# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_dap _shelx_title ' [C3N2P2O7.XH2O]' _shelx_refln_list_code 4 _shelx_F_calc_maximum 255.49 _exptl_crystal_F_000 856.00 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8096.52 12045.53 30.73 o 4 0 0 100.76 73.50 1.27 o 6 0 0 3819.42 3785.03 5.19 o 8 0 0 1000.66 995.86 3.70 o 1 1 0 3530.21 5317.69 3.60 o 3 1 0 25964.55 27420.43 57.69 o 5 1 0 1446.08 1498.61 2.94 o 7 1 0 367.96 340.90 1.76 o 9 1 0 1171.07 1203.54 2.95 o 0 2 0 697.17 1385.20 1.66 o 2 2 0 1914.23 2359.18 2.76 o 4 2 0 2738.99 3108.99 3.83 o 6 2 0 198.24 181.12 1.24 o 8 2 0 37.83 37.21 0.63 o 1 3 0 257.83 325.65 1.00 o 3 3 0 771.27 898.06 1.91 o 5 3 0 928.26 1011.18 2.39 o 7 3 0 525.07 506.27 2.10 o 9 3 0 803.18 823.29 2.40 o 0 4 0 48727.02 46262.57 75.44 o 2 4 0 5343.19 6522.85 3.36 o 4 4 0 9222.08 8342.66 7.02 o 6 4 0 1402.39 1428.57 3.26 o 8 4 0 40.24 42.22 0.96 o 1 5 0 20766.71 22379.12 50.69 o 3 5 0 11898.63 11944.69 7.84 o 5 5 0 2317.20 2188.82 3.90 o 7 5 0 840.54 840.60 2.65 o 0 6 0 3921.86 5227.75 4.29 o 2 6 0 514.89 660.69 4.47 o 4 6 0 3849.28 4170.04 6.29 o 6 6 0 112.91 106.77 0.98 o 8 6 0 189.16 183.68 1.25 o 1 7 0 705.98 828.00 2.68 o 3 7 0 1341.59 1483.88 1.98 o 5 7 0 1934.72 1852.82 12.19 o 7 7 0 110.88 111.42 1.01 o 9 7 0 52.44 53.20 0.64 o 0 8 0 75.04 92.83 0.63 o 2 8 0 645.05 742.87 1.41 o 4 8 0 1237.13 1267.11 6.25 o 6 8 0 869.40 840.62 2.70 o 8 8 0 620.28 604.75 2.15 o 1 9 0 541.37 573.41 3.74 o 3 9 0 1965.94 2002.00 2.55 o 5 9 0 26.14 31.13 1.13 o 7 9 0 690.07 681.44 2.37 o 0 10 0 225.67 251.99 1.18 o 2 10 0 8.29 16.03 0.63 o 4 10 0 1340.43 1354.46 5.22 o 6 10 0 1.37 3.69 0.23 o 8 10 0 103.24 111.88 0.85 o 1 11 0 123.77 132.65 0.67 o 3 11 0 2.29 5.38 0.11 o 5 11 0 1706.80 1631.37 3.77 o 7 11 0 87.79 82.20 3.00 o 0 12 0 781.27 910.20 2.44 o 2 12 0 3053.47 3068.06 4.90 o 4 12 0 532.29 528.58 3.48 o 6 12 0 53.42 54.85 2.28 o 1 13 0 520.61 481.34 6.11 o 3 13 0 1994.97 1990.85 5.22 o 5 13 0 15.56 16.27 0.44 o 7 13 0 3.93 5.68 0.65 o 0 14 0 292.22 306.16 1.60 o 2 14 0 539.60 534.35 2.02 o 4 14 0 90.98 101.14 0.64 o 6 14 0 177.85 209.07 3.70 o 1 15 0 87.44 85.54 0.65 o 3 15 0 442.18 424.31 1.37 o 5 15 0 7.09 7.61 0.83 o 0 16 0 1389.09 1346.06 3.35 o 2 16 0 1083.59 1031.79 6.32 o 4 16 0 66.93 68.12 0.52 o 1 17 0 33.56 31.75 0.59 o 3 17 0 833.81 870.94 4.40 o 0 18 0 38.05 38.98 0.58 o 2 18 0 102.10 105.89 0.60 o -9 1 1 501.91 450.86 1.96 o -7 1 1 1168.67 1077.85 3.08 o -5 1 1 626.07 647.80 1.95 o -3 1 1 2156.31 2870.52 3.13 o -1 1 1 8829.75 14957.66 31.30 o 1 1 1 272.30 305.86 1.03 o 3 1 1 2696.27 2804.20 3.48 o 5 1 1 4601.78 4699.61 5.32 o 7 1 1 794.87 804.44 2.58 o 9 1 1 275.91 308.46 1.32 o -8 2 1 90.60 89.24 0.93 o -6 2 1 1597.06 1560.33 3.36 o -4 2 1 3734.61 4456.83 4.37 o -2 2 1 3582.45 4648.86 3.82 o 0 2 1 10482.44 17075.16 34.18 o 2 2 1 27491.24 16255.52 10.51 o 4 2 1 759.51 819.73 2.05 o 6 2 1 2611.25 2695.36 4.46 o 8 2 1 1041.46 1083.35 2.97 o -9 3 1 90.54 85.76 0.86 o -7 3 1 737.92 707.07 2.49 o -5 3 1 1432.65 1539.15 2.99 o -3 3 1 506.23 632.08 1.50 o -1 3 1 4687.38 6932.84 4.22 o 1 3 1 6435.19 8260.40 5.02 o 3 3 1 6930.95 5488.77 5.81 o 5 3 1 9287.73 8690.44 7.68 o 7 3 1 94.77 95.15 0.93 o 9 3 1 247.53 290.67 0.93 o -8 4 1 463.28 458.60 1.97 o -6 4 1 244.12 239.02 1.37 o -4 4 1 991.94 1120.53 2.32 o -2 4 1 267.03 326.12 1.07 o 0 4 1 589.16 881.68 1.55 o 2 4 1 7992.27 8990.85 5.91 o 4 4 1 59.93 64.84 0.61 o 6 4 1 861.08 867.99 2.60 o 8 4 1 134.50 135.51 1.07 o -9 5 1 428.22 427.38 1.72 o -7 5 1 2184.85 2080.74 4.27 o -5 5 1 1948.92 1966.54 3.60 o -3 5 1 471.82 657.67 1.52 o -1 5 1 7182.29 8355.45 5.59 o 1 5 1 1436.69 1893.74 2.56 o 3 5 1 824.87 794.41 2.10 o 5 5 1 2293.35 2014.54 3.95 o 7 5 1 4.63 5.52 0.26 o 9 5 1 120.22 141.15 0.89 o -8 6 1 424.61 394.24 1.86 o -6 6 1 5468.26 5197.75 6.53 o -4 6 1 3775.40 4005.25 4.76 o -2 6 1 15056.47 17310.62 45.58 o 0 6 1 224.09 215.83 1.01 o 2 6 1 39.93 27.29 0.51 o 4 6 1 83.82 112.90 0.74 o 6 6 1 6366.31 5307.04 7.17 o 8 6 1 719.95 727.34 2.34 o -9 7 1 724.30 746.98 2.14 o -7 7 1 884.59 865.15 2.72 o -5 7 1 184.42 220.04 1.17 o -3 7 1 5083.65 5515.77 5.32 o -1 7 1 921.90 1069.25 2.15 o 1 7 1 4509.10 4850.77 4.70 o 3 7 1 5900.08 6159.05 5.82 o 5 7 1 1202.69 1200.50 3.02 o 7 7 1 1377.71 1285.24 3.40 o -8 8 1 1.31 1.42 0.33 o -6 8 1 124.42 131.62 1.07 o -4 8 1 143.90 168.55 1.00 o -2 8 1 2375.02 2643.92 3.66 o 0 8 1 204.22 224.33 1.04 o 2 8 1 7506.28 7621.30 6.63 o 4 8 1 6.70 6.78 0.31 o 6 8 1 1407.12 1394.59 3.43 o 8 8 1 11.19 13.16 0.38 o -7 9 1 754.97 748.69 2.53 o -5 9 1 61.86 68.37 0.74 o -3 9 1 28.71 28.81 0.49 o -1 9 1 2.07 3.15 0.15 o 1 9 1 2866.46 3038.29 4.05 o 3 9 1 1943.40 1960.67 3.66 o 5 9 1 1069.51 1083.80 2.93 o 7 9 1 697.07 697.50 2.34 o -8 10 1 304.15 304.21 1.44 o -6 10 1 344.86 327.09 1.74 o -4 10 1 3605.49 3515.99 5.33 o -2 10 1 9.41 20.50 0.27 o 0 10 1 603.29 657.81 1.92 o 2 10 1 3463.93 3462.67 4.89 o 4 10 1 103.41 114.11 0.92 o 6 10 1 1079.01 1052.90 3.01 o 8 10 1 612.95 687.63 1.95 o -7 11 1 1216.64 1213.85 2.99 o -5 11 1 89.29 88.80 0.90 o -3 11 1 1878.50 1786.79 3.76 o -1 11 1 1900.32 1946.67 3.59 o 1 11 1 78.68 81.73 0.77 o 3 11 1 291.42 266.07 1.51 o 5 11 1 685.33 669.78 2.45 o 7 11 1 133.19 123.80 1.01 o -6 12 1 1.30 1.76 0.16 o -4 12 1 329.32 343.92 1.70 o -2 12 1 509.01 481.48 2.00 o 0 12 1 244.09 273.21 1.36 o 2 12 1 3754.73 3523.98 5.42 o 4 12 1 136.62 139.18 1.09 o 6 12 1 104.98 120.47 0.92 o -7 13 1 49.98 60.80 0.62 o -5 13 1 292.67 282.83 1.58 o -3 13 1 630.82 639.22 2.35 o -1 13 1 53.04 56.12 0.69 o 1 13 1 963.32 949.23 2.79 o 3 13 1 355.36 335.44 1.76 o 5 13 1 9.15 11.11 0.37 o -6 14 1 126.46 143.99 0.95 o -4 14 1 15.04 17.40 0.42 o -2 14 1 1050.13 1041.81 2.96 o 0 14 1 4867.98 4550.83 6.38 o 2 14 1 2610.18 2441.75 4.66 o 4 14 1 13.13 13.91 0.44 o 6 14 1 120.61 145.19 0.90 o -5 15 1 92.33 94.81 0.84 o -3 15 1 3754.09 3479.40 5.51 o -1 15 1 98.91 102.69 0.95 o 1 15 1 26.55 30.98 0.53 o 3 15 1 215.97 240.48 1.36 o 5 15 1 242.49 260.12 1.28 o -4 16 1 56.25 54.37 0.71 o -2 16 1 0.43 2.02 0.09 o 0 16 1 7.29 9.57 0.34 o 2 16 1 369.23 364.74 1.75 o 4 16 1 11.89 11.22 0.41 o -3 17 1 119.82 128.01 0.94 o -1 17 1 65.03 67.30 0.76 o 1 17 1 61.54 70.65 0.73 o 3 17 1 30.16 31.81 0.53 o -2 18 1 198.34 199.32 1.15 o 0 18 1 393.01 402.45 1.63 o 2 18 1 491.56 498.87 1.78 o -10 0 2 220.30 199.97 1.18 o -8 0 2 715.84 741.13 2.50 o -6 0 2 8.72 13.18 0.29 o -4 0 2 189.30 211.26 1.00 o -2 0 2 4316.47 5013.29 4.28 o 0 0 2 1763.85 2565.62 2.70 o 2 0 2 2525.51 2962.99 3.24 o 4 0 2 15683.51 14189.39 9.45 o 6 0 2 1974.37 1974.17 3.85 o 8 0 2 1936.81 1942.14 3.97 o -9 1 2 9.91 10.41 0.39 o -7 1 2 208.87 205.33 1.30 o -5 1 2 176.83 213.89 1.04 o -3 1 2 3175.20 3601.37 3.76 o -1 1 2 6136.94 8191.99 5.00 o 1 1 2 99.79 156.19 0.64 o 3 1 2 104.35 119.00 0.71 o 5 1 2 383.58 351.17 1.60 o 7 1 2 1444.22 1418.63 3.47 o 9 1 2 12.49 15.73 0.37 o -8 2 2 45.56 46.76 0.67 o -6 2 2 59.97 61.72 0.69 o -4 2 2 797.00 949.28 2.02 o -2 2 2 805.60 1013.86 1.85 o 0 2 2 137.01 216.07 0.76 o 2 2 2 74.97 83.18 0.59 o 4 2 2 1477.28 1467.25 2.87 o 6 2 2 859.32 818.62 2.60 o 8 2 2 69.95 77.05 0.79 o -9 3 2 159.82 162.00 1.11 o -7 3 2 5170.32 4716.64 6.46 o -5 3 2 1068.76 1199.43 2.59 o -3 3 2 923.14 1022.36 2.10 o -1 3 2 33573.07 36583.77 62.50 o 1 3 2 5629.00 6173.71 4.81 o 3 3 2 2407.36 2265.67 3.43 o 5 3 2 97.87 103.82 0.84 o 7 3 2 62.15 57.25 0.77 o 9 3 2 35.10 41.73 0.53 o -8 4 2 11.30 13.26 0.37 o -6 4 2 2317.21 2328.06 4.12 o -4 4 2 10457.40 10497.00 7.54 o -2 4 2 3141.56 4037.67 3.77 o 0 4 2 3595.88 5023.19 3.81 o 2 4 2 5010.51 5098.37 4.87 o 4 4 2 1031.94 934.31 2.49 o 6 4 2 1786.54 1634.43 3.81 o 8 4 2 2489.25 2414.20 4.44 o -9 5 2 66.72 65.54 0.75 o -7 5 2 271.81 269.81 1.54 o -5 5 2 4212.19 4262.80 5.30 o -3 5 2 683.60 730.42 1.89 o -1 5 2 1755.45 2185.16 2.81 o 1 5 2 333.17 465.23 1.24 o 3 5 2 1724.04 1908.72 3.06 o 5 5 2 3703.59 3278.60 5.22 o 7 5 2 1286.38 1226.66 3.28 o 9 5 2 14.95 16.26 0.41 o -8 6 2 168.65 164.50 1.20 o -6 6 2 12.45 16.64 0.37 o -4 6 2 85.45 96.57 0.74 o -2 6 2 3051.83 3479.38 3.92 o 0 6 2 67.62 76.24 0.56 o 2 6 2 6.28 9.02 0.22 o 4 6 2 736.32 787.85 2.22 o 6 6 2 1693.99 1559.58 3.77 o 8 6 2 83.06 94.07 0.83 o -9 7 2 1106.94 1141.83 2.69 o -7 7 2 2347.48 2201.92 4.42 o -5 7 2 195.92 197.06 1.23 o -3 7 2 1995.99 2284.22 3.32 o -1 7 2 483.67 589.44 1.59 o 1 7 2 1636.54 2024.14 2.87 o 3 7 2 2441.81 2609.73 3.91 o 5 7 2 675.41 663.77 2.30 o 7 7 2 1.26 3.78 0.15 o -8 8 2 7.07 7.54 0.37 o -6 8 2 10520.46 9306.90 9.40 o -4 8 2 6399.46 6465.63 6.64 o -2 8 2 8044.07 8270.02 6.69 o 0 8 2 1608.95 1789.70 2.97 o 2 8 2 31.73 37.50 0.45 o 4 8 2 9.62 11.64 0.31 o 6 8 2 1899.77 1743.51 3.98 o 8 8 2 1440.29 1640.94 3.13 o -7 9 2 810.76 818.86 2.62 o -5 9 2 1564.60 1564.74 3.49 o -3 9 2 1819.61 1978.52 3.47 o -1 9 2 6386.57 6561.73 6.22 o 1 9 2 1227.37 1294.41 2.70 o 3 9 2 1639.71 1713.27 3.42 o 5 9 2 887.09 884.79 2.73 o 7 9 2 33.32 34.41 0.59 o -8 10 2 60.69 64.18 0.71 o -6 10 2 10.91 12.95 0.39 o -4 10 2 1929.15 1874.30 3.90 o -2 10 2 2993.99 3042.95 4.44 o 0 10 2 253.71 262.17 1.27 o 2 10 2 522.89 580.47 1.93 o 4 10 2 33.23 39.38 0.56 o 6 10 2 0.87 1.50 0.12 o -7 11 2 4.21 3.45 0.27 o -5 11 2 6.20 7.72 0.32 o -3 11 2 434.29 415.82 1.85 o -1 11 2 216.81 228.49 1.24 o 1 11 2 1.80 1.08 0.37 o 3 11 2 933.68 933.59 2.76 o 5 11 2 611.38 599.07 2.31 o 7 11 2 3.07 2.36 0.45 o -6 12 2 1493.06 1422.53 3.50 o -4 12 2 1207.79 1226.44 3.18 o -2 12 2 770.57 742.39 2.46 o 0 12 2 1968.54 1921.44 3.86 o 2 12 2 2050.08 1991.33 4.08 o 4 12 2 18.60 17.96 0.48 o 6 12 2 281.76 306.80 1.45 o -7 13 2 303.59 341.13 1.39 o -5 13 2 111.27 127.83 0.97 o -3 13 2 2695.45 2600.73 4.74 o -1 13 2 4004.00 3839.20 5.69 o 1 13 2 952.53 935.25 2.83 o 3 13 2 2006.64 1817.77 4.09 o 5 13 2 164.01 167.86 1.17 o -6 14 2 396.38 398.23 1.67 o -4 14 2 266.76 259.78 1.50 o -2 14 2 145.51 133.35 1.15 o 0 14 2 603.30 585.96 2.30 o 2 14 2 516.41 530.42 2.12 o 4 14 2 179.35 186.83 1.21 o 6 14 2 154.26 167.49 0.98 o -5 15 2 30.76 28.79 0.57 o -3 15 2 25.35 28.15 0.53 o -1 15 2 264.82 285.40 1.52 o 1 15 2 1001.73 963.31 2.90 o 3 15 2 53.48 52.89 0.73 o 5 15 2 86.18 89.61 0.80 o -4 16 2 545.52 577.09 1.99 o -2 16 2 377.33 345.32 1.76 o 0 16 2 113.29 109.99 1.01 o 2 16 2 1239.29 1239.87 3.14 o 4 16 2 16.83 15.14 0.48 o -3 17 2 111.92 115.98 0.91 o -1 17 2 1191.53 1172.13 2.97 o 1 17 2 41.44 48.39 0.60 o 3 17 2 637.16 676.82 2.00 o -2 18 2 100.13 107.21 0.82 o 0 18 2 125.69 139.12 0.93 o 2 18 2 976.43 1060.63 2.40 o -9 1 3 5.86 5.04 0.35 o -7 1 3 376.58 333.59 1.75 o -5 1 3 270.97 288.01 1.28 o -3 1 3 32.74 41.09 0.40 o -1 1 3 9768.76 10121.63 6.16 o 1 1 3 65274.31 42093.68 88.78 o 3 1 3 1351.39 1393.23 2.63 o 5 1 3 1254.11 1238.00 2.99 o 7 1 3 488.04 423.82 2.06 o 9 1 3 39.07 33.37 0.61 o -10 2 3 537.02 527.09 1.84 o -8 2 3 2373.44 2096.37 4.45 o -6 2 3 87.54 93.72 0.81 o -4 2 3 2151.91 2306.53 3.40 o -2 2 3 11223.80 11876.61 6.83 o 0 2 3 6494.93 6841.66 5.08 o 2 2 3 5341.21 4777.13 5.06 o 4 2 3 6919.86 6178.60 6.43 o 6 2 3 2.39 3.59 0.13 o 8 2 3 775.60 741.32 2.43 o -9 3 3 14.46 11.09 0.47 o -7 3 3 60.97 66.81 0.75 o -5 3 3 28.50 26.24 0.47 o -3 3 3 21174.62 22280.52 53.47 o -1 3 3 17821.37 19441.70 46.52 o 1 3 3 11807.15 10369.56 7.37 o 3 3 3 226.26 199.75 1.12 o 5 3 3 6899.61 5768.67 6.96 o 7 3 3 1112.47 1024.86 3.05 o -8 4 3 140.61 124.09 1.14 o -6 4 3 2597.04 2555.90 4.35 o -4 4 3 192.27 190.17 1.05 o -2 4 3 67.64 97.35 0.56 o 0 4 3 11357.14 11395.04 6.93 o 2 4 3 16202.74 12789.81 9.00 o 4 4 3 3713.65 3266.17 4.89 o 6 4 3 2795.74 2365.49 4.85 o 8 4 3 262.10 258.48 1.43 o -9 5 3 375.62 361.95 1.68 o -7 5 3 601.65 601.56 2.24 o -5 5 3 214.23 207.80 1.19 o -3 5 3 270.57 257.70 1.21 o -1 5 3 4546.57 5379.95 4.51 o 1 5 3 1529.88 1544.67 2.73 o 3 5 3 36.83 48.64 0.48 o 5 5 3 281.79 251.10 1.50 o 7 5 3 25.77 18.05 0.62 o -8 6 3 276.70 262.25 1.53 o -6 6 3 2905.82 2870.03 4.77 o -4 6 3 7189.03 7204.72 6.52 o -2 6 3 5056.55 5607.28 5.11 o 0 6 3 513.69 586.19 1.62 o 2 6 3 728.46 666.55 1.98 o 4 6 3 1489.43 1421.38 3.18 o 6 6 3 3.32 3.19 0.19 o 8 6 3 451.56 460.99 1.77 o -9 7 3 759.67 810.78 2.22 o -7 7 3 462.82 439.17 2.01 o -5 7 3 3325.02 3332.84 4.94 o -3 7 3 454.69 570.59 1.62 o -1 7 3 730.35 711.44 1.97 o 1 7 3 3864.43 4053.49 4.59 o 3 7 3 2311.07 2129.60 3.84 o 5 7 3 988.48 902.89 2.83 o 7 7 3 137.24 139.07 1.09 o -8 8 3 10.91 8.90 0.40 o -6 8 3 647.73 649.14 2.33 o -4 8 3 296.52 309.58 1.42 o -2 8 3 1594.03 1692.99 3.03 o 0 8 3 4083.54 4231.96 4.78 o 2 8 3 154.92 174.97 1.00 o 4 8 3 447.79 391.62 1.88 o 6 8 3 1.99 2.44 0.14 o 8 8 3 599.16 710.96 1.91 o -7 9 3 1317.19 1303.42 3.33 o -5 9 3 12.88 10.64 0.48 o -3 9 3 452.52 436.91 1.77 o -1 9 3 1945.59 2075.20 3.49 o 1 9 3 1638.95 1744.74 3.26 o 3 9 3 0.92 2.03 0.10 o 5 9 3 1183.77 1119.49 3.14 o 7 9 3 90.36 97.23 0.86 o -8 10 3 34.10 34.21 0.57 o -6 10 3 474.99 447.99 2.04 o -4 10 3 6822.19 6413.58 7.32 o -2 10 3 121.18 118.63 0.94 o 0 10 3 2.90 3.70 0.19 o 2 10 3 3064.55 2981.95 4.75 o 4 10 3 110.13 96.68 1.01 o 6 10 3 25.21 29.63 0.51 o -7 11 3 1141.12 1154.34 2.96 o -5 11 3 93.29 100.74 0.92 o -3 11 3 1066.30 1052.41 2.89 o -1 11 3 5920.59 5874.89 6.61 o 1 11 3 1077.70 1086.48 2.80 o 3 11 3 450.01 398.99 1.95 o 5 11 3 156.07 158.64 1.17 o 7 11 3 3.86 3.96 0.23 o -6 12 3 2.91 3.92 0.18 o -4 12 3 289.01 311.58 1.59 o -2 12 3 234.15 228.36 1.38 o 0 12 3 99.84 127.74 0.89 o 2 12 3 57.39 58.19 0.74 o 4 12 3 99.57 85.68 0.95 o 6 12 3 185.02 181.32 1.16 o -7 13 3 145.52 152.45 0.99 o -5 13 3 1.99 3.02 0.14 o -3 13 3 1576.89 1545.19 3.63 o -1 13 3 2078.61 2045.25 4.09 o 1 13 3 208.26 198.48 1.32 o 3 13 3 154.97 157.79 1.16 o 5 13 3 3.89 6.06 0.25 o -6 14 3 64.15 62.89 0.71 o -4 14 3 497.70 477.43 2.05 o -2 14 3 174.02 167.27 1.26 o 0 14 3 774.53 743.62 2.60 o 2 14 3 988.63 927.54 2.87 o 4 14 3 1494.07 1464.47 3.37 o -5 15 3 857.23 904.58 2.44 o -3 15 3 1484.96 1430.18 3.48 o 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