Acta Crystallographica Section C

Crystal Structure Communications

Volume 53, Part 3 (March 1997)

Cover illustration: A New Mixed Oxide with (Bi12O14)n Columns: PbBi12Mo5O34, see Enjalbert, Hasselmann & Galy, pages 269-272. Projection of the structure on the (010) plane (left) and arrangement of the Bi atoms at the corners of octahedra in the (Bi12O14) columns (right).

• inorganic compounds
• metal-organic compounds
• organic compounds
• addenda and errata

inorganic compounds

 

Caesium Gadolinium Tetratelluride

W. Bensch and P. Dürichen

Synopsis: CsGdTe₄ comprises [GdTe₄]_n^n- layers separated by Cs⁺ ions. Each Gd cation is in a square-antiprismatic environment of Te atoms.

Formula: CsGdTe₄

 

A New Mixed Oxide with (Bi₁₂O₁₄)_n Columns: PbBi₁₂Mo₅O₃₄

R. Enjalbert, G. Hasselmann and J. Galy

Synopsis: The structure of PbBi₁₂Mo₅O₃₄ consists of (Bi₁₂O₁₄)_n columns surrounded by MoO₄ tetrahedra. The Pb atoms occupy specific sites between four tetrahedra.

Formula: PbBi₁₂Mo₅O₃₄

metal-organic compounds

 

Tetra(p-chlorophenyl)tin

S. W. Ng

Formula: [Sn(C₆H₄Cl)₄]

 

[Bis(N,N-dimethylthiocarbamoylthio)acetato-O]triphenyl(quinoline N-oxide-O)tin

S. W. Ng

Formula: [Sn(C₆H₅)₃(C₈H₁₃N₂O₂S₄)(C₉H₇NO)]

 

(Diethylenetriamine)(imidazole)(thiocyanato)copper(II) Perchlorate

H.-M. Hu, H.-S. Sun, X.-H. Chen, Q. Zhao, Y. Pan, X.-Y. Huang and X.-Z. You

Formula: [Cu(NCS)(C₄H₁₃N₃)(C₃H₄N₂)]ClO₄

 

[-(1,4-Dibenzylpiperazine)-N:N']bis(trimethylindium) Dibenzene Solvate

X. Ma, Y. Pan, L. Wu, X. Huang, H. Sun and C. Zhu

Formula: [In₂(C₁₈H₂₂N₂)(CH₃)₆].2C₆H₆

 

trans-Diiodobis(triphenylarsine-As)platinum(II)

S. Otto and A. Roodt

Formula: [PtI₂(C₁₈H₁₅As)₂]

 

Bis(6-chloro-2-pyridonato-N,O)(4,4'-dimethyl-2,2'-bipyridine-N,N')zinc(II) Hydrate at 150 K

C. G. Mowat, S. Parsons, G. A. Solan and R. E. P. Winpenny

Formula: [Zn(C₅H₃ClNO)₂(C₁₂H₁₂N₂)].H₂O

 

Disodium Fluorescein Octahydrate

K. Yamaguchi, Z. Tamura and M. Maeda

Formula: 2Na⁺.C₂₀H₁₀O₅^2-.8H₂O

 

Tetracarbonyl-1²C,2²C--diphenylphosphido-P:P--iodo-bis(triphenylphosphine)-1P,2P-diosmium(Os-Os) Benzene Solvate

A. W. Herlinger and A. L. Rheingold

Formula: [Os₂I(C₁₂H₁₀P)(C₁₈H₁₅P)₂(CO)₄].C₆H₆

 

Hetero-Ring Oxygen Coordination to Strontium in Strontium Bis(2-furancarboxylate)

B. Paluchowska, J. K. Maurin and J. Leciejewicz

Formula: [Sr(C₅H₃O₃)₂]

 

[Bis(thiodiphenylphosphino-S)amido]chlorobis(dimethylphenylphosphine-P)nitridorhenium(V)

U. Abram, E. Schulz Lang and J. R. Dilworth

Formula: [ReNCl(C₂₄H₂₀NP₂S₂)(C₈H₁₁P)₂]

 

cis-Di(nitrato-O,O')bis(tricyclohexylphosphine oxide-O)nickel(II)

A. R. Kennedy, S. W. Sloss and M. D. Spicer

Formula: [Ni(NO₃)₂(C₁₈H₃₃OP)₂]

 

Bis[tris(2-hydroxyethyl)ammonium] Hexachloroplatinate(IV)

V. T. Yilmaz, H. Içbudak and R. A. Howie

Formula: (C₆H₁₆NO₃)₂[PtCl₆]

 

trans-Diaquabis(pyridine-2-carboxamide-N¹,O)copper(II) Dichloride and Dibromide

L. Sieron and M. Bukowska-Strzyzewska

Formula: [Cu(C₆H₆N₂O)₂(H₂O)₂]Cl₂ and [Cu(C₆H₆N₂O)₂(H₂O)₂]Br₂

 

(Benzoylacetonato-O,O')(2,2'-bipyridine-N,N')(nitrato-O)copper(II)

L. Zhang, D. Xu, Y. Xu and J. Gu

Formula: [Cu(C₁₀H₉O₂)(NO₃)(C₁₀H₈N₂)]

 

(Acetonitrile-N)(⁵-cyclopentadienyl)bis(triphenylphosphine-P)ruthenium(II) Tetrafluoroborate

O. Y. Carreón, M. A. Leyva, J. M. Fernández-G. and A. Pénicaud

Formula: [Ru(C₅H₅)(C₂H₃N)(C₁₈H₁₅P)₂]BF₄

 

Nonacarbonyl[₃-(1,2-diphenylethyl)phenylphosphinito]triosmium(2 Os-Os)

M. V. Capparelli, Y. De Sanctis, A. J. Arce and E. Spodine

Formula: [Os₃(C₂₀H₁₅OP)(CO)₉]

 

Hexakis(dimethylformamide)bis(hexaphenylcyclohexasiloxanehexaolato)hexacopper(II) Dimethylformamide Solvate

S. V. Lindeman, O. I. Shchegolikhina, Y. A. Molodtsova and A. A. Zhdanov

Formula: [Cu₆(C₃₆H₃₀O₁₂Si₆)₂(C₃H₇NO)₆].4C₃H₇NO

organic compounds

 

Bis[(E)-2-(2,4-dichloro-5-nitrostyryl)-1,3-benzothiazole] Hydrate

O. Cox, M. Cordero, S. Piñeiro and S. D. Huang

Formula: 2C₁₅H₈Cl₂N₂O₂S.H₂O

 

Euniciniatin

A. D. Rodríguez, E. González and S. D. Huang

Formula: C₂₀H₃₀O₃

 

(±)-2-[Hydroxy(4-methoxyphenyl)methyl]-2H-1,4-benzothiazin-3(4H)-one Hydrate

P. Kumaradhas and K. A. Nirmala

Formula: C₁₆H₁₅NO₃S.H₂O

 

(±)-trans-3-Hydroxy-2-(4-methoxyphenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepine 1-Oxide

P. Kumaradhas and K. A. Nirmala

Formula: C₁₆H₁₅NO₄S

 

Bis(N,N,N',N'-tetramethylethylenediammonium) Cyclotetraphosphate Tetrahydrate

H. Thabet, A. Jouini and S. El Hassane

Formula: 2C₆H₁₈N₂²⁺.P₄O₁₂^4-.4H₂O

 

3-Anilino-N-phenyl-1H-indole-2-carbothioamide

L. Jing, F. He-Liang, S. Jie and C. Wei-Xing

Formula: C₂₁H₁₇N₃S

 

meso-1,11-Dimethylcyclotrideca-2,9-diyne-1,11-diol

C. Boss, H. Stoeckli-Evans and R. Keese

Formula: C₁₅H₂₂O₂

 

2-Amino-5-methyl-10bH-1,3,4-thiadiazolo[3,2-c]quinazolin-6-ium-10b-carboxylate Hydrate

Q. Zhang, S. Li, L. Wang, J. Liu and X. Huang

Formula: C₁₁H₁₀N₄O₂S.H₂O

 

1-Acetyl-4-[(1R,2S,5R)-3-menthyloxycarbonyl]piperazine-2,5-dione

B. A. Burkett, C. L. L. Chai and D. C. R. Hockless

Formula: C₁₇H₂₆N₂O₅

 

Glimepiride

M. Iwata, H. Nagase, T. Endo and H. Ueda

Formula: C₂₄H₃₄N₄O₅S

 

N-(Carbamoylmethyl)pyridinium Perchlorate and N-(Carbamoylmethyl)-N'-methyl-4,4'-bipyridinium Diperchlorate Hydrate

K. Sakai, Y. Ikuta, M. Shiomi, T. Tamane, Y. Tomita, T. Tsubomura and N. Nemoto

Formula: C₇H₉N₂O⁺.ClO₄^- and C₁₃H₁₅N₃O²⁺.2ClO₄^-.H₂O

 

Hydrated Structures of N-Methylated Cholamide Derivatives

M. C. Wahle and S. R. Byrn

Formula: C₂₅H₄₃NO₄.0.25H₂O, C₂₅H₄₃NO₄.1.5H₂O and C₂₆H₄₅NO₄.0.5H₂O

 

Twinned Crystal Structure of Bis(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexenyl)phenylmethane at 150K

M. Bolte, A. Degen and S. Rühl

Formula: C₂₃H₂₈O₄

 

Bis(p-methoxyphenyl) Telluride

J. Farran, A. Alvarez-Larena, J. F. Piniella, M. V. Capparelli and L. Torres-Castellanos

Formula: C₁₄H₁₄O₂Te

 

2,2-Dimethyl-2,3-dihydro-1H-2-silacyclopenta[l]phenanthrene

T. Wagner, H.-W. Marx and S. Moss

Formula: C₁₈H₁₈Si

 

1,3-Bis(p-fluorophenyl)triazene

R. Anulewicz

Formula: C₁₂H₉F₂N₃

 

3,4-Epoxy-5-androstan-17-one

J. A. Paixão, M. Ramos Silva, M. J. de Almeida, E. J. Tavares da Silva, M. L. Sá e Melo and A. S. Campos Neves

Formula: C₁₉H₂₈O₂

 

Succinyl Oleanolic Acid

J. Yang, J. W. Quail and Z. Jia

Formula: C₃₄H₅₂O₆

 

Inclusion Complex of (S)-1,3-Butanediol with (S,S)-(+)-trans-2,3-Bis(hydroxydiphenylmethyl)-1,4-dioxaspiro[4.4]nonane

K. Nishikawa, A. Matsumoto, H. Tsukada, M. Shiro and F. Toda

Formula: C₃₃H₃₂O₄.C₄H₁₀O₂

 

A 2H-Pyrano[3,2-a]indolizine Derivative

A. Kakehi, K. Kitajima, S. Ito and K. Matsubara

Formula: C₁₄H₁₀N₂O₂

 

(1R*,3R*,4S*)-4-(tert-Butyldiphenylsilyloxy)-6,7-dimethoxy-1-methyl-3-phenyl-1,2,3,4-tetrahydroisoquinoline

J. L. Pizarro, M. I. Arriortua, I. Tellitu, D. Badía, E. Domínguez, L. Ochando, J. M. Amigó and T. Debaerdemaeker

Formula: C₃₄H₃₉NO₃Si

 

Novel Protective Group in -Lactam Chemistry: 3-Phenoxy-4-phenyl-N-[-(phenylthio)benzyl]azetidin-2-one

V. Srirajan, B. M. Bhawal and V. G. Puranik

Formula: C₂₈H₂₃NO₂S

 

2-[1-(Thiosemicarbazono)ethyl]pyridinium Chloride

S. Abram and U. Abram

Formula: C₈H₁₁N₄S⁺.Cl^-

 

N-Phenylsulfonyl-3-methylbenz[f]indole

T. S. Yokum and F. R. Fronczek

Formula: C₁₉H₁₅NO₂S

 

4'-Hydroxy-3'-methoxy-N-methyl-4-stilbazolium Tosylate Hydrate, C₁₅H₁₆NO₂⁺.C₇H₇O₃S^-.H₂O

D.-C. Zhang, T.-Z. Zhang, Y.-Q. Zhang, Z.-H. Fei and K.-B. Yu

Formula: C₁₅H₁₆NO₂⁺.C₇H₇O₃S^-.H₂O

 

Extended Conformation of Putrescine Occurring on a Center of Symmetry in its 1:2 Complex with Malonic Acid

A. M. Babu, T. J. R. Weakley and M. R. N. Murthy

Formula: C₄H₁₄N₂²⁺.2C₃H₃O₄^-

 

Imidazole-4-acetic Acid-Picric Acid (1/1) Complex

Y. In, H. Nagata, M. Doi, T. Ishida and A. Wakahara

Formula: C₅H₇N₂O₂⁺.C₆H₂N₃O₇^-

 

Hydrogen-Bonding Pattern of a Bicyclic -Keto Acid: (-)-anti-Isoketopinic Acid

R. A. Lalancette, M. L. Coté and H. W. Thompson

Formula: C₁₀H₁₄O₃

 

2-(3-Methoxy-2-hydroxyphenyl)benzimidazole

Y. Elerman and M. Kabak

Formula: C₁₄H₁₂N₂O₂

 

3-Hydroxy-N,N-dimethyl-2-butenethioamide

K. Honda and T. Tsuchiya

Formula: C₆H₁₁NOS

 

N,N'-Bis(4-chlorobenzylidene)-2,2'-diaminodiphenyl disulfide

S. Ide, G. Öztas, N. Ancin and M. Tüzün

Formula: C₂₆H₁₈Cl₂N₂S₂

 

N-Acetyl-2,3,4,6-tetra-O-acetyl-N-benzyl--D-glucopyranosylamine

M. Jesús Diánez, M. D. Estrada, A. López-Castro and S. Pérez-Garrido

Formula: C₂₃H₂₉NO₁₀

 

Diethyl 3-(1-Morpholinyl)-2,8-cyclooctadiene-1,2-dicarboxylate

S. Özbey and N. Tunouglu

Formula: C₁₈H₂₇NO₅

 

2-Amino-6-fluorobenzothiazole

J. Jai-nhuknan, A. G. Karipides, J. M. Hughes and J. S. Cantrell

Formula: C₇H₅FN₂S

 

3-(E)-But-2-enoxy-1,2-benzisothiazole 1,1-Dioxide: Unusual C-O-C Ether Bond Lengths and Reactivity

J. V. Barkley, M. L. S. Cristiano, R. A. W. Johnstone and R. M. S. Loureiro

Formula: C₁₁H₁₁NO₃S

 

(1,4a,9a)-4a-Acetoxy-9a-chloro-1-methoxy-3-trimethylsiloxy-1,4,4a,9,9a,10-hexahydroanthracene-9,10-dione

J. M. White, A. G. Riches, D. W. Cameron and P. G. Griffiths

Formula: C₂₀H₂₃ClO₆Si

 

(1R,1R')-2-exo-Mercapto-2'-thioxo-3-exo,3'-exo-bibornane, 2-Dehydro-2,2'-exo-epidithio-3,3'-bibornane and 2-endo,2'- exo-Epidithio-3,3'-bibornanylidene. Potential Antiviral Agents

W. Kwiatkowski, T. S. Cameron, P. Salama and M. Poirier

Formula: C₂₀H₃₂S₂, C₂₀H₃₀S₂ and C₂₀H₃₀S₂

 

5-(p-Tolylamino)benzo-1,3-dioxole

F. Chatel, G. Boyer and J. P. Galy

Formula: C₁₄H₁₃NO₂

addenda and errata

 

3,4-Dihydroxy-5-androstan-17-one. Erratum

M. Ramos Silva, J. A. Paixão, M.-J. M. de Almeida, E. J. Tavares da Silva, M. L. Sá e Melo and A. S. Campos Neves

Synopsis: Erratum to Acta Cryst. (1996), C52, 2892-2894.

Formula:

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