



Acta Cryst. (1996). C52, 2703-2705    [ doi:10.1107/S0108270196007998 ]

Bis[(1,2,5,6-[bold eta])-1,5-cyclooctadiene]-di-[bold mu]-ethoxo-dirhodium(I)

M. Ramm and D. Selent

Formula: [Rh2(C2H5O)2(C8H12)2]



Acta Cryst. (1996). C52, 2705-2707    [ doi:10.1107/S0108270196008281 ]

[N-(2-Mercaptophenyl)-2-hydroxynaphthaldiminato](pyridine)nickel(II)

Y. Elerman and I. Svoboda

Formula: [Ni(C17H11NOS)(C5H5N)]



Acta Cryst. (1996). C52, 2707-2710    [ doi:10.1107/S0108270196008116 ]

Chloro(2,3,7,8,12,13,17,18-octaethylporphinato)gallium(III)

K. E. Brancato-Buentello, A. G. Coutsolelos and W. R. Scheidt

Formula: [Ga(C36H44N4)Cl].1.45CH2Cl2



Acta Cryst. (1996). C52, 2710-2713    [ doi:10.1107/S010827019600950X ]

3-Chloro-3,3-bis(triphenylphosphine-P)-1,2-dicarba-3-rhoda-closo-dodecaborane- Dichloromethane (1/1.1)

G. Ferguson, P. A. McEneaney and T. R. Spalding

Formula: [RhCl(C2H11B9)(C18H15P)2].1.1CH2Cl2



Acta Cryst. (1996). C52, 2713-2716    [ doi:10.1107/S0108270196009183 ]

(4-Nitrophenyl 1,3,5,8,12-pentaazacyclotetradec-3-yl ketone-N1,N5,N8,N12)copper(II) Dinitrate

N. Sardone and M. Licchelli

Formula: [Cu(C16H26N6O3)](NO3)2



Acta Cryst. (1996). C52, 2716-2720    [ doi:10.1107/S0108270196007044 ]

Ammonium, Potassium and Lithium Salts of D, L-Glyceric Acid

T. Popek and T. Lis

Formula: NH4+.C3H5O4-, K+.C3H5O4- and Li+.C3H5O4-



Acta Cryst. (1996). C52, 2720-2724    [ doi:10.1107/S0108270196007445 ]

Acid Salts of Phosphoenolpyruvic Acid (H3PEP): NaH5(PEP)2.2H2O and KH5(PEP)2

T. Lis

Formula: Na+.C6H9O12P2-.2H2O and K+.C3H4O6P-.C3H5O6P



Acta Cryst. (1996). C52, 2724-2726    [ doi:10.1107/S0108270196004040 ]

(Dimercaptomethylenepropanedinitrilato-S,S')(pyridine)(triphenylphosphine)palladium(II)-Acetonitrile (1/1)

D.-L. Long, X.-Q. Xin and X.-Y. Huang

Formula: [Pd(C4N2S2)(C5H5N)(C18H15P)].C2H3N



Acta Cryst. (1996). C52, 2726-2728    [ doi:10.1107/S0108270196007640 ]

1-Hydroxy-2,1[bold lambda]5-benzoxarsol-3-one Monohydrate

M. S. Hundal, G. Hundal and S. S. Parmar

Formula: C7H5AsO3.H2O



Acta Cryst. (1996). C52, 2729-2731    [ doi:10.1107/S0108270196006786 ]

Caesium Iodide Complex of 1,3-Calix[4]-bis-crown-6

P. Thuéry, M. Nierlich, V. Lamare, J.-F. Dozol, Z. Asfari and J. Vicens

Formula: [Cs2I2(C48H60O12)].2C2H3N



Acta Cryst. (1996). C52, 2731-2734    [ doi:10.1107/S0108270196001308 ]

A Mixed-Metal Pentanuclear Complex Containing Linked NiIIN2S2 and CuII Units

S. Fox, R. T. Stibrany, J. A. Potenza and H. J. Schugar

Formula: [Cu3Ni2I3(C14H28N2S2)2].2C2H3N



Acta Cryst. (1996). C52, 2734-2736    [ doi:10.1107/S0108270196008785 ]

Tris{2-[(4-chlorophenyl)iminomethyl]pyrrolato-N,N'}cobalt(III)

J. A. Castro, J. Romero, J. A. García-Vázquez, A. Sousa and A. Castiñeiras

Formula: [Co(C11H8ClN2)3]



Acta Cryst. (1996). C52, 2736-2738    [ doi:10.1107/S0108270196009079 ]

7-Methyl-3-adeninium Trichloro(7-methyladenine-N9)zinc(II) Hydrate

C. L. Price and M. R. Taylor

Formula: (C6H8N5)[ZnCl3(C6H7N5)].H2O



Acta Cryst. (1996). C52, 2738-2740    [ doi:10.1107/S0108270196008608 ]

Bis(pyridine-2-thione)-2[bold kappa]S;3[bold kappa]S-tetra-[bold mu]-sulfido-1:2[bold kappa]4S;1:3[bold kappa]4S-bis(triphenylphosphine)-2[bold kappa]P;3[bold kappa]P-dicoppermolybdenum Bis(dichloromethane) Solvate

Q. Wang, X. Wu, Q. Huang and T. Sheng

Formula: [Cu2MoS4(C5H5NS)2(C18H15P)2].2CH2Cl2



Acta Cryst. (1996). C52, 2740-2742    [ doi:10.1107/S0108270196008852 ]

Aquatris(2,6-difluorobenzoato)praseodymium(III)

A. G. Karipides, J. Jai-nhuknan and J. S. Cantrell

Formula: [Pr(C7H3F2O2)3(H2O)]



Acta Cryst. (1996). C52, 2742-2745    [ doi:10.1107/S010827019600933X ]

Dichloro[N,N'-ethylenebis(3-tert-butyl-5-methylsalicylideneiminato)-N,N',O,O']titanium(IV), [TiCl2(C26H34N2O2)]

T. Repo, M. Klinga, M. Leskelä, P. Pietikäinen and G. Brunow

Formula: [TiCl2(C26H34N2O2)]



Acta Cryst. (1996). C52, 2745-2747    [ doi:10.1107/S0108270196009651 ]

Dicyano(2,9-dimethyl-1,10-phenanthroline-N,N')([bold eta]2-ethene)platinum(II)

A. Tuzi and B. Panunzi

Formula: [Pt(CN)2(C2H4)(C14H12N2)]



Acta Cryst. (1996). C52, 2747-2750    [ doi:10.1107/S0108270196009286 ]

An Unexpected Trimethylstannylpyrrole from a Stannylated Derivative of Tosylmethyl Isocyanide (TosMIC) and Chalcone

A. Meetsma, H. P. Dijkstra, R. ten Have and A. M. van Leusen

Formula: [Sn(CH3)3(C22H20NO3)]



Acta Cryst. (1996). C52, 2750-2752    [ doi:10.1107/S0108270196008359 ]

N-Chloro(methyl)arsino-N,N'-dimethyl-N'-(p-tolylthio)urea

P. G. Jones, A. K. Fischer, C. Müller, V. A. Pinchuk and R. Schmutzler

Formula: C11H16AsClN2OS



Acta Cryst. (1996). C52, 2752-2754    [ doi:10.1107/S0108270196005793 ]

A [bold mu]-Oxamidato-Bridged Dinuclear Copper(II) Complex

Z.-N. Chen, Q. Jun, W.-X. Tang, J. Chen and P.-J. Zheng

Formula: [Cu2(C6H12N4O2)(C8H6N2)2(H2O)2](ClO4)2



Acta Cryst. (1996). C52, 2754-2757    [ doi:10.1107/S0108270196008037 ]

Triple-Decker [Cp*Fe(C8H6)Fe(C8H7)]

A. Alvarez-Larena, J. L. Briansó, J. F. Piniella, J. Farran, J. M. Manríquez, I. Chávez, B. Oelckers, E. Molins and C. Miravitlles

Formula: [Fe2(C8H7)(C10H15)(C8H6)]



Acta Cryst. (1996). C52, 2757-2760    [ doi:10.1107/S0108270196010165 ]

(SS*,1S*,2R*)-1-(Hydroxymethyl)-2-(p-tolylsulfinyl)ferrocene

P. D. Robinson, D. H. Hua, N. M. Lagneau and J. Chen

Formula: [Fe(C13H13O2S)(C5H5)]



Acta Cryst. (1996). C52, 2760-2763    [ doi:10.1107/S010827019600858X ]

Hydrogen Bis[(8-quinolinol-N)(8-quinolinolato-N,O)(triphenylphosphine-P)silver(I)] Acetate Monohydrate

A. H. Othman, S.-C. Goh, H.-K. Fun and K. Sivakumar

Formula: [Ag2H(C9H6NO)2(C9H7NO)2(C18H15P)2](C2H3O2).H2O



Acta Cryst. (1996). C52, 2763-2766    [ doi:10.1107/S0108270196008578 ]

Aqua(3,5-dimethylpyrazole)(N-salicylideneglycinato)copper(II)

S. A. Warda, C. Friebel, J. Sivý, G. Plesch and O. Svajlenová

Formula: [Cu(C9H7NO3)(C5H8N2)(H2O)]



Acta Cryst. (1996). C52, 2766-2768    [ doi:10.1107/S010827019600577X ]

mer-Triaqua(chloranilato-O,O')chloroiron(III) Pentahydrate

B. F. Abrahams, B. F. Hoskins and R. Robson

Formula: [FeCl(C6Cl2O4)(H2O)3].5H2O



Acta Cryst. (1996). C52, 2768-2770    [ doi:10.1107/S0108270196006579 ]

Chloro[N,N'-ethylenebis(3-imino-1-phenyl-1-butanonato-N,O)]manganese(III), [MnCl(C22H22N2O2)]

Y.-L. Feng and S.-X. Liu

Formula: [MnCl(C22H22N2O2)]


organic compounds



Acta Cryst. (1996). C52, 2771-2772    [ doi:10.1107/S0108270196007317 ]

3-Benzyl-5-(2-fluorobenzylidene)imidazolidine-2,4-dione

C. A. De Simone, M. A. Pereira, C. Luu-Duc, I. R. Pitta, S. L. Galdino, E. H. C. Menezes and J. Zukerman-Schpector

Formula: C17H13FN2O2



Acta Cryst. (1996). C52, 2772-2774    [ doi:10.1107/S0108270196008256 ]

(Z)-1-(Dichloro-p-methoxyphenyltelluro)-1-phenyl-2-thiophenylethene

J. Zukerman-Schpector, I. Caracelli, M. J. Dabdoub, V. B. Dabdoub and M. A. Pereira

Formula: C21H18Cl2OSTe



Acta Cryst. (1996). C52, 2775-2777    [ doi:10.1107/S0108270196008487 ]

The Acetyl Derivative of a Novel Fries Rearrangement Product

S. C. Jain, S. Talwar, R. Kumar, B. R. Babu and W. Errington

Formula: C26H18O8



Acta Cryst. (1996). C52, 2777-2779    [ doi:10.1107/S0108270196007159 ]

2-{1-[(2-Amino-4,5-dimethylphenyl)imino]ethyl}phenol

J. P. Corden, P. R. Bishop, W. Errington and M. G. H. Wallbridge

Formula: C16H18N2O



Acta Cryst. (1996). C52, 2779-2781    [ doi:10.1107/S0108270196010153 ]

A Sulfonyl-Substituted Aziridine

W. Clegg, S. L. Heath, L. Horsburgh, R. F. W. Jackson and A. Wood

Formula: C14H19NO4S



Acta Cryst. (1996). C52, 2781-2783    [ doi:10.1107/S0108270196010141 ]

A Sulfoximidooxirane

W. Clegg, M. R. J. Elsegood, R. F. W. Jackson, P. L. Bailey and A. D. Briggs

Formula: C16H17NO4S2



Acta Cryst. (1996). C52, 2783-2785    [ doi:10.1107/S0108270196008347 ]

trans-4-tert-Butylcyclohexyl 2,4-Dinitrobenzenesulfenate

J. M. White, J. Giordano and A. J. Green

Formula: C16H22N2O5S



Acta Cryst. (1996). C52, 2785-2787    [ doi:10.1107/S0108270196008062 ]

3-[1,2-Dicarba-closo-dodecacarboranyl(methyleneoxy)]benzonitrile

J. M. White, S. A. Bateman, D. P. Kelly and R. F. Martin

Formula: C10H17B10NO



Acta Cryst. (1996). C52, 2787-2789    [ doi:10.1107/S0108270196001746 ]

Studies on Condensed Heterocyclic Compounds. XIII. 6-(4-Methylphenyl)-3-(1-naphthylmethylene)-s-triazolo[3,4-b][1,3,4]thiadiazole

Z.-Y. Zhang, N. Zou, Y. Zhu, L. Zhao and M. Li

Formula: C21H16N4S



Acta Cryst. (1996). C52, 2789-2791    [ doi:10.1107/S0108270196007597 ]

(2,4-Dinitrophenyl)(10-methyl-3-phenothiazinyl)diazene Hemimethanol Solvate

Y. Zhu, B. Liu, Q.-X. Guo and Y.-C. Liu

Formula: C19H13N5O4S.0.5CH4O



Acta Cryst. (1996). C52, 2791-2793    [ doi:10.1107/S010827019600131X ]

A Pyridine-2,6(1H,3H)-dione Alkaloid

Y. Zhu, Z.-J. Jia, J.-G. Shi and H.-Q. Wang

Formula: C10H13NO5



Acta Cryst. (1996). C52, 2793-2795    [ doi:10.1107/S0108270196007962 ]

1,7-Dimethyl-5-phenyl-2-(3-thenoylaminomethyl)-2,3-dihydro-1H-1,4-benzodiazepin-4-ium Chloride

N. M. Blaton, O. M. Peeters and C. J. De Ranter

Formula: C23H24N3OS+.Cl-



Acta Cryst. (1996). C52, 2795-2797    [ doi:10.1107/S010827019600710X ]

(-)-(R)-N-[(3,4-Dihydro-2H-1-benzopyran-2-yl)methyl]-N'-(1,4,5,6-tetrahydro-2-pyrimidyl)-1,3-propanediaminium Dibromide

O. M. Peeters, N. M. Blaton and C. J. De Ranter

Formula: C17H28N4O2+.2Br-



Acta Cryst. (1996). C52, 2797-2800    [ doi:10.1107/S0108270196005197 ]

Two Photoproducts Derived from 11,12-Dibenzoyl-9,10-dihydro-9,10-dimethoxy-9,10-ethenoanthracene

S. A. Kumar, T. Mathew, S. Das, N. P. Rath and M. V. George

Formula: C32H24O4.0.5CH4O and C33H28O5



Acta Cryst. (1996). C52, 2800-2802    [ doi:10.1107/S0108270196007238 ]

The Photoproduct Derived from 9-Cyanodibenzobarrelene

M. Muneer, M. V. George and N. P. Rath

Formula: C31H19NO2



Acta Cryst. (1996). C52, 2802-2805    [ doi:10.1107/S0108270196003770 ]

Bis(o-aminophénylammonium) Bis(o-phénylènediammonium) cyclo-Hexaphosphate Dihydrate

E. H. Soumhi et T. Jouini

Formula: 2C6H9N2+.2C6H10N22+.P6O186-.2H2O



Acta Cryst. (1996). C52, 2805-2806    [ doi:10.1107/S0108270196008840 ]

(1S,5R,6R,8R,10R,12R)-5,8,15,15-Tetramethyl-6-phenyl-7,9-dioxa-3-thia-4-azatetracyclo[10.2.1.01,10.04,8]pentadecane 3,3-Dioxide

M. Bolte and C. Strahringer

Formula: C21H29NO4S



Acta Cryst. (1996). C52, 2807-2809    [ doi:10.1107/S0108270196007913 ]

Two Nitro-[alpha]-methoxy-trans-chalcones

M. Bolte, G. Schütz and H. J. Bader

Formula: Two isomers of C16H13NO4



Acta Cryst. (1996). C52, 2810-2811    [ doi:10.1107/S0108270196006865 ]

1,3-Bis(2,6-diisopropylphenyl)-2,2,4,4-tetramethyl-1,3-diaza-2,4-disilacyclobutane

S. A. A. Shah, H. W. Roesky, P. Lubini and H.-G. Schmidt

Formula: C28H46N2Si2



Acta Cryst. (1996). C52, 2811-2814    [ doi:10.1107/S0108270196008530 ]

3,3,6,6-Tetramethyl-9-(2-nitrophenyl)-3,4,5,6,9,10-hexahydroacridine-1,8(2H,7H)-dione

M. Brito-Arias, G. Ramirez, R. E. Rivas, E. Molins and W. Maniukiewicz

Formula: C23H26N2O4



Acta Cryst. (1996). C52, 2814-2818    [ doi:10.1107/S0108270196007020 ]

Two C-Unsubstituted Enaminals

A. J. Blake, H. McNab, L. C. Monahan, S. Parsons and E. Stevenson

Formula: C9H17NO and C12H13NO



Acta Cryst. (1996). C52, 2818-2822    [ doi:10.1107/S0108270196008232 ]

4-Methyl-1,2,4-triazole and 1-Methyltetrazole

M. H. Palmer and S. Parsons

Formula: C3H5N3 and C2H4N4



Acta Cryst. (1996). C52, 2822-2826    [ doi:10.1107/S0108270196008499 ]

17[beta]-Isopropylsparteine and 17[beta]-Isopropyllupanine Perchlorates

I. Wolska, T. Borowiak and Wl. Boczon

Formula: C18H34N22+.2ClO4- and C18H31N2O+.ClO4-.H2O



Acta Cryst. (1996). C52, 2826-2830    [ doi:10.1107/S010827019600697X ]

A Triphenylboroxin Derivative Possessing Two Intramolecular Chelates

P. D. Robinson, M. P. Groziak and L. Yi

Formula: C27H33B3N6O3



Acta Cryst. (1996). C52, 2830-2832    [ doi:10.1107/S0108270196008268 ]

Tetra-n-butylammonium Chloride-Thiourea (1/2), a Layer-Type Inclusion Compound

Q. Li and T. C. W. Mak

Formula: C16H36N+.Cl-.2CH4N2S



Acta Cryst. (1996). C52, 2832-2835    [ doi:10.1107/S0108270196008013 ]

2-(2,5-Dichlorophenylhydrazono)glutaric Acid and 2-(3,5-Dichlorophenylhydrazono)glutaric Acid

S. Antolic, B. Kojic-Prodic and J. D. Cohen

Formula: Two isomers of C11H10Cl2N2O4



Acta Cryst. (1996). C52, 2836-2837    [ doi:10.1107/S0108270196007676 ]

5,5,8,8-Tetrafluoro-6-methoxy-5,8-dihydroquinoline

K. Kato, H. Morikawa, H. Kimoto and K. Momota

Formula: C10H7F4NO



Acta Cryst. (1996). C52, 2837-2839    [ doi:10.1107/S0108270196007639 ]

A Highly Strained Tertiary Acetate: 2,2'-Spirobiadamant-1-yl Acetate

J. Vaissermann and J. S. Lomas

Formula: C21H30O2



Acta Cryst. (1996). C52, 2839-2841    [ doi:10.1107/S0108270196007615 ]

2,6-Dibenzoylhydroquinone

K. Biradha, G. R. Desiraju, H. L. Carrell and A. K. Katz

Formula: C20H14O4



Acta Cryst. (1996). C52, 2841-2844    [ doi:10.1107/S0108270196007019 ]

Balancing Conjugational Stabilization and Torsional Strain. The Solid-State Structure of a 2-Thioalkyl-Substituted Pyridine N-Oxide

J. Hartung, I. Svoboda and H. Fuess

Formula: C16H17NOS



Acta Cryst. (1996). C52, 2844-2847    [ doi:10.1107/S0108270196008104 ]

Three 1,4-trans-Substituted Cyclohexanes

D. C. Swenson, C. R. Davis and D. J. Burton

Formula: C12H16F4O4, C10H14F6 and C10H12F8



Acta Cryst. (1996). C52, 2847-2849    [ doi:10.1107/S0108270196007536 ]

[alpha],[alpha]'-Bis(2-pyridylseleno)-p-xylene

C. O. Kienitz, C. Thöne and P. G. Jones

Formula: C18H16N2Se2



Acta Cryst. (1996). C52, 2849-2851    [ doi:10.1107/S0108270196007548 ]

(8R,8aS)-Indolizidine-1-spiro-2'-(1',3'-dithiane)-8-carbonitrile

F. F. Fleming, Z. Hussain, M. Mullaney, R. E. Norman and S.-C. Chang

Formula: C12H18N2S2



Acta Cryst. (1996). C52, 2851-2853    [ doi:10.1107/S0108270196008244 ]

9-Dicyclohexylphenylphosphino-arachno-6-thiadecaborane(11)

G. M. Rosair, A. J. Welch and A. S. Weller

Formula: C18H38B9PS



Acta Cryst. (1996). C52, 2853-2857    [ doi:10.1107/S010827019600827X ]

Directly Linked C-Disaccharides: Structures of Two 3,4-Dihydro-2H-pyran Derivatives

S. Ianelli and M. Nardelli

Formula: C21H29NO7S.H2O and C19H28O8



Acta Cryst. (1996). C52, 2857-2859    [ doi:10.1107/S0108270196007755 ]

C38H54N3O9P, a New Compound in Diazadihydrophosphinine Chemistry

S. García-Granda, R. Santiago-García and K. Bieger

Formula: C38H54N3O9P



Acta Cryst. (1996). C52, 2859-2861    [ doi:10.1107/S0108270196007561 ]

Methyl Triphenylphosphoranylideneacetate: a Redetermination

P. D. Boyle

Formula: C21H19O2P



Acta Cryst. (1996). C52, 2862-2864    [ doi:10.1107/S0108270196008876 ]

2-Naphthoic Acid at 153K

A. C. Blackburn, L. J. Fitzgerald and R. E. Gerkin

Formula: C11H8O2



Acta Cryst. (1996). C52, 2865-2868    [ doi:10.1107/S0108270196008335 ]

2-Methyl-3-phenyl-2,5-dihydro-1,2,4-triazin-6(1H)-one Methanol Solvate and 4-Methyl-3-phenyl-4,5-dihydro-1,2,4-triazin-6(1H)-one

D. J. Collins, T. C. Hughes, W. M. Johnson and M. F. Mackay

Formula: C10H11N3O.CH4O and C10H11N3O



Acta Cryst. (1996). C52, 2868-2871    [ doi:10.1107/S0108270196008864 ]

p-Nitroaniline-3,5-Dinitromethyl Salicylate (1:1) Co-Crystal

K.-S. Huang, D. Britton and M. C. Etter

Formula: C6H6N2O2.C8H6N2O7



Acta Cryst. (1996). C52, 2871-2873    [ doi:10.1107/S0108270196007743 ]

L-Leucyl-L-alanine Dimethyl Sulfoxide Solvate

S. N. Mitra, L. Govindasamy and E. Subramanian

Formula: C9H18N2O3.C2H6OS



Acta Cryst. (1996). C52, 2873-2875    [ doi:10.1107/S0108270196007652 ]

Dalspinosin

S. Lakshmi, S. Kumar, J. Senthilselvan and K. Subramanian

Formula: C18H16O7



Acta Cryst. (1996). C52, 2875-2878    [ doi:10.1107/S0108270196008360 ]

Acetoxymethyl 4-Chloro-N-furfuryl-5-sulfamoylanthranilate, an Absorption Furosemide Prodrug

O. A. González, A. W. Mombrú, L. P. Suescun, R. A. Mariezcurrena, E. Manta and C. Prandi

Formula: C15H15ClN2O7S



Acta Cryst. (1996). C52, 2878-2880    [ doi:10.1107/S0108270196007457 ]

2-(p-Diethylaminobenzylidene)-1,3-indandione

V. Khodorkovsky, R. A. Mazor and A. Ellern

Formula: C20H19NO2



Acta Cryst. (1996). C52, 2880-2882    [ doi:10.1107/S0108270196007688 ]

3-(4-Nitrobenzyloximino)hexahydroazepin-2-one

D. Tranqui, H. Elfrom, H. Pera and G. Leclerc

Formula: C13H15N3O4



Acta Cryst. (1996). C52, 2882-2883    [ doi:10.1107/S0108270196008001 ]

1,1'-Diacetyl-2,2'-biimidazole

P. M. Secondo, C. A. Hester, H. L. Collier, R. G. Baughman and A. W. Cordes

Formula: C10H10N4O2



Acta Cryst. (1996). C52, 2883-2885    [ doi:10.1107/S0108270196008323 ]

Methyl 2-Benzoyloxy-3-oxo-3-phenylpropanoate

J. P. Shaw, E. W. Tan and A. G. Blackman

Formula: C17H14O5



Acta Cryst. (1996). C52, 2885-2887    [ doi:10.1107/S0108270196008207 ]

2-Butyne-1,4-diol

Th. Steiner

Formula: C4H6O2



Acta Cryst. (1996). C52, 2887-2889    [ doi:10.1107/S0108270196007299 ]

Octakis(3,5-dimethylphenylthio)naphthalene

G. A. Downing, D. D. MacNicol, P. R. Mallinson and P. K. Milligan

Formula: C74H72S8



Acta Cryst. (1996). C52, 2890-2891    [ doi:10.1107/S0108270196008189 ]

Diethyl 3-Piperidino-2,7-cycloheptadiene-1,2-dicarboxylate

S. Özbey, A. Temel, N. Tunouglu and N. Uludaug

Formula: C18H27NO4



Acta Cryst. (1996). C52, 2892-2894    [ doi:10.1107/S0108270196008839 ]

3[beta],4[alpha]-Dihydroxy-5[beta]-androstan-17-one

M. Ramos Silva, J. A. Paixão, M.-J. M. de Almeida, E. J. Tavares da Silva, M. L. Sá e Melo and A. S. Campos Neves

Formula: C19H30O3



Acta Cryst. (1996). C52, 2894-2896    [ doi:10.1107/S0108270196007068 ]

5-Phenylindazole

O. Hager, C. Foces-Foces, N. Jagerovic, J. Elguero and S. Trofimenko

Formula: C13H10N2



Acta Cryst. (1996). C52, 2896-2899    [ doi:10.1107/S0108270196007664 ]

2-Hydroxy-1,4-naphthoquinone

J. Dekkers, H. Kooijman, J. Kroon and E. Grech

Formula: C10H6O3



Acta Cryst. (1996). C52, 2899-2903    [ doi:10.1107/S0108270196006440 ]

Three Testosterone Derivatives

Z. Böcskei, T. Gérczei, A. Bodor, R. Schwartz and G. Náray-Szabó

Formula: C21H30O3, C28H37NO3 and C28H37NO3



Acta Cryst. (1996). C52, 2903-2905    [ doi:10.1107/S0108270196008025 ]

Boc-Phe-Aminomalonaldehyde

J. Sopková, I. Císarová and Z. Arnold

Formula: C17H22N2O5



Acta Cryst. (1996). C52, 2905-2907    [ doi:10.1107/S0108270196007809 ]

Methyl 7[alpha],12[alpha]-Dihydroxy-3[alpha]-methacryloylamino-5[beta]-cholan-24-oate

M. Akram, J. K. Denike, F. Bélanger-Gariépy and X.-X. Zhu

Formula: C29H47NO5



Acta Cryst. (1996). C52, 2908-2910    [ doi:10.1107/S0108270196008591 ]

2-(2-Thioxo-1,3-thiazolidin-3-yl)-4,5-dihydro-1,3-thiazol-1-ium Chloride, C6H9N2S3+.Cl-

E. S. Raper, M. Kubiak and T. Glowiak

Formula: C6H9N2S3+.Cl-



Acta Cryst. (1996). C52, 2910-2912    [ doi:10.1107/S0108270196007895 ]

2-(7,9-Diphenylcyclopenta[a]acenaphthadien-6b-yl)-2-phenylethanol

T. Repo, M. Klinga, M. Leskelä, M. Polamo and B. Rieger

Formula: C35H26O



Acta Cryst. (1996). C52, 2912-2915    [ doi:10.1107/S0108270196008220 ]

cis-Aconitic Acid at 150K

N. Nagel, U. Endruschat and H. Bock

Formula: C6H6O6



Acta Cryst. (1996). C52, 2915-2917    [ doi:10.1107/S0108270196006968 ]

N-[2-(1-Hydrazonoethyl)-3-benzofuranyl]-p-toluenesulfonamide

F. Bachechi, V. M. Coiro and M. Delfini

Formula: C17H17N3O3S



Acta Cryst. (1996). C52, 2917-2920    [ doi:10.1107/S0108270196007081 ]

Two Polymorphic Forms of 3-Hydroxy-2-methyl-4H-pyran-4-one (Maltol)

J. Burgess, J. Fawcett, D. R. Russell, R. C. Hider, M. B. Hossain, C. R. Stoner and D. van der Helm

Formula: Two polymorphs of C6H6O3



Acta Cryst. (1996). C52, 2920-2922    [ doi:10.1107/S0108270196008475 ]

2,2-Dimethyl-6-nitro-3,4-dihydro-2H-benzo[b]pyran-4-one O-Benzoyloxime

Q.-C. Yang, H.-M. Li, Y.-Q. Tang and W.-L. Huang

Formula: C18H16N2O5



Acta Cryst. (1996). C52, 2922-2924    [ doi:10.1107/S0108270196008517 ]

4-Octyloxybiphenyl-4'-yl 4-Methoxybenzoate

K. Hori and Y. Nishiura

Formula: C28H32O4



Acta Cryst. (1996). C52, 2924-2927    [ doi:10.1107/S0108270196008906 ]

Tris[2-(2-methoxyethoxy)phenyl]phosphine Oxide Monohydrate

P. D. Livant, J. Mao and T. R. Webb

Formula: C27H33O7P.H2O



Acta Cryst. (1996). C52, 2927-2929    [ doi:10.1107/S010827019600889X ]

Torturing the 7-Oxabicyclo[2.2.1]heptane Skeleton with an Oxetane Ring: 4,7-Dioxatricyclo[3.2.1.03,6]octane at 190K

A. A. Pinkerton, C. le Drian and P. Vogel

Formula: C6H8O2



Acta Cryst. (1996). C52, 2929-2932    [ doi:10.1107/S0108270196008736 ]

2,4-Dinitrophenyl Phenyl Sulfone

J. Ellena, G. Punte and N. S. Nudelman

Formula: C12H8N2O6S



Acta Cryst. (1996). C52, 2932-2936    [ doi:10.1107/S0108270196005677 ]

Inclusion of the Main Pheromone Component of Dacus oleae, 1,7-Dioxaspiro[5,5]undecane, in [beta]-Cyclodextrin

N. Rysanek, G. Le Bas, F. Villain and G. Tsoucaris

Formula: C42H70O35.C9H16O2.9H2O



Acta Cryst. (1996). C52, 2936-2939    [ doi:10.1107/S0108270196006944 ]

cis-4,5-Dihydroxy-2,3,4,5-tetraphenylcyclopent-2-enone

M. J. Jedrzejas, M. D. Rubin, R. J. Baker, J. Masnovi and R. L. R. Towns

Formula: C29H22O3



Acta Cryst. (1996). C52, 2939-2941    [ doi:10.1107/S0108270196007135 ]

A Potential Antiprotozoal Drug Containing Acridine and Thiadiazole Moieties

J. Karolak-Wojciechowska, A. Mrozek, P. Amiel, P. Brouant and J. Barbe

Formula: C22H23ClN4OS3



Acta Cryst. (1996). C52, 2941-2942    [ doi:10.1107/S0108270196007147 ]

N'-[Bis(methylthio)methylene]cyanoacetohydrazide

R. Pomes Hernandez, A. Gómez González, A. Rosado Pérez, B. M. Nápoles Frías, R. A. Toscano and J. Quincoces Suárez

Formula: C6H9N3OS2



Acta Cryst. (1996). C52, 2943-2945    [ doi:10.1107/S0108270196007007 ]

4(5)-(p-Methoxyphenylazo)-2-methylimidazole

R. Anulewicz and D. Maciejewska

Formula: C11H12N4O



Acta Cryst. (1996). C52, 2945-2946    [ doi:10.1107/S0108270196010827 ]

(Z)-2-(Benzoyl-aci-nitro)-2-phenylacetonitrile

D. R. Powell, P. E. Hanson and S. H. Gellman

Formula: C15H10N2O3


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