Acta Crystallographica Section C

Crystal Structure Communications

Volume 52, Part 12 (December 1996)


Cover illustrationCover illustration: A Homoleptic Cuprate(II) with Deprotonated 1,6-Anhydro-beta-D-glucose Ligands, see Gack & Klüfers, pages 2972-2975. Displacement ellipsoids are shown at the 50% probability level.

inorganic compounds



Acta Cryst. (1996). C52, 2947-2949    [ doi:10.1107/S0108270196008700 ]

K2MoO2(MoO2As2O7)2

M. F. Zid and T. Jouini

Synopsis: The structure of K2MoO2(MoO2As2O7)2 is built up from As2O7 groups and corner-sharing MoO6 octahedra to form a three- dimensional framework with intersecting tunnels where the K+ ions reside.

Formula: K2MoO2(MoO2As2O7)2



Acta Cryst. (1996). C52, 2949-2951    [ doi:10.1107/S0108270196009626 ]

NaYP2O7

A. Hamady and T. Jouini

Synopsis: NaYP2O7 crystallizes in the non-centrosymmetric space group P21. The structure consists of corner-sharing YO6 octahedra and P2O7 groups with alternate stacking of octahedral and phosphate layers. The framework delimits intersecting tunnels where the Na+ ions are located.

Formula: NaYP2O7



Acta Cryst. (1996). C52, 2951-2954    [ doi:10.1107/S0108270196008827 ]

A New Langbeinite: Dipotassium Dimanganese Tetrafluoroberyllate

A. Guelylah, T. Breczewski and G. Madariaga

Synopsis: K2Mn2(BeF4)3 has a langbeinite-type structure. Each Mn2+ cation is surrounded by six F- anions in the form of a distorted octahedron, each F- ion belonging to a different BeF42- tetrahedron. The K+ ions are nine-coordinate.

Formula: K2Mn2(BeF4)3



Acta Cryst. (1996). C52, 2954-2956    [ doi:10.1107/S0108270196008815 ]

Langbeinite-Type Cubic Dithallium Dicadmium Sulfate

A. Guelylah, G. Madariaga and T. Breczewski

Synopsis: Tl2Cd2(SO4)3 has a langbeinite-type structure in which each Tl+ ion is surrounded by nine O atoms, forming an irregular polyhedron. Each Cd2+ ion is coordinated by six O atoms in the form of a distorted octahedron, each O atom belonging to a different sulfate ion.

Formula: Tl2Cd2(SO4)3



Acta Cryst. (1996). C52, 2956-2959    [ doi:10.1107/S0108270196010840 ]

Gadolinium Potassium Hexacyanoferrate(II) Trihydrate

D. F. Mullica, J. L. Ward and E. L. Sappenfield

Synopsis: The structure of GdKFe(CN)6.3H2O contains non-linear cyanide bridges which link octahedrally coordinated Fe atoms and eight-coordinate Gd atoms. Cavities within the structure are occupied by K+ ions and zeolitic water molecules.

Formula: GdKFe(CN)6.3H2O



Acta Cryst. (1996). C52, 2959-2960    [ doi:10.1107/S0108270196011006 ]

Chlorapatite: Ca5(AsO4)3Cl

T. A. Wardojo and S.-J. Hwu

Synopsis: Ca5(AsO4)3Cl crystallizes in the hexagonal system and is closely related to its phosphate analogs Ca5(PO4)3X (X = Cl, OH), but has a slightly modified structure in terms of the anion sites.

Formula: Ca5(AsO4)3Cl



Acta Cryst. (1996). C52, 2960-2963    [ doi:10.1107/S0108270196002739 ]

A Mixed Nickel-Lithium Pyrophosphate, LiNi1.5P2O7

K. Rissouli, K. Benkhouja, A. Sadel, M. Bettach, M. Zahir, M. Giorgi and M. Pierrot

Synopsis: The structure of LiNi1.5P2O7 is composed of [P2O7] layers separated by chains of [NiO6] octahedra. The Li+ sites are six-coordinate with four short and two long Li-O bonds.

Formula: LiNi1.5P2O7



Acta Cryst. (1996). C52, 2963-2964    [ doi:10.1107/S0108270196010104 ]

Rubidium Indium Antimonide, Rb2In2Sb3

O. Gourdon, F. Boucher, J. Gareh, M. Evain, C. O'Connor and J. Jin-Seung

Synopsis: The structure of rubidium indium antimonide, a layered material isotypic with A2In2Sb3 (A = Na, K, Cs), is reported.

Formula: Rb2In2Sb3



Acta Cryst. (1996). C52, 2964-2967    [ doi:10.1107/S0108270196008694 ]

Triclinic Fe3Al2Si3 and Orthorhombic Fe3Al2Si4 with New Structure Types

T. I. Yanson, M. B. Manyako, O. I. Bodak, N. V. German, O. S. Zarechnyuk, R. Cerný, J. V. Pacheco and K. Yvon

Synopsis: Fe3Al2Si3 contains three iron, two aluminium and three silicon sites whose atomic environments derive from icosahedra. Fe3Al2Si4 contains two iron, one aluminium and three silicon sites whose atomic environments derive from hexagonal cuboctahedra.

Formula: Fe3Al2Si3 and Fe3Al2Si4



Acta Cryst. (1996). C52, 2967-2969    [ doi:10.1107/S0108270196008153 ]

La Phase Monoclinique Li2Nb0,5In1,5(PO4)3

X. Cieren, S. Jaulmes, J. Angenault, J. C. Couturier and M. Quarton

Synopsis: Li2Nb0.5In1.5(PO4)3 contains PO4 tetrahedra and distorted MO6 octahedra with a statistical distribution of Nb and In atoms over the M sites. The framework contains cavities, one of which is fully occupied by Li+ while the other two are occupied by 1/3Li+ and 2/3Li+.

Formula: Li2Nb0.5In1.5(PO4)3


metal-organic compounds



Acta Cryst. (1996). C52, 2970-2972    [ doi:10.1107/S0108270196009043 ]

The Sodium Salt of N1-Deprotonated Inosine, Na+.C10H11N4O5-.2.5H2O

P. Klüfers and P. Mayer

Formula: Na+.C10H11N4O5-.2.5H2O



Acta Cryst. (1996). C52, 2972-2975    [ doi:10.1107/S010827019600947X ]

A Homoleptic Cuprate(II) Complex with Deprotonated 1,6-Anhydro-[beta]-D-glucose (Levoglucosan) Ligands

C. Gack and P. Klüfers

Formula: Li2[Cu(C6H8O5)2].8H2O



Acta Cryst. (1996). C52, 2975-2977    [ doi:10.1107/S0108270196010347 ]

Tetrachloro[2-(phenylamino)pyridinato]titanate(IV) with a 2-(Phenylamino)pyridinium Counterion

M. Polamo and M. Leskelä

Formula: (C11H11N2)[TiCl4(C11H9N2)]



Acta Cryst. (1996). C52, 2977-2980    [ doi:10.1107/S0108270196011328 ]

Trichlorobis[2,6-di(phenylamino)pyridinato-N,N']tantalum(V) Toluene Solvate (1/1)

M. Polamo

Formula: [TaCl3(C17H14N3)2].C7H8



Acta Cryst. (1996). C52, 2980-2982    [ doi:10.1107/S010827019601027X ]

mer-Trichloro[2-(phenylamino)pyridinato]oxotungsten(VI)

M. Polamo

Formula: [WCl3(O)(C11H9N2)]



Acta Cryst. (1996). C52, 2982-2984    [ doi:10.1107/S010827019601030X ]

Ruthenium(II) Complex Containing a New Hybrid Bidentate Phosphine-Thioether Ligand: [(p-Cymene)RuCl(Me2PCH2CH2SMe)][BPh4].0.5CH2Cl2

T. Suzuki, N. Taguchi and K. Kashiwabara

Formula: [RuCl(C10H14)(C5H13PS)](C24H20B).0.5CH2Cl2



Acta Cryst. (1996). C52, 2984-2987    [ doi:10.1107/S0108270196010426 ]

cis-Diaquabis(2,2'-bipyrimidine-N,N')cobalt(II) Diperchlorate Dihydrate, [Co(C8H6N4)2(H2 O)2](ClO4)2.2H2O

J. Brunzelle, A. Fitch, Y. Wang and S. F. Pavkovic

Formula: [Co(C8H6N4)2(H2O)2](ClO4)2.2H2O



Acta Cryst. (1996). C52, 2987-2989    [ doi:10.1107/S0108270196010700 ]

[2,2'-Oxybis(1,1,1,3,3,3-hexafluoro-2-propanolato-O)](N,N,N',N'-tetramethylethylenediamine-N,N')copper(II) Hemibenzene Solvate

C. George and A. P. Purdy

Formula: [Cu(C6F12O3)(C6H16N2)].0.5C6H6



Acta Cryst. (1996). C52, 2990-2992    [ doi:10.1107/S0108270196011286 ]

Bis(dicyclohexylammonium) Aquadimethyldi(oxalato-O,O')stannate Ethanol Solvate

S. W. Ng

Formula: (C12H24N)2[Sn(C2O4)2(CH3)2(H2O)].C2H6O



Acta Cryst. (1996). C52, 2992-2994    [ doi:10.1107/S0108270196010815 ]

Solvate-Dependent Polymorphism: Crystallization of [{Mn(CO)3}2{[bold mu]-([bold eta]5-C6H6-[bold eta]5-C6H6)}] from CH2Cl2 as a Mono-Solvate in the Rare Tetragonal Space Group P42/mbc

T. L. Utz, S. J. Geib and N. J. Cooper

Formula: [Mn2(C12H12)(CO)6].CH2Cl2



Acta Cryst. (1996). C52, 2994-2996    [ doi:10.1107/S0108270196011407 ]

Aqua[2,6-diacetylpyridinedi(benzoic acid hydrazone)]nitratocobalt(II) Nitrate at 173K

K. A. Abboud, R. C. Palenik and G. J. Palenik

Formula: [Co(NO3)(C23H21N5O2)(H2O)]NO3



Acta Cryst. (1996). C52, 2996-2999    [ doi:10.1107/S0108270196010049 ]

Triaqua(oxydiacetato-O,O',O'')strontium(II) Monohydrate

R. Baggio, M. Perec and M. T. Garland

Formula: [Sr(C4H4O5)(H2O)3].H2O



Acta Cryst. (1996). C52, 3000-3002    [ doi:10.1107/S0108270196004258 ]

(E)-1,3-Diferrocenyl-2-buten-1-one-Water (4/1)

J. J. C. Erasmus, G. J. Lamprecht, J. C. Swarts, A. Roodt and Å. Oskarsson

Formula: [Fe2(C5H5)2(C14H12O)].0.25H2O



Acta Cryst. (1996). C52, 3002-3005    [ doi:10.1107/S0108270196009493 ]

(trans-1R,2R-Cyclohexanediamine-N,N')(L-ascorbato-C2,O5)platinum(II)-Water (1/3)

H. Yuge and T. K. Miyamoto

Formula: [Pt(C6H6O6)(C6H14N2)].3H2O



Acta Cryst. (1996). C52, 3005-3007    [ doi:10.1107/S0108270196008682 ]

An Oxo-Centered Trinuclear Cobalt(II)-Diiron(III) Acetate-Aqua Complex

T. Sato and F. Ambe

Formula: [CoFe2O(C2H3O2)6(H2O)3].2H2O



Acta Cryst. (1996). C52, 3007-3009    [ doi:10.1107/S010827019600978X ]

Di-[bold mu]-chloro-bis[(diethylenetriamine)copper(II)] Dinitrate

M. K. Urtiaga, M. I. Arriortua, R. Cortés and T. Rojo

Formula: [Cu2Cl2(C4H13N3)2](NO3)2



Acta Cryst. (1996). C52, 3009-3013    [ doi:10.1107/S010827019601075X ]

A Paucity of Hydrogen Bonds in Ferrocene-1,1'-diylbis[bis(4-methoxyphenyl)methanol]- Methanol (3/2)

W. Bell, G. Ferguson and C. Glidewell

Formula: 3[Fe(C20H19O3)2].2CH4O



Acta Cryst. (1996). C52, 3013-3016    [ doi:10.1107/S0108270196011249 ]

Pentaammine-2[bold kappa]5N-([bold mu]-4,4'-bipyridine-1[bold kappa]N:2[bold kappa]N')(2,2'-bipyridine-1[bold kappa]2N,N')(2,2':6',2''-terpyridine-1[bold kappa]3N,N',N'')diruthenium Tetrakis(hexafluorophosphate) Acetonitrile Solvate

D. J. Szalda, F. Fagalde and N. E. Katz

Formula: [Ru2(C10H8N2)2(C15H11N3)(NH3)5](PF6)4.CH3CN



Acta Cryst. (1996). C52, 3016-3018    [ doi:10.1107/S0108270196010293 ]

A 1:2 Adduct of Tetrakis([bold mu]-thiobenzoato-O,S)dimolybdenum(II)(Mo-Mo) with Triphenylphosphine Oxide, [Mo2(C7H5OS)4].2[(C6H5)3OP]

M. Cindric, V. Vrdoljak, D. Matkovic-Calogovic and B. Kamenar

Formula: [Mo2(C7H5OS)4].2C18H15OP



Acta Cryst. (1996). C52, 3019-3020    [ doi:10.1107/S0108270196010311 ]

trans-Bis(dicyanamido-N)tetrakis(4-methylimidazole-N1)nickel(II)

J. Kozísek, H. Paulus, M. Danková and M. Hvastijová

Formula: [Ni(C2N3)2(C4H6N2)4]



Acta Cryst. (1996). C52, 3020-3024    [ doi:10.1107/S0108270196010748 ]

8-[1,2-Bis(diphenylphosphino)ethane]-9,10-[bold mu]-hydrido-8-rhoda-7-thia-nido-undecaborane(10)-Dichloromethane (2/1)

G. M. Rosair, A. J. Welch and A. S. Weller

Formula: [Rh(B9H10S)(C26H24P2)]2.CH2Cl2



Acta Cryst. (1996). C52, 3024-3025    [ doi:10.1107/S0108270196010463 ]

Linear-Chain Structure of Bis(O,O'-dimethyldithiophosphato)cadmium(II)

T. Ito and M. Otake

Formula: [Cd(C2H6O2PS2)2]



Acta Cryst. (1996). C52, 3025-3027    [ doi:10.1107/S0108270196012115 ]

Chlorotris(m-methoxyphenyl)tin(IV)

I. Wharf and A.-M. Lebuis

Formula: [SnCl(C7H7O)3]



Acta Cryst. (1996). C52, 3028-3030    [ doi:10.1107/S0108270196011122 ]

Bis(1,1,1,5,5,5-hexafluoro-2,4-pentanedionato)(2,5,8,11,14,17-hexaoxaoctadecane)barium

M. Motevalli, P. O'Brien and I. M. Watson

Formula: [Ba(C5HF6O2)2(C12H26O6)]



Acta Cryst. (1996). C52, 3030-3033    [ doi:10.1107/S0108270196009663 ]

Tris(N,N-diethyldithiocarbamato-S,S')nickel(IV) 1,1,2,3,3-Pentacyanopropenide

W. Chen, H. Li, Z.-J. Zhong, K. Zhang and X.-Z. You

Formula: [Ni(C5H10NS2)3](C8N5)



Acta Cryst. (1996). C52, 3033-3035    [ doi:10.1107/S0108270196010608 ]

[beta]-meso-(5,7,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane)nickel(II) Diperchlorate Monohydrate

A. Wang, T.-J. Lee, B.-H. Chen, Y.-Z. Yuan and C.-S. Chung

Formula: [Ni(C16H36N4)](ClO4)2.H2O



Acta Cryst. (1996). C52, 3035-3037    [ doi:10.1107/S0108270196009389 ]

[1,8-Bis(2-hydroxyethyl)-1,3,6,8,10,13-hexaazacyclotetradecane]nickel(II) Bis(maleonitriledithiolato)nickelate(II)

B.-Z. Shan, X.-Z. You, H.-K. Fun and K. Sivakumar

Formula: [Ni(C12H30N6O2)][Ni(C4N2S2)2]



Acta Cryst. (1996). C52, 3037-3038    [ doi:10.1107/S0108270196011365 ]

Trichloro[[bold eta]5-(trimethylstannyl)cyclopentadienyl]titanium

A. V. Churakov and L. G. Kuz'mina

Formula: [TiCl3(C8H13Sn)]



Acta Cryst. (1996). C52, 3039-3040    [ doi:10.1107/S0108270196010128 ]

cis-Tetracarbonyldi(pyridine-N)tungsten(0), [W(CO)4(py)2]

J. Holzbock, W. Sawodny, E. Grosse, M. Haseidl and L. Walz

Formula: [W(C5H5N)2(CO)4]



Acta Cryst. (1996). C52, 3040-3043    [ doi:10.1107/S0108270196010062 ]

Nitrato(2,3,7,8,12,13,17,18-octaethylporphyrinato)iron(III)

M. K. Ellison, M. Shang, J. Kim and W. R. Scheidt

Formula: [Fe(C36H44N4)(NO3)]



Acta Cryst. (1996). C52, 3043-3045    [ doi:10.1107/S0108270196009833 ]

A Cadmium(II) Complex of Creatinine, [Cd(C2H3O2)2(C4H7N3O)2].0.5H2O

R. Chotalia, T. W. Hambley, D. D. Ridley and P. Turner

Formula: [Cd(C2H3O2)2(C4H7N3O)2].0.5H2O



Acta Cryst. (1996). C52, 3045-3047    [ doi:10.1107/S0108270196006956 ]

Bis(triethylsulfonium) Tetraiodocadmate(II)

L. Bengtsson-Kloo, J. Berglund, H. Stegemann, C. Svensson and P. H. Svensson

Formula: (C6H15S)2[CdI4]



Acta Cryst. (1996). C52, 3047-3049    [ doi:10.1107/S0108270196009961 ]

Triple-Decker Pentalene Complex of Iron and Cobalt

C. Miravitlles, E. Molins, W. Maniukiewicz, M. Mas, J. M. Manríquez, I. Chávez, B. Oelckers, A. Alvarez-Larena and J. L. Briansó

Formula: [CoFe(C8H7)(C10H15)(C8H6)]



Acta Cryst. (1996). C52, 3049-3051    [ doi:10.1107/S0108270196007354 ]

Restricting Chelate Ring Flipping in CuII Complexes. I. Non-Thermochromic Bis(o-phenylenediamine-N,N')copper(II) Bis(tetrafluoroborate)

B. Narayanan and M. M. Bhadbhade

Formula: [Cu(C6H8N2)2](BF4)2


organic compounds



Acta Cryst. (1996). C52, 3052-3055    [ doi:10.1107/S010827019601133X ]

Piperazine-4,4'-Sulfonyldiphenol (1/2): a Self-Assembled Channel Structure

P. I. Coupar, G. Ferguson and C. Glidewell

Formula: C4H12N22+.2C12H9O4S-



Acta Cryst. (1996). C52, 3055-3057    [ doi:10.1107/S010827019601013X ]

N-H...pi(arene) Hydrogen Bonding in 4,4'-Thiodiphenol-Piperazine (1/1)

P. I. Coupar, G. Ferguson and C. Glidewell

Formula: C4H10N2.C12H10O2S



Acta Cryst. (1996). C52, 3057-3062    [ doi:10.1107/S0108270196011377 ]

Two- and Three-Dimensional Hydrogen-Bonding Networks in the Structures of 4,4'-Dihydroxybenzophenone and 4,4'-Thiodiphenol

G. Ferguson and C. Glidewell

Formula: C13H10O3 and C12H10O2S



Acta Cryst. (1996). C52, 3062-3064    [ doi:10.1107/S0108270196012012 ]

4,7-Bis(2-thiophenoyl)-1-thia-4,7-diazacyclononane

A. J. Blake, J. P. Danks, S. Parsons and M. Schröder

Formula: C16H18N2O2S3



Acta Cryst. (1996). C52, 3064-3067    [ doi:10.1107/S0108270196010256 ]

An Unusual 3H-Pyrrole at 150K

X. L. M. Despinoy, H. McNab and S. Parsons

Formula: C19H18N2O7



Acta Cryst. (1996). C52, 3067-3069    [ doi:10.1107/S010827019601178X ]

The Major Isoxazoline Cycloadduct from Reaction of a Xylopyranosylnitrile Oxide with a Hex-5-enopyranoside

W. J. Ferguson, S. Parsons and R. M. Paton

Formula: C22H31NO12



Acta Cryst. (1996). C52, 3069-3073    [ doi:10.1107/S0108270196009080 ]

The First Crystal Structure Analysis of Cyclododeca-2,8-diyne-1,10-diols

C. Boss, H. Stoeckli-Evans and R. Keese

Formula: C12H16O2 and C14H20O2



Acta Cryst. (1996). C52, 3073-3075    [ doi:10.1107/S0108270196010943 ]

Tetraprotonated Tetra(2-pyridyl)pyrazine: Pyrazine-2,3,5,6-tetra(2-pyridinium) Tetrachloride Dihydrate

M. Graf and H. Stoeckli-Evans

Formula: C24H20N64+.4Cl-.2H2O



Acta Cryst. (1996). C52, 3075-3078    [ doi:10.1107/S0108270196010001 ]

[bold gamma]-Aminobutyric Acid: a Novel Tetragonal Phase

A. J. Dobson and R. E. Gerkin

Formula: C4H9NO2



Acta Cryst. (1996). C52, 3078-3081    [ doi:10.1107/S0108270196010414 ]

2-Acetylbenzoic Acid: Phthalide Form

A. J. Dobson and R. E. Gerkin

Formula: C9H8O3



Acta Cryst. (1996). C52, 3081-3083    [ doi:10.1107/S0108270196010852 ]

Coumarin-3-carboxylic Acid

A. J. Dobson and R. E. Gerkin

Formula: C10H6O4



Acta Cryst. (1996). C52, 3083-3086    [ doi:10.1107/S0108270196009547 ]

4-(2-Naphthyl)butanoic Acid

A. J. Dobson and R. E. Gerkin

Formula: C14H14O2



Acta Cryst. (1996). C52, 3086-3088    [ doi:10.1107/S0108270196010013 ]

sym-Hexahydropyrene

A. J. Dobson and R. E. Gerkin

Formula: C16H16



Acta Cryst. (1996). C52, 3088-3091    [ doi:10.1107/S0108270196010530 ]

2-Hydroxybiphenyl-3-carboxylic Acid (3-Phenylsalicylic Acid)

A. J. Dobson and R. E. Gerkin

Formula: C13H10O3



Acta Cryst. (1996). C52, 3091-3093    [ doi:10.1107/S0108270196011432 ]

9,10-Bis(1-pyridiniomethyl)anthracene Dichloride-Methanol-Water (1/2/1)

J. C. Bryan, A. A. Gakh and R. A. Sachleben

Formula: C26H22N22+.2Cl-.2CH4O.H2O



Acta Cryst. (1996). C52, 3093-3095    [ doi:10.1107/S0108270196010694 ]

9,10-Bis(7-fluoro-2,5-dioxaheptyl)triptycene

A. A. Gakh, J. C. Bryan and R. A. Sachleben

Formula: C30H32F2O4



Acta Cryst. (1996). C52, 3095-3097    [ doi:10.1107/S0108270196011055 ]

3,4,5,6,9,10-Hexahydro-14,16-dihydroxy-3-methyl-1H-2-benzoxacyclotetradecin-1,7(8H)-dione (Zearalenone)

K. Panneerselvam, E. Rudiño-Piñera and M. Soriano-García

Formula: C18H22O5



Acta Cryst. (1996). C52, 3098-3100    [ doi:10.1107/S0108270196011067 ]

The 1:1 Molecular Complex of N,N'-Bis(4-methoxybenzylidene)ethylenediamine and Hydroquinone

K. Panneerselvam, M. Soriano-García, A. Reyes-Arellano, J. Tamariz-Mascarúa and R. I. Mendoza-Sánchez

Formula: C18H20N2O2.C6H6O2



Acta Cryst. (1996). C52, 3100-3102    [ doi:10.1107/S0108270196009559 ]

6-Ammonio-(1H+)-1,4,8,11-tetraazacyclotridecane-5,7-dione Dichloride Methanol Solvate: an Amino-Pendant Tetraazacyclotridecane Derivative

A. K. Mishra, J. F. Gestin, A. Faivre-Chauvet, J. F. Chatal and M. Evain

Formula: C9H21N5O22+.2Cl-.CH4O



Acta Cryst. (1996). C52, 3102-3104    [ doi:10.1107/S0108270196009444 ]

A Corticosteroid Ester

J. Negriolli, M. Evain and F. André

Formula: C23H29FO5



Acta Cryst. (1996). C52, 3104-3105    [ doi:10.1107/S0108270196007172 ]

(E)-3-(4-Chlorophenyl)-3-cyclopropyl-2-(phenylthio)acrylonitrile

D. Roche, J. Métin and M. Madesclaire

Formula: C18H14ClNS



Acta Cryst. (1996). C52, 3106-3108    [ doi:10.1107/S0108270196010050 ]

(Dicyclohexylphosphino)borane, BH3PH(C6H11)2, a Precursor to Water-Soluble Phosphine Ligands

M. W. Day, B. Mohr and R. H. Grubbs

Formula: C12H26BP



Acta Cryst. (1996). C52, 3108-3110    [ doi:10.1107/S0108270196008888 ]

6-Bromo-2H-3,1-benzoxazine-2,4(1H)-dione at 153K

P. Lubini and J. Wouters

Formula: C8H4BrNO3



Acta Cryst. (1996). C52, 3110-3112    [ doi:10.1107/S0108270196010773 ]

6-Amino-1,3-dimethyl-5-(4-oxo-2-penten-2-yl)aminouracil

S. B. Jimenez-Pulido, J. N. Low, G. Ferguson, M. N. Moreno-Carretero and F. Hueso-Ureña

Formula: C11H16N4O3



Acta Cryst. (1996). C52, 3112-3114    [ doi:10.1107/S0108270196009262 ]

A Cyclic Side-Chain-Linked Biphenyl Ether Tripeptide: H3N+-cyclo-[Phe(4-O)-Phe-Phe(3-O)]-OMe.Cl-

J. W. Janetka, K. A. Satyshur and D. H. Rich

Formula: C28H30N3O5+.Cl-



Acta Cryst. (1996). C52, 3114-3116    [ doi:10.1107/S0108270196010542 ]

meso-(3,5-Di-tert-butylphenyl)-2,2'-dipyrromethane

K.-J. Lin, J.-Y. Wu and C.-T. Chen

Formula: C23H30N2



Acta Cryst. (1996). C52, 3116-3118    [ doi:10.1107/S010827019601102X ]

[alpha],[alpha]-Diacetoxy-2,4-dichloro-5-nitrobenzaldehyde

S. D. Huang, O. Cox, M. Cordero and S. Piñeiro

Formula: C11H9Cl2NO6



Acta Cryst. (1996). C52, 3118-3121    [ doi:10.1107/S0108270196011079 ]

(Z)-2-Acetoxy-3,3',4'-trimethoxystilbene

S. Li, K. Lundquist and R. Stomberg

Formula: C19H20O5



Acta Cryst. (1996). C52, 3121-3124    [ doi:10.1107/S0108270196009572 ]

Quitenidinium Ethyl Ester Ethyl Sulfate

K. Lewinski, W. Nitek, B. J. Oleksyn, A. Kostrzewa, T. Lipinska and A. Suszko-Purzycka

Formula: C21H27N2O4+.C2H5SO4-



Acta Cryst. (1996). C52, 3124-3126    [ doi:10.1107/S0108270196011092 ]

Columnar Stacking of 1,3-Diphenyl-1,2,4-benzotriazin-4(1H)-yl Radicals

C. Krieger and F. A. Neugebauer

Formula: C19H14N3



Acta Cryst. (1996). C52, 3127-3128    [ doi:10.1107/S0108270196011250 ]

Ethyl 2-Fluoro-3-oxo-2-(p-toluoyl)-3-(p-tolyl)propanoate, C20H19O4F

M.-J. Kim, J.-C. Shin, J.-H. Lee, D.-Y. Rhie, D.-Y. Kim, I.-H. Suh, S.-S. Choi, W. P. Jensen and D. E. Lewis

Formula: C20H19O4F



Acta Cryst. (1996). C52, 3129-3131    [ doi:10.1107/S010827019600916X ]

4-[5'-Oxo-1',3'-diphenyl-4'-(p-tolylmethyl)]-1,3-diphenyl-4-(p-tolylmethyl)pyrazol-5-one: Product of a Reductive Dimerization Reaction

G. Bruno, G. Grassi, F. Nicoló, F. Risitano and R. Scopelliti

Formula: C46H38N4O2



Acta Cryst. (1996). C52, 3131-3133    [ doi:10.1107/S0108270196009249 ]

12-(N-Benzoylimino)-11,12-dihydrobenzimidazo[2,1-b][1,3,5]benzothiadiazepine

C. E. Song, B. W. Jin and J. H. Jeong

Formula: C21H14N4OS



Acta Cryst. (1996). C52, 3133-3135    [ doi:10.1107/S0108270196009304 ]

Ethyl {[N-(2-Hydroxyethyl)amino](2-hydroxy-1-naphthyl)methyl}phosphonate

M. N. Tahir, D. Ülkü, H. Yilmaz and H. Nazir

Formula: C15H20NO5P



Acta Cryst. (1996). C52, 3135-3138    [ doi:10.1107/S0108270196009109 ]

1-Diphenylphosphino-2-phenyl-1,2-dicarba-closo-dodecaborane(12)

M. A. McWhannell, G. M. Rosair, A. J. Welch, F. Teixidor and C. Viñas

Formula: C20H25B10P



Acta Cryst. (1996). C52, 3138-3140    [ doi:10.1107/S0108270196009195 ]

Tetraethyl (1Z,3Z)-Buta-1,3-diene-1,2,3,4-tetracarboxylate

K. Tani, T. Yamagata and Y. Kataoka

Formula: C16H22O8



Acta Cryst. (1996). C52, 3140-3142    [ doi:10.1107/S0108270196010244 ]

10-(N-Carboxymethylcarbamoyl)-3,7-bis(dimethylamino)phenothiazine (CCAP)-Ethanol (1/1), C19H22N4O3S.C2H6O

I. Fujii, N. Hirayama, N. Aoyama and A. Miike

Formula: C19H22N4O3S.C2H6O



Acta Cryst. (1996). C52, 3142-3144    [ doi:10.1107/S0108270196009250 ]

Penicillin V Benzhydryl Ester Sulfoxide Monohydrate

T.-S. Yoon and W. Shin

Formula: C29H28N2O6S.H2O



Acta Cryst. (1996). C52, 3145-3146    [ doi:10.1107/S0108270196009377 ]

1-(2-Naphthyl)-3-(4-nitrophenyl)prop-2-en-1-one

S. S. S. Raj, M. N. Ponnuswamy, G. Shanmugam and S. Nanjundan

Formula: C19H13NO3



Acta Cryst. (1996). C52, 3147-3150    [ doi:10.1107/S0108270196009614 ]

(S)-5,6-Dimethoxy-1,2,3,4-tetrahydro-2-naphthalenamine- L-(+)-Mandelic Acid (1/1): the Absolute Configuration of a Precursor of the Active Stereoisomer of 5,6-ADTN, an Important Dopaminergic Agonist

M. Fantucci, S. Montanari, F. Santangelo, S. Ianelli and M. Nardelli

Formula: C12H18NO2+C8H7O3-



Acta Cryst. (1996). C52, 3150-3152    [ doi:10.1107/S0108270196009158 ]

(3R*,4S*)-4-[(S*)-2-Cyclohexyl-2-(tert-butyldimethylsiloxy)ethyl]-3-hexyl-3-(trimethylsilyl)oxetan-2-one

P. J. Kocienski, B. Pelotier and M. Webster

Formula: C26H52O3Si2



Acta Cryst. (1996). C52, 3152-3154    [ doi:10.1107/S0108270196010931 ]

1,3-Diphenyl-4-imidazoline-2-thione

P. J. Cox, B. Sohal, G. G. Skellern, S. W. Love and N. Shankland

Formula: C15H12N2S



Acta Cryst. (1996). C52, 3154-3157    [ doi:10.1107/S0108270196009584 ]

2,2':6',2''-Terpyridinium Trifluoromethanesulfonate, [terpyH](CF3SO3)

A. Hergold-Brundic, Z. Popovic and D. Matkovic-Calogovic

Formula: C15H12N3+.CF3O3S-



Acta Cryst. (1996). C52, 3157-3159    [ doi:10.1107/S0108270196009110 ]

An 18-Chloro-4[alpha]-hydroxy Derivative of 19-Acetylteupolin IV: a Neo-clerodane Diterpenoid of Biological Interest

G. Hundal (née Sood) and M. Martinez-Ripoll

Formula: C24H29ClO9



Acta Cryst. (1996). C52, 3159-3162    [ doi:10.1107/S0108270196008980 ]

Hydrogen Bonding in 4,4-Dimethylcyclohexane-1,3-dione and 2,5,5-Trimethylcyclohexane-1,3-dione Monohydrate

J. C. Barnes

Formula: C8H12O2 and C9H14O2.H2O



Acta Cryst. (1996). C52, 3163-3165    [ doi:10.1107/S0108270196010839 ]

5-(2-Naphthyl)thio-1-phenyltetrazole: Chemical Reactivity and Electronic Effects of Conjugation through Sulfur

J. A. C. Alves, C. J. Dillon and R. A. W. Johnstone

Formula: C17H12N4S



Acta Cryst. (1996). C52, 3165-3167    [ doi:10.1107/S0108270196009754 ]

(3S,5S,1'S)-3-Benzyl-5-[1'-(tert-butoxycarbonylamino)-2'-phenylethyl]-4,5-dihydrofuran-2(3H)-one

J. Sopková, P. Vojtísek, J. Litera and M. Soucek

Formula: C24H29NO4



Acta Cryst. (1996). C52, 3167-3169    [ doi:10.1107/S0108270196009535 ]

Ethylmethylglyoxal Bis(amidinohydrazonium) Dichloride-Water (1/2)

J. Koskinen, M. Koskinen, I. Mutikainen, B. Mannfors and H. Elo

Formula: C7H18N82+.2Cl-.2H2O



Acta Cryst. (1996). C52, 3169-3171    [ doi:10.1107/S0108270196009857 ]

N-(tert-Butoxycarbonyl)-2-phenylglycine

A. M. González-Cameno, D. Badía, E. Domínguez, M. I. Arriortua, M. K. Urtiaga and X. Solans

Formula: C13H17NO4



Acta Cryst. (1996). C52, 3171-3173    [ doi:10.1107/S0108270196009419 ]

o-Cyanophenol

C. Beswick, M. Kubicki and P. W. Codding

Formula: C7H5NO



Acta Cryst. (1996). C52, 3173-3177    [ doi:10.1107/S0108270196009481 ]

2',3'-Dideoxy-3'-nitrothymidine and 2'-Propoxy-3'-nitrothymidine

S. Neidle, J. P. Chattopadhyaya, N. Hossain and A. Papchikhin

Formula: C10H13N3O6 and C13H19N3O7



Acta Cryst. (1996). C52, 3177-3179    [ doi:10.1107/S0108270196009456 ]

1-Methyl-2-phenyldecahydroquinolin-4-one Oxime

V. K. Ganesh, D. Velmurugan, A. Thiruvalluvar, V. Parthasarathi, N. Ramasubbu and D. Natarajan

Formula: C16H22N2O



Acta Cryst. (1996). C52, 3179-3181    [ doi:10.1107/S0108270196009432 ]

An Optically Active Pentacoordinate Silicate: (+)-Bis(triethylammonium) Bis[(R,R)-tartrato(4-)]diphenyldisilicate

Z.-G. Wang, S.-G. Liu, D. Wang and X.-M. Sui

Formula: 2C6H16N+.C20H14O12Si22-



Acta Cryst. (1996). C52, 3181-3183    [ doi:10.1107/S0108270196005562 ]

Oxopregnenyl 4-Allyloxybenzoate

D. W. Tomlin, T. J. Bunning, C. M. McHugh and W. W. Adams

Formula: C31H40O4



Acta Cryst. (1996). C52, 3183-3185    [ doi:10.1107/S0108270196009821 ]

A Bicyclo[2.2.1]heptenone System

K. A. Wheeler and C. J. Carrow

Formula: C36H27NO



Acta Cryst. (1996). C52, 3185-3188    [ doi:10.1107/S0108270196010980 ]

Tetraphenylphosphonium Perchlorate

J. J. Vittal and P. A. W. Dean

Formula: C24H20P+.ClO4-



Acta Cryst. (1996). C52, 3188-3190    [ doi:10.1107/S0108270196009882 ]

Mannose Phenylhydrazone, an Acyclic Monosaccharide Derivative

W. H. Ojala and W. B. Gleason

Formula: C12H18N2O5



Acta Cryst. (1996). C52, 3190-3193    [ doi:10.1107/S0108270196011900 ]

(±)-1,11-Dimethyl-3,9-dinitro-5,7-dihydrodibenz[c,e]oxepine

A. W. Roszak, V. E. Williams and R. P. Lemieux

Formula: C16H14N2O5



Acta Cryst. (1996). C52, 3193-3195    [ doi:10.1107/S0108270196005392 ]

(-)-Thebaine

C. H. Mahler, E. D. Stevens, M. L. Trudell and S. P. Nolan

Formula: C19H21NO3



Acta Cryst. (1996). C52, 3195-3196    [ doi:10.1107/S0108270196010360 ]

(Z)-N-Formylnornuciferin Isolated from Piper argyrophylum

O. Simonsen, S. K. Singh, J. Wengel and V. S. Parmar

Formula: C19H19NO3



Acta Cryst. (1996). C52, 3197-3198    [ doi:10.1107/S0108270196009687 ]

Chiral Hydroxylamines. III. 1-(N-Benzyl-N-hydroxyamino)-1-deoxy-1-(2-furyl)-2,3:4,5-di-O-isopropylidene-L-manno-pentitol

P. Merino, F. Junquera, F. L. Merchan and T. Tejero

Formula: C22H29NO6



Acta Cryst. (1996). C52, 3199-3202    [ doi:10.1107/S0108270196011134 ]

Two Schiff Base Ligands Derived from 2,2-Dimethyl-1,3-propanediamine

J. P. Corden, W. Errington, P. Moore, P. R. Phillips and M. G. H. Wallbridge

Formula: C23H30N2O2 and C31H30N2O2



Acta Cryst. (1996). C52, 3202-3204    [ doi:10.1107/S0108270196009171 ]

3-Methoxy-1,4-benzoquinone 4-Oxime

N. Sardone, O. Carugo, J. Charalambous and D. V. Raghvani

Formula: C7H7NO3



Acta Cryst. (1996). C52, 3204-3207    [ doi:10.1107/S0108270196009912 ]

cis- and trans-4-tert-Butylcyclohexyl p-Nitrobenzenesulfonate at 130K

J. M. White, J. Giordano and A. J. Green

Formula: cis- and trans-C16H23NO5S



Acta Cryst. (1996). C52, 3207-3210    [ doi:10.1107/S0108270196009948 ]

Stereochemistry of Chiral Sulfoxides used for the Synthesis of Antitumor Antibiotic Analogues of Sparsomycin

A. Hempel, N. Camerman, J. Grierson, D. Mastropaolo and A. Camerman

Formula: C18H27NO2S, C18H27NO2S and C16H15NO3S



Acta Cryst. (1996). C52, 3210-3213    [ doi:10.1107/S0108270196010281 ]

Methyl (1R,2R)- and (1S,2S)-1-Cyano-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]cyclopropane-1-carboxylate

C. Cativiela, M. D. Díaz-de-Villegas, J. A. Gálvez, A. I. Jiménez and M. P. López

Formula: Two isomers of C11H15NO4



Acta Cryst. (1996). C52, 3213-3215    [ doi:10.1107/S0108270196009675 ]

A Strained Tricyclic Product of a Dipolar 1,3-Cycloaddition Reaction of Diazepine

A. Hasnaoui, M. El Messaoudi, J. P. Lavergne, M. Giorgi and M. Pierrot

Formula: C27H28Cl2N6O4



Acta Cryst. (1996). C52, 3216-3217    [ doi:10.1107/S0108270196010475 ]

Glycoric Acid, a New Degraded Carotenoid from Glycosmis arborea

T. Kiyotani, K. Masuda, H. Ageta, A. K. Chakravarty and B. Das

Formula: C12H20O4



Acta Cryst. (1996). C52, 3218-3219    [ doi:10.1107/S0108270196009122 ]

Methyl [alpha]-D-Lyxopyranoside

A. G. Evdokimov and F. Frolow

Formula: C6H12O5



Acta Cryst. (1996). C52, 3219-3222    [ doi:10.1107/S0108270196012152 ]

A Strained Cyclononadienyne

W. Clegg, A. R. Al Dulayymi and M. S. Baird

Formula: C12H11ClO2



Acta Cryst. (1996). C52, 3222-3224    [ doi:10.1107/S0108270196009845 ]

(E)- and (Z)-4-Ethynyl-4'-nitrostilbene

D. C. R. Hockless, I. R. Whittall and M. G. Humphrey

Formula: Two isomers of C16H11NO2



Acta Cryst. (1996). C52, 3225-3227    [ doi:10.1107/S0108270196009523 ]

Trinitrophloroglucinol

J. J. Wolff, F. Gredel, H. Irngartinger and T. Dreier

Formula: C6H3N3O9



Acta Cryst. (1996). C52, 3227-3229    [ doi:10.1107/S0108270196011158 ]

(S),(E)-5-Methoxycarbonyl-2-triphenylmethylaminohex-4-en-4-olide

V. Nastopoulos, C. Athanassopoulos, D. Papaioannou and E. Gavuzzo

Formula: C27H25NO4



Acta Cryst. (1996). C52, 3229-3232    [ doi:10.1107/S0108270196010037 ]

2,4,6-Tri-O-benzyl-myo-inositol 1,3,5-Tris(dibenzylphosphate)

V. Graingeot, C. Brigando, B. Faure and D. Benlian

Formula: C69H69O15P3



Acta Cryst. (1996). C52, 3232-3234    [ doi:10.1107/S0108270196011031 ]

Conformation of Crystalline 3-(4-Methoxyphenyl)-2,2,4,4-tetramethylpentane

D. J. Collins, G. D. Fallon and H. A. Jacobs

Formula: C16H26O



Acta Cryst. (1996). C52, 3234-3236    [ doi:10.1107/S0108270196009973 ]

4,4'-[1,6-Hexanediylbis(oxy)]bisbenzaldehyde

F. Artzner, P.-A. Albouy, G. Berruyer, M. Veber, C. Mérienne and F. Robert

Formula: C20H22O4



Acta Cryst. (1996). C52, 3236-3238    [ doi:10.1107/S0108270196011912 ]

5-(2-Aminophenyl)-1,3,4-oxadiazol-2(3H)-one

J. S. Davidson and J. Trotter

Formula: C8H7N3O2



Acta Cryst. (1996). C52, 3238-3240    [ doi:10.1107/S0108270196011274 ]

3,3-(Oxydiethyl)-1,2-di(o-methylphenyl)guanidinium Chloride Monohydrate

L. Sudha, K. Subramanian, J. Senthil Selvan, Th. Steiner, G. Koellner, K. Ramdas and N. Srinivasan

Formula: C19H24N3O+.Cl-.H2O



Acta Cryst. (1996). C52, 3240-3243    [ doi:10.1107/S0108270196008797 ]

2[alpha],3[alpha]:7[alpha],8[alpha]-Diépoxy-cis-himachalane

A. Chiaroni, C. Riche, E. Lassaba et A. Benharref

Formula: C15H24O2



Acta Cryst. (1996). C52, 3243-3246    [ doi:10.1107/S0108270196009420 ]

2-(2,6-Di-tert-butyl-4-methylphenoxy)-2,4,4,6,6,8,8-heptachlorocyclo-2[bold lambda]5,4[bold lambda]5,6[bold lambda]5,8[bold lambda]5-tetraphosphazatetraene

T. Hökelek, A. Kiliç, S. Begeç, Z. Kiliç and M. Yildiz

Formula: C15H23Cl7N4OP4



Acta Cryst. (1996). C52, 3246-3248    [ doi:10.1107/S0108270196011146 ]

1,1,3,3-Tetramethylurea

C. S. Frampton and K. E. B. Parkes

Formula: C5H12N2O



Acta Cryst. (1996). C52, 3248-3250    [ doi:10.1107/S0108270196010232 ]

An Inorganic N-Amino Analogue of Pyrrole: a Five-Membered Ring with Methylhydrazine and Two B Atoms as Building Blocks

U. Engelhardt and S. S. Park

Formula: C14H18B2N4



Acta Cryst. (1996). C52, 3250-3252    [ doi:10.1107/S0108270196010797 ]

3,7-Bis(2-thienyl)-1,5,2,4,6,8-dithiatetrazocine

T. M. Barclay, A. W. Cordes, R. T. Oakley and K. E. Preuss

Formula: C10H6N4S4



Acta Cryst. (1996). C52, 3252-3256    [ doi:10.1107/S0108270196010219 ]

Crystalline Complexes Involving Amino Acids. I. L-Argininium Hydrogen Squarate

O. Angelova, V. Velikova, T. Kolev and V. Radomirska

Formula: C6H15N4O2+.C4HO4-



Acta Cryst. (1996). C52, 3256-3258    [ doi:10.1107/S0108270196010268 ]

5-Chloro-2-[(2-hydroxybenzylidene)aminomethyl]phenol

S. Kevran, A. Elmali and Y. Elerman

Formula: C14H12ClNO2



Acta Cryst. (1996). C52, 3258-3260    [ doi:10.1107/S0108270196011754 ]

4,5-Dihydroxy-1-nitroanthracene-9,10-dione

A. V. Yatsenko, K. A. Paseshnichenko and S. I. Popov

Formula: C14H7NO6


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Acta Cryst. (1996). C52, 3261-3262    [ doi:10.1107/S0108270196099726 ]

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