Acta Crystallographica Section C

Crystal Structure Communications

Volume 53, Part 3 (March 1997)

Cover illustrationCover illustration: A New Mixed Oxide with (Bi12O14)n Columns: PbBi12Mo5O34, see Enjalbert, Hasselmann & Galy, pages 269-272. Projection of the structure on the (010) plane (left) and arrangement of the Bi atoms at the corners of octahedra in the (Bi12O14) columns (right).

inorganic compounds

Acta Cryst. (1997). C53, 267-269    [ doi:10.1107/S0108270196012309 ]

Caesium Gadolinium Tetratelluride

W. Bensch and P. Dürichen

Synopsis: CsGdTe4 comprises [GdTe4]nn- layers separated by Cs+ ions. Each Gd cation is in a square-antiprismatic environment of Te atoms.

Formula: CsGdTe4

Acta Cryst. (1997). C53, 269-272    [ doi:10.1107/S0108270196013698 ]

A New Mixed Oxide with (Bi12O14)n Columns: PbBi12Mo5O34

R. Enjalbert, G. Hasselmann and J. Galy

Synopsis: The structure of PbBi12Mo5O34 consists of (Bi12O14)n columns surrounded by MoO4 tetrahedra. The Pb atoms occupy specific sites between four tetrahedra.

Formula: PbBi12Mo5O34

metal-organic compounds

Acta Cryst. (1997). C53, 273-274    [ doi:10.1107/S0108270196013716 ]


S. W. Ng

Formula: [Sn(C6H4Cl)4]

Acta Cryst. (1997). C53, 274-276    [ doi:10.1107/S0108270196013704 ]

[Bis(N,N-dimethylthiocarbamoylthio)acetato-O]triphenyl(quinoline N-oxide-O)tin

S. W. Ng

Formula: [Sn(C6H5)3(C8H13N2O2S4)(C9H7NO)]

Acta Cryst. (1997). C53, 276-278    [ doi:10.1107/S0108270196013893 ]

(Diethylenetriamine)(imidazole)(thiocyanato)copper(II) Perchlorate

H.-M. Hu, H.-S. Sun, X.-H. Chen, Q. Zhao, Y. Pan, X.-Y. Huang and X.-Z. You

Formula: [Cu(NCS)(C4H13N3)(C3H4N2)]ClO4

Acta Cryst. (1997). C53, 278-279    [ doi:10.1107/S0108270196013169 ]

[[bold mu]-(1,4-Dibenzylpiperazine)-N:N']bis(trimethylindium) Dibenzene Solvate

X. Ma, Y. Pan, L. Wu, X. Huang, H. Sun and C. Zhu

Formula: [In2(C18H22N2)(CH3)6].2C6H6

Acta Cryst. (1997). C53, 280-282    [ doi:10.1107/S0108270196013844 ]


S. Otto and A. Roodt

Formula: [PtI2(C18H15As)2]

Acta Cryst. (1997). C53, 282-283    [ doi:10.1107/S0108270196013868 ]

Bis(6-chloro-2-pyridonato-N,O)(4,4'-dimethyl-2,2'-bipyridine-N,N')zinc(II) Hydrate at 150 K

C. G. Mowat, S. Parsons, G. A. Solan and R. E. P. Winpenny

Formula: [Zn(C5H3ClNO)2(C12H12N2)].H2O

Acta Cryst. (1997). C53, 284-285    [ doi:10.1107/S0108270196010487 ]

Disodium Fluorescein Octahydrate

K. Yamaguchi, Z. Tamura and M. Maeda

Formula: 2Na+.C20H10O52-.8H2O

Acta Cryst. (1997). C53, 285-287    [ doi:10.1107/S0108270196013911 ]

Tetracarbonyl-1[bold kappa]2C,2[bold kappa]2C-[bold mu]-diphenylphosphido-P:P-[bold mu]-iodo-bis(triphenylphosphine)-1[bold kappa]P,2[bold kappa]P-diosmium(Os-Os) Benzene Solvate

A. W. Herlinger and A. L. Rheingold

Formula: [Os2I(C12H10P)(C18H15P)2(CO)4].C6H6

Acta Cryst. (1997). C53, 287-289    [ doi:10.1107/S0108270196011018 ]

Hetero-Ring Oxygen Coordination to Strontium in Strontium Bis(2-furancarboxylate)

B. Paluchowska, J. K. Maurin and J. Leciejewicz

Formula: [Sr(C5H3O3)2]

Acta Cryst. (1997). C53, 289-292    [ doi:10.1107/S0108270196013790 ]


U. Abram, E. Schulz Lang and J. R. Dilworth

Formula: [ReNCl(C24H20NP2S2)(C8H11P)2]

Acta Cryst. (1997). C53, 292-293    [ doi:10.1107/S0108270196014229 ]

cis-Di(nitrato-O,O')bis(tricyclohexylphosphine oxide-O)nickel(II)

A. R. Kennedy, S. W. Sloss and M. D. Spicer

Formula: [Ni(NO3)2(C18H33OP)2]

Acta Cryst. (1997). C53, 294-296    [ doi:10.1107/S0108270196011341 ]

Bis[tris(2-hydroxyethyl)ammonium] Hexachloroplatinate(IV)

V. T. Yilmaz, H. Içbudak and R. A. Howie

Formula: (C6H16NO3)2[PtCl6]

Acta Cryst. (1997). C53, 296-298    [ doi:10.1107/S0108270196013364 ]

trans-Diaquabis(pyridine-2-carboxamide-N1,O)copper(II) Dichloride and Dibromide

L. Sieron and M. Bukowska-Strzyzewska

Formula: [Cu(C6H6N2O)2(H2O)2]Cl2 and [Cu(C6H6N2O)2(H2O)2]Br2

Acta Cryst. (1997). C53, 299-301    [ doi:10.1107/S0108270196012358 ]


L. Zhang, D. Xu, Y. Xu and J. Gu

Formula: [Cu(C10H9O2)(NO3)(C10H8N2)]

Acta Cryst. (1997). C53, 301-302    [ doi:10.1107/S0108270196013674 ]

(Acetonitrile-N)([bold eta]5-cyclopentadienyl)bis(triphenylphosphine-P)ruthenium(II) Tetrafluoroborate

O. Y. Carreón, M. A. Leyva, J. M. Fernández-G. and A. Pénicaud

Formula: [Ru(C5H5)(C2H3N)(C18H15P)2]BF4

Acta Cryst. (1997). C53, 302-305    [ doi:10.1107/S0108270196008219 ]

Nonacarbonyl[[bold mu]3-(1,2-diphenylethyl)phenylphosphinito]triosmium(2 Os-Os)

M. V. Capparelli, Y. De Sanctis, A. J. Arce and E. Spodine

Formula: [Os3(C20H15OP)(CO)9]

Acta Cryst. (1997). C53, 305-309    [ doi:10.1107/S0108270196010761 ]

Hexakis(dimethylformamide)bis(hexaphenylcyclohexasiloxanehexaolato)hexacopper(II) Dimethylformamide Solvate

S. V. Lindeman, O. I. Shchegolikhina, Y. A. Molodtsova and A. A. Zhdanov

Formula: [Cu6(C36H30O12Si6)2(C3H7NO)6].4C3H7NO

organic compounds

Acta Cryst. (1997). C53, 310-311    [ doi:10.1107/S0108270196013352 ]

Bis[(E)-2-(2,4-dichloro-5-nitrostyryl)-1,3-benzothiazole] Hydrate

O. Cox, M. Cordero, S. Piñeiro and S. D. Huang

Formula: 2C15H8Cl2N2O2S.H2O

Acta Cryst. (1997). C53, 311-313    [ doi:10.1107/S010827019601308X ]


A. D. Rodríguez, E. González and S. D. Huang

Formula: C20H30O3

Acta Cryst. (1997). C53, 313-315    [ doi:10.1107/S0108270196011857 ]

(±)-2-[Hydroxy(4-methoxyphenyl)methyl]-2H-1,4-benzothiazin-3(4H)-one Hydrate

P. Kumaradhas and K. A. Nirmala

Formula: C16H15NO3S.H2O

Acta Cryst. (1997). C53, 315-318    [ doi:10.1107/S0108270196011845 ]

(±)-trans-3-Hydroxy-2-(4-methoxyphenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepine 1-Oxide

P. Kumaradhas and K. A. Nirmala

Formula: C16H15NO4S

Acta Cryst. (1997). C53, 318-320    [ doi:10.1107/S0108270196012139 ]

Bis(N,N,N',N'-tetramethylethylenediammonium) Cyclotetraphosphate Tetrahydrate

H. Thabet, A. Jouini and S. El Hassane

Formula: 2C6H18N22+.P4O124-.4H2O

Acta Cryst. (1997). C53, 320-322    [ doi:10.1107/S0108270196012668 ]


L. Jing, F. He-Liang, S. Jie and C. Wei-Xing

Formula: C21H17N3S

Acta Cryst. (1997). C53, 322-325    [ doi:10.1107/S0108270196013789 ]


C. Boss, H. Stoeckli-Evans and R. Keese

Formula: C15H22O2

Acta Cryst. (1997). C53, 325-327    [ doi:10.1107/S0108270196013935 ]

2-Amino-5-methyl-10bH-1,3,4-thiadiazolo[3,2-c]quinazolin-6-ium-10b-carboxylate Hydrate

Q. Zhang, S. Li, L. Wang, J. Liu and X. Huang

Formula: C11H10N4O2S.H2O

Acta Cryst. (1997). C53, 327-329    [ doi:10.1107/S0108270196013753 ]


B. A. Burkett, C. L. L. Chai and D. C. R. Hockless

Formula: C17H26N2O5

Acta Cryst. (1997). C53, 329-331    [ doi:10.1107/S0108270196002363 ]


M. Iwata, H. Nagase, T. Endo and H. Ueda

Formula: C24H34N4O5S

Acta Cryst. (1997). C53, 331-334    [ doi:10.1107/S010827019601311X ]

N-(Carbamoylmethyl)pyridinium Perchlorate and N-(Carbamoylmethyl)-N'-methyl-4,4'-bipyridinium Diperchlorate Hydrate

K. Sakai, Y. Ikuta, M. Shiomi, T. Tamane, Y. Tomita, T. Tsubomura and N. Nemoto

Formula: C7H9N2O+.ClO4- and C13H15N3O2+.2ClO4-.H2O

Acta Cryst. (1997). C53, 334-339    [ doi:10.1107/S0108270196013145 ]

Hydrated Structures of N-Methylated Cholamide Derivatives

M. C. Wahle and S. R. Byrn

Formula: C25H43NO4.0.25H2O, C25H43NO4.1.5H2O and C26H45NO4.0.5H2O

Acta Cryst. (1997). C53, 340-342    [ doi:10.1107/S0108270196013078 ]

Twinned Crystal Structure of Bis(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexenyl)phenylmethane at 150K

M. Bolte, A. Degen and S. Rühl

Formula: C23H28O4

Acta Cryst. (1997). C53, 342-343    [ doi:10.1107/S0108270196013194 ]

Bis(p-methoxyphenyl) Telluride

J. Farran, A. Alvarez-Larena, J. F. Piniella, M. V. Capparelli and L. Torres-Castellanos

Formula: C14H14O2Te

Acta Cryst. (1997). C53, 344-345    [ doi:10.1107/S0108270196013315 ]


T. Wagner, H.-W. Marx and S. Moss

Formula: C18H18Si

Acta Cryst. (1997). C53, 345-346    [ doi:10.1107/S0108270196013881 ]


R. Anulewicz

Formula: C12H9F2N3

Acta Cryst. (1997). C53, 347-349    [ doi:10.1107/S0108270196014394 ]


J. A. Paixão, M. Ramos Silva, M. J. de Almeida, E. J. Tavares da Silva, M. L. Sá e Melo and A. S. Campos Neves

Formula: C19H28O2

Acta Cryst. (1997). C53, 349-351    [ doi:10.1107/S0108270196013923 ]

Succinyl Oleanolic Acid

J. Yang, J. W. Quail and Z. Jia

Formula: C34H52O6

Acta Cryst. (1997). C53, 351-353    [ doi:10.1107/S0108270196014175 ]

Inclusion Complex of (S)-1,3-Butanediol with (S,S)-(+)-trans-2,3-Bis(hydroxydiphenylmethyl)-1,4-dioxaspiro[4.4]nonane

K. Nishikawa, A. Matsumoto, H. Tsukada, M. Shiro and F. Toda

Formula: C33H32O4.C4H10O2

Acta Cryst. (1997). C53, 353-355    [ doi:10.1107/S0108270196012644 ]

A 2H-Pyrano[3,2-a]indolizine Derivative

A. Kakehi, K. Kitajima, S. Ito and K. Matsubara

Formula: C14H10N2O2

Acta Cryst. (1997). C53, 355-358    [ doi:10.1107/S0108270196013376 ]


J. L. Pizarro, M. I. Arriortua, I. Tellitu, D. Badía, E. Domínguez, L. Ochando, J. M. Amigó and T. Debaerdemaeker

Formula: C34H39NO3Si

Acta Cryst. (1997). C53, 358-360    [ doi:10.1107/S0108270196011973 ]

Novel Protective Group in [beta]-Lactam Chemistry: 3-Phenoxy-4-phenyl-N-[[alpha]-(phenylthio)benzyl]azetidin-2-one

V. Srirajan, B. M. Bhawal and V. G. Puranik

Formula: C28H23NO2S

Acta Cryst. (1997). C53, 360-362    [ doi:10.1107/S0108270196014114 ]

2-[1-(Thiosemicarbazono)ethyl]pyridinium Chloride

S. Abram and U. Abram

Formula: C8H11N4S+.Cl-

Acta Cryst. (1997). C53, 362-363    [ doi:10.1107/S0108270196014187 ]


T. S. Yokum and F. R. Fronczek

Formula: C19H15NO2S

Acta Cryst. (1997). C53, 364-365    [ doi:10.1107/S010827019601414X ]

4'-Hydroxy-3'-methoxy-N-methyl-4-stilbazolium Tosylate Hydrate, C15H16NO2+.C7H7O3S-.H2O

D.-C. Zhang, T.-Z. Zhang, Y.-Q. Zhang, Z.-H. Fei and K.-B. Yu

Formula: C15H16NO2+.C7H7O3S-.H2O

Acta Cryst. (1997). C53, 365-367    [ doi:10.1107/S010827019601342X ]

Extended Conformation of Putrescine Occurring on a Center of Symmetry in its 1:2 Complex with Malonic Acid

A. M. Babu, T. J. R. Weakley and M. R. N. Murthy

Formula: C4H14N22+.2C3H3O4-

Acta Cryst. (1997). C53, 367-369    [ doi:10.1107/S0108270196012899 ]

Imidazole-4-acetic Acid-Picric Acid (1/1) Complex

Y. In, H. Nagata, M. Doi, T. Ishida and A. Wakahara

Formula: C5H7N2O2+.C6H2N3O7-

Acta Cryst. (1997). C53, 370-372    [ doi:10.1107/S0108270196013959 ]

Hydrogen-Bonding Pattern of a Bicyclic [bold gamma]-Keto Acid: (-)-anti-Isoketopinic Acid

R. A. Lalancette, M. L. Coté and H. W. Thompson

Formula: C10H14O3

Acta Cryst. (1997). C53, 372-374    [ doi:10.1107/S0108270196013972 ]


Y. Elerman and M. Kabak

Formula: C14H12N2O2

Acta Cryst. (1997). C53, 374-376    [ doi:10.1107/S0108270196013686 ]


K. Honda and T. Tsuchiya

Formula: C6H11NOS

Acta Cryst. (1997). C53, 376-378    [ doi:10.1107/S0108270196013832 ]

N,N'-Bis(4-chlorobenzylidene)-2,2'-diaminodiphenyl disulfide

S. Ide, G. Öztas, N. Ancin and M. Tüzün

Formula: C26H18Cl2N2S2

Acta Cryst. (1997). C53, 378-379    [ doi:10.1107/S0108270196014230 ]


M. Jesús Diánez, M. D. Estrada, A. López-Castro and S. Pérez-Garrido

Formula: C23H29NO10

Acta Cryst. (1997). C53, 380-381    [ doi:10.1107/S0108270196013091 ]

Diethyl 3-(1-Morpholinyl)-2,8-cyclooctadiene-1,2-dicarboxylate

S. Özbey and N. Tunouglu

Formula: C18H27NO5

Acta Cryst. (1997). C53, 381-383    [ doi:10.1107/S0108270196014369 ]


J. Jai-nhuknan, A. G. Karipides, J. M. Hughes and J. S. Cantrell

Formula: C7H5FN2S

Acta Cryst. (1997). C53, 383-386    [ doi:10.1107/S0108270196014151 ]

3-(E)-But-2-enoxy-1,2-benzisothiazole 1,1-Dioxide: Unusual C-O-C Ether Bond Lengths and Reactivity

J. V. Barkley, M. L. S. Cristiano, R. A. W. Johnstone and R. M. S. Loureiro

Formula: C11H11NO3S

Acta Cryst. (1997). C53, 386-387    [ doi:10.1107/S0108270196013595 ]


J. M. White, A. G. Riches, D. W. Cameron and P. G. Griffiths

Formula: C20H23ClO6Si

Acta Cryst. (1997). C53, 387-391    [ doi:10.1107/S0108270196012085 ]

(1R,1R')-2-exo-Mercapto-2'-thioxo-3-exo,3'-exo-bibornane, 2-Dehydro-2,2'-exo-epidithio-3,3'-bibornane and 2-endo,2'- exo-Epidithio-3,3'-bibornanylidene. Potential Antiviral Agents

W. Kwiatkowski, T. S. Cameron, P. Salama and M. Poirier

Formula: C20H32S2, C20H30S2 and C20H30S2

Acta Cryst. (1997). C53, 391-393    [ doi:10.1107/S010827019601267X ]


F. Chatel, G. Boyer and J. P. Galy

Formula: C14H13NO2

addenda and errata

Acta Cryst. (1997). C53, 394    [ doi:10.1107/S0108270197001510 ]

3[beta],4[alpha]-Dihydroxy-5[beta]-androstan-17-one. Erratum

M. Ramos Silva, J. A. Paixão, M.-J. M. de Almeida, E. J. Tavares da Silva, M. L. Sá e Melo and A. S. Campos Neves

Synopsis: Erratum to Acta Cryst. (1996), C52, 2892-2894.


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