Acta Crystallographica Section C

Crystal Structure Communications

Volume 53, Part 2 (February 1997)

Cover illustration: A Tetranuclear Iron Cluster Complex: \[{Fe(CO)₃}₃{mu₃-CC\[Fe(CO)₂(eta⁵-C₅H₅)\]C(CF₃)}\], see Muir, Manojlovic-Muir, Morrice, Guennou, Pétillon & Rumin, pages 219-222. Displacement ellipsoids are shown at the 30% probability level.

inorganic compounds
metal-organic compounds
organic compounds

inorganic compounds

Acta Cryst. (1997). C53, 163-165 [ doi:10.1107/S0108270196011687 ]

Ba₆V₄O₅S₁₁

J. B. Litteer, J. C. Fettinger and B. W. Eichhorn

Synopsis: The structure of Ba₆V₄O₅S₁₁ contains isolated VS₄^3-, VOS₃^3- and VO₂S₂^3- tetrahedra separated by nine- and ten-coordinate Ba²⁺ ions.

Formula: Ba₆V₄O₅S₁₁

Acta Cryst. (1997). C53, 165-167 [ doi:10.1107/S0108270196013765 ]

K₂WSe₄

D. Röhnert, C. Näther and W. Bensch

Synopsis: K₂WSe₄ has a structure based on isolated slightly distorted WSe₄ tetrahedra joined via K⁺ ions. The compound is isotypic with the previously reported Rb and Cs analogues and crystallizes in the [beta] -K₂SO₄ structure type.

Formula: K₂WSe₄

Acta Cryst. (1997). C53, 167-169 [ doi:10.1107/S0108270196011869 ]

A New Polymorph of Li₄P₂O₇

A. Daidouh, M. L. Veiga, C. Pico and M. Martinez-Ripoll

Synopsis: The structure of this new polymorph of Li₄P₂O₇ consists of Li-O tetrahedra and pyrophosphate groups connected to each other through edges and vertices.

Formula: Li₄P₂O₇

metal-organic compounds

Acta Cryst. (1997). C53, 170-171 [ doi:10.1107/S0108270196013480 ]

A New Decavanadate with Mixed Cations, [Li(H₂O)₄]₂[N(CH₃)₄]₄[V₁₀O₂₈].4H₂O

P. Y. Zavalij, T. Chirayil, M. S. Whittingham, V. K. Pecharsky and R. A. Jacobson

Formula: (C₄H₁₂N)₄[Li(H₂O)₄]₂[V₁₀O₂₈].4H₂O

Acta Cryst. (1997). C53, 172-174 [ doi:10.1107/S0108270196011948 ]

The First Example of a cis-Platinum Analogue with Two Directly Bridged Imidazoles: [Pt(mimim)Cl₂].Et₄NCl

S. Karentzopoulos, H. Engelking, B. Bremer, N. Paschke and B. Krebs

Formula: (C₈H₂₀N)[PtCl₂(C₇H₈N₄)]Cl

Acta Cryst. (1997). C53, 174-176 [ doi:10.1107/S0108270196013200 ]

fac-Tris(6-methyl-2-mercaptopyridinato)cobalt(III) at 150K

C. Fielding, S. Parsons and R. E. P. Winpenny

Formula: [Co(C₆H₆NS)₃]

Acta Cryst. (1997). C53, 176-179 [ doi:10.1107/S0108270196011572 ]

Tetraaquabis(p-nitrosalicylato) Complexes of Zinc(II) and Cobalt(II)

M. N. Tahir, D. Ülkü, E. M. Movsumov and T. Hökelek

Formula: [Co(C₇H₄NO₅)₂(H₂O)₄] and [Zn(C₇H₄NO₅)₂(H₂O)₄]

Acta Cryst. (1997). C53, 179-181 [ doi:10.1107/S0108270196012590 ]

Bis{2-[(2-hydroxybenzyl)iminomethyl]phenolato(2 -)-O:O,N,O'}dicopper(II)

D. Ülkü, F. Ercan, O. Atakol, I. Ercan and A. Gencer

Formula: [Cu₂(C₁₄H₁₁NO₂)₂]

Acta Cryst. (1997). C53, 181-183 [ doi:10.1107/S0108270196012966 ]

Bis{2-[(3-aminopropyl)iminomethyl]-4,6-dinitrophenolato-O,N,N'}nickel(II)

M. N. Tahir, D. Ülkü, H. Nazir and O. Atakol

Formula: [Ni(C₁₀H₁₁N₄O₅)₂]

Acta Cryst. (1997). C53, 183-185 [ doi:10.1107/S0108270196013157 ]

2-[(2,3-Dimethylphenyl)amino]benzoato-O:O'}-trimethyltin(IV)

M. N. Tahir, D. Ülkü, M. Danish, S. Ali, A. Badshah and M. Mazhar

Formula: [Sn(C₁₅H₁₄NO₂)(CH₃)₃]

Acta Cryst. (1997). C53, 185-187 [ doi:10.1107/S0108270196012723 ]

Tetracarbonyl(^2:2-1,5-cyclooctadiene)molybdenum(0)

D. Ülkü, M. N. Tahir and S. Özkar

Formula: [Mo(C₈H₁₂)(CO)₄]

Acta Cryst. (1997). C53, 187-189 [ doi:10.1107/S0108270196013170 ]

Diaquabis(N,N-diethylnicotinamide-N¹)bis(2-hydroxybenzoato-O)cobalt(II)

T. Hökelek and H. Necefouglu

Formula: [Co(C₇H₅O₃)₂(C₁₀H₁₄N₂O)₂(H₂O)₂]

Acta Cryst. (1997). C53, 190-191 [ doi:10.1107/S0108270196011705 ]

[(Carbazolylmethyl)dimethylamine-N]trimethylgallium

W. Gu, Y. Pan, Y. Shen, X. Huang, H. Sun and X. Sun

Formula: [Ga(CH₃)₃(C₁₅H₁₆N₂)]

Acta Cryst. (1997). C53, 191-193 [ doi:10.1107/S0108270196012796 ]

Tetrachlorobis(N,N,N',N'-tetramethylethylenediamine-N,N')thorium(IV)

D. Rabinovich, G. L. Schimek, W. T. Pennington, J. B. Nielsen and K. D. Abney

Formula: [ThCl₄(C₆H₁₆N₂)₂]

Acta Cryst. (1997). C53, 193-195 [ doi:10.1107/S0108270196012395 ]

Metal-,-Dicarboxylate Complexes. I. Aqua(2,2'-bipyridyl-N,N')(malonato-O,O')copper(II) Monohydrate

E. Suresh and M. M. Bhadbhade

Formula: [Cu(C₃H₂O₄)(C₁₀H₈N₂)(H₂O)].H₂O

Acta Cryst. (1997). C53, 195-197 [ doi:10.1107/S0108270196012486 ]

Luminescent Tris(3-ethyl-1,5-diaza-3-azonia-7-phosphatricyclo[3.3.1.1^3,7]decane-P)gold(I) Tetraiodide Trihydrate, [(EtTPA)₃Au]I₄.3H₂O

J. M. Forward, R. J. Staples, C. W. Liu and J. P. Fackler Jnr

Formula: [Au(C₈H₁₇N₃P)₃]I₄.3H₂O

Acta Cryst. (1997). C53, 197-200 [ doi:10.1107/S0108270196013108 ]

-Chloro-1:2²Cl-trichloro-2³Cl-(2,4-dimethyl-5,8-diazadec-4-ene-2,10-diamine-1⁴N,N',N'',N''')copper(II)zinc(II)

O. P. Gladkikh, N. F. Curtis and S. L. Heath

Formula: [CuZnCl₄(C₁₀H₂₄N₄)]

Acta Cryst. (1997). C53, 200-202 [ doi:10.1107/S0108270196012024 ]

Bis(piperazinium) Pentakis(trioxomolybdo)bis(ethylphosphonate) Dihydrate

W. T. A. Harrison, L. L. Dussack and A. J. Jacobson

Formula: (C₄H₁₂N₂)₂[Mo₅O₁₅(C₂H₅O₃P)₂].2H₂O

Acta Cryst. (1997). C53, 202-204 [ doi:10.1107/S0108270196012875 ]

Dichloro(⁵-cyclopentadienyl)(phenylimido)vanadium(V)

M. C. W. Chan, J. M. Cole, V. C. Gibson and J. A. K. Howard

Formula: [VCl₂(C₅H₅)(C₆H₅N)]

Acta Cryst. (1997). C53, 204-206 [ doi:10.1107/S0108270196006129 ]

Copper(II) and Nickel(II) Complexes of 4-Methyl-4,7-diazadecane-1,10-diamine

T.-H. Lu, T. H. Tahirov, K. Shu and C.-S. Chung

Formula: [Cu(C₉H₂₄N₄)(ClO₄)]ClO₄ and [Ni(C₉H₂₄N₄)](ClO₄)₂

Acta Cryst. (1997). C53, 207-209 [ doi:10.1107/S0108270196012978 ]

[6-(2-Pyridylmethyl)-2,6,10-triazaundecane-1,11-diylbis(2-phenolato)(1 -)]copper(II) Tetrafluoroborate Methanol Acetonitrile Solvate (1/1/0.3/0.7)

D. E. Fenton, Q.-Y. He and V. McKee

Formula: [Cu(C₂₆H₃₃N₄O₂)]BF₄.0.3CH₄O.0.7C₂H₃N

Acta Cryst. (1997). C53, 209-212 [ doi:10.1107/S0108270196011699 ]

Disorder in Bis(tetraethylammonium) Bis(-sulfido)bis[(1,2,3,4-tetrathiabutane-1,4-diyl-S,S)thiotungstate(V)]

A. K. Mukherjee, P. K. Das, M. Mukherjee, P. K. Chakraborty and R. Bhattacharya

Formula: (C₈H₂₀N)₂[W₂S₁₂]

Acta Cryst. (1997). C53, 212-213 [ doi:10.1107/S0108270196012292 ]

The First Example of a Discrete Di(carboxylato)triorganostannate: Tetramethylammonium Triphenylbis(trifluoroacetato)stannate

S. W. Ng and V. G. Kumar Das

Formula: (C₄H₁₂N)[Sn(C₂F₃O₂)₂(C₆H₅)₃]

Acta Cryst. (1997). C53, 213-215 [ doi:10.1107/S0108270196013571 ]

A Pteridin-6-yl Alkene-1,2-dithiolate Complex of Cobalt

R. L. Beddoes, A. Dinsmore, M. Helliwell, C. D. Garner and J. A. Joule

Formula: [Co(C₅H₅)(C₁₂H₁₂N₆OS₂)].H₂O

Acta Cryst. (1997). C53, 216-217 [ doi:10.1107/S0108270196013479 ]

(+)₅₈₉--Amminebromobis(ethylenediamine-N,N')cobalt(III) Dibromide

H. Nakagawa, S. Ohba, K. Asakura, T. Miura, A. Tanaka and S. Osanai

Formula: [CoBr(C₂H₈N₂)₂(NH₃)]Br₂

Acta Cryst. (1997). C53, 217-219 [ doi:10.1107/S0108270196013030 ]

Chelation of 2,6-Bis(hydroxymethyl)pyridine in cis-Dichloro(triphenylphosphine-P)[2-(oxymethylene-O)-6-(hydroxymethyl)pyridine-N]oxorhenium(V)-Water (2/1)

T. I. A. Gerber, J. Perils, J. G. H. Du Preez and G. Bandoli

Formula: 2[ReCl₂O(C₇H₈NO₂)(C₁₈H₁₅P)].H₂O

Acta Cryst. (1997). C53, 219-222 [ doi:10.1107/S0108270196012632 ]

A Tetranuclear Iron Cluster Complex: [{Fe(CO)₃}₃{₃-CC[Fe(CO)₂(⁵-C₅H₅)]C(CF₃)}]

K. W. Muir, L. Manojlovic-Muir, F. Morrice, K. Guennou, F. Pétillon and R. Rumin

Formula: [Fe₄(C₅H₅)(C₄F₃)(CO)₁₁]

organic compounds

Acta Cryst. (1997). C53, 223-225 [ doi:10.1107/S010827019601147X ]

The Unusual Structure of a C-Arylated Gibberellin Bis--lactone Formed from a Free Radical-Initiated Cyclization

L. N. Mander, M. S. Sherburn and A. C. Willis

Formula: C₂₉H₃₀O₈.C₂H₃N

Acta Cryst. (1997). C53, 225-227 [ doi:10.1107/S0108270196012656 ]

4-Bromo-2,6-dichlorobenzonitrile

D. Britton

Formula: C₇H₂BrCl₂N

Acta Cryst. (1997). C53, 227-229 [ doi:10.1107/S0108270196012310 ]

2,4-Dinitro-trans-cinnamic Acid

V. R. Thalladi, C. V. K. Sharma and G. R. Desiraju

Formula: C₉H₆N₂O₆

Acta Cryst. (1997). C53, 229-231 [ doi:10.1107/S0108270196013303 ]

[Ph₃PH][nido-B₁₁H₁₄]

T. D. McGrath and A. J. McGrathand

Formula: C₁₈H₁₆P⁺.B₁₁H₁₄^-

Acta Cryst. (1997). C53, 231-234 [ doi:10.1107/S0108270196012504 ]

Tetrakis(p-dimethylaminophenyl)ethylene Hemibenzene Solvate

C. Näther and H. Bock

Formula: C₃₄H₄₀N₄.0.5C₆H₆

Acta Cryst. (1997). C53, 234-236 [ doi:10.1107/S0108270196012693 ]

,-Trehalose Monohydrate

T. Taga, Y. Miwa and Z. Min

Formula: C₁₂H₂₂O₁₁.H₂O

Acta Cryst. (1997). C53, 236-238 [ doi:10.1107/S0108270196012851 ]

(6S)-8-C-Chloro-6,7,8-trideoxy-1,2:3,4-di-O-isopropylidene--D-galacto-octa-6,7-dienopyranose

D. Horton, Q. Liu, R. L. Luck and J. V. Silverton

Formula: C₁₄H₁₉ClO₅

Acta Cryst. (1997). C53, 238-239 [ doi:10.1107/S0108270196012802 ]

9,10-Dihydro-9-oxo-10-acridineacetic Acid

D. Dobrzynska and I. Turowska-Tyrk

Formula: C₁₅H₁₁NO₃

Acta Cryst. (1997). C53, 240-241 [ doi:10.1107/S0108270196013121 ]

cis-1,1'-Dimethyl-3,3'-diphenyl-2,2'-biimidazolidinylidene

D. Ülkü, M. N. Tahir, B. Çetinkaya and I. Özdemir

Formula: C₂₀H₂₄N₄

Acta Cryst. (1997). C53, 241-243 [ doi:10.1107/S0108270196012620 ]

9,10-Bis{2-[4-(N,N-diphenylamino)phenyl]ethynyl}anthracene

D. Venkataraman, P.-W. Wang and J. S. Moore

Formula: C₅₄H₃₆N₂

Acta Cryst. (1997). C53, 243-245 [ doi:10.1107/S0108270196013224 ]

A Novel Tricyclic Cyclobutanone Ketal

J. F. Britten, K. Kassam and J. Warkentin

Formula: C₁₅H₂₂O₅

Acta Cryst. (1997). C53, 245-247 [ doi:10.1107/S0108270196012498 ]

3-Acetamido-5-O-acetyl-1,2-O-isopropylidene-D-ribofuranose

K. A. Abboud, I. B. Parr and B. A. Horenstein

Formula: C₁₂H₁₉NO₆

Acta Cryst. (1997). C53, 247-248 [ doi:10.1107/S010827019601298X ]

Bis[(S)-(-)--methylbenzyl]thiourea

P. J. Bailey, K. J. Grant and S. Parsons

Formula: C₁₇H₂₀N₂S

Acta Cryst. (1997). C53, 248-251 [ doi:10.1107/S0108270196013467 ]

2',3'-Diphenyl-Substituted p-Terphenyls

V. Nastopoulos, J. Kallitsis, H. Naarmann, O. Dideberg and L. Dupont

Formula: C₃₁H₂₄O and C₃₂H₂₆O₂

Acta Cryst. (1997). C53, 251-253 [ doi:10.1107/S0108270196011420 ]

A Functionalized Dimethyl 1,3-Butadiene-2,3-dicarboxylate

D. Zellmer, R. Niewa, H. Preut and R. P. Kreher

Formula: C₂₁H₂₇NO₄

Acta Cryst. (1997). C53, 253-255 [ doi:10.1107/S010827019601390X ]

1,13-Tridecanediol

N. Nakamura, Y. Tanihara and T. Takayama

Formula: C₁₃H₂₈O₂

Acta Cryst. (1997). C53, 255-257 [ doi:10.1107/S0108270196010682 ]

L-Histidylglycinium Dichloride

Th. Steiner

Formula: C₈H₁₄N₄O₃²⁺.2Cl^-

Acta Cryst. (1997). C53, 257-261 [ doi:10.1107/S010827019601181X ]

3-Ethoxycarbonyl-5-methoxycarbonyl-2,6-dimethyl-4-(3-nitrophenyl)pyridinium Nitrate, Dineopentyl 2,6-Dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate and Dihexyl 2,6-Dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate

K. R. Rowan and E. M. Holt

Formula: C₁₈H₁₉N₂O₆⁺.NO₃^-, C₂₅H₃₂N₂O₆ and C₂₇H₃₆N₂O₆

Acta Cryst. (1997). C53, 261-264 [ doi:10.1107/S0108270196012887 ]

Triterpenoide. X. Über neue isomere Triterpenlactone

A. Gzella, L. Zaprutko und U. Wrzeciono

Formula: Three isomers of C₂₉H₄₂O₆

Acta Cryst. (1997). C53, 264-266 [ doi:10.1107/S0108270196012863 ]

Methyl 3-Deoxy--D-arabino-hexopyranoside

A. G. Evdokimov and F. Frolow

Formula: C₇H₁₄O₅