# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_snpic _shelx_title ' [(Bu2SnO2C-2-C5H4NO)2O]2 hydrate in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 428.21 _exptl_crystal_F_000 1548.00 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3414.69 3441.85 93.81 o 4 0 0 4999.30 4156.03 136.50 o 5 0 0 2441.75 2490.13 152.34 o 6 0 0 11552.87 12443.05 266.99 o 7 0 0 190.49 284.23 129.69 o 8 0 0 6064.25 5447.90 237.13 o 9 0 0 36.05 75.37 151.34 o 10 0 0 43.13 131.49 152.14 o 11 0 0 215.80 534.39 174.79 o 12 0 0 0.29 104.63 162.56 o 13 0 0 48.91 181.60 155.55 o 14 0 0 164.24 294.65 155.95 o -13 1 0 224.20 154.94 170.38 o -12 1 0 56.82 44.70 161.16 o -11 1 0 0.62 25.26 166.17 o -10 1 0 763.19 784.34 178.60 o -9 1 0 2093.87 2313.34 197.64 o -8 1 0 3838.15 4201.94 207.46 o -7 1 0 1741.61 1904.83 148.53 o -6 1 0 1773.13 2487.33 185.81 o -5 1 0 6167.11 6197.57 221.29 o -4 1 0 36297.91 35345.73 342.56 o -3 1 0 85444.88 79451.33 2370.67 o -2 1 0 3399.61 3969.82 112.65 o -1 1 0 16150.78 18064.94 150.33 o 1 1 0 107757.72 113439.25 1684.34 o 2 1 0 246.73 346.97 69.96 o 3 1 0 2387.37 2138.75 118.66 o 4 1 0 2298.76 3065.01 122.67 o 5 1 0 17989.38 18641.42 275.81 o 6 1 0 1964.92 1767.73 169.18 o 7 1 0 2402.83 2730.07 168.37 o 8 1 0 12.37 143.32 133.50 o 9 1 0 844.79 853.50 156.35 o 10 1 0 346.29 465.23 169.58 o 11 1 0 1301.46 1466.86 202.45 o 12 1 0 38.39 1.60 148.73 o 13 1 0 57.34 126.68 132.29 o 14 1 0 1150.09 983.99 172.18 o -13 2 0 165.79 96.21 159.55 o -12 2 0 187.28 174.59 169.98 o -11 2 0 836.17 1143.14 206.06 o -10 2 0 99.96 159.55 171.98 o -9 2 0 3086.10 3474.12 244.54 o -8 2 0 11289.94 11454.45 325.12 o -7 2 0 6035.62 5350.89 214.08 o -6 2 0 4595.74 4804.07 190.02 o -5 2 0 5483.92 5921.96 214.68 o -4 2 0 7843.82 8177.97 191.83 o -3 2 0 43461.23 41153.44 344.97 o -2 2 0 38.24 173.18 117.86 o -1 2 0 2586.54 2443.43 98.62 o 0 2 0 13802.25 14963.11 223.70 o 1 2 0 16513.68 17522.33 170.38 o 2 2 0 27.27 36.08 77.77 o 3 2 0 851.81 953.32 139.51 o 4 2 0 87.11 37.08 86.59 o 5 2 0 102.88 115.46 116.06 o 6 2 0 5452.61 5821.94 210.27 o 7 2 0 2631.10 2580.13 166.37 o 8 2 0 1.48 -32.07 127.28 o 9 2 0 24.83 81.58 143.52 o 10 2 0 3518.35 3309.95 220.89 o 11 2 0 2662.51 2253.21 220.29 o 12 2 0 2875.38 2952.76 240.33 o 13 2 0 66.03 -48.11 149.13 o 14 2 0 363.82 511.94 176.79 o -13 3 0 990.29 1004.43 193.83 o -12 3 0 1533.57 1598.35 213.67 o -11 3 0 1473.70 1456.24 208.66 o -10 3 0 1563.95 1449.62 218.69 o -9 3 0 98.99 29.47 171.18 o -8 3 0 10046.41 8706.14 307.88 o -7 3 0 13355.87 12935.34 327.13 o -6 3 0 703.50 702.36 140.71 o -5 3 0 5766.36 5973.67 227.31 o -4 3 0 17223.81 18314.09 319.51 o -3 3 0 9151.49 9456.21 205.06 o -2 3 0 8680.21 7926.61 171.78 o -1 3 0 2518.15 2451.65 156.95 o 0 3 0 628.25 440.60 73.98 o 1 3 0 26168.90 26425.71 256.17 o 2 3 0 297.37 244.14 138.31 o 3 3 0 2610.29 3074.03 125.28 o 4 3 0 2.16 10.02 101.83 o 5 3 0 69.25 148.73 150.73 o 6 3 0 3228.30 3513.81 193.03 o 7 3 0 1253.37 1302.29 152.54 o 8 3 0 4054.78 3720.47 199.24 o 9 3 0 396.01 511.54 152.74 o 10 3 0 69.96 125.68 147.33 o 11 3 0 6315.62 5582.40 295.26 o 12 3 0 4188.60 3696.01 266.39 o 13 3 0 309.30 369.22 153.14 o 14 3 0 122.91 -13.23 149.73 o -12 4 0 574.20 409.71 200.24 o -11 4 0 6528.69 6070.29 320.91 o -10 4 0 2080.09 2434.61 226.50 o -9 4 0 521.93 293.65 160.76 o -8 4 0 1183.10 1132.12 193.03 o -7 4 0 7805.91 8521.33 288.84 o -6 4 0 14595.87 13645.92 327.13 o -5 4 0 1210.10 1668.51 153.14 o -4 4 0 7328.72 7329.69 233.72 o -3 4 0 22146.05 22653.13 341.76 o -2 4 0 225.09 211.07 108.04 o -1 4 0 2987.07 3218.35 132.69 o 0 4 0 41376.38 42001.58 253.56 o 1 4 0 28961.56 30773.78 309.09 o 2 4 0 2630.17 2496.75 117.46 o 3 4 0 3633.59 3767.97 154.14 o 4 4 0 26.52 -47.91 109.64 o 5 4 0 6509.43 6901.73 217.08 o 6 4 0 8650.20 8263.76 239.93 o 7 4 0 5356.42 5871.45 227.10 o 8 4 0 3883.47 3992.07 220.09 o 9 4 0 1067.19 1047.93 177.59 o 10 4 0 2.56 -66.95 147.33 o 11 4 0 2210.18 2271.45 223.90 o 12 4 0 7728.74 7221.85 336.35 o 13 4 0 1840.18 1801.20 207.86 o 14 4 0 14.60 48.91 155.14 o -12 5 0 1165.91 1077.19 230.91 o -11 5 0 2038.92 1795.19 244.14 o -10 5 0 6383.76 6157.08 327.73 o -9 5 0 1448.16 1818.84 223.10 o -8 5 0 0.78 38.49 159.35 o -7 5 0 634.09 558.84 170.98 o -6 5 0 8320.54 8774.50 279.22 o -5 5 0 593.39 545.41 150.13 o -4 5 0 441.21 470.65 128.08 o -3 5 0 3375.22 3841.33 202.05 o -2 5 0 8435.58 7541.96 235.12 o -1 5 0 9.41 61.14 146.12 o 0 5 0 941.82 1073.49 93.16 o 1 5 0 6238.17 5466.55 176.19 o 2 5 0 26412.89 28381.06 345.17 o 3 5 0 13451.00 13901.69 276.21 o 4 5 0 3991.37 3917.91 194.43 o 5 5 0 1932.08 1799.80 182.00 o 6 5 0 565.02 564.45 141.71 o 7 5 0 12044.65 12104.90 315.70 o 8 5 0 12475.66 12276.68 331.94 o 9 5 0 4467.97 4212.96 247.15 o 10 5 0 504.32 501.31 175.19 o 11 5 0 335.65 117.66 163.76 o 12 5 0 5432.33 5255.28 307.28 o 13 5 0 2153.31 1907.24 217.88 o 14 5 0 1169.39 1336.77 193.23 o -11 6 0 1519.26 1046.53 234.12 o -10 6 0 2256.44 1990.22 253.16 o -9 6 0 2828.07 2701.20 256.77 o -8 6 0 61.75 143.72 176.59 o -7 6 0 125.43 124.48 160.96 o -6 6 0 1305.15 1173.61 193.63 o -5 6 0 5148.70 4787.64 235.52 o -4 6 0 2829.25 3063.01 198.44 o -3 6 0 5020.28 4962.03 205.26 o -2 6 0 590.82 654.85 138.91 o -1 6 0 951.82 1310.51 179.60 o 0 6 0 71.99 91.20 108.29 o 1 6 0 12249.89 12252.62 280.62 o 2 6 0 2149.54 2187.26 184.61 o 3 6 0 493.07 497.10 151.74 o 4 6 0 20996.99 20808.03 347.17 o 5 6 0 6848.89 6489.82 227.91 o 6 6 0 798.50 741.65 149.53 o 7 6 0 1.25 -59.93 172.18 o 8 6 0 12359.83 13478.75 355.39 o 9 6 0 7114.01 6743.18 280.42 o 10 6 0 1680.00 1640.44 199.44 o 11 6 0 3.11 -64.74 171.58 o 12 6 0 371.96 381.45 185.41 o 13 6 0 5175.11 5219.00 304.08 o 14 6 0 215.89 163.76 184.01 o -11 7 0 293.14 111.05 203.05 o -10 7 0 351.10 476.06 206.46 o -9 7 0 985.99 1009.64 222.29 o -8 7 0 1199.34 1086.61 225.30 o -7 7 0 67.84 79.98 189.22 o -6 7 0 0.33 -125.88 170.58 o -5 7 0 856.87 961.34 197.04 o -4 7 0 3130.65 3100.29 224.90 o -3 7 0 12894.46 12679.97 328.73 o -2 7 0 6200.41 5833.56 231.92 o -1 7 0 758.40 880.16 141.71 o 0 7 0 2372.81 2482.54 122.28 o 1 7 0 8424.84 8683.89 248.35 o 2 7 0 172.73 337.95 129.09 o 3 7 0 1853.72 1741.47 152.74 o 4 7 0 10876.37 11361.44 284.23 o 5 7 0 11152.54 11100.66 295.26 o 6 7 0 6214.05 6007.15 244.34 o 7 7 0 205.38 135.90 163.56 o 8 7 0 1914.86 2039.13 206.06 o 9 7 0 7219.01 7447.55 305.48 o 10 7 0 2520.68 2675.34 227.51 o 11 7 0 610.27 479.47 179.40 o 12 7 0 82.42 144.92 205.26 o 13 7 0 52.99 46.90 183.21 o -10 8 0 218.67 268.00 206.66 o -9 8 0 1.10 20.24 195.23 o -8 8 0 4.71 -43.70 189.62 o -7 8 0 147.70 229.11 192.63 o -6 8 0 107.71 175.59 173.99 o -5 8 0 121.61 47.31 162.96 o -4 8 0 3053.67 3058.60 237.13 o -3 8 0 64.06 6.82 170.78 o -2 8 0 14911.30 14283.54 353.79 o -1 8 0 3709.56 3588.37 223.50 o 0 8 0 5547.83 5829.95 177.45 o 1 8 0 1261.13 1005.03 166.37 o 2 8 0 18411.97 17951.49 363.81 o 3 8 0 6285.48 6751.20 250.56 o 4 8 0 166.97 33.47 160.36 o 5 8 0 9275.83 8821.00 293.25 o 6 8 0 10031.85 10288.26 317.51 o 7 8 0 515.61 714.39 182.61 o 8 8 0 2.71 -41.09 170.78 o 9 8 0 633.97 938.89 188.02 o 10 8 0 1471.89 1203.67 211.07 o 11 8 0 455.97 680.71 172.58 o 12 8 0 243.88 392.47 169.38 o 13 8 0 181.57 93.21 164.16 o -9 9 0 179.80 165.77 199.84 o -8 9 0 256.74 130.69 185.21 o -7 9 0 333.67 468.24 190.62 o -6 9 0 348.42 447.59 191.83 o -5 9 0 180.54 -13.03 190.62 o -4 9 0 176.21 132.69 186.41 o -3 9 0 8314.30 7150.69 324.12 o -2 9 0 1010.10 1078.40 205.86 o -1 9 0 2333.71 1922.47 215.88 o 0 9 0 5497.47 4546.87 699.65 o 1 9 0 9655.61 9486.68 305.88 o 2 9 0 221.73 142.72 183.81 o 3 9 0 16515.86 15753.40 382.25 o 4 9 0 1784.85 1521.58 200.24 o 5 9 0 78.65 183.21 169.38 o 6 9 0 3940.43 3719.06 239.53 o 7 9 0 1964.05 2131.14 222.69 o 8 9 0 47.64 134.30 176.39 o 9 9 0 251.48 297.46 188.62 o 10 9 0 140.11 204.86 184.21 o 11 9 0 413.24 517.15 173.18 o 12 9 0 82.56 22.45 169.38 o 13 9 0 20.24 33.67 164.57 o -8 10 0 239.93 188.42 233.32 o -7 10 0 2143.04 1885.99 250.96 o -6 10 0 264.74 252.96 207.06 o -5 10 0 70.98 61.74 187.42 o -4 10 0 498.01 597.73 184.41 o -3 10 0 2989.39 2873.58 251.36 o -2 10 0 4652.80 4502.60 282.83 o -1 10 0 1050.59 858.91 207.26 o 0 10 0 209.16 236.95 135.17 o 1 10 0 2389.40 1956.95 234.12 o 2 10 0 7771.71 7162.92 316.90 o 3 10 0 38.80 -45.50 192.83 o 4 10 0 3219.94 3022.32 234.12 o 5 10 0 155.05 139.11 167.57 o 6 10 0 2207.71 2033.92 227.71 o 7 10 0 49.58 108.64 188.62 o 8 10 0 1019.84 1036.10 231.51 o 9 10 0 143.59 88.60 198.84 o 10 10 0 41.02 190.22 179.80 o 11 10 0 17.05 9.82 174.59 o 12 10 0 131.67 -53.12 186.01 o -7 11 0 18.15 162.16 213.88 o -6 11 0 2162.99 2392.72 288.44 o -5 11 0 347.02 430.36 222.69 o -4 11 0 98.22 59.13 198.44 o -3 11 0 180.80 263.18 188.42 o -2 11 0 14164.53 12939.55 437.57 o -1 11 0 1.27 171.98 209.06 o 0 11 0 152.91 277.92 144.42 o 1 11 0 199.83 194.03 182.00 o 2 11 0 1594.94 1318.73 213.67 o 3 11 0 1895.50 1929.29 239.73 o 4 11 0 1340.36 1861.34 215.08 o 5 11 0 892.45 847.08 201.85 o 6 11 0 35.88 -97.82 184.81 o 7 11 0 499.42 596.12 195.03 o 8 11 0 117.68 172.38 214.48 o 9 11 0 21.77 61.54 178.40 o 10 11 0 15.26 113.85 196.64 o 11 11 0 43.62 22.05 190.22 o -5 12 0 2591.69 2731.47 293.05 o -4 12 0 115.55 20.85 210.07 o -3 12 0 1418.42 1166.19 233.72 o -2 12 0 526.68 630.20 228.51 o -1 12 0 11227.51 9717.59 418.13 o 0 12 0 79.57 115.13 155.68 o 1 12 0 608.42 778.73 203.25 o 2 12 0 248.25 24.65 214.28 o 3 12 0 2367.93 2093.65 252.36 o 4 12 0 595.59 641.02 226.30 o 5 12 0 458.26 411.71 193.83 o 6 12 0 0.22 83.59 180.20 o 7 12 0 0.68 17.24 198.24 o 8 12 0 74.84 231.11 187.62 o 9 12 0 781.79 526.37 226.50 o 10 12 0 262.38 175.79 210.07 o -4 13 0 977.57 1403.52 261.58 o -3 13 0 234.21 148.93 222.29 o -2 13 0 1088.07 1232.54 255.17 o -1 13 0 887.74 974.57 268.80 o 0 13 0 5432.13 4584.38 249.14 o 1 13 0 62.52 -63.94 211.67 o 2 13 0 50.66 82.18 204.25 o 3 13 0 1490.35 1265.41 232.92 o 4 13 0 1567.75 1488.31 256.77 o 5 13 0 3673.17 3523.83 298.46 o 6 13 0 91.57 230.51 208.06 o 7 13 0 99.46 50.31 205.26 o 8 13 0 76.97 96.61 209.26 o 9 13 0 843.43 926.86 243.94 o -1 14 0 170.71 268.40 240.33 o 0 14 0 55.76 -102.25 166.10 o 1 14 0 23.36 284.63 238.73 o 2 14 0 201.19 117.86 214.28 o 3 14 0 50.51 131.89 212.47 o 4 14 0 1397.91 1399.71 261.18 o 5 14 0 116.28 -15.03 227.51 o 6 14 0 2043.44 2306.52 313.50 o 7 14 0 0.21 48.11 237.53 o -7 -14 1 339.34 592.12 243.94 o -6 -14 1 80.69 282.43 225.90 o -5 -14 1 2569.63 2265.63 288.84 o -4 -14 1 31.95 43.30 210.87 o -3 -14 1 254.40 195.43 235.12 o -2 -14 1 623.08 393.67 248.15 o -1 -14 1 774.39 960.53 243.54 o 0 -14 1 18.84 -90.26 163.63 o 1 -14 1 5.09 0.00 223.30 o -9 -13 1 1097.72 1237.55 243.54 o -8 -13 1 825.05 928.66 232.12 o -7 -13 1 51.35 -99.62 198.64 o -6 -13 1 2112.82 1935.10 276.82 o -5 -13 1 8.31 69.96 227.51 o -4 -13 1 3404.84 3260.44 304.28 o -3 -13 1 165.72 147.13 196.44 o -2 -13 1 22.59 22.45 212.87 o -1 -13 1 282.62 279.42 234.92 o 0 -13 1 1612.72 1502.59 187.52 o 1 -13 1 890.29 865.92 240.73 o 2 -13 1 268.82 117.06 208.86 o 3 -13 1 272.00 179.80 223.50 o 4 -13 1 240.68 65.55 240.53 o -10 -12 1 1128.15 1575.90 244.14 o -9 -12 1 1312.05 1263.41 228.11 o -8 -12 1 829.00 724.41 224.50 o -7 -12 1 139.67 337.15 188.82 o -6 -12 1 149.24 134.70 195.23 o -5 -12 1 2960.54 3110.11 287.04 o -4 -12 1 144.40 273.01 193.23 o -3 -12 1 1139.39 1299.29 218.89 o -2 -12 1 321.42 312.90 209.67 o -1 -12 1 870.36 793.76 212.87 o 0 -12 1 8254.58 7405.77 257.80 o 1 -12 1 1255.55 1493.72 260.78 o 2 -12 1 2525.23 2289.89 270.80 o 3 -12 1 10.04 217.28 216.68 o 4 -12 1 2017.55 1876.17 266.19 o 5 -12 1 76.13 81.58 223.10 o 6 -12 1 1408.00 1259.20 276.21 o -11 -11 1 272.62 196.84 179.00 o -10 -11 1 179.07 317.10 207.06 o -9 -11 1 1233.52 1465.06 230.71 o -8 -11 1 654.28 575.48 218.69 o -7 -11 1 74.16 103.83 174.79 o -6 -11 1 41.16 124.08 184.81 o -5 -11 1 23.81 91.40 182.41 o -4 -11 1 295.11 282.03 180.80 o -3 -11 1 1331.92 1253.38 206.06 o -2 -11 1 0.10 6.82 177.19 o -1 -11 1 17.89 32.27 170.98 o 0 -11 1 174.57 222.55 138.96 o 1 -11 1 15199.61 14256.48 448.40 o 2 -11 1 766.93 773.12 225.50 o 3 -11 1 1007.74 972.36 229.11 o 4 -11 1 0.93 -72.76 204.86 o 5 -11 1 3261.39 2857.15 290.45 o 6 -11 1 205.41 180.60 230.51 o 7 -11 1 3027.28 2927.71 306.28 o -12 -10 1 848.36 1342.38 232.12 o -11 -10 1 348.05 436.37 181.80 o -10 -10 1 0.19 -61.34 181.40 o -9 -10 1 168.67 195.84 213.27 o -8 -10 1 721.21 337.55 209.67 o -7 -10 1 577.84 897.59 204.25 o -6 -10 1 185.82 219.89 172.18 o -5 -10 1 472.18 309.69 180.20 o -4 -10 1 372.31 430.36 172.78 o -3 -10 1 4610.51 5008.13 267.59 o -2 -10 1 73.92 80.18 194.83 o -1 -10 1 92.12 -6.41 182.81 o 0 -10 1 389.66 259.91 133.65 o 1 -10 1 2894.83 2660.91 241.74 o 2 -10 1 5887.10 5231.62 290.45 o 3 -10 1 914.78 873.74 207.26 o 4 -10 1 985.78 1181.02 216.08 o 5 -10 1 244.68 187.62 172.98 o 6 -10 1 4868.21 4981.27 325.72 o 7 -10 1 67.47 -60.33 222.09 o 8 -10 1 1808.88 1726.24 249.55 o -12 -9 1 140.83 182.20 194.43 o -11 -9 1 183.30 165.97 187.02 o -10 -9 1 61.61 87.80 177.39 o -9 -9 1 58.98 211.87 190.62 o -8 -9 1 17.31 -43.70 179.60 o -7 -9 1 16.93 30.27 168.37 o -6 -9 1 503.74 251.76 178.60 o -5 -9 1 1325.12 1058.55 194.83 o -4 -9 1 6678.81 6672.83 276.61 o -3 -9 1 124.69 130.29 177.59 o -2 -9 1 14445.83 13269.28 363.41 o -1 -9 1 3985.99 3881.83 239.93 o 0 -9 1 87.97 92.13 122.37 o 1 -9 1 79.70 183.61 182.61 o 2 -9 1 10269.16 9004.21 336.55 o 3 -9 1 2373.83 2148.37 226.50 o 4 -9 1 2819.20 3004.88 239.93 o 5 -9 1 233.77 157.15 176.59 o 6 -9 1 728.30 942.69 193.23 o 7 -9 1 2722.28 2533.63 261.78 o 8 -9 1 0.19 -80.58 203.45 o 9 -9 1 320.15 421.94 206.86 o -13 -8 1 58.78 52.12 159.55 o -12 -8 1 11.55 -19.44 177.19 o -11 -8 1 254.45 114.65 186.61 o -10 -8 1 8.42 33.47 165.17 o -9 -8 1 183.75 104.63 170.58 o -8 -8 1 55.67 52.52 164.97 o -7 -8 1 1978.23 1976.59 214.48 o -6 -8 1 5941.19 6434.50 275.41 o -5 -8 1 1439.38 1622.81 180.60 o -4 -8 1 5525.48 5443.09 245.14 o -3 -8 1 20834.97 21713.04 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