# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # # #_reflns_d_resolution_high 0.8406 # #loop_ # _symmetry_equiv_pos_as_xyz # 'x, y, z' # '-x, y+1/2, -z' # #_cell_length_a 4.8789 #_cell_length_b 15.0112 #_cell_length_c 9.2835 #_cell_angle_alpha 90.000 #_cell_angle_beta 99.459 #_cell_angle_gamma 90.000 data_14s4co _shelx_title ' 14S4CO #520 in P2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 95.66 _exptl_crystal_F_000 300.00 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -17 0 123.29 130.38 4.28 o 0 -16 0 1104.87 1149.87 11.15 o 1 -16 0 288.84 274.18 5.68 o 2 -16 0 8.20 8.42 2.16 o 1 -15 0 49.93 51.14 2.72 o 2 -15 0 731.47 721.41 8.92 o 3 -15 0 147.23 142.24 4.53 o 0 -14 0 33.58 33.73 2.22 o 1 -14 0 54.08 46.79 2.54 o 2 -14 0 47.69 42.51 2.65 o 3 -14 0 108.50 106.71 3.83 o 1 -13 0 661.29 667.62 7.59 o 2 -13 0 56.21 56.15 2.77 o 3 -13 0 558.94 552.63 7.78 o 0 -12 0 134.56 127.01 3.28 o 1 -12 0 16.99 17.68 1.74 o 2 -12 0 4.57 4.36 1.55 o 3 -12 0 214.27 212.51 4.77 o 4 -12 0 137.36 134.36 4.32 o 1 -11 0 100.67 93.99 2.84 o 2 -11 0 421.08 396.63 5.66 o 3 -11 0 1.17 3.29 1.62 o 4 -11 0 271.21 271.61 5.69 o 0 -10 0 33.49 31.71 1.83 o 1 -10 0 1352.10 1335.54 9.10 o 2 -10 0 214.24 202.22 4.01 o 3 -10 0 248.55 235.74 4.71 o 4 -10 0 83.42 79.43 3.22 o 1 -9 0 222.67 218.94 3.60 o 2 -9 0 35.62 37.75 1.97 o 3 -9 0 102.38 101.23 3.16 o 4 -9 0 492.19 486.51 7.16 o 0 -8 0 5357.52 5419.35 17.53 o 1 -8 0 242.97 238.40 3.60 o 2 -8 0 19.11 20.88 1.61 o 3 -8 0 35.52 36.15 2.10 o 4 -8 0 314.81 312.72 5.62 o 5 -8 0 22.86 26.04 2.49 o 1 -7 0 112.11 113.42 2.46 o 2 -7 0 1338.55 1289.49 8.46 o 3 -7 0 1212.03 1178.92 9.15 o 4 -7 0 66.40 63.74 2.84 o 5 -7 0 95.96 104.10 3.80 o 0 -6 0 179.20 210.20 2.80 o 1 -6 0 5.26 1.10 1.15 o 2 -6 0 85.93 72.43 2.24 o 3 -6 0 661.46 620.36 6.52 o 4 -6 0 78.58 79.97 2.98 o 5 -6 0 109.81 105.89 3.79 o 1 -5 0 2563.74 2541.56 9.69 o 2 -5 0 1819.80 1841.78 9.23 o 3 -5 0 717.49 679.27 6.60 o 4 -5 0 311.80 294.83 5.13 o 5 -5 0 30.78 27.04 2.42 o 0 -4 0 2858.08 2963.22 9.58 o 1 -4 0 61.46 63.74 1.62 o 2 -4 0 74.79 69.71 2.06 o 3 -4 0 162.82 171.92 3.36 o 4 -4 0 91.57 90.36 3.05 o 5 -4 0 36.78 32.15 2.49 o 1 -3 0 3904.17 3754.00 12.38 o 2 -3 0 1249.19 1154.60 6.78 o 3 -3 0 829.88 839.72 6.96 o 4 -3 0 230.50 225.79 4.42 o 5 -3 0 92.68 87.10 3.39 o 0 -2 0 482.82 496.75 2.41 o 1 -2 0 9148.87 8291.24 30.48 o 2 -2 0 665.83 662.25 5.00 o 3 -2 0 1110.38 1063.70 7.74 o 4 -2 0 187.25 189.15 4.01 o 5 -2 0 180.69 178.72 4.57 o 1 -1 0 630.28 579.17 3.34 o 2 -1 0 1836.29 1814.55 8.15 o 3 -1 0 357.90 317.24 4.26 o 4 -1 0 209.81 194.77 4.06 o 5 -1 0 169.99 182.49 4.55 o 1 0 0 82.25 76.55 2.15 o 2 0 0 234.17 253.03 2.49 o 3 0 0 2.55 2.03 0.84 o 4 0 0 670.97 678.41 16.85 o 5 0 0 2.95 2.39 1.13 o 1 1 0 627.13 595.74 9.24 o 2 1 0 1831.26 1876.51 8.34 o 3 1 0 358.78 351.34 4.45 o 4 1 0 209.22 201.23 4.10 o 5 1 0 169.48 179.80 4.55 o 0 2 0 484.53 490.55 6.69 o 1 2 0 9150.33 8509.50 29.90 o 2 2 0 668.67 685.52 5.05 o 3 2 0 1110.58 1143.78 8.02 o 4 2 0 187.52 192.61 4.03 o 5 2 0 179.68 176.40 4.57 o 1 3 0 3891.01 3917.17 17.93 o 2 3 0 1248.50 1205.18 6.87 o 3 3 0 829.95 877.68 7.05 o 4 3 0 231.44 237.38 4.46 o 5 3 0 92.10 95.97 3.54 o 0 4 0 2861.25 2938.52 9.79 o 1 4 0 60.22 61.23 1.14 o 2 4 0 73.66 72.73 2.03 o 3 4 0 164.47 180.92 3.37 o 4 4 0 92.09 93.81 3.10 o 5 4 0 37.25 37.17 2.49 o 1 5 0 2565.55 2586.16 20.62 o 2 5 0 1808.91 1904.15 9.44 o 3 5 0 717.18 705.30 6.66 o 4 5 0 314.54 317.59 5.34 o 5 5 0 31.01 32.73 2.47 o 0 6 0 179.45 203.91 1.95 o 1 6 0 4.95 3.91 0.82 o 2 6 0 87.12 85.81 2.28 o 3 6 0 659.34 658.73 6.62 o 4 6 0 77.58 83.57 3.02 o 5 6 0 110.22 114.53 3.90 o 1 7 0 109.50 115.27 1.75 o 2 7 0 1341.46 1391.62 8.66 o 3 7 0 1213.19 1228.82 9.33 o 4 7 0 66.17 76.03 2.95 o 5 7 0 96.41 104.22 3.79 o 0 8 0 5342.37 5359.20 20.59 o 1 8 0 242.83 254.96 7.38 o 2 8 0 20.99 27.28 1.69 o 3 8 0 34.86 33.24 2.10 o 4 8 0 312.96 312.80 5.64 o 5 8 0 23.72 22.03 2.40 o 1 9 0 222.99 223.08 2.59 o 2 9 0 36.58 40.80 2.00 o 3 9 0 102.18 100.54 3.11 o 4 9 0 493.53 501.82 7.17 o 0 10 0 34.73 35.37 1.37 o 1 10 0 1350.13 1336.81 21.01 o 2 10 0 215.78 217.82 4.08 o 3 10 0 245.89 253.57 4.82 o 4 10 0 84.15 74.61 3.25 o 1 11 0 101.28 97.03 3.19 o 2 11 0 418.72 422.75 5.82 o 3 11 0 1.49 0.00 1.70 o 4 11 0 272.37 275.17 5.70 o 0 12 0 132.97 124.86 2.30 o 1 12 0 17.56 15.43 1.19 o 2 12 0 4.74 2.50 1.49 o 3 12 0 215.22 204.38 4.72 o 4 12 0 136.58 119.85 4.29 o 1 13 0 657.91 664.55 6.43 o 2 13 0 55.98 57.61 2.72 o 3 13 0 559.98 580.02 7.94 o 0 14 0 34.04 34.83 2.99 o 1 14 0 53.81 44.77 1.83 o 2 14 0 48.45 52.39 2.67 o 3 14 0 109.11 114.75 3.91 o 1 15 0 49.81 52.91 2.54 o 2 15 0 728.93 754.79 9.05 o 3 15 0 147.36 151.53 4.51 o 0 16 0 1103.04 1127.99 7.78 o 1 16 0 288.77 274.41 5.90 o 2 16 0 7.98 7.28 2.05 o 1 17 0 122.96 128.58 3.00 o -1 -17 1 154.78 154.76 4.68 o 0 -17 1 7.25 8.63 2.03 o 1 -17 1 267.63 267.89 5.89 o -2 -16 1 392.40 393.31 6.88 o -1 -16 1 12.07 13.10 2.07 o 0 -16 1 600.14 609.65 8.24 o 1 -16 1 222.81 231.98 5.22 o 2 -16 1 25.14 25.21 2.47 o -3 -15 1 13.40 7.43 2.05 o -2 -15 1 45.06 45.89 2.70 o -1 -15 1 287.72 297.05 5.65 o 0 -15 1 3.42 2.92 1.73 o 1 -15 1 29.83 31.43 2.40 o 2 -15 1 47.56 49.82 2.89 o -3 -14 1 11.58 11.32 2.10 o -2 -14 1 57.82 55.85 2.77 o -1 -14 1 827.04 828.43 8.75 o 0 -14 1 162.79 188.29 4.37 o 1 -14 1 452.18 459.35 6.63 o 2 -14 1 33.36 32.59 2.40 o 3 -14 1 526.56 502.51 7.82 o -3 -13 1 12.97 13.41 2.02 o -2 -13 1 6.67 8.98 1.70 o -1 -13 1 68.89 69.13 2.76 o 0 -13 1 320.22 325.09 5.35 o 1 -13 1 114.97 117.84 3.46 o 2 -13 1 19.51 20.45 1.99 o 3 -13 1 180.11 172.99 4.59 o -4 -12 1 182.15 188.14 4.92 o -3 -12 1 65.95 67.21 2.96 o -2 -12 1 230.25 217.59 4.51 o -1 -12 1 32.92 31.74 2.02 o 0 -12 1 1425.00 1375.71 10.25 o 1 -12 1 6.22 4.69 1.43 o 2 -12 1 3.48 4.86 1.55 o 3 -12 1 39.17 40.28 2.47 o 4 -12 1 749.47 710.87 9.42 o -4 -11 1 2.60 0.19 1.73 o -3 -11 1 203.24 208.57 4.61 o -2 -11 1 547.07 548.13 6.61 o -1 -11 1 5.88 5.94 1.37 o 0 -11 1 1.30 2.58 1.30 o 1 -11 1 786.91 741.52 7.28 o 2 -11 1 2053.28 1979.65 12.69 o 3 -11 1 190.17 187.72 4.37 o 4 -11 1 1.13 0.91 1.75 o -4 -10 1 313.05 318.11 5.94 o -3 -10 1 1.67 1.80 1.48 o -2 -10 1 692.34 705.07 7.10 o -1 -10 1 387.71 392.85 5.04 o 0 -10 1 219.42 236.37 3.88 o 1 -10 1 406.93 396.37 5.08 o 2 -10 1 195.30 184.96 3.89 o 3 -10 1 91.09 95.23 3.17 o 4 -10 1 34.09 31.08 2.43 o -5 -9 1 7.26 1.76 1.92 o -4 -9 1 31.10 33.71 2.41 o -3 -9 1 270.15 272.39 4.80 o -2 -9 1 746.04 763.50 7.11 o -1 -9 1 567.84 599.93 5.82 o 0 -9 1 324.78 327.67 4.24 o 1 -9 1 3200.23 3283.49 14.19 o 2 -9 1 1196.30 1159.00 8.94 o 3 -9 1 1305.11 1248.81 10.24 o 4 -9 1 54.69 51.04 2.76 o -5 -8 1 0.93 -2.06 1.69 o -4 -8 1 29.04 36.51 2.28 o -3 -8 1 1194.00 1174.55 9.45 o -2 -8 1 245.11 250.22 3.98 o -1 -8 1 19.45 20.10 1.51 o 0 -8 1 708.34 722.44 5.85 o 1 -8 1 283.61 290.12 3.94 o 2 -8 1 242.35 259.21 4.14 o 3 -8 1 549.49 526.70 6.46 o 4 -8 1 57.56 57.50 2.84 o 5 -8 1 30.30 35.13 2.70 o -5 -7 1 149.52 143.25 4.35 o -4 -7 1 129.21 128.09 3.75 o -3 -7 1 265.76 261.06 4.43 o -2 -7 1 598.34 617.84 5.82 o -1 -7 1 799.24 826.57 6.02 o 0 -7 1 683.38 755.20 5.61 o 1 -7 1 1289.35 1262.19 7.71 o 2 -7 1 3360.63 3281.54 14.03 o 3 -7 1 188.47 194.56 3.90 o 4 -7 1 60.72 63.66 2.82 o 5 -7 1 173.22 164.22 4.75 o -5 -6 1 176.11 183.68 4.80 o -4 -6 1 14.02 14.30 1.83 o -3 -6 1 24.37 24.25 1.78 o -2 -6 1 77.47 77.07 2.22 o -1 -6 1 1317.32 1310.04 7.17 o 0 -6 1 3208.42 3484.51 11.95 o 1 -6 1 2508.82 2602.97 10.62 o 2 -6 1 61.48 59.10 2.04 o 3 -6 1 593.01 590.03 6.43 o 4 -6 1 69.96 70.62 3.01 o 5 -6 1 549.07 544.72 8.10 o -5 -5 1 178.22 184.35 4.69 o -4 -5 1 175.44 166.91 3.93 o -3 -5 1 109.80 118.55 2.94 o -2 -5 1 175.77 170.98 2.96 o -1 -5 1 53.29 52.00 1.64 o 0 -5 1 159.15 186.32 2.49 o 1 -5 1 1637.64 1726.77 7.97 o 2 -5 1 203.08 220.11 3.41 o 3 -5 1 94.92 95.85 2.79 o 4 -5 1 86.29 79.54 2.95 o 5 -5 1 49.78 46.77 2.74 o -5 -4 1 1.57 -0.73 1.70 o -4 -4 1 222.43 221.18 4.38 o -3 -4 1 42.26 44.36 1.97 o -2 -4 1 140.29 120.96 2.46 o -1 -4 1 193.62 199.36 2.54 o 0 -4 1 2927.73 2981.71 9.92 o 1 -4 1 257.10 264.94 2.95 o 2 -4 1 51.83 56.00 1.88 o 3 -4 1 267.74 250.26 4.06 o 4 -4 1 2455.37 2295.57 14.03 o 5 -4 1 128.26 114.13 3.94 o -5 -3 1 466.38 468.39 7.11 o -4 -3 1 30.62 41.33 2.26 o -3 -3 1 146.23 132.66 2.94 o -2 -3 1 361.10 358.14 3.85 o -1 -3 1 48.35 52.04 1.46 o 0 -3 1 2912.72 2964.51 9.48 o 1 -3 1 449.01 450.97 3.57 o 2 -3 1 323.43 305.15 3.65 o 3 -3 1 113.63 109.40 2.78 o 4 -3 1 76.62 81.00 2.90 o 5 -3 1 39.43 37.00 2.48 o -5 -2 1 75.72 82.53 3.20 o -4 -2 1 249.93 268.59 4.68 o -3 -2 1 104.01 97.52 2.56 o -2 -2 1 1245.87 1346.51 7.05 o -1 -2 1 1771.73 1809.53 6.62 o 0 -2 1 62.33 66.20 1.22 o 1 -2 1 5030.87 4783.17 17.91 o 2 -2 1 61.03 55.23 1.88 o 3 -2 1 269.87 253.17 3.99 o 4 -2 1 202.49 190.58 4.14 o 5 -2 1 213.42 203.71 4.94 o -5 -1 1 18.74 16.06 2.05 o -4 -1 1 168.94 161.19 3.64 o -3 -1 1 173.94 152.98 3.04 o -2 -1 1 1368.65 1364.94 6.99 o -1 -1 1 3783.12 3808.17 12.14 o 0 -1 1 78.53 77.28 1.04 o 1 -1 1 979.46 990.06 4.75 o 2 -1 1 3045.44 2898.29 11.09 o 3 -1 1 700.17 635.61 6.09 o 4 -1 1 63.10 64.39 2.63 o 5 -1 1 162.77 164.33 4.44 o -5 0 1 33.25 32.17 2.21 o -4 0 1 47.00 49.02 1.34 o -3 0 1 3490.98 3586.25 60.52 o -2 0 1 134.52 139.20 1.65 o -1 0 1 4417.81 4060.56 35.86 o 1 0 1 57.95 76.10 1.60 o 2 0 1 0.13 3.12 3.52 o 3 0 1 154.51 149.63 6.07 o 4 0 1 0.25 -2.22 2.43 o 5 0 1 197.72 192.07 5.25 o -5 1 1 17.68 14.20 2.77 o -4 1 1 168.56 157.74 2.57 o -3 1 1 169.51 139.90 3.34 o -2 1 1 1369.12 1325.08 44.31 o -1 1 1 3788.59 3738.24 34.63 o 0 1 1 83.65 88.90 4.57 o 1 1 1 978.79 1022.75 4.81 o 2 1 1 3040.07 3057.14 11.37 o 3 1 1 706.11 687.15 6.31 o 4 1 1 62.31 67.33 2.65 o 5 1 1 164.72 186.16 4.59 o -5 2 1 76.94 76.78 5.38 o -4 2 1 251.19 256.88 7.20 o -3 2 1 104.10 96.74 5.33 o -2 2 1 1240.96 1302.47 33.29 o -1 2 1 1784.59 1812.59 17.84 o 0 2 1 62.15 63.33 0.83 o 1 2 1 5016.35 4968.77 18.24 o 2 2 1 61.15 65.50 1.90 o 3 2 1 269.61 265.17 4.02 o 4 2 1 202.54 197.34 4.17 o 5 2 1 214.27 216.41 5.02 o -5 3 1 465.12 456.87 13.00 o -4 3 1 30.82 41.01 1.58 o -3 3 1 145.17 129.31 2.06 o -2 3 1 355.05 353.22 8.19 o -1 3 1 49.05 47.79 1.49 o 0 3 1 2916.77 2924.81 12.40 o 1 3 1 452.43 463.41 3.57 o 2 3 1 330.71 320.40 3.76 o 3 3 1 111.91 106.04 2.76 o 4 3 1 76.72 80.46 2.94 o 5 3 1 40.23 41.30 2.72 o -5 4 1 1.59 -0.54 4.59 o -4 4 1 224.19 214.18 7.45 o -3 4 1 41.81 44.12 1.39 o -2 4 1 146.27 125.41 2.98 o -1 4 1 192.28 195.05 2.66 o 0 4 1 2920.98 2983.76 11.57 o 1 4 1 257.15 268.80 2.96 o 2 4 1 51.81 61.51 1.96 o 3 4 1 269.86 260.67 4.15 o 4 4 1 2453.70 2433.30 14.45 o 5 4 1 127.47 138.34 4.12 o -5 5 1 176.51 179.37 3.26 o -4 5 1 173.47 169.24 2.79 o -3 5 1 111.16 114.43 3.40 o -2 5 1 177.96 167.30 4.04 o -1 5 1 55.09 51.87 1.96 o 0 5 1 157.36 181.18 4.72 o 1 5 1 1640.96 1790.82 8.15 o 2 5 1 201.88 217.67 3.35 o 3 5 1 93.79 100.76 2.84 o 4 5 1 86.36 78.68 2.98 o 5 5 1 50.60 53.21 2.88 o -5 6 1 177.20 179.94 4.48 o -4 6 1 12.38 6.83 1.19 o -3 6 1 24.67 21.77 1.25 o -2 6 1 80.66 77.23 1.75 o -1 6 1 1320.67 1278.68 20.41 o 0 6 1 3208.21 3458.44 33.36 o 1 6 1 2502.21 2659.71 10.62 o 2 6 1 61.09 62.36 2.10 o 3 6 1 593.23 608.77 6.50 o 4 6 1 70.36 70.00 2.90 o 5 6 1 549.24 556.92 8.15 o -5 7 1 149.11 137.71 3.02 o -4 7 1 129.68 124.93 2.58 o -3 7 1 268.30 255.15 4.34 o -2 7 1 601.06 608.48 18.09 o -1 7 1 797.10 826.36 23.81 o 0 7 1 686.96 755.01 8.33 o 1 7 1 1289.27 1277.63 7.59 o 2 7 1 3355.00 3411.11 14.26 o 3 7 1 185.42 200.76 4.02 o 4 7 1 61.73 69.09 2.93 o 5 7 1 172.71 186.88 4.94 o -5 8 1 0.79 -4.18 4.19 o -4 8 1 28.43 32.70 1.57 o -3 8 1 1195.73 1139.55 39.69 o -2 8 1 245.11 243.02 2.76 o -1 8 1 20.34 20.24 2.10 o 0 8 1 708.00 721.96 4.14 o 1 8 1 285.28 295.69 3.94 o 2 8 1 244.44 274.68 4.20 o 3 8 1 549.37 551.25 6.59 o 4 8 1 57.35 55.43 2.76 o 5 8 1 30.26 26.72 2.49 o -5 9 1 7.07 4.23 1.47 o -4 9 1 32.06 32.65 2.12 o -3 9 1 273.37 261.64 12.03 o -2 9 1 748.18 728.33 10.25 o -1 9 1 567.25 584.81 6.34 o 0 9 1 326.66 314.17 11.23 o 1 9 1 3200.96 3343.69 14.06 o 2 9 1 1190.14 1196.57 8.96 o 3 9 1 1302.79 1302.10 10.37 o 4 9 1 53.87 61.15 2.94 o -4 10 1 312.46 309.48 7.10 o -3 10 1 2.18 1.63 1.29 o -2 10 1 696.38 697.86 14.07 o -1 10 1 388.11 393.81 6.10 o 0 10 1 218.19 234.31 2.72 o 1 10 1 405.46 394.43 5.07 o 2 10 1 194.30 199.65 3.95 o 3 10 1 90.47 97.43 3.27 o 4 10 1 33.69 28.20 2.42 o -4 11 1 2.59 4.36 1.99 o -3 11 1 205.80 197.04 5.26 o -2 11 1 548.39 527.50 14.00 o -1 11 1 6.11 6.37 0.98 o 0 11 1 1.40 2.58 5.08 o 1 11 1 788.35 761.44 7.31 o 2 11 1 2051.29 2069.40 12.89 o 3 11 1 186.52 173.95 4.29 o 4 11 1 1.02 5.04 1.68 o -4 12 1 183.76 186.33 5.44 o -3 12 1 66.79 65.25 5.44 o -2 12 1 231.72 223.58 8.87 o -1 12 1 33.91 34.47 1.51 o 0 12 1 1423.23 1390.56 7.18 o 1 12 1 5.87 5.27 1.49 o 2 12 1 3.36 3.94 1.56 o 3 12 1 39.17 37.50 2.41 o 4 12 1 746.63 760.28 9.68 o -3 13 1 13.09 15.11 3.09 o -2 13 1 6.49 4.44 1.26 o -1 13 1 69.64 66.74 1.93 o 0 13 1 321.16 322.13 10.98 o 1 13 1 113.88 112.89 3.40 o 2 13 1 18.82 19.42 2.02 o 3 13 1 180.32 175.18 4.63 o -3 14 1 11.49 13.96 5.95 o -2 14 1 58.57 55.04 4.45 o -1 14 1 830.10 825.86 18.49 o 0 14 1 162.57 190.01 3.07 o 1 14 1 450.37 464.67 6.65 o 2 14 1 32.84 31.76 2.42 o 3 14 1 524.34 510.72 7.82 o -3 15 1 13.02 10.65 1.44 o -2 15 1 45.02 49.50 1.93 o -1 15 1 287.62 293.32 6.58 o 0 15 1 4.07 7.63 1.22 o 1 15 1 29.98 26.49 2.22 o 2 15 1 46.87 42.18 2.78 o -2 16 1 393.53 377.91 4.79 o -1 16 1 12.66 12.09 1.38 o 0 16 1 599.69 596.68 5.71 o 1 16 1 222.04 223.81 5.12 o 2 16 1 25.48 23.63 2.41 o -1 17 1 153.74 146.50 3.21 o 0 17 1 7.29 10.48 2.19 o 1 17 1 269.31 267.81 4.16 o -1 -17 2 68.12 74.12 3.36 o 0 -17 2 153.89 159.44 4.67 o 1 -17 2 70.64 73.07 3.49 o -2 -16 2 1.79 -0.11 1.72 o -1 -16 2 95.50 95.51 3.64 o 0 -16 2 356.05 364.96 6.49 o 1 -16 2 12.82 14.78 1.97 o 2 -16 2 146.85 134.29 4.36 o -3 -15 2 53.83 60.44 3.19 o -2 -15 2 93.74 94.22 3.60 o -1 -15 2 27.70 25.60 2.31 o 0 -15 2 31.32 29.21 2.36 o 1 -15 2 50.94 51.37 2.84 o 2 -15 2 586.54 601.52 8.39 o -3 -14 2 131.28 126.83 4.07 o -2 -14 2 144.69 144.00 4.17 o -1 -14 2 6.94 10.89 1.73 o 0 -14 2 67.48 72.80 2.97 o 1 -14 2 13.95 15.24 1.91 o 2 -14 2 538.33 532.33 7.58 o 3 -14 2 168.85 151.97 4.65 o -3 -13 2 159.59 164.21 4.41 o -2 -13 2 173.61 169.57 4.21 o -1 -13 2 20.83 21.87 1.90 o 0 -13 2 3.91 6.64 1.62 o 1 -13 2 399.58 425.93 6.15 o 2 -13 2 185.86 185.31 4.42 o 3 -13 2 402.45 388.96 6.76 o -4 -12 2 5.08 5.41 1.87 o -3 -12 2 215.46 220.16 4.85 o -2 -12 2 96.14 94.68 3.16 o -1 -12 2 104.87 96.65 3.01 o 0 -12 2 82.71 78.94 2.73 o 1 -12 2 565.64 618.92 7.11 o 2 -12 2 88.93 92.34 3.21 o 3 -12 2 46.29 36.54 2.56 o -4 -11 2 183.58 190.50 4.91 o -3 -11 2 83.46 95.37 3.24 o -2 -11 2 108.09 98.65 3.08 o -1 -11 2 653.77 672.62 6.96 o 0 -11 2 295.83 281.01 4.53 o 1 -11 2 4.66 4.48 1.49 o 2 -11 2 453.30 449.55 6.22 o 3 -11 2 150.19 140.96 3.96 o 4 -11 2 11.37 15.16 2.08 o -4 -10 2 65.48 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