Acta Crystallographica Section C

Crystal Structure Communications

Volume 53, Part 4 (April 1997)


Cover illustrationCover illustration: Intra- and Intermolecular Hydrogen Bonding in a Tetrahydroxycalix\[4\]arene, see Böhmer, Ferguson, Grüttner and Vogt, pages 469-472. Displacement ellipsoids are shown at the 30% probability level: H atoms and the solvent molecule have been omitted for clarity.

inorganic compounds



Acta Cryst. (1997). C53, 395-397    [ doi:10.1107/S0108270196014102 ]

The Mixed Anionic Framework in the Structure of Na2{MnF[PO4]

O. V. Yakubovich, O. V. Karimova and O. K. Mel'nikov

Synopsis: Na2{MnF[PO4]} is isotypic with Na2{ZrO[XO4]} (X = Si, Ge) and comprises (Mn2F2O8) octahedral chains connected by corner-sharing PO4 tetrahedra to form a three-dimensional framework with Na+ ions in the channels.

Formula: Na2{MnF[PO4]}



Acta Cryst. (1997). C53, 397-399    [ doi:10.1107/S0108270196007226 ]

Na4Ce(As2O7)2

W. Belam, H. Boughzala and T. Jouini

Synopsis: The structure of Na4Ce(As2O7)2 is built from CeO8 antiprisms and As2O7 diarsenate groups connected by Ce-O-As mixed bridges to form a three-dimensional framework with Na+ cations located in the tunnels. The As2O7 groups have a nearly eclipsed confomation.

Formula: Na4Ce(As2O7)2



Acta Cryst. (1997). C53, 399-401    [ doi:10.1107/S0108270196013960 ]

Strontium Metagermanate, SrGeO3

F. Nishi

Synopsis: The structure of SrGeO3 consists of ternary rings of GeO4 groups and close-packed Sr atoms stacked alternately along the [001] direction to form a six-layer structure.

Formula: SrGeO3


metal-organic compounds



Acta Cryst. (1997). C53, 402-404    [ doi:10.1107/S010827019601459X ]

trans-Diaquabis(hexafluoroacetylacetonato-O,O')manganese(II) Monohydrate

M. H. Dickman

Formula: [Mn(C5HF6O2)2(H2O)2].H2O



Acta Cryst. (1997). C53, 404-406    [ doi:10.1107/S0108270196014291 ]

[bold mu]-Hydrido-[bold mu]-dicyclohexylphosphido-bis[dicyclohexylphosphine(tricarbonyl)rhenium]

U. Flörke and H.-J. Haupt

Formula: [Re2H(C12H22P)(C12H23P)2(CO)6]



Acta Cryst. (1997). C53, 406-408    [ doi:10.1107/S0108270196015132 ]

Dichlorodimethylbis(3-methyladenine-N7)tin(IV)

A. Hazell, J. Ouyang and L. E. Khoo

Formula: [SnCl2(CH3)2(C6H7N5)2]



Acta Cryst. (1997). C53, 409-410    [ doi:10.1107/S0108270196014692 ]

Tetramethylammonium Tris(thiobenzoato-O,S)mercury(II)

J. J. Vittal and P. A. W. Dean

Formula: (C4H12N)[Hg(C7H5OS)3]



Acta Cryst. (1997). C53, 411-413    [ doi:10.1107/S0108270196013297 ]

Bis[bis(2-aminoethyl-N)sulfide-S]nickel(II) Bis(hexafluorophosphate)

A. J. Blake, J. P. Danks, S. Parsons and M. Schröder

Formula: [Ni(C4H12N2S)2](PF6)2



Acta Cryst. (1997). C53, 413-414    [ doi:10.1107/S0108270196015405 ]

Tetraphenylphosphonium (Hydrogensulfido-S)trisulfidotungstate(VI)

M. Parvez, P. M. Boorman and M. Wang

Formula: (C24H20P)[W(HS)S3]



Acta Cryst. (1997). C53, 415-416    [ doi:10.1107/S0108270196013984 ]

Dichlorobis[1-methyl-3-(prop-2-enyl)imidazole-2(3H)-thione-S]zinc(II)

D. J. Williams, T. A. Ly, J. W. Mudge, W. T. Pennington and G. L. Schimek

Formula: [ZnCl2(C7H10N2S)2]



Acta Cryst. (1997). C53, 416-419    [ doi:10.1107/S0108270196014199 ]

The isonido-Metalladicarbaborane [1,1,1-H{P(CH3)3}2-6-Cl-1,2,4-IrC2B8H9]

J. Bould, N. P. Rath and L. Barton

Formula: [IrH(C3H9P)2(C2B8H9Cl)]



Acta Cryst. (1997). C53, 419-422    [ doi:10.1107/S0108270196014412 ]

Bis{[bold mu]-[1-(N-Methylsulfonimidoyl)-2,2-diphenylethene]}-1[bold kappa]2C1,N:2[bold kappa]O;1[bold kappa]O:2[bold kappa]2C1,N-bis[(tetrahydrofuran-O)lithium] Tetrahydrofuran Solvate and 1-(N-Methylphenylsulfonimidoyl)-2,2-diphenylethene

M. Zehnder, J. F. K. Müller and M. Neuburger

Formula: [Li2(C21H19NOS)2(C4H8O)2].C4H8O and C21H19NOS



Acta Cryst. (1997). C53, 422-425    [ doi:10.1107/S0108270196014138 ]

Metal-[alpha],[omega]-Dicarboxylate Complexes. II. catena-Poly[bis(imidazole-N3)copper(II)-di-[bold mu]-adipato(1 -)-O1:O6;O6:O1]

E. Suresh and M. M. Bhadbhade

Formula: [Cu(C6H9O4)2(C3H4N2)2]



Acta Cryst. (1997). C53, 425-428    [ doi:10.1107/S010827019601503X ]

[bold mu]-1,4-Bis(diphenylphosphino)phenylene-P:P'-bis[[bold mu]3-benzylidyne-octacarbonyl-triangulo-tricobalt(3 Co-Co)]

N. C. Alexander, B. H. Robinson and J. Simpson

Formula: [Co6(C7H5)2(C30H24P2)(CO)16]



Acta Cryst. (1997). C53, 428-430    [ doi:10.1107/S0108270196014680 ]

Reinvestigation of mer,trans-(Acetonitrile)trichlorobis(triphenylphosphine)rhenium(III)

M. Davis, F. Bélanger-Gariépy, D. Zargarian and A. L. Beauchamp

Formula: [ReCl3(C2H3N)(C18H15P)2]



Acta Cryst. (1997). C53, 430-432    [ doi:10.1107/S0108270196014333 ]

Aqua(2,2'-bipyridyl-N,N')trichloromanganese(III)

A. Tesouro, M. Corbella and H. Stoeckli-Evans

Formula: [MnCl3(C10H8N2)(H2O)]



Acta Cryst. (1997). C53, 432-434    [ doi:10.1107/S0108270196013327 ]

Sodium trans-Bis(methyliminodiacetato-O,N,O)chromate(III), Na[Cr(C5H7NO4)2]

J.-S. Suh, S.-J. Park, K.-W. Lee, I.-H. Suh, J.-H. Lee, J.-H. Song and M.-R. Oh

Formula: Na[Cr(C5H7NO4)2]



Acta Cryst. (1997). C53, 434-436    [ doi:10.1107/S0108270196015028 ]

trans-Bis[4-amino-3,5-bis(2-pyridyl)-1,2,4-triazole-N1,N']copper(II) Bis(tetrafluoroborate)

A. J. Jircitano, S. O. Sommerer and K. A. Abboud

Formula: [Cu(C12H10N6)2](BF4)2



Acta Cryst. (1997). C53, 436-438    [ doi:10.1107/S0108270196014370 ]

A Chelate-Stabilized Tungsten-Imido-Monoalkyl Complex, [WCl(PhN)(CH2CMe3){o-C6H4(NSiMe3)2}]

S.-Y. S. Wang, J. M. Boncella and K. A. Abboud

Formula: [WCl(C5H11)(C6H5N)(C12H22N2Si2)]



Acta Cryst. (1997). C53, 438-443    [ doi:10.1107/S0108270196012772 ]

The Mercury(II) Trifluoroacetate-Bipyridyl System

J. Halfpenny and R. W. H. Small

Formula: [Hg(C2F3O2)(C10H8N2)][Hg(C2F3O2)4]0.5, [Hg(C2F3O2)(C10H8N2)2][Hg(C2F3O2)3(C10H8N2)] and [Hg(C10H8N2)2](C2F3O2)2



Acta Cryst. (1997). C53, 443-445    [ doi:10.1107/S010827019601284X ]

Structural Investigation of NiII Complexes. XI. Dichlorobis(4-methylpiperidine-N)(4-methylpyridine-N)nickel(II)

M. Koman, E. Jóna and I. Kopál

Formula: [NiCl2(C6H7N)(C6H13N)2]



Acta Cryst. (1997). C53, 445-447    [ doi:10.1107/S0108270196014916 ]

(SR,1R,2S)-1-(tert-Butylsulfinyl)2-(hydroxymethyl)ferrocene

P. D. Robinson, D. H. Hua, N. M. Lagneau, P. M. Robben and C. Y. Meyers

Formula: [Fe(C5H5)(C10H15O2S)]



Acta Cryst. (1997). C53, 447-449    [ doi:10.1107/S0108270196014643 ]

Tricarbonyl[3-([bold eta]5-cyclopentadienylcarbonylamino)propionic acid]rhenium

A. Bennouna, A. Mousser, A. Gorfti, M. Salmain, C. Cabestaing and G. Jaouen

Formula: [Re(C9H10NO3)(CO)3]



Acta Cryst. (1997). C53, 449-451    [ doi:10.1107/S0108270196014874 ]

Epimer B of Tetraphenylarsonium (Mercaptoacetylalanylglycylglycinato-N,N',N'',S)oxotechnetate(V) (99Tc) Chloroform Solvate

N. M. Blaton, G. Bormans, O. M. Peeters and A. Verbruggen

Formula: (C24H20As)[TcO(C9H11N3O5S)].CHCl3



Acta Cryst. (1997). C53, 452-453    [ doi:10.1107/S0108270196015016 ]

[bold mu]-Acetato-O:O'-[bold mu]-oxo-bis{[tris(2-pyridylmethyl)amine-N,N',N'',N''']iron(III)} Tris(trifluoromethanesulfonate) Dihydrate

R. E. Norman, N. L. Peterson and S.-C. Chang

Formula: [Fe2O(C2H3O2)(C18H18N4)2](CF3O3S)3.2H2O


organic compounds



Acta Cryst. (1997). C53, 454-455    [ doi:10.1107/S0108270196014825 ]

1-Adeninium 2-Fluorobenzoate Monohydrate

J. Jai-nhuknan, A. G. Karipides and J. S. Cantrell

Formula: C5H6N5+.C7H4FO2-.H2O



Acta Cryst. (1997). C53, 455-457    [ doi:10.1107/S010827019601428X ]

N,N'-Bis(pentafluorophenyl)urea

J. Jai-nhuknan, A. G. Karipides, J. M. Hughes and J. S. Cantrell

Formula: C13H2F10N2O



Acta Cryst. (1997). C53, 457-459    [ doi:10.1107/S0108270196014461 ]

(3R,2'S)-2'-N-Dibenzylamino-1,2:5,6-di-O-isopropylidène-[alpha]-D-allofuranose-3-spiro-3'-[beta]-propiolactone

A. Chiaroni, C. Riche, S. Bouifraden, J.-P. Lavergne and P. Viallefont

Formula: C28H33NO7



Acta Cryst. (1997). C53, 459-461    [ doi:10.1107/S0108270196014606 ]

Méthyl N-[(2R,5S)-1-N-Benzyl-5-méthoxycarbonylprolyl]-(S)-phénylalaninate

A. Chiaroni, C. Riche, T. Zair, F. Guenoun, R. Lazaro et P. Viallefont

Formula: C24H28N2O5



Acta Cryst. (1997). C53, 461-463    [ doi:10.1107/S0108270196014448 ]

(N-Hydroxy-2-méthylpyrrolidin-2-yl)phosphonate de Diéthyle

S. Barbati, D. Siri, P. Tordo et J.-P. Reboul

Formula: C9H20NO4P



Acta Cryst. (1997). C53, 463-465    [ doi:10.1107/S0108270196012127 ]

Bis(propane-1,3-diammonium) Diphosphate Tetrahydrate

M. Charfi and A. Jouini

Formula: 2C3H12N2^2+.P2O7^4-.4H2O



Acta Cryst. (1997). C53, 465-467    [ doi:10.1107/S0108270196014709 ]

1,4-Phenylenebis(diphenylphosphine oxide)

N. C. Alexander, B. H. Robinson and J. Simpson

Formula: C30H24O2P2



Acta Cryst. (1997). C53, 467-469    [ doi:10.1107/S0108270196005604 ]

2-(Diphenylphosphinoyl)-1,3-dioxane

W. R. Majzner, M. W. Wieczorek, M. Mikolajczyk and P. P. Graczyk

Formula: C16H17O3P



Acta Cryst. (1997). C53, 469-472    [ doi:10.1107/S0108270196015508 ]

Intra- and Intermolecular Hydrogen Bonding in a Tetrahydroxycalix[4]arene

V. Böhmer, G. Ferguson, C. Grüttner and W. Vogt

Formula: C45H49NO6.0.5CHCl3



Acta Cryst. (1997). C53, 472-474    [ doi:10.1107/S0108270196015521 ]

A Calix[4]arene with Diethylthiocarbamoylmethyloxy Substituents in the 1,3 Positions

M. G. B. Drew, P. D. Beer and M. I. Ogden

Formula: C56H78N2O4S2



Acta Cryst. (1997). C53, 474-476    [ doi:10.1107/S0108270196015545 ]

meta-Nitroacetophenone at 173K

M. Bolte and M. Scholtyssik

Formula: C8H7NO3



Acta Cryst. (1997). C53, 476-477    [ doi:10.1107/S0108270196014928 ]

2-Methylamino-5-chlorobenzophenone

P. J. Cox, A. T. Md. Anisuzzaman, G. G. Skellern, R. H. Pryce-Jones, A. J. Florence and N. Shankland

Formula: C14H12ClNO



Acta Cryst. (1997). C53, 477-480    [ doi:10.1107/S0108270196014655 ]

The Dipeptide pGlu-Pro-NH2

J. Wouters, B. Norberg and G. Evrard

Formula: C10H15N3O3.H2O



Acta Cryst. (1997). C53, 480-482    [ doi:10.1107/S0108270196014382 ]

Cholamide Dihydrate

M. C. Wahle, P. E. Fanwick and S. R. Byrn

Formula: C24H41NO4.2H2O



Acta Cryst. (1997). C53, 482-486    [ doi:10.1107/S0108270196013649 ]

Anti-Inflammatory Drugs. V. [Tris-(2-hydroxymethyl)methyl]ammonium 2-[(2,6-Dichlorophenyl)amino]phenylacetate (TRISH. D)

C. Castellari and S. Ottani

Formula: C4H12NO3+.C14H10Cl2NO2- and C4H11NO3



Acta Cryst. (1997). C53, 486-488    [ doi:10.1107/S0108270196014473 ]

Two Schiff Base Ligands Derived from 1,2-Diaminoethane

J. P. Corden, W. Errington, P. Moore and M. G. H. Wallbridge

Formula: C20H24N2O2 and C28H24N2O2



Acta Cryst. (1997). C53, 488-490    [ doi:10.1107/S0108270196015399 ]

Low-Temperature Phase of Tetraethylammonium Bromide

M. Ralle, J. C. Bryan, A. Habenschuss and B. Wunderlich

Formula: C8H20N+.Br-



Acta Cryst. (1997). C53, 490-491    [ doi:10.1107/S0108270196013583 ]

Ethyl N-Methyl-2-pyrrolylcarbonylhydrazinocarboxylate

M. Liu-Gonzalez, F. Sanz-Ruiz, M. E. Gonzalez-Rosende, O. Lozano-Lucía, E. Zaballos-García and J. Sepulveda-Arqués

Formula: C9H13N3O3



Acta Cryst. (1997). C53, 492-493    [ doi:10.1107/S0108270196014679 ]

N-(5-Nitro-2-pyrrolidinylphenyl)trifluoroacetamide

C. Yanes, M. Torres, M. López-Rodríguez, P. Núñez and I. Brito

Formula: C12H12F3N3O3



Acta Cryst. (1997). C53, 494-496    [ doi:10.1107/S0108270196015296 ]

2,4-Dibromo-5-hydroxybenzaldehyde

A. Matos Beja, J. A. Paixão, M. Ramos Silva, L. Alte da Veiga, A. M. d'A. Rocha Gonsalves, M. M. Pereira and A. C. Serra

Formula: C7H4Br2O2



Acta Cryst. (1997). C53, 496-498    [ doi:10.1107/S0108270196015284 ]

13-Phenyl-11,13,15-triazatricyclo[8.5.2.011,15]heptadec-16-ene-12,14-dione

M. N. Tahir, D. Ülkü, A. S. Demir, M. Mohammadi and E. Özgül

Formula: C20H25N3O2



Acta Cryst. (1997). C53, 498-499    [ doi:10.1107/S010827019601548X ]

4,4'-Dimethyl-2,2'-bipyridine 1,1'-Dioxide

H. Kanno and K. Iijima

Formula: C12H12N2O2



Acta Cryst. (1997). C53, 499-504    [ doi:10.1107/S0108270196015090 ]

meso-2,2,2',2'-Tetrachloro-1,1'-diphenyl-1,1'-bicyclopropyl and meso-2,2,2',2'-Tetrabromo-1,1'-diphenyl-1,1'-bicyclopropyl

Y.-L. Lam, L.-L. Koh and H.-H. Huang

Formula: C18H14Cl4 and C18H14Br4



Acta Cryst. (1997). C53, 504-506    [ doi:10.1107/S0108270196014886 ]

(E)-3-(2,2-Dibromospiro[2.4]heptan-1-yl)propenenitrile

M. G. Banwell, D. C. R. Hockless and A. W. Wu

Formula: C10H11Br2N



Acta Cryst. (1997). C53, 506-508    [ doi:10.1107/S0108270196015934 ]

Antazoline

M. Parvez

Formula: C17H19N3



Acta Cryst. (1997). C53, 508-511    [ doi:10.1107/S0108270196014588 ]

Disorder in 13-cis-Retinoic Acid

L. Malpezzi, C. Fuganti and P. Grasselli

Formula: C20H28O2



Acta Cryst. (1997). C53, 511-513    [ doi:10.1107/S010827019601445X ]

Absolute Structure of (Thian-5-one 1,1-dioxide)-3-spiro-3'-(5'-O-tert-butyldimethylsilyl-3'-deoxy-1',2'-O-isopropylidene-[alpha]-D-xylo-pentofuranose), a Novel Type of Spirosugar

G. Bernardinelli, J. M. J. Tronchet and I. Kovacs

Formula: C18H32O7SSi



Acta Cryst. (1997). C53, 513-515    [ doi:10.1107/S0108270197000255 ]

A Novel Function of an Atropisomeric Flavin Model as a Host Compound

Y. Kawai, J. Kunitomo and A. Ohno

Formula: C28H23N3O4.CH4O



Acta Cryst. (1997). C53, 515-517    [ doi:10.1107/S010827019601579X ]

Configurations of Cycloadducts Formed in Asymmetric Intramolecular Diels-Alder Reactions

J. Breu, T. Butz, K.-J. Range and J. Sauer

Formula: C21H30O5 and C14H18O5



Acta Cryst. (1997). C53, 517-519    [ doi:10.1107/S0108270196015156 ]

4-(9-Fluorenoxy)-2-phenylphthalazin-1(2H)-one

M. J. Bausch, P. D. Robinson and Y. Gong

Formula: C27H18N2O2



Acta Cryst. (1997). C53, 519-521    [ doi:10.1107/S0108270196013777 ]

(±)-N-[1,8(10)-Menthadien-3-yl]toluenesulfonamide

A. Stepien and A. M. Osinska

Formula: C17H23NO2S



Acta Cryst. (1997). C53, 521-522    [ doi:10.1107/S0108270196015569 ]

4-(1,7,8,9,10,10-Hexachloro-3,5-dioxo-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)butyric Acid Toluene Solvate

B. Bartkowska, F. M. Bohnen, C. Krüger and W. F. Maier

Formula: C13H9Cl6NO4.C7H8


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