# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # #_reflns_d_resolution_high 0.8402 # #loop_ # _symmetry_equiv_pos_as_xyz # 'x, y, z' # '-x, y+1/2, -z+1/2' # '-x, -y, -z' # 'x, -y-1/2, z-1/2' # #_cell_length_a 14.6120 #_cell_length_b 10.7150 #_cell_length_c 20.6360 #_cell_angle_alpha 90.000 #_cell_angle_beta 92.878 #_cell_angle_gamma 90.000 # data_nitrs3 _shelx_title ' NITRS3 (#163) FOR NRC/MS in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 325.73 _exptl_crystal_F_000 1400.00 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12866.97 12875.62 60.70 o 3 0 0 157.45 111.84 19.99 o 4 0 0 13122.16 12696.49 85.47 o 5 0 0 81.50 36.89 22.43 o 6 0 0 16269.67 17560.30 123.21 o 7 0 0 449.89 212.19 29.23 o 8 0 0 1824.33 1499.26 48.16 o 9 0 0 208.60 244.30 30.40 o 10 0 0 5087.71 5256.73 92.06 o 11 0 0 22.86 -45.50 27.00 o 12 0 0 2195.35 2012.73 69.10 o 13 0 0 224.29 167.44 36.89 o 14 0 0 2638.12 2390.98 80.48 o 15 0 0 16.79 115.32 25.51 o 16 0 0 43.16 103.16 65.38 o 17 0 0 62.16 18.04 24.03 o 2 1 0 1419.18 1478.53 26.36 o 3 1 0 11332.63 10857.79 73.25 o 4 1 0 3.92 -8.50 20.84 o 5 1 0 4173.06 4391.06 61.13 o 6 1 0 1723.83 2354.94 51.03 o 7 1 0 254.05 233.13 29.13 o 8 1 0 1435.33 1181.19 43.59 o 9 1 0 75.37 121.19 27.85 o 10 1 0 21.45 50.50 27.53 o 11 1 0 519.35 478.92 40.08 o 12 1 0 147.30 164.25 36.36 o 13 1 0 0.31 -56.98 32.21 o 14 1 0 132.11 83.24 37.00 o 15 1 0 62.57 73.23 21.07 o 16 1 0 215.73 239.46 39.39 o 17 1 0 99.54 133.57 24.35 o 0 2 0 46289.17 46752.31 138.41 o 1 2 0 2973.55 3133.11 38.70 o 2 2 0 10344.85 11192.34 73.88 o 3 2 0 9311.38 8992.71 73.35 o 4 2 0 1812.84 1764.61 40.40 o 5 2 0 2451.27 2423.51 49.65 o 6 2 0 2236.10 1993.81 49.43 o 7 2 0 26.49 82.50 25.62 o 8 2 0 6310.56 5881.71 88.66 o 9 2 0 1136.89 1201.07 47.52 o 10 2 0 1271.31 1116.87 49.65 o 11 2 0 216.57 206.24 34.98 o 12 2 0 3618.31 3857.29 90.57 o 13 2 0 205.66 304.47 39.97 o 14 2 0 298.23 301.68 41.89 o 15 2 0 103.06 71.87 21.53 o 16 2 0 585.04 647.90 36.46 o 17 2 0 79.52 41.67 22.77 o 1 3 0 8034.67 7576.05 68.36 o 2 3 0 2949.02 2984.50 46.78 o 3 3 0 2155.49 2122.44 43.27 o 4 3 0 115.99 85.90 23.60 o 5 3 0 453.63 469.14 29.55 o 6 3 0 1.95 49.65 23.92 o 7 3 0 51.49 42.42 23.60 o 8 3 0 1179.79 1002.06 43.37 o 9 3 0 432.36 446.92 34.87 o 10 3 0 50.89 -21.47 29.34 o 11 3 0 127.45 89.41 32.00 o 12 3 0 270.59 350.07 42.42 o 13 3 0 7.00 -17.22 30.30 o 14 3 0 105.99 89.70 49.91 o 15 3 0 11.66 -39.84 19.92 o 16 3 0 25.84 -6.26 22.66 o 0 4 0 16.66 31.15 20.62 o 1 4 0 133.98 256.10 26.05 o 2 4 0 5755.55 5633.48 70.06 o 3 4 0 824.95 790.29 34.98 o 4 4 0 23147.94 22620.15 150.43 o 5 4 0 1521.10 1750.47 49.11 o 6 4 0 5086.76 5044.64 79.94 o 7 4 0 378.72 587.57 35.61 o 8 4 0 1585.80 1631.41 54.22 o 9 4 0 10.89 1.59 27.85 o 10 4 0 1018.09 883.42 47.63 o 11 4 0 897.71 1013.12 54.32 o 12 4 0 965.76 984.31 56.98 o 13 4 0 65.78 114.40 24.13 o 14 4 0 1001.69 1049.37 51.29 o 15 4 0 171.76 211.79 23.53 o 16 4 0 799.64 736.34 44.44 o 1 5 0 213.77 334.13 29.66 o 2 5 0 766.54 722.47 34.98 o 3 5 0 31.86 22.22 24.66 o 4 5 0 7535.44 7376.40 93.87 o 5 5 0 249.58 232.81 29.34 o 6 5 0 4004.81 3677.20 73.25 o 7 5 0 550.66 521.87 38.16 o 8 5 0 47.35 91.21 30.51 o 9 5 0 140.49 170.84 32.85 o 10 5 0 391.84 364.85 40.61 o 11 5 0 881.70 1010.14 54.96 o 12 5 0 798.13 832.39 55.49 o 13 5 0 0.21 -10.89 36.73 o 14 5 0 0.08 13.62 61.98 o 15 5 0 0.87 -14.76 21.87 o 0 6 0 3209.71 3428.65 67.82 o 1 6 0 393.51 431.61 32.53 o 2 6 0 12844.48 12303.36 124.91 o 3 6 0 352.95 319.35 31.57 o 4 6 0 1416.08 1473.96 49.86 o 5 6 0 6.37 -51.03 25.51 o 6 6 0 2471.21 2312.20 64.42 o 7 6 0 338.13 411.41 38.06 o 8 6 0 2005.46 1895.37 64.00 o 9 6 0 187.72 212.62 37.85 o 10 6 0 1593.83 1785.66 68.25 o 11 6 0 5.62 0.00 31.25 o 12 6 0 1479.94 1564.58 39.09 o 13 6 0 8.32 31.02 21.22 o 14 6 0 556.85 584.91 89.14 o 15 6 0 51.49 84.31 22.73 o 1 7 0 925.92 872.05 43.69 o 2 7 0 501.69 571.83 39.33 o 3 7 0 630.73 655.60 40.72 o 4 7 0 22.43 0.00 26.58 o 5 7 0 868.04 990.37 47.41 o 6 7 0 823.44 794.97 45.82 o 7 7 0 112.76 185.30 32.00 o 8 7 0 1233.72 1064.04 54.96 o 9 7 0 414.88 343.59 42.84 o 10 7 0 218.97 316.48 40.72 o 11 7 0 14.00 11.26 19.76 o 12 7 0 7.90 29.04 20.52 o 13 7 0 0.86 47.13 33.65 o 14 7 0 35.24 -17.04 62.67 o 0 8 0 79.74 70.59 28.49 o 1 8 0 1103.47 1198.84 50.50 o 2 8 0 2938.82 2691.30 72.50 o 3 8 0 20.72 46.14 29.23 o 4 8 0 1603.68 1824.04 62.40 o 5 8 0 105.47 38.91 33.17 o 6 8 0 819.79 818.04 49.33 o 7 8 0 568.61 545.57 46.78 o 8 8 0 1113.25 894.48 56.77 o 9 8 0 100.36 108.01 28.07 o 10 8 0 3531.22 3787.02 81.33 o 11 8 0 14.60 45.61 27.96 o 12 8 0 1287.78 1335.55 57.19 o 13 8 0 1.13 41.78 31.36 o 1 9 0 77.08 160.42 33.49 o 2 9 0 545.79 575.98 45.82 o 3 9 0 444.86 396.32 42.84 o 4 9 0 1755.10 1704.86 67.82 o 5 9 0 221.28 211.13 38.06 o 6 9 0 25.15 100.25 33.70 o 7 9 0 119.84 169.24 30.51 o 8 9 0 0.01 11.69 25.94 o 9 9 0 115.09 159.89 30.72 o 10 9 0 369.87 372.18 38.27 o 11 9 0 7.15 39.23 30.09 o 12 9 0 149.68 192.42 34.98 o 0 10 0 344.62 314.03 39.97 o 1 10 0 459.33 466.91 44.76 o 2 10 0 1155.60 1092.85 58.68 o 3 10 0 18.21 114.39 33.91 o 4 10 0 3223.58 3092.93 72.93 o 5 10 0 58.23 56.24 29.55 o 6 10 0 2403.52 2507.92 68.46 o 7 10 0 724.81 726.72 45.39 o 8 10 0 509.94 604.04 40.61 o 9 10 0 8.40 -55.81 28.92 o 10 10 0 525.91 503.16 43.37 o 1 11 0 13.80 91.00 26.90 o 2 11 0 82.96 91.53 27.85 o 3 11 0 1.26 15.31 29.98 o 4 11 0 422.40 403.33 38.38 o 5 11 0 60.69 54.11 28.81 o 6 11 0 351.08 366.13 39.12 o 7 11 0 32.92 39.23 29.13 o 8 11 0 5.49 27.96 30.19 o 0 12 0 1023.51 1066.48 50.82 o 1 12 0 96.86 37.42 30.09 o 2 12 0 424.10 485.83 39.97 o 3 12 0 86.17 127.68 32.32 o 4 12 0 579.53 710.56 45.61 o 5 12 0 505.75 454.57 43.27 o -17 1 1 75.60 35.77 72.13 o -16 1 1 132.07 109.27 37.53 o -15 1 1 58.63 131.29 20.15 o -14 1 1 382.51 334.45 44.65 o -13 1 1 399.54 300.00 40.72 o -12 1 1 2428.83 2632.30 77.18 o -11 1 1 3.82 -2.23 29.66 o -10 1 1 348.39 354.86 35.08 o -9 1 1 732.19 676.01 39.23 o -8 1 1 216.47 277.46 30.30 o -7 1 1 706.77 859.40 37.95 o -6 1 1 27397.12 24846.98 148.41 o -5 1 1 4003.97 4767.18 61.77 o -4 1 1 35095.67 35748.35 150.21 o -3 1 1 18918.85 19177.67 96.10 o -2 1 1 10388.00 10095.66 60.49 o -1 1 1 60.23 91.43 11.91 o 1 1 1 69.92 94.93 12.33 o 2 1 1 47202.75 49091.62 140.86 o 3 1 1 315.55 277.04 21.79 o 4 1 1 233.17 55.49 22.01 o 5 1 1 3766.41 4014.30 58.04 o 6 1 1 24.55 34.76 24.56 o 7 1 1 28.59 18.92 24.24 o 8 1 1 316.31 433.21 33.91 o 9 1 1 2402.89 2497.39 62.83 o 10 1 1 11145.71 11204.88 133.42 o 11 1 1 1.22 32.96 27.75 o 12 1 1 3623.86 3376.24 84.62 o 13 1 1 344.26 483.17 43.48 o 14 1 1 1365.43 1603.74 39.31 o 15 1 1 375.62 362.05 32.11 o 16 1 1 196.58 137.27 48.80 o 17 1 1 1.35 -48.94 63.36 o -17 2 1 40.62 12.89 21.59 o -16 2 1 159.99 138.07 23.38 o -15 2 1 17.54 24.84 20.86 o -14 2 1 93.62 62.24 21.88 o -13 2 1 224.89 191.89 38.70 o -12 2 1 441.11 415.24 41.78 o -11 2 1 2.52 -30.94 28.38 o -10 2 1 82.53 182.42 31.04 o -9 2 1 107.81 145.75 28.38 o -8 2 1 4121.07 3883.54 73.57 o -7 2 1 5002.83 5229.62 77.82 o -6 2 1 232.18 274.91 26.79 o -5 2 1 690.94 752.45 31.89 o -4 2 1 6760.48 6660.31 69.31 o -3 2 1 242.69 239.62 24.24 o -2 2 1 1251.99 1265.70 31.36 o -1 2 1 16586.64 16715.58 84.83 o 0 2 1 50.51 53.47 18.50 o 1 2 1 341.12 298.94 20.41 o 2 2 1 1162.85 1404.44 32.21 o 3 2 1 14133.60 13892.46 91.32 o 4 2 1 1110.64 1192.03 35.08 o 5 2 1 570.46 666.45 33.06 o 6 2 1 1513.87 1693.81 45.82 o 7 2 1 1110.82 1427.40 46.35 o 8 2 1 102.15 83.24 27.53 o 9 2 1 58.00 51.35 26.79 o 10 2 1 2016.64 1953.63 61.87 o 11 2 1 6.34 -6.38 30.83 o 12 2 1 166.20 99.19 36.78 o 13 2 1 274.53 225.59 38.38 o 14 2 1 33.16 15.12 35.67 o 15 2 1 5.66 37.45 20.63 o 16 2 1 10.40 -10.32 57.46 o 17 2 1 6.53 62.27 66.44 o -16 3 1 909.20 898.81 35.38 o -15 3 1 170.79 119.76 22.73 o -14 3 1 914.27 839.69 43.32 o -13 3 1 254.60 143.20 37.85 o -12 3 1 657.41 811.03 49.75 o -11 3 1 2721.10 2796.65 77.07 o -10 3 1 3188.29 3205.51 77.07 o -9 3 1 582.32 635.40 39.02 o -8 3 1 3116.63 3050.09 66.44 o -7 3 1 1615.11 1879.85 51.67 o -6 3 1 5460.16 5866.40 79.62 o -5 3 1 2588.04 2675.35 52.62 o -4 3 1 5658.29 5352.40 67.19 o -3 3 1 6528.43 7143.38 72.50 o -2 3 1 16575.32 16172.45 101.74 o -1 3 1 1797.16 1981.58 38.80 o 0 3 1 9442.29 9203.95 73.78 o 1 3 1 8.15 15.63 20.30 o 2 3 1 354.62 321.90 24.66 o 3 3 1 4409.46 3999.21 56.02 o 4 3 1 4847.87 5141.06 67.08 o 5 3 1 156.04 108.33 23.49 o 6 3 1 2122.03 1850.29 48.80 o 7 3 1 494.67 607.44 34.34 o 8 3 1 2149.61 2168.47 58.26 o 9 3 1 8.38 -52.30 26.15 o 10 3 1 4794.67 4598.15 89.72 o 11 3 1 1843.78 1461.63 58.89 o 12 3 1 887.84 564.18 49.86 o 13 3 1 212.15 151.06 40.82 o 14 3 1 1851.03 1886.27 42.81 o 15 3 1 447.87 410.17 48.32 o 16 3 1 835.36 835.05 34.66 o -16 4 1 31.37 43.37 43.16 o -15 4 1 152.89 172.35 23.27 o -14 4 1 134.35 191.76 21.64 o -13 4 1 206.20 141.63 21.99 o -12 4 1 1120.19 1144.19 59.00 o -11 4 1 156.47 188.17 34.66 o -10 4 1 1239.09 1423.25 57.19 o -9 4 1 202.55 189.33 31.25 o -8 4 1 5.16 -24.56 27.21 o -7 4 1 30.05 -53.37 26.68 o -6 4 1 3102.70 3523.80 67.08 o -5 4 1 6598.57 7078.74 87.70 o -4 4 1 2181.26 1946.93 47.63 o -3 4 1 1464.87 1436.44 41.03 o -2 4 1 377.78 237.17 25.62 o -1 4 1 1009.90 1080.94 35.29 o 0 4 1 637.41 748.62 32.21 o 1 4 1 756.53 831.65 34.34 o 2 4 1 502.68 284.16 27.75 o 3 4 1 6707.24 7395.22 84.20 o 4 4 1 347.46 415.03 30.72 o 5 4 1 641.21 537.81 32.96 o 6 4 1 1110.33 1043.73 41.46 o 7 4 1 2.56 -50.39 25.20 o 8 4 1 818.77 875.34 44.44 o 9 4 1 39.43 52.62 29.34 o 10 4 1 19.32 50.82 32.74 o 11 4 1 512.12 314.99 39.65 o 12 4 1 37.77 99.61 33.06 o 13 4 1 23.56 19.67 20.52 o 14 4 1 81.02 106.35 50.34 o 15 4 1 19.78 18.30 25.78 o 16 4 1 4.08 101.30 22.81 o -15 5 1 0.15 -64.49 38.70 o -14 5 1 1145.16 1101.88 37.09 o -13 5 1 20.28 20.74 20.17 o -12 5 1 1371.82 1284.95 63.25 o -11 5 1 0.11 2.98 30.30 o -10 5 1 36.49 62.62 31.04 o -9 5 1 143.02 54.64 30.83 o -8 5 1 1253.18 1172.26 52.41 o -7 5 1 487.33 531.54 38.70 o -6 5 1 3127.05 3289.71 69.74 o -5 5 1 322.85 329.24 31.68 o -4 5 1 5109.38 5047.30 79.09 o -3 5 1 587.07 569.39 34.87 o -2 5 1 25044.32 25040.57 163.71 o -1 5 1 2318.46 1928.32 48.69 o 0 5 1 9241.23 8713.34 94.19 o 1 5 1 627.78 934.98 37.21 o 2 5 1 1594.17 1818.93 48.90 o 3 5 1 103.10 115.13 27.11 o 4 5 1 5039.17 5092.05 80.69 o 5 5 1 2112.83 2122.44 56.45 o 6 5 1 8399.14 7848.20 105.67 o 7 5 1 503.77 515.38 37.95 o 8 5 1 4092.48 3802.32 83.13 o 9 5 1 0.28 13.18 28.07 o 10 5 1 330.47 136.39 38.38 o 11 5 1 6.09 -58.68 29.34 o 12 5 1 838.10 871.94 56.45 o 13 5 1 171.28 129.55 21.90 o 14 5 1 223.45 265.32 26.03 o 15 5 1 210.68 272.39 82.81 o -15 6 1 13.85 -2.88 21.36 o -14 6 1 68.30 46.59 42.84 o -13 6 1 67.02 52.41 21.49 o -12 6 1 75.82 177.24 28.49 o -11 6 1 2.97 -35.93 35.61 o -10 6 1 89.78 89.51 35.83 o -9 6 1 19.37 58.04 30.51 o -8 6 1 198.64 112.05 34.76 o -7 6 1 55.82 112.58 30.83 o -6 6 1 93.70 62.08 29.34 o -5 6 1 234.51 237.60 29.98 o -4 6 1 1860.01 1696.36 52.73 o -3 6 1 200.68 203.69 31.89 o -2 6 1 1196.38 1459.19 48.58 o -1 6 1 9.89 8.82 23.28 o 0 6 1 551.18 623.71 35.72 o 1 6 1 437.95 415.98 33.91 o 2 6 1 4028.15 3799.03 71.55 o 3 6 1 899.86 944.34 41.46 o 4 6 1 2127.81 2088.85 58.15 o 5 6 1 23.17 33.59 25.83 o 6 6 1 732.27 816.66 43.80 o 7 6 1 76.11 23.92 27.21 o 8 6 1 16.72 13.08 28.81 o 9 6 1 0.00 26.05 33.81 o 10 6 1 236.53 291.92 39.23 o 11 6 1 31.00 -13.61 32.96 o 12 6 1 41.10 18.74 22.01 o 13 6 1 12.87 -43.60 37.15 o 14 6 1 89.41 129.94 33.97 o 15 6 1 42.95 -45.33 22.66 o -14 7 1 1041.46 915.53 51.24 o -13 7 1 0.36 49.33 29.55 o -12 7 1 1974.56 1921.84 61.77 o -11 7 1 210.63 372.29 34.76 o -10 7 1 1397.79 1484.38 65.59 o -9 7 1 28.49 35.51 32.53 o -8 7 1 929.45 1217.12 56.98 o -7 7 1 132.31 150.00 32.21 o -6 7 1 628.70 582.04 43.37 o -5 7 1 236.91 122.04 31.36 o -4 7 1 2032.99 2147.21 63.25 o -3 7 1 16.56 93.13 27.11 o -2 7 1 7040.45 6681.15 101.31 o -1 7 1 135.37 159.14 29.23 o 0 7 1 4051.99 3945.20 77.82 o 1 7 1 121.69 177.11 28.28 o 2 7 1 2610.13 2941.65 69.95 o 3 7 1 167.74 200.28 33.06 o 4 7 1 2502.70 2266.92 64.95 o 5 7 1 19.48 -53.15 26.58 o 6 7 1 2840.81 3326.70 81.11 o 7 7 1 0.23 69.42 30.51 o 8 7 1 1645.26 1547.63 64.00 o 9 7 1 26.30 67.40 34.12 o 10 7 1 536.09 411.52 46.67 o 11 7 1 217.88 275.99 67.98 o 12 7 1 1959.25 2005.88 45.66 o 13 7 1 41.14 3.78 42.20 o 14 7 1 475.89 520.44 39.28 o -13 8 1 2.78 14.35 29.98 o -12 8 1 2.21 64.32 29.77 o -11 8 1 100.03 129.59 31.36 o -10 8 1 29.10 43.05 27.96 o -9 8 1 2.37 -52.73 27.00 o -8 8 1 276.80 303.94 41.99 o -7 8 1 45.75 -37.10 31.68 o -6 8 1 28.13 69.21 33.17 o -5 8 1 1057.76 1210.85 54.43 o -4 8 1 73.62 81.43 32.53 o -3 8 1 0.12 -16.16 28.49 o -2 8 1 0.00 -4.46 27.75 o -1 8 1 1000.09 989.73 48.16 o 0 8 1 7.37 -30.72 26.90 o 1 8 1 622.68 684.31 41.78 o 2 8 1 46.00 13.08 27.21 o 3 8 1 63.72 136.29 30.51 o 4 8 1 751.31 824.42 46.46 o 5 8 1 116.13 45.29 31.89 o 6 8 1 57.19 4.57 30.94 o 7 8 1 54.41 117.26 35.51 o 8 8 1 936.40 1150.04 56.56 o 9 8 1 204.01 147.87 30.30 o 10 8 1 109.69 127.36 28.92 o 11 8 1 6.81 -30.72 27.32 o 12 8 1 5.58 -17.97 28.28 o 13 8 1 122.81 237.28 33.59 o -12 9 1 452.37 464.04 43.27 o -11 9 1 4.54 49.11 29.98 o -10 9 1 2223.18 2166.67 66.55 o -9 9 1 725.88 715.45 43.59 o -8 9 1 1948.32 2124.57 63.78 o -7 9 1 75.18 -21.90 26.36 o -6 9 1 59.33 57.30 35.19 o -5 9 1 27.37 -67.93 34.76 o -4 9 1 1559.95 1460.46 63.57 o -3 9 1 625.36 574.38 47.09 o -2 9 1 1066.89 893.95 53.15 o -1 9 1 18.81 44.12 29.66 o 0 9 1 3677.14 3305.12 85.15 o 1 9 1 147.06 229.52 35.40 o 2 9 1 700.31 679.42 47.73 o 3 9 1 56.57 69.10 30.09 o 4 9 1 935.09 826.86 51.56 o 5 9 1 148.85 127.04 34.98 o 6 9 1 1737.81 1798.73 70.91 o 7 9 1 1.93 47.52 26.47 o 8 9 1 1515.91 1556.99 56.34 o 9 9 1 780.61 787.85 46.14 o 10 9 1 952.93 951.14 49.96 o 11 9 1 15.74 -15.10 29.34 o 12 9 1 306.97 307.44 40.82 o -10 10 1 4.48 -29.45 31.57 o -9 10 1 1.23 -1.70 28.81 o -8 10 1 159.07 178.60 33.06 o -7 10 1 22.89 -16.90 28.92 o -6 10 1 336.94 316.27 37.63 o 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33.06 o -3 12 1 28.70 -6.27 31.57 o -2 12 1 287.55 224.20 38.16 o -1 12 1 42.09 86.32 32.53 o 0 12 1 7.41 -46.24 27.85 o 1 12 1 6.62 -57.62 28.81 o 2 12 1 57.54 196.46 32.74 o 3 12 1 0.05 -55.92 27.96 o 4 12 1 241.51 363.79 36.78 o 5 12 1 0.37 8.40 30.94 o -17 0 2 11.79 23.77 20.09 o -16 0 2 4.63 25.06 41.35 o -15 0 2 476.77 403.27 63.15 o -14 0 2 1564.87 1685.41 70.16 o -13 0 2 56.42 139.69 36.46 o -12 0 2 484.14 550.46 44.44 o -11 0 2 959.08 893.84 46.78 o -10 0 2 9283.35 9251.26 119.92 o -9 0 2 4827.23 5007.43 85.90 o -8 0 2 1849.92 1954.48 52.84 o -7 0 2 247.40 123.00 27.53 o -6 0 2 70.74 24.45 23.71 o -5 0 2 7103.71 7037.18 73.03 o -4 0 2 14858.63 13658.58 90.68 o -3 0 2 3953.25 4159.94 46.24 o -2 0 2 43910.71 45112.08 129.48 o 2 0 2 7903.26 7298.27 52.41 o 3 0 2 85455.31 86098.56 227.18 o 4 0 2 20527.52 20406.17 112.79 o 5 0 2 21049.71 20158.58 123.64 o 6 0 2 2936.09 2410.11 50.92 o 7 0 2 554.66 320.52 28.92 o 8 0 2 850.93 1087.21 44.22 o 9 0 2 2074.22 2184.74 59.75 o 10 0 2 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