Acta Crystallographica Section C

Crystal Structure Communications

Volume 54, Part 4 (April 1998)

Cover illustration Cover illustration: An Exact Quasi-Ferrodistortive Ordering in (N,N'-Di-n-butylthiourea-S)(N-salicylideneglycinato-O,N,O')copper(II), see Warda, pages 460-462. Displacement ellipsoids are shown at the 40% probability level for non-H atoms.

cif-access (inorganic compounds)

Acta Cryst. (1998). C54, IUC9800010    [ doi:10.1107/S0108270198099776 ]

Luminescent CuI Clusters. Bis({tris[2-(2-methoxyethoxy)ethyl]amine}potassium) Hexaiodotetracuprate(I)

J. T. Mague

Synopsis: The [Cu4I6]2- ion in this compound has twofold rotation symmetry while the seven-coordinate K+ ion has a geometry midway between capped octahedral and end-capped trigonal prismatic.

Formula: [K(C15H33NO6)]2[Cu4I6]

cif-access (organic compounds)

Acta Cryst. (1998). C54, IUC9800008    [ doi:10.1107/S0108270198099764 ]

A Neutral Triphenylphosphine-Substituted closo-Decaborane: 1,6-(PPh3)2B10H8

H.-J. Yao, C.-H. Hu, J.-M. Dou, J. Sun, J.-D. Wei, Z.-E. Huang, R.-S. Jin and P.-J. Zheng

Synopsis: 1,6-Bis(triphenylphosphino)-closo-decaborane is substituted at an apical and an equatorial position of the closo-decaborane framework by triphenylphosphine groups with B-P bond lengths of 1.879 (6) and 1.925 (6) Å.

Formula: C36H38B10P2

Acta Cryst. (1998). C54, IUC9800009    [ doi:10.1107/S0108270198099752 ]

The (1S,9aR) and (1S,9aS) Relative Configurations of 3-Fluoro-1,9a-dihydro-1-phenyl-1,2-bis(trifluoromethyl)-4H-quinolizin-4-one

D. C. Swenson, M. Yamamoto and D. J. Burton

Synopsis: Cycloaddition of (Z)-1,1,2,5,5,5-hexafluoro-4-phenyl-3-trifluoromethyl-1,3-pentadiene with pyridine gave the (1S,9aR) racemate as the major product and the (1S,9aS) racemate as the minor product, as determined by the crystal structures of the title compounds.

Formula: Two diastereomers of C17H10F7NO

inorganic compounds

Acta Cryst. (1998). C54, 445-447    [ doi:10.1107/S0108270197015989 ]

Re-Refinement of [alpha]-(AlMnSi)

K. Sugiyama, N. Kaji and K. Hiraga

Synopsis: The structure of [alpha]-(AlMnSi) is reproduced by the connection of two large atom clusters with icosahedral symmetry (a Mackay icosahedron and a double-Mackay icosahedron). Si and Mn atoms are proposed to constitute icosahedral arrangements in the atom clusters.

Formula: Al4Mn1.01Si0.74

metal-organic compounds

Acta Cryst. (1998). C54, 448-449    [ doi:10.1107/S0108270197015965 ]

Bis(2-chloro-1H-imidazol-3-ium) Hexachloroplatinate(IV), (C3H4ClN2)2[PtCl6]

G. Valle and R. Ettorre

Formula: (C3H4ClN2)2[PtCl6]

Acta Cryst. (1998). C54, 449-451    [ doi:10.1107/S0108270197016958 ]

Bis(acetylacetonato-O,O')([bold eta]4-trans-2,4-hexadiene)ruthenium(II) 1/6-Ethanol Solvate

E. Meléndez, R. Ilarraza, G. P. A. Yap and A. L. Rheingold

Formula: [Ru(C5H7O2)2(C6H10)].1/6C2H6O

Acta Cryst. (1998). C54, 451-453    [ doi:10.1107/S0108270197016405 ]

catena-Poly[[(di-2-pyridyl-N-amine)(propionato-O,O')copper(II)]-[bold mu]-nitrato-O:O']

S. Youngme, C. Pakawatchai and H.-K. Fun

Formula: [Cu(NO3)(C3H5O2)(C10H9N3)]

Acta Cryst. (1998). C54, 453-456    [ doi:10.1107/S0108270197016764 ]

Tris(N,N'-diethylthiourea-S)iodocopper(I) and Tris(N,N'-diethylthiourea-S)iodosilver(I)

H.-K. Fun, I. A. Razak, C. Pakawatchai, C. Khaokong, S. Chantrapromma and S. Saithong

Formula: [CuI(C5H12N2S)3] and [AgI(C5H12N2S)3]

Acta Cryst. (1998). C54, 456-458    [ doi:10.1107/S0108270197012912 ]

Magnesium Sulfate Tetraurea Monohydrate

T. Todorov, R. Petrova, K. Kossev, J. Macícek and O. Angelova

Formula: [Mg(SO4)(CH4N2O)4(H2O)]

Acta Cryst. (1998). C54, 458-460    [ doi:10.1107/S0108270197016594 ]

[1,2-Bis(2-methoxyethyl-O)-[bold eta]5-cyclopentadienyl]trichlorozirconium(IV)

A. A. H. van der Zeijden, C. Mattheis and R. Fröhlich

Formula: [ZrCl3(C11H17O2)]

Acta Cryst. (1998). C54, 460-462    [ doi:10.1107/S0108270197016582 ]

An Exact Quasi-Ferrodistortive Ordering in (N,N'-Di-n-butylthiourea-S)(N-salicylideneglycinato-O,N,O')copper(II)

S. A. Warda

Formula: [Cu(C9H7NO3)(C9H20N2S)]

Acta Cryst. (1998). C54, 462-464    [ doi:10.1107/S010827019701442X ]


H. Zhang, Y. Lu and E. Biehl

Formula: [Fe(C5H5)(C23H22NO4)]

Acta Cryst. (1998). C54, 464-468    [ doi:10.1107/S0108270197016284 ]

Bis(1,10-phenanthroline-N,N')copper(II) Tetrathionate and Tris(1,10-phenanthroline-N,N')copper(II) Tetrathionate Pentahydrate

E. Freire, S. Baggio, R. Baggio and M. T. Garland

Formula: [Cu(C12H8N2)2(S4O6)] and [Cu(C12H8N2)3](S4O6).5H2O

Acta Cryst. (1998). C54, 468-470    [ doi:10.1107/S0108270197013218 ]

Bis[[bold mu]-N,N'-bis(salicylidene)-1,3-propanediaminato]bis(dimethylformamide)di([bold mu]-nitrito)copper(II)dinickel(II)-Dimethylformamide (1/2)

M. N. Tahir, D. Ülkü, O. Atakol and O. Çakirer

Formula: [CuNi2(NO2)2(C17H16N2O2)2(C3H7NO)2].2C3H7NO

Acta Cryst. (1998). C54, 470-473    [ doi:10.1107/S0108270197016971 ]

Bis(tetra-n-butylammonium) Bis[(4-cyanophenyl)dithiocarbimato(2-)-S,S']nickel(II)

S. B. Schougaard, T. Pittelkow, F. Krebs, S. Larsen, H. O. Sørensen, D. R. Greve and T. Bjørnholm

Formula: (C16H36N)2[Ni(C8H4N2S2)2]

Acta Cryst. (1998). C54, 473-475    [ doi:10.1107/S0108270197015898 ]

A cis-Dioxomolybdenum(VI) Complex, [Mo{N2C3H3C(Me)2O}2(O)2]

M. K. Ehlert, S. J. Rettig, A. Storr and J. Trotter

Formula: [Mo(O)2(C6H9N2O)2]

Acta Cryst. (1998). C54, 475-476    [ doi:10.1107/S0108270197005842 ]

Tetrakis[1-(1-phenylcyclohexyl)piperidinium] Tetrachloromanganate(II) Dichloride

N.-L. Chang, V. M. Lynch and S. H. Simonsen

Formula: (C17H26N)4[MnCl4]Cl2

Acta Cryst. (1998). C54, 476-479    [ doi:10.1107/S0108270197015485 ]

Diiodotetrakis[tris(dimethylamino)phosphine oxide-O]bismuth(III) Pentaiodide, [BiI2{OP(NMe2)3}4][I5]

L. J. Farrugia, N. C. Norman and N. L. Pickett

Formula: [BiI2(C6H18N3OP)4](I5)

Acta Cryst. (1998). C54, 479-481    [ doi:10.1107/S0108270197016375 ]


Z.-N. Chen, A. Siu, C.-Y. Su, I. Williams and B.-S. Kang

Formula: [Co(N3)3(C10H8N2)(C5H5N)]

Acta Cryst. (1998). C54, 481-483    [ doi:10.1107/S0108270197017174 ]

Dipyridiniomethane cis-Dibromotetrafluoroosmate(IV), cis-[(C5H5 N)2CH2][OsBr2F4]

M. Höhling and W. Preetz

Formula: (C11H12N2)[OsBr2F4]

Acta Cryst. (1998). C54, 483-485    [ doi:10.1107/S0108270197016867 ]

(Phthalocyaninato)antimony Iodide

R. Kubiak and M. Razik

Formula: [Sb(C32H16N8)]I

Acta Cryst. (1998). C54, 485-487    [ doi:10.1107/S0108270198000511 ]

Dichloro[6,7-dimethyl-2,3-bis(2-pyridyl-N)quinoxaline]palladium(II) Monohydrate

F. Nicoló, M. Cusumano, M. L. Di Pietro, R. Scopelliti and G. Bruno

Formula: [PdCl2(C20H16N4)].H2O

organic compounds

Acta Cryst. (1998). C54, 488-489    [ doi:10.1107/S010827019701545X ]


Ç. Tarimci, F. Ercan, M. Koçoglu and I. Ören

Formula: C14H12ClNO2S

Acta Cryst. (1998). C54, 489-491    [ doi:10.1107/S0108270197012407 ]


J. G. Garcia, B. Asfaw, A. Rodriguez and F. R. Fronczek

Formula: C11H13NO2Si

Acta Cryst. (1998). C54, 491-496    [ doi:10.1107/S0108270197015862 ]

Structure and Photochemistry of Four Adamantylacetophenones

T. Y. Fu, J. R. Scheffer, J. Trotter and J. Yang

Formula: C18H21FO, C19H21NO, C20H23NO and C20H24O3

Acta Cryst. (1998). C54, 496-497    [ doi:10.1107/S0108270197015904 ]


T. Y. Fu, J. R. Scheffer and J. Trotter

Formula: C18H17NS

Acta Cryst. (1998). C54, 497-499    [ doi:10.1107/S0108270197015461 ]

Mephentermine Hemisulfate Monohydrate: an Adrenergic Agent

R. Sengupta, R. Banerjee and J. K. Dattagupta

Formula: C11H18N+.0.5SO42-.H2O

Acta Cryst. (1998). C54, 499-501    [ doi:10.1107/S0108270197014674 ]

D-Phenylglycine Hydrochloride

S. Ravichandran, J. K. Dattagupta and C. Chakrabarti

Formula: C8H10NO2+.Cl-

Acta Cryst. (1998). C54, 501-504    [ doi:10.1107/S010827019701651X ]

A Low-Temperature Phase of 2-Pyrrolidone

R. Goddard, O. Heinemann, C. Krüger, I. Magdó, F. Mark and K. Schaffner

Formula: C4H7NO

Acta Cryst. (1998). C54, 504-507    [ doi:10.1107/S0108270197016314 ]

Polysulfonylamines. C. Bis(4-nitrobenzenesulfonyl)amine Monohydrate

O. Moers, P. G. Jones and A. Blaschette

Formula: C12H9N3O8S2.H2O

Acta Cryst. (1998). C54, 507-509    [ doi:10.1107/S0108270197016570 ]

(R)- and (S)-2-(4-Bromophenyl)-2-oxoethyl 2-Methoxymethylpyrrolidine-1-dithiocarboxylate

M. Biedermann, H. Hartung, W. Dölling and P. Verjus

Formula: C15H18BrNO2S2

Acta Cryst. (1998). C54, 509-513    [ doi:10.1107/S010827019701439X ]

Nonstereospecific 1,3-Dipolar Cycloaddition Reactions of Azomethine Ylides: Proof of the Structures for Four Diastereoisomeric [3+2] Cycloadducts

J. Breu, K.-J. Range, A. Weber and J. Sauer

Formula: C29H33N5, C29H33N5, C29H32N4O and C34H39N5

Acta Cryst. (1998). C54, 513-515    [ doi:10.1107/S0108270197013474 ]

Pyridine N-Oxide and 4-Nitrophenol (1:1 Complex)

R. Moreno-Fuquen, R. H. De Almeida Santos and R. H. P. Francisco

Formula: C5H5NO.C6H5NO3

Acta Cryst. (1998). C54, 515-517    [ doi:10.1107/S0108270197016260 ]

2:1 Complex of 3-Picoline N-Oxide and Hydroquinone

R. Moreno-Fuquen, M. T. doP. Gambardella and J. Valderrama-N

Formula: 2C6H7NO.C6H6O2

Acta Cryst. (1998). C54, 517-519    [ doi:10.1107/S0108270197016272 ]

1:1 Complex of 2-Aminobenzoic Acid and 3-Methyl-4-nitropyridine N-Oxide

R. Moreno-Fuquen, R. H. De Almeida Santos and E. V. R. De Castro

Formula: C7H7NO2.C6H6N2O3

Acta Cryst. (1998). C54, 519-521    [ doi:10.1107/S0108270197016491 ]

Some 1,3-Dipolar Adducts from Benzodiazepine. I. Condensation of Nitrilimines with 2-Methyl-4-phenyl-1,5-benzodiazepines

M. Essaber, A. Baouid, A. Hasnaoui, M. Giorgi and M. Pierrot

Formula: C26H23N5O4 and C27H25ClN4O2

Acta Cryst. (1998). C54, 521-523    [ doi:10.1107/S010827019701737X ]


A. Kuhl, D. Schollmeyer, M. Schürmann, H. Preut and W. Kreiser

Formula: C25H27ClO3

Acta Cryst. (1998). C54, 523-525    [ doi:10.1107/S0108270197016983 ]


T. Hökelek, Z. Kiliç and H. Dal

Formula: C6H14Cl4N2OP2

Acta Cryst. (1998). C54, 525-527    [ doi:10.1107/S0108270197015631 ]

p-Toluidinium 2'-Hydroxy-3'-methoxy-5'-flavonesulfonate Hydrate

G. Pèpe, J.-C. Wallet, A. Habsaoui and E. M. Gaydou

Formula: C7H10N+.C16H11O7S-.H2O

Acta Cryst. (1998). C54, 527-529    [ doi:10.1107/S0108270197015928 ]

Thiophene-2-carbaldehyde N-(2,4-Dinitrophenyl)-N-methylhydrazone

M. Aygün, S. Isik, N. Öcal, M. N. Tahir, S. Kaban and O. Büyükgüngör

Formula: C12H10N4O4S

Acta Cryst. (1998). C54, 529-531    [ doi:10.1107/S0108270197013991 ]


Y. Elerman and A. Elmali

Formula: C16H14N2OS

Acta Cryst. (1998). C54, 531-533    [ doi:10.1107/S0108270197015874 ]

[alpha]-(2H-1-Benzopyran-2-ylidene)-[alpha]-(methylthio)acetonitrile, a Chromylidene Acetonitrile

F. Pochat and P. L'Haridon

Formula: C12H9NOS

Acta Cryst. (1998). C54, 533-534    [ doi:10.1107/S0108270197015138 ]


M. Barrot, G. Fabrias, F. Camps, E. Molins, A. Roig and W. Maniukiewicz

Formula: C9H16S4

Acta Cryst. (1998). C54, 535-539    [ doi:10.1107/S0108270197015771 ]

Phenolphthalein and 3',3''-Dinitrophenolphthalein

L. J. Fitzgerald and R. E. Gerkin

Formula: C20H14O4 and C20H12N2O8

Acta Cryst. (1998). C54, 539-540    [ doi:10.1107/S0108270197013930 ]

8-Hydroxyquinolinium-Salicylate-Salicylic Acid (1/1/1) Complex, C9H8NO+.C7H5O3-.C7H6O3

J. R. Jebamony and P. Thomas Muthiah

Formula: C9H8NO+.C7H5O3-.C7H6O3

Acta Cryst. (1998). C54, 541-542    [ doi:10.1107/S0108270197015953 ]


S. Shanmuga Sundara Raj, M. N. Ponnuswamy, G. Shanmugam and S. Nanjundan

Formula: C19H13NO3

Acta Cryst. (1998). C54, 542-544    [ doi:10.1107/S0108270197016508 ]

4-Methyl-7,10-dihydrobenzo[h]coumarin and 4-Methyl-7,8,9,10-tetrahydro-8,9-epoxybenzo[h]coumarin

K. Chinnakali, H.-K. Fun, K. Sriraghavan and V. T. Ramakrishnan

Formula: C14H12O2 and C14H12O3

Acta Cryst. (1998). C54, 544-547    [ doi:10.1107/S0108270197016557 ]

Two Dyotropomers Resulting from Irreversible Thermal (4[bold sigma]+2[bold pi]) 2H Group Transfer

C. Wilson and J. A. K. Howard

Formula: C16H8Cl10 and C20H16Cl4

Acta Cryst. (1998). C54, 547-550    [ doi:10.1107/S0108270197016521 ]

Two New Structures of 5-Nitrouracil

A. R. Kennedy, M. O. Okoth, D. B. Sheen, J. N. Sherwood and R. M. Vrcelj

Formula: C4H3N3O4 and C4H3N3O4.C2H6OS

Acta Cryst. (1998). C54, 550-553    [ doi:10.1107/S0108270197016533 ]

3-Methylthio-1,2,4-triazine: a Comparison of Experimental and Theoretical Structures

M. H. Palmer, S. Parsons, S. Smith, A. J. Blake and M. F. Guest

Formula: C4H5N3S

Acta Cryst. (1998). C54, 553-555    [ doi:10.1107/S0108270197016302 ]


S. Wang, F. Brisse, F. Bélanger-Gariépy, A. Donat-Bouillud and M. Leclerc

Formula: C36H50S4

Acta Cryst. (1998). C54, 555-557    [ doi:10.1107/S0108270197014406 ]


M. S. Løiten, B. Dalhus, B. Fjærtoft and J. Klaveness

Formula: C4H6I2O2

Acta Cryst. (1998). C54, 557-559    [ doi:10.1107/S0108270197016727 ]


V. K. Ganesh, D. Velmurugan, M. Bidya Sagar and P. Murugan

Formula: C25H32N2O2

Acta Cryst. (1998). C54, 559-561    [ doi:10.1107/S0108270197016776 ]

L-Histidinol Phosphate Tetrahydrate: Redetermination at 110 and 240K

T. Lis, J. Mazurek and N. Okabe

Formula: C6H12N3O4P.4H2O

addenda and errata

Acta Cryst. (1998). C54, 562    [ doi:10.1107/S0108270198003357 ]

N-Phenyl-N-(phenylthioxomethyl)benzamide. Erratum

T. Y. Fu, J. R. Scheffer and J. Trotter


Acta Cryst. (1998). C54, 562    [ doi:10.1107/S0108270198003369 ]

Complex Network of Hydrogen Bonds in 3-Aminopyrazole-4-carboxylic Acid. Erratum

A. J. Dobson and R. E. Gerkin


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