Acta Crystallographica Section C

Crystal Structure Communications

Volume 53, Part 3 (March 1997)


Cover illustrationCover illustration: A New Mixed Oxide with (Bi12O14)n Columns: PbBi12Mo5O34, see Enjalbert, Hasselmann & Galy, pages 269-272. Projection of the structure on the (010) plane (left) and arrangement of the Bi atoms at the corners of octahedra in the (Bi12O14) columns (right).

inorganic compounds



Acta Cryst. (1997). C53, 267-269    [ doi:10.1107/S0108270196012309 ]

Caesium Gadolinium Tetratelluride

W. Bensch and P. Dürichen

Synopsis: CsGdTe4 comprises [GdTe4]nn- layers separated by Cs+ ions. Each Gd cation is in a square-antiprismatic environment of Te atoms.

Formula: CsGdTe4



Acta Cryst. (1997). C53, 269-272    [ doi:10.1107/S0108270196013698 ]

A New Mixed Oxide with (Bi12O14)n Columns: PbBi12Mo5O34

R. Enjalbert, G. Hasselmann and J. Galy

Synopsis: The structure of PbBi12Mo5O34 consists of (Bi12O14)n columns surrounded by MoO4 tetrahedra. The Pb atoms occupy specific sites between four tetrahedra.

Formula: PbBi12Mo5O34


metal-organic compounds



Acta Cryst. (1997). C53, 273-274    [ doi:10.1107/S0108270196013716 ]

Tetra(p-chlorophenyl)tin

S. W. Ng

Formula: [Sn(C6H4Cl)4]



Acta Cryst. (1997). C53, 274-276    [ doi:10.1107/S0108270196013704 ]

[Bis(N,N-dimethylthiocarbamoylthio)acetato-O]triphenyl(quinoline N-oxide-O)tin

S. W. Ng

Formula: [Sn(C6H5)3(C8H13N2O2S4)(C9H7NO)]



Acta Cryst. (1997). C53, 276-278    [ doi:10.1107/S0108270196013893 ]

(Diethylenetriamine)(imidazole)(thiocyanato)copper(II) Perchlorate

H.-M. Hu, H.-S. Sun, X.-H. Chen, Q. Zhao, Y. Pan, X.-Y. Huang and X.-Z. You

Formula: [Cu(NCS)(C4H13N3)(C3H4N2)]ClO4



Acta Cryst. (1997). C53, 278-279    [ doi:10.1107/S0108270196013169 ]

[[bold mu]-(1,4-Dibenzylpiperazine)-N:N']bis(trimethylindium) Dibenzene Solvate

X. Ma, Y. Pan, L. Wu, X. Huang, H. Sun and C. Zhu

Formula: [In2(C18H22N2)(CH3)6].2C6H6



Acta Cryst. (1997). C53, 280-282    [ doi:10.1107/S0108270196013844 ]

trans-Diiodobis(triphenylarsine-As)platinum(II)

S. Otto and A. Roodt

Formula: [PtI2(C18H15As)2]



Acta Cryst. (1997). C53, 282-283    [ doi:10.1107/S0108270196013868 ]

Bis(6-chloro-2-pyridonato-N,O)(4,4'-dimethyl-2,2'-bipyridine-N,N')zinc(II) Hydrate at 150 K

C. G. Mowat, S. Parsons, G. A. Solan and R. E. P. Winpenny

Formula: [Zn(C5H3ClNO)2(C12H12N2)].H2O



Acta Cryst. (1997). C53, 284-285    [ doi:10.1107/S0108270196010487 ]

Disodium Fluorescein Octahydrate

K. Yamaguchi, Z. Tamura and M. Maeda

Formula: 2Na+.C20H10O52-.8H2O



Acta Cryst. (1997). C53, 285-287    [ doi:10.1107/S0108270196013911 ]

Tetracarbonyl-1[bold kappa]2C,2[bold kappa]2C-[bold mu]-diphenylphosphido-P:P-[bold mu]-iodo-bis(triphenylphosphine)-1[bold kappa]P,2[bold kappa]P-diosmium(Os-Os) Benzene Solvate

A. W. Herlinger and A. L. Rheingold

Formula: [Os2I(C12H10P)(C18H15P)2(CO)4].C6H6



Acta Cryst. (1997). C53, 287-289    [ doi:10.1107/S0108270196011018 ]

Hetero-Ring Oxygen Coordination to Strontium in Strontium Bis(2-furancarboxylate)

B. Paluchowska, J. K. Maurin and J. Leciejewicz

Formula: [Sr(C5H3O3)2]



Acta Cryst. (1997). C53, 289-292    [ doi:10.1107/S0108270196013790 ]

[Bis(thiodiphenylphosphino-S)amido]chlorobis(dimethylphenylphosphine-P)nitridorhenium(V)

U. Abram, E. Schulz Lang and J. R. Dilworth

Formula: [ReNCl(C24H20NP2S2)(C8H11P)2]



Acta Cryst. (1997). C53, 292-293    [ doi:10.1107/S0108270196014229 ]

cis-Di(nitrato-O,O')bis(tricyclohexylphosphine oxide-O)nickel(II)

A. R. Kennedy, S. W. Sloss and M. D. Spicer

Formula: [Ni(NO3)2(C18H33OP)2]



Acta Cryst. (1997). C53, 294-296    [ doi:10.1107/S0108270196011341 ]

Bis[tris(2-hydroxyethyl)ammonium] Hexachloroplatinate(IV)

V. T. Yilmaz, H. Içbudak and R. A. Howie

Formula: (C6H16NO3)2[PtCl6]



Acta Cryst. (1997). C53, 296-298    [ doi:10.1107/S0108270196013364 ]

trans-Diaquabis(pyridine-2-carboxamide-N1,O)copper(II) Dichloride and Dibromide

L. Sieron and M. Bukowska-Strzyzewska

Formula: [Cu(C6H6N2O)2(H2O)2]Cl2 and [Cu(C6H6N2O)2(H2O)2]Br2



Acta Cryst. (1997). C53, 299-301    [ doi:10.1107/S0108270196012358 ]

(Benzoylacetonato-O,O')(2,2'-bipyridine-N,N')(nitrato-O)copper(II)

L. Zhang, D. Xu, Y. Xu and J. Gu

Formula: [Cu(C10H9O2)(NO3)(C10H8N2)]



Acta Cryst. (1997). C53, 301-302    [ doi:10.1107/S0108270196013674 ]

(Acetonitrile-N)([bold eta]5-cyclopentadienyl)bis(triphenylphosphine-P)ruthenium(II) Tetrafluoroborate

O. Y. Carreón, M. A. Leyva, J. M. Fernández-G. and A. Pénicaud

Formula: [Ru(C5H5)(C2H3N)(C18H15P)2]BF4



Acta Cryst. (1997). C53, 302-305    [ doi:10.1107/S0108270196008219 ]

Nonacarbonyl[[bold mu]3-(1,2-diphenylethyl)phenylphosphinito]triosmium(2 Os-Os)

M. V. Capparelli, Y. De Sanctis, A. J. Arce and E. Spodine

Formula: [Os3(C20H15OP)(CO)9]



Acta Cryst. (1997). C53, 305-309    [ doi:10.1107/S0108270196010761 ]

Hexakis(dimethylformamide)bis(hexaphenylcyclohexasiloxanehexaolato)hexacopper(II) Dimethylformamide Solvate

S. V. Lindeman, O. I. Shchegolikhina, Y. A. Molodtsova and A. A. Zhdanov

Formula: [Cu6(C36H30O12Si6)2(C3H7NO)6].4C3H7NO


organic compounds



Acta Cryst. (1997). C53, 310-311    [ doi:10.1107/S0108270196013352 ]

Bis[(E)-2-(2,4-dichloro-5-nitrostyryl)-1,3-benzothiazole] Hydrate

O. Cox, M. Cordero, S. Piñeiro and S. D. Huang

Formula: 2C15H8Cl2N2O2S.H2O



Acta Cryst. (1997). C53, 311-313    [ doi:10.1107/S010827019601308X ]

Euniciniatin

A. D. Rodríguez, E. González and S. D. Huang

Formula: C20H30O3



Acta Cryst. (1997). C53, 313-315    [ doi:10.1107/S0108270196011857 ]

(±)-2-[Hydroxy(4-methoxyphenyl)methyl]-2H-1,4-benzothiazin-3(4H)-one Hydrate

P. Kumaradhas and K. A. Nirmala

Formula: C16H15NO3S.H2O



Acta Cryst. (1997). C53, 315-318    [ doi:10.1107/S0108270196011845 ]

(±)-trans-3-Hydroxy-2-(4-methoxyphenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepine 1-Oxide

P. Kumaradhas and K. A. Nirmala

Formula: C16H15NO4S



Acta Cryst. (1997). C53, 318-320    [ doi:10.1107/S0108270196012139 ]

Bis(N,N,N',N'-tetramethylethylenediammonium) Cyclotetraphosphate Tetrahydrate

H. Thabet, A. Jouini and S. El Hassane

Formula: 2C6H18N22+.P4O124-.4H2O



Acta Cryst. (1997). C53, 320-322    [ doi:10.1107/S0108270196012668 ]

3-Anilino-N-phenyl-1H-indole-2-carbothioamide

L. Jing, F. He-Liang, S. Jie and C. Wei-Xing

Formula: C21H17N3S



Acta Cryst. (1997). C53, 322-325    [ doi:10.1107/S0108270196013789 ]

meso-1,11-Dimethylcyclotrideca-2,9-diyne-1,11-diol

C. Boss, H. Stoeckli-Evans and R. Keese

Formula: C15H22O2



Acta Cryst. (1997). C53, 325-327    [ doi:10.1107/S0108270196013935 ]

2-Amino-5-methyl-10bH-1,3,4-thiadiazolo[3,2-c]quinazolin-6-ium-10b-carboxylate Hydrate

Q. Zhang, S. Li, L. Wang, J. Liu and X. Huang

Formula: C11H10N4O2S.H2O



Acta Cryst. (1997). C53, 327-329    [ doi:10.1107/S0108270196013753 ]

1-Acetyl-4-[(1R,2S,5R)-3-menthyloxycarbonyl]piperazine-2,5-dione

B. A. Burkett, C. L. L. Chai and D. C. R. Hockless

Formula: C17H26N2O5



Acta Cryst. (1997). C53, 329-331    [ doi:10.1107/S0108270196002363 ]

Glimepiride

M. Iwata, H. Nagase, T. Endo and H. Ueda

Formula: C24H34N4O5S



Acta Cryst. (1997). C53, 331-334    [ doi:10.1107/S010827019601311X ]

N-(Carbamoylmethyl)pyridinium Perchlorate and N-(Carbamoylmethyl)-N'-methyl-4,4'-bipyridinium Diperchlorate Hydrate

K. Sakai, Y. Ikuta, M. Shiomi, T. Tamane, Y. Tomita, T. Tsubomura and N. Nemoto

Formula: C7H9N2O+.ClO4- and C13H15N3O2+.2ClO4-.H2O



Acta Cryst. (1997). C53, 334-339    [ doi:10.1107/S0108270196013145 ]

Hydrated Structures of N-Methylated Cholamide Derivatives

M. C. Wahle and S. R. Byrn

Formula: C25H43NO4.0.25H2O, C25H43NO4.1.5H2O and C26H45NO4.0.5H2O



Acta Cryst. (1997). C53, 340-342    [ doi:10.1107/S0108270196013078 ]

Twinned Crystal Structure of Bis(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexenyl)phenylmethane at 150K

M. Bolte, A. Degen and S. Rühl

Formula: C23H28O4



Acta Cryst. (1997). C53, 342-343    [ doi:10.1107/S0108270196013194 ]

Bis(p-methoxyphenyl) Telluride

J. Farran, A. Alvarez-Larena, J. F. Piniella, M. V. Capparelli and L. Torres-Castellanos

Formula: C14H14O2Te



Acta Cryst. (1997). C53, 344-345    [ doi:10.1107/S0108270196013315 ]

2,2-Dimethyl-2,3-dihydro-1H-2-silacyclopenta[l]phenanthrene

T. Wagner, H.-W. Marx and S. Moss

Formula: C18H18Si



Acta Cryst. (1997). C53, 345-346    [ doi:10.1107/S0108270196013881 ]

1,3-Bis(p-fluorophenyl)triazene

R. Anulewicz

Formula: C12H9F2N3



Acta Cryst. (1997). C53, 347-349    [ doi:10.1107/S0108270196014394 ]

3[alpha],4[alpha]-Epoxy-5[alpha]-androstan-17-one

J. A. Paixão, M. Ramos Silva, M. J. de Almeida, E. J. Tavares da Silva, M. L. Sá e Melo and A. S. Campos Neves

Formula: C19H28O2



Acta Cryst. (1997). C53, 349-351    [ doi:10.1107/S0108270196013923 ]

Succinyl Oleanolic Acid

J. Yang, J. W. Quail and Z. Jia

Formula: C34H52O6



Acta Cryst. (1997). C53, 351-353    [ doi:10.1107/S0108270196014175 ]

Inclusion Complex of (S)-1,3-Butanediol with (S,S)-(+)-trans-2,3-Bis(hydroxydiphenylmethyl)-1,4-dioxaspiro[4.4]nonane

K. Nishikawa, A. Matsumoto, H. Tsukada, M. Shiro and F. Toda

Formula: C33H32O4.C4H10O2



Acta Cryst. (1997). C53, 353-355    [ doi:10.1107/S0108270196012644 ]

A 2H-Pyrano[3,2-a]indolizine Derivative

A. Kakehi, K. Kitajima, S. Ito and K. Matsubara

Formula: C14H10N2O2



Acta Cryst. (1997). C53, 355-358    [ doi:10.1107/S0108270196013376 ]

(1R*,3R*,4S*)-4-(tert-Butyldiphenylsilyloxy)-6,7-dimethoxy-1-methyl-3-phenyl-1,2,3,4-tetrahydroisoquinoline

J. L. Pizarro, M. I. Arriortua, I. Tellitu, D. Badía, E. Domínguez, L. Ochando, J. M. Amigó and T. Debaerdemaeker

Formula: C34H39NO3Si



Acta Cryst. (1997). C53, 358-360    [ doi:10.1107/S0108270196011973 ]

Novel Protective Group in [beta]-Lactam Chemistry: 3-Phenoxy-4-phenyl-N-[[alpha]-(phenylthio)benzyl]azetidin-2-one

V. Srirajan, B. M. Bhawal and V. G. Puranik

Formula: C28H23NO2S



Acta Cryst. (1997). C53, 360-362    [ doi:10.1107/S0108270196014114 ]

2-[1-(Thiosemicarbazono)ethyl]pyridinium Chloride

S. Abram and U. Abram

Formula: C8H11N4S+.Cl-



Acta Cryst. (1997). C53, 362-363    [ doi:10.1107/S0108270196014187 ]

N-Phenylsulfonyl-3-methylbenz[f]indole

T. S. Yokum and F. R. Fronczek

Formula: C19H15NO2S



Acta Cryst. (1997). C53, 364-365    [ doi:10.1107/S010827019601414X ]

4'-Hydroxy-3'-methoxy-N-methyl-4-stilbazolium Tosylate Hydrate, C15H16NO2+.C7H7O3S-.H2O

D.-C. Zhang, T.-Z. Zhang, Y.-Q. Zhang, Z.-H. Fei and K.-B. Yu

Formula: C15H16NO2+.C7H7O3S-.H2O



Acta Cryst. (1997). C53, 365-367    [ doi:10.1107/S010827019601342X ]

Extended Conformation of Putrescine Occurring on a Center of Symmetry in its 1:2 Complex with Malonic Acid

A. M. Babu, T. J. R. Weakley and M. R. N. Murthy

Formula: C4H14N22+.2C3H3O4-



Acta Cryst. (1997). C53, 367-369    [ doi:10.1107/S0108270196012899 ]

Imidazole-4-acetic Acid-Picric Acid (1/1) Complex

Y. In, H. Nagata, M. Doi, T. Ishida and A. Wakahara

Formula: C5H7N2O2+.C6H2N3O7-



Acta Cryst. (1997). C53, 370-372    [ doi:10.1107/S0108270196013959 ]

Hydrogen-Bonding Pattern of a Bicyclic [bold gamma]-Keto Acid: (-)-anti-Isoketopinic Acid

R. A. Lalancette, M. L. Coté and H. W. Thompson

Formula: C10H14O3



Acta Cryst. (1997). C53, 372-374    [ doi:10.1107/S0108270196013972 ]

2-(3-Methoxy-2-hydroxyphenyl)benzimidazole

Y. Elerman and M. Kabak

Formula: C14H12N2O2



Acta Cryst. (1997). C53, 374-376    [ doi:10.1107/S0108270196013686 ]

3-Hydroxy-N,N-dimethyl-2-butenethioamide

K. Honda and T. Tsuchiya

Formula: C6H11NOS



Acta Cryst. (1997). C53, 376-378    [ doi:10.1107/S0108270196013832 ]

N,N'-Bis(4-chlorobenzylidene)-2,2'-diaminodiphenyl disulfide

S. Ide, G. Öztas, N. Ancin and M. Tüzün

Formula: C26H18Cl2N2S2



Acta Cryst. (1997). C53, 378-379    [ doi:10.1107/S0108270196014230 ]

N-Acetyl-2,3,4,6-tetra-O-acetyl-N-benzyl-[beta]-D-glucopyranosylamine

M. Jesús Diánez, M. D. Estrada, A. López-Castro and S. Pérez-Garrido

Formula: C23H29NO10



Acta Cryst. (1997). C53, 380-381    [ doi:10.1107/S0108270196013091 ]

Diethyl 3-(1-Morpholinyl)-2,8-cyclooctadiene-1,2-dicarboxylate

S. Özbey and N. Tunouglu

Formula: C18H27NO5



Acta Cryst. (1997). C53, 381-383    [ doi:10.1107/S0108270196014369 ]

2-Amino-6-fluorobenzothiazole

J. Jai-nhuknan, A. G. Karipides, J. M. Hughes and J. S. Cantrell

Formula: C7H5FN2S



Acta Cryst. (1997). C53, 383-386    [ doi:10.1107/S0108270196014151 ]

3-(E)-But-2-enoxy-1,2-benzisothiazole 1,1-Dioxide: Unusual C-O-C Ether Bond Lengths and Reactivity

J. V. Barkley, M. L. S. Cristiano, R. A. W. Johnstone and R. M. S. Loureiro

Formula: C11H11NO3S



Acta Cryst. (1997). C53, 386-387    [ doi:10.1107/S0108270196013595 ]

(1[alpha],4a[beta],9a[beta])-4a-Acetoxy-9a-chloro-1-methoxy-3-trimethylsiloxy-1,4,4a,9,9a,10-hexahydroanthracene-9,10-dione

J. M. White, A. G. Riches, D. W. Cameron and P. G. Griffiths

Formula: C20H23ClO6Si



Acta Cryst. (1997). C53, 387-391    [ doi:10.1107/S0108270196012085 ]

(1R,1R')-2-exo-Mercapto-2'-thioxo-3-exo,3'-exo-bibornane, 2-Dehydro-2,2'-exo-epidithio-3,3'-bibornane and 2-endo,2'- exo-Epidithio-3,3'-bibornanylidene. Potential Antiviral Agents

W. Kwiatkowski, T. S. Cameron, P. Salama and M. Poirier

Formula: C20H32S2, C20H30S2 and C20H30S2



Acta Cryst. (1997). C53, 391-393    [ doi:10.1107/S010827019601267X ]

5-(p-Tolylamino)benzo-1,3-dioxole

F. Chatel, G. Boyer and J. P. Galy

Formula: C14H13NO2


addenda and errata



Acta Cryst. (1997). C53, 394    [ doi:10.1107/S0108270197001510 ]

3[beta],4[alpha]-Dihydroxy-5[beta]-androstan-17-one. Erratum

M. Ramos Silva, J. A. Paixão, M.-J. M. de Almeida, E. J. Tavares da Silva, M. L. Sá e Melo and A. S. Campos Neves

Synopsis: Erratum to Acta Cryst. (1996), C52, 2892-2894.

Formula:


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