Acta Crystallographica Section C

Crystal Structure Communications

Volume 53, Part 2 (February 1997)


Cover illustrationCover illustration: A Tetranuclear Iron Cluster Complex: \[{Fe(CO)3}3{mu3-CC\[Fe(CO)2(eta5-C5H5)\]C(CF3)}\], see Muir, Manojlovic-Muir, Morrice, Guennou, Pétillon & Rumin, pages 219-222. Displacement ellipsoids are shown at the 30% probability level.

inorganic compounds



Acta Cryst. (1997). C53, 163-165    [ doi:10.1107/S0108270196011687 ]

Ba6V4O5S11

J. B. Litteer, J. C. Fettinger and B. W. Eichhorn

Synopsis: The structure of Ba6V4O5S11 contains isolated VS43-, VOS33- and VO2S23- tetrahedra separated by nine- and ten-coordinate Ba2+ ions.

Formula: Ba6V4O5S11



Acta Cryst. (1997). C53, 165-167    [ doi:10.1107/S0108270196013765 ]

K2WSe4

D. Röhnert, C. Näther and W. Bensch

Synopsis: K2WSe4 has a structure based on isolated slightly distorted WSe4 tetrahedra joined via K+ ions. The compound is isotypic with the previously reported Rb and Cs analogues and crystallizes in the [beta]-K2SO4 structure type.

Formula: K2WSe4



Acta Cryst. (1997). C53, 167-169    [ doi:10.1107/S0108270196011869 ]

A New Polymorph of Li4P2O7

A. Daidouh, M. L. Veiga, C. Pico and M. Martinez-Ripoll

Synopsis: The structure of this new polymorph of Li4P2O7 consists of Li-O tetrahedra and pyrophosphate groups connected to each other through edges and vertices.

Formula: Li4P2O7


metal-organic compounds



Acta Cryst. (1997). C53, 170-171    [ doi:10.1107/S0108270196013480 ]

A New Decavanadate with Mixed Cations, [Li(H2O)4]2[N(CH3)4]4[V10O28].4H2O

P. Y. Zavalij, T. Chirayil, M. S. Whittingham, V. K. Pecharsky and R. A. Jacobson

Formula: (C4H12N)4[Li(H2O)4]2[V10O28].4H2O



Acta Cryst. (1997). C53, 172-174    [ doi:10.1107/S0108270196011948 ]

The First Example of a cis-Platinum Analogue with Two Directly Bridged Imidazoles: [Pt(mimim)Cl2].Et4NCl

S. Karentzopoulos, H. Engelking, B. Bremer, N. Paschke and B. Krebs

Formula: (C8H20N)[PtCl2(C7H8N4)]Cl



Acta Cryst. (1997). C53, 174-176    [ doi:10.1107/S0108270196013200 ]

fac-Tris(6-methyl-2-mercaptopyridinato)cobalt(III) at 150K

C. Fielding, S. Parsons and R. E. P. Winpenny

Formula: [Co(C6H6NS)3]



Acta Cryst. (1997). C53, 176-179    [ doi:10.1107/S0108270196011572 ]

Tetraaquabis(p-nitrosalicylato) Complexes of Zinc(II) and Cobalt(II)

M. N. Tahir, D. Ülkü, E. M. Movsumov and T. Hökelek

Formula: [Co(C7H4NO5)2(H2O)4] and [Zn(C7H4NO5)2(H2O)4]



Acta Cryst. (1997). C53, 179-181    [ doi:10.1107/S0108270196012590 ]

Bis{2-[(2-hydroxybenzyl)iminomethyl]phenolato(2 -)-O:O,N,O'}dicopper(II)

D. Ülkü, F. Ercan, O. Atakol, I. Ercan and A. Gencer

Formula: [Cu2(C14H11NO2)2]



Acta Cryst. (1997). C53, 181-183    [ doi:10.1107/S0108270196012966 ]

Bis{2-[(3-aminopropyl)iminomethyl]-4,6-dinitrophenolato-O,N,N'}nickel(II)

M. N. Tahir, D. Ülkü, H. Nazir and O. Atakol

Formula: [Ni(C10H11N4O5)2]



Acta Cryst. (1997). C53, 183-185    [ doi:10.1107/S0108270196013157 ]

2-[(2,3-Dimethylphenyl)amino]benzoato-O:O'}-trimethyltin(IV)

M. N. Tahir, D. Ülkü, M. Danish, S. Ali, A. Badshah and M. Mazhar

Formula: [Sn(C15H14NO2)(CH3)3]



Acta Cryst. (1997). C53, 185-187    [ doi:10.1107/S0108270196012723 ]

Tetracarbonyl([bold eta]2:2-1,5-cyclooctadiene)molybdenum(0)

D. Ülkü, M. N. Tahir and S. Özkar

Formula: [Mo(C8H12)(CO)4]



Acta Cryst. (1997). C53, 187-189    [ doi:10.1107/S0108270196013170 ]

Diaquabis(N,N-diethylnicotinamide-N1)bis(2-hydroxybenzoato-O)cobalt(II)

T. Hökelek and H. Necefouglu

Formula: [Co(C7H5O3)2(C10H14N2O)2(H2O)2]



Acta Cryst. (1997). C53, 190-191    [ doi:10.1107/S0108270196011705 ]

[(Carbazolylmethyl)dimethylamine-N]trimethylgallium

W. Gu, Y. Pan, Y. Shen, X. Huang, H. Sun and X. Sun

Formula: [Ga(CH3)3(C15H16N2)]



Acta Cryst. (1997). C53, 191-193    [ doi:10.1107/S0108270196012796 ]

Tetrachlorobis(N,N,N',N'-tetramethylethylenediamine-N,N')thorium(IV)

D. Rabinovich, G. L. Schimek, W. T. Pennington, J. B. Nielsen and K. D. Abney

Formula: [ThCl4(C6H16N2)2]



Acta Cryst. (1997). C53, 193-195    [ doi:10.1107/S0108270196012395 ]

Metal-[alpha],[omega]-Dicarboxylate Complexes. I. Aqua(2,2'-bipyridyl-N,N')(malonato-O,O')copper(II) Monohydrate

E. Suresh and M. M. Bhadbhade

Formula: [Cu(C3H2O4)(C10H8N2)(H2O)].H2O



Acta Cryst. (1997). C53, 195-197    [ doi:10.1107/S0108270196012486 ]

Luminescent Tris(3-ethyl-1,5-diaza-3-azonia-7-phosphatricyclo[3.3.1.13,7]decane-P)gold(I) Tetraiodide Trihydrate, [(EtTPA)3Au]I4.3H2O

J. M. Forward, R. J. Staples, C. W. Liu and J. P. Fackler Jnr

Formula: [Au(C8H17N3P)3]I4.3H2O



Acta Cryst. (1997). C53, 197-200    [ doi:10.1107/S0108270196013108 ]

[bold mu]-Chloro-1:2[bold kappa]2Cl-trichloro-2[bold kappa]3Cl-(2,4-dimethyl-5,8-diazadec-4-ene-2,10-diamine-1[bold kappa]4N,N',N'',N''')copper(II)zinc(II)

O. P. Gladkikh, N. F. Curtis and S. L. Heath

Formula: [CuZnCl4(C10H24N4)]



Acta Cryst. (1997). C53, 200-202    [ doi:10.1107/S0108270196012024 ]

Bis(piperazinium) Pentakis(trioxomolybdo)bis(ethylphosphonate) Dihydrate

W. T. A. Harrison, L. L. Dussack and A. J. Jacobson

Formula: (C4H12N2)2[Mo5O15(C2H5O3P)2].2H2O



Acta Cryst. (1997). C53, 202-204    [ doi:10.1107/S0108270196012875 ]

Dichloro([bold eta]5-cyclopentadienyl)(phenylimido)vanadium(V)

M. C. W. Chan, J. M. Cole, V. C. Gibson and J. A. K. Howard

Formula: [VCl2(C5H5)(C6H5N)]



Acta Cryst. (1997). C53, 204-206    [ doi:10.1107/S0108270196006129 ]

Copper(II) and Nickel(II) Complexes of 4-Methyl-4,7-diazadecane-1,10-diamine

T.-H. Lu, T. H. Tahirov, K. Shu and C.-S. Chung

Formula: [Cu(C9H24N4)(ClO4)]ClO4 and [Ni(C9H24N4)](ClO4)2



Acta Cryst. (1997). C53, 207-209    [ doi:10.1107/S0108270196012978 ]

[6-(2-Pyridylmethyl)-2,6,10-triazaundecane-1,11-diylbis(2-phenolato)(1 -)]copper(II) Tetrafluoroborate Methanol Acetonitrile Solvate (1/1/0.3/0.7)

D. E. Fenton, Q.-Y. He and V. McKee

Formula: [Cu(C26H33N4O2)]BF4.0.3CH4O.0.7C2H3N



Acta Cryst. (1997). C53, 209-212    [ doi:10.1107/S0108270196011699 ]

Disorder in Bis(tetraethylammonium) Bis([bold mu]-sulfido)bis[(1,2,3,4-tetrathiabutane-1,4-diyl-S,S)thiotungstate(V)]

A. K. Mukherjee, P. K. Das, M. Mukherjee, P. K. Chakraborty and R. Bhattacharya

Formula: (C8H20N)2[W2S12]



Acta Cryst. (1997). C53, 212-213    [ doi:10.1107/S0108270196012292 ]

The First Example of a Discrete Di(carboxylato)triorganostannate: Tetramethylammonium Triphenylbis(trifluoroacetato)stannate

S. W. Ng and V. G. Kumar Das

Formula: (C4H12N)[Sn(C2F3O2)2(C6H5)3]



Acta Cryst. (1997). C53, 213-215    [ doi:10.1107/S0108270196013571 ]

A Pteridin-6-yl Alkene-1,2-dithiolate Complex of Cobalt

R. L. Beddoes, A. Dinsmore, M. Helliwell, C. D. Garner and J. A. Joule

Formula: [Co(C5H5)(C12H12N6OS2)].H2O



Acta Cryst. (1997). C53, 216-217    [ doi:10.1107/S0108270196013479 ]

(+)589-[Lambda]-Amminebromobis(ethylenediamine-N,N')cobalt(III) Dibromide

H. Nakagawa, S. Ohba, K. Asakura, T. Miura, A. Tanaka and S. Osanai

Formula: [CoBr(C2H8N2)2(NH3)]Br2



Acta Cryst. (1997). C53, 217-219    [ doi:10.1107/S0108270196013030 ]

Chelation of 2,6-Bis(hydroxymethyl)pyridine in cis-Dichloro(triphenylphosphine-P)[2-(oxymethylene-O)-6-(hydroxymethyl)pyridine-N]oxorhenium(V)-Water (2/1)

T. I. A. Gerber, J. Perils, J. G. H. Du Preez and G. Bandoli

Formula: 2[ReCl2O(C7H8NO2)(C18H15P)].H2O



Acta Cryst. (1997). C53, 219-222    [ doi:10.1107/S0108270196012632 ]

A Tetranuclear Iron Cluster Complex: [{Fe(CO)3}3{[bold mu]3-CC[Fe(CO)2([bold eta]5-C5H5)]C(CF3)}]

K. W. Muir, L. Manojlovic-Muir, F. Morrice, K. Guennou, F. Pétillon and R. Rumin

Formula: [Fe4(C5H5)(C4F3)(CO)11]


organic compounds



Acta Cryst. (1997). C53, 223-225    [ doi:10.1107/S010827019601147X ]

The Unusual Structure of a C-Arylated Gibberellin Bis-[bold gamma]-lactone Formed from a Free Radical-Initiated Cyclization

L. N. Mander, M. S. Sherburn and A. C. Willis

Formula: C29H30O8.C2H3N



Acta Cryst. (1997). C53, 225-227    [ doi:10.1107/S0108270196012656 ]

4-Bromo-2,6-dichlorobenzonitrile

D. Britton

Formula: C7H2BrCl2N



Acta Cryst. (1997). C53, 227-229    [ doi:10.1107/S0108270196012310 ]

2,4-Dinitro-trans-cinnamic Acid

V. R. Thalladi, C. V. K. Sharma and G. R. Desiraju

Formula: C9H6N2O6



Acta Cryst. (1997). C53, 229-231    [ doi:10.1107/S0108270196013303 ]

[Ph3PH][nido-B11H14]

T. D. McGrath and A. J. McGrathand

Formula: C18H16P+.B11H14-



Acta Cryst. (1997). C53, 231-234    [ doi:10.1107/S0108270196012504 ]

Tetrakis(p-dimethylaminophenyl)ethylene Hemibenzene Solvate

C. Näther and H. Bock

Formula: C34H40N4.0.5C6H6



Acta Cryst. (1997). C53, 234-236    [ doi:10.1107/S0108270196012693 ]

[alpha],[beta]-Trehalose Monohydrate

T. Taga, Y. Miwa and Z. Min

Formula: C12H22O11.H2O



Acta Cryst. (1997). C53, 236-238    [ doi:10.1107/S0108270196012851 ]

(6S)-8-C-Chloro-6,7,8-trideoxy-1,2:3,4-di-O-isopropylidene-[alpha]-D-galacto-octa-6,7-dienopyranose

D. Horton, Q. Liu, R. L. Luck and J. V. Silverton

Formula: C14H19ClO5



Acta Cryst. (1997). C53, 238-239    [ doi:10.1107/S0108270196012802 ]

9,10-Dihydro-9-oxo-10-acridineacetic Acid

D. Dobrzynska and I. Turowska-Tyrk

Formula: C15H11NO3



Acta Cryst. (1997). C53, 240-241    [ doi:10.1107/S0108270196013121 ]

cis-1,1'-Dimethyl-3,3'-diphenyl-2,2'-biimidazolidinylidene

D. Ülkü, M. N. Tahir, B. Çetinkaya and I. Özdemir

Formula: C20H24N4



Acta Cryst. (1997). C53, 241-243    [ doi:10.1107/S0108270196012620 ]

9,10-Bis{2-[4-(N,N-diphenylamino)phenyl]ethynyl}anthracene

D. Venkataraman, P.-W. Wang and J. S. Moore

Formula: C54H36N2



Acta Cryst. (1997). C53, 243-245    [ doi:10.1107/S0108270196013224 ]

A Novel Tricyclic Cyclobutanone Ketal

J. F. Britten, K. Kassam and J. Warkentin

Formula: C15H22O5



Acta Cryst. (1997). C53, 245-247    [ doi:10.1107/S0108270196012498 ]

3-Acetamido-5-O-acetyl-1,2-O-isopropylidene-D-ribofuranose

K. A. Abboud, I. B. Parr and B. A. Horenstein

Formula: C12H19NO6



Acta Cryst. (1997). C53, 247-248    [ doi:10.1107/S010827019601298X ]

Bis[(S)-(-)-[alpha]-methylbenzyl]thiourea

P. J. Bailey, K. J. Grant and S. Parsons

Formula: C17H20N2S



Acta Cryst. (1997). C53, 248-251    [ doi:10.1107/S0108270196013467 ]

2',3'-Diphenyl-Substituted p-Terphenyls

V. Nastopoulos, J. Kallitsis, H. Naarmann, O. Dideberg and L. Dupont

Formula: C31H24O and C32H26O2



Acta Cryst. (1997). C53, 251-253    [ doi:10.1107/S0108270196011420 ]

A Functionalized Dimethyl 1,3-Butadiene-2,3-dicarboxylate

D. Zellmer, R. Niewa, H. Preut and R. P. Kreher

Formula: C21H27NO4



Acta Cryst. (1997). C53, 253-255    [ doi:10.1107/S010827019601390X ]

1,13-Tridecanediol

N. Nakamura, Y. Tanihara and T. Takayama

Formula: C13H28O2



Acta Cryst. (1997). C53, 255-257    [ doi:10.1107/S0108270196010682 ]

L-Histidylglycinium Dichloride

Th. Steiner

Formula: C8H14N4O32+.2Cl-



Acta Cryst. (1997). C53, 257-261    [ doi:10.1107/S010827019601181X ]

3-Ethoxycarbonyl-5-methoxycarbonyl-2,6-dimethyl-4-(3-nitrophenyl)pyridinium Nitrate, Dineopentyl 2,6-Dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate and Dihexyl 2,6-Dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate

K. R. Rowan and E. M. Holt

Formula: C18H19N2O6+.NO3-, C25H32N2O6 and C27H36N2O6



Acta Cryst. (1997). C53, 261-264    [ doi:10.1107/S0108270196012887 ]

Triterpenoide. X. Über neue isomere Triterpenlactone

A. Gzella, L. Zaprutko und U. Wrzeciono

Formula: Three isomers of C29H42O6



Acta Cryst. (1997). C53, 264-266    [ doi:10.1107/S0108270196012863 ]

Methyl 3-Deoxy-[alpha]-D-arabino-hexopyranoside

A. G. Evdokimov and F. Frolow

Formula: C7H14O5


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