Acta Crystallographica Section C

Crystal Structure Communications

Volume 54, Part 8 (August 1998)

Cover illustration Cover illustration: 3,4-Bis(1-adamantyl)-1,2-dithiete: the First Structurally Characterized Dithiete Unsupported by a Ring or Benzenoid Frame, see Donahue & Holm, pages 1175-1178. One of the two independent molecules in the unit cell is shown with displacement ellipsoids plotted at the 50% probability level and H atoms omitted for clarity.

cif-access (inorganic compounds)

Acta Cryst. (1998). C54, IUC9800043    [ doi:10.1107/S0108270198099508 ]

A Sanidine Feldspar Analogue: KFeGe3O8

D. Lévy and J. Barbier

Synopsis: The crystal structure of the sanidine feldspar analogue potassium iron germanate, quenched from 873 K, has been determined in the C2/m space group using a flux-grown single crystal. A partial ordering of Fe is observed on the two tetrahedral sites, with a preferential occupancy for the T1 site (32%) over the T2 site (18%). This ordering is also reflected by the difference in the size of the tetrahedral sites [mean <<span class="it">T1-O> 1.765 (2) Å versus <<span class="it">T2-O> 1.749 (2) Å].

Formula: KFeGe3O8

cif-access (metal-organic compounds)

Acta Cryst. (1998). C54, IUC9800034    [ doi:10.1107/S0108270198099491 ]

Redetermination of Bis(1,2-ethanediammonium) Dichloride Tetrachloromercurate(II)

R. Spengler, R. Zouari, A. Ben Salah, H. Zimmermann and H. Burzlaff

Synopsis: The structure of bis(1,2-ethanediammonium) dichloride tetrachloromercurate, originally determined at 153 K [Wen et al. (1992). Inorg. Chim. Acta, 193, 77-85], has been redetermined with room-temperature data carefully corrected for absorption effects.

Formula: (C2H10N2)2Cl2[HgCl4]

Acta Cryst. (1998). C54, IUC9800035    [ doi:10.1107/S010827019809948X ]

[N,N'-Bis(trimethylsilyl)-o-phenylenediamido](1,4-butanediyl)(phenylimido)tungsten(VI), a Deactivation Product from Olefin Metathesis Polymerization

S.-Y. S. Wang, J. M. Boncella and K. A. Abboud

Synopsis: This compound was isolated as a deactivation product from olefin metathesis polymerization and its crystal structure was determined. The W atom has a square-pyramidal coordination geometry with the phenylimido ligand occupying the apical position. A relatively short W-N(imido) bond, 1.736 (3) Å, is interpreted as arising from the interaction of the lone pair of N(imido) and the W metal center.

Formula: [W(C4H8)(C6H5N)(C12H22N2Si2)]

Acta Cryst. (1998). C54, IUC9800036    [ doi:10.1107/S0108270198099478 ]


A. Deák, L. Párkányi, A. Kálmán, M. Venter and I. Haiduc

Synopsis: This complex is isostructural with the analogous nickel complex but has slightly longer metal-oxygen bonds. The crystal is built up from infinite one-dimensional chains of hydrogen-bonded molecules.

Formula: [Co(C6H5N2O2)2(CH4O)2]

Acta Cryst. (1998). C54, IUC9800037    [ doi:10.1107/S0108270198099466 ]

[N,N'-Bis(2-pyridylmethyl)ethylenediaminediacetato]cobalt(III) Perchlorate Monohydrate

P. Caravan, C. Orvig and S. J. Rettig

Synopsis: The structure of [Co(C18H20N4O4)]ClO4.H2O is isomorphous with that of the corresponding tetrafluoroborate monohydrate [Mandel & Douglas (1989). Inorg. Chim. Acta, 155, 55-69]. The cobalt(III) atom has distorted octahedral coordination with trans carboxylato groups.

Formula: [Co(C18H20N4O4)]ClO4.H2O

Acta Cryst. (1998). C54, IUC9800040    [ doi:10.1107/S0108270198099454 ]

Tetraphenylphosphonium Tetrachloroaluminate

N. Burford, D. J. LeBlanc and A. J. Lough

Synopsis: The crystal structure of tetraphenylphosphonium tetrachloroaluminate was determined at 150 K. Bond lengths and angles are normal.

Formula: (C24H20P)[AlCl4]

Acta Cryst. (1998). C54, IUC9800044    [ doi:10.1107/S0108270198099442 ]

A New Polymorph of Bis(di-n-propyldithiocarbamato-S,S')nickel(II)

F.-F. Jian, Z.-X. Wang, H.-K. Fun, Z.-P. Bai, X.-Z. You, I. A. Razak and K. Chinnakali

Synopsis: The structure of bis(di-n-propyldithiocarbamato-S,S')nickel(II) has been reported previously in the rhombohedral space group R-3. The new triclinic polymorph shows similar structural features with a square-planar environment for the Ni atoms.

Formula: [Ni(C7H14NS2)2]

cif-access (organic compounds)

Acta Cryst. (1998). C54, IUC9800038    [ doi:10.1107/S0108270198099430 ]

(2S,3S,5R)-2-Benzyl-N-(tert-butoxycarbonyl)-3-hydroxy-5-methylpyrrolidine at 158K

J. W. Bats, T. Heinrich and M. Reggelin

Synopsis: The pyrrolidine ring has an envelope conformation. The crystal packing is stabilized by an intermolecular hydrogen bond.

Formula: C17H25NO3

Acta Cryst. (1998). C54, IUC9800039    [ doi:10.1107/S0108270198099429 ]

(2S,3R,5S)-2-Benzyl-N-(tert-butoxycarbonyl)-3-hydroxy-5-methylpyrrolidine at 158K

J. W. Bats, T. Heinrich and M. Reggelin

Synopsis: The pyrrolidine ring has a conformation intermediate between a twist and an envelope. The crystal packing is stabilized by an intermolecular hydrogen bond.

Formula: C17H25NO3

Acta Cryst. (1998). C54, IUC9800041    [ doi:10.1107/S0108270198099417 ]

Disorder in Tris(2-methyl-1,2-propanediammonium) cyclo-Hexaphosphate Trihydrate

M. Charfi, A. Jouini and M. Pierrot

Synopsis: 3C4H14N22+.P6O186-.3H2O contains tetragonal channels parallel to the a direction of the unit cell built up by four rows of P6O18 rings and completed by organic groups. The condensed phosphoric groups are centrosymmetric, while the three independent organic cations have no internal symmetry.

Formula: 3C4H14N22+.P6O186-.3H2O

Acta Cryst. (1998). C54, IUC9800042    [ doi:10.1107/S0108270198099405 ]

Piperazine-1,4-diium Dihydrogendiphosphate

M. Charfi, A. Jouini and M. Pierrot

Synopsis: C4H12N22+.H2P2O72- has a typical layer structure composed of organic and inorganic groups centred on planes parallel to (100). The formula unit consists of one acidic anion and two crystallographically independent organic half cations. The H2P2O72- anions have no internal symmetry whereas the piperazinium cations are centrosymmetric.

Formula: C4H12N22+.H2P2O72-

inorganic compounds

Acta Cryst. (1998). C54, 1053-1055    [ doi:10.1107/S0108270198002145 ]

The Layered Perovskite K2Nd2Ti3O10

G. Amow and J. E. Greedan

Synopsis: The preparation of single crystals of the layered perovskite K2Nd2Ti3O10 and the characterization of its structure are described.

Formula: K2Nd2Ti3O10

Acta Cryst. (1998). C54, 1055-1057    [ doi:10.1107/S0108270197020076 ]


C. R. Feger and J. W. Kolis

Synopsis: Na3Mn4Te2O12 has a superstructure of the CaFe2O4 structure type. A tripling of the b axis arises because of significant differences in the oxidation states of tellurium and manganese within their respective octahedra.

Formula: Na3Mn4Te2O12

Acta Cryst. (1998). C54, 1057-1059    [ doi:10.1107/S0108270197019306 ]

A Neodymium-Substituted Britholite Compound

L. Boyer, J.-M. Savariault, J. Carpena and J.-L. Lacout

Synopsis: Ca9Nd(PO4)5(SiO4)F1.5O0.25 belongs to the britholite family and is isostructural with apatite. The neodymium ions are distributed over the two calcium sites but are mainly localized in calcium site II.

Formula: (Ca9.02.Nd0.98)[(PO4)5.1.(SiO4)0.9]F1.53O0.27

Acta Cryst. (1998). C54, 1059-1062    [ doi:10.1107/S0108270198002820 ]

A Mixed Zinc-Cobalt Diphosphate, ZnCoP2O7

M. Bettach, K. Benkhouja, M. Zahir, K. Rissouli, A. Sadel, M. Giorgi and M. Pierrot

Synopsis: The structure of the mixed zinc cobalt diphosphate ZnCoP2O7 presents a low-dimensional system not previously observed in the diphosphates of 3d transition elements.

Formula: ZnCoP2O7

Acta Cryst. (1998). C54, 1062-1064    [ doi:10.1107/S0108270198001000 ]


P. Vassilev and D. Nihtianova

Synopsis: The crystal structure of pentalead molybdenum octaoxide is a 4:3:2 superstructure of tetragonal [alpha]-PbO (litharge).

Formula: Pb5MoO8

Acta Cryst. (1998). C54, 1064-1066    [ doi:10.1107/S010827019800167X ]

Neutron Powder Diffraction Study on Highly Deuterated Ca(IO3)2.D2O

S. Peter, E. Suchanek, T. Roisnel and H. D. Lutz

Synopsis: Neutron powder diffraction studies confirm the results of a previous X-ray single-crystal study of the protonated compound. The water molecules form hydrogen bonds of different strengths. Deviation from a random distribution of the H atoms (H/D enrichment effect) has been established.

Formula: Ca(IO3)2.D2O

metal-organic compounds

Acta Cryst. (1998). C54, 1067-1068    [ doi:10.1107/S0108270198002753 ]


T.-H. Lu, J.-M. Lo, B.-H. Chen, M.-Y. Yeh, S.-F. Tung, W.-T. Huang and H.-H. Yao

Formula: [Zn(NCS)2(C4H13N3)]

Acta Cryst. (1998). C54, 1069-1070    [ doi:10.1107/S0108270198002947 ]

[7-Methyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene-[bold kappa]4N](nitrato-[bold kappa]O)copper(II) Nitrate Hydrate

T.-H. Lu, S.-F. Tung, T.-Y. Chi and C.-S. Chung

Formula: [Cu(NO3)(C14H24N4)]NO3.H2O

Acta Cryst. (1998). C54, 1071-1072    [ doi:10.1107/S0108270198001711 ]

(Isothiocyanato-[bold kappa]N)(1,4,8,11-tetramethyl-1,4,8,11-tetraazacyclotetradecane-[bold kappa]4N)copper(II) Perchlorate

T.-H. Lu, W.-Z. Shui, S.-F. Tung, T.-Y. Chi, F.-L. Liao and C.-S. Chung

Formula: [Cu(NCS)(C14H32N4)]ClO4

Acta Cryst. (1998). C54, 1072-1074    [ doi:10.1107/S0108270198003345 ]


Y. Elerman, A. Elmali and S. Özbey

Formula: [Cu(C18H13BrNO)2]

Acta Cryst. (1998). C54, 1075-1076    [ doi:10.1107/S0108270198005228 ]

Rerefinement of {1-[(2-Hydroxybenzylidene)aminomethyl]naphthalen-2-olato(2 -)-N,O,O'}(piperidine-N)nickel(II)

H. Paulus, I. Svoboda and H. Fuess

Formula: [Ni(C18H13NO2)(C5H11N)]

Acta Cryst. (1998). C54, 1076-1078    [ doi:10.1107/S0108270198002534 ]


Y. Elerman, A. Elmali, I. Svoboda and H. Fuess

Formula: [Ni(C15H16NO)2]

Acta Cryst. (1998). C54, 1078-1081    [ doi:10.1107/S0108270198002406 ]

A Silver(I) Complex of a Tube-Shaped Hydrocarbon

S. Kammermeier, P. G. Jones, I. Dix and R. Herges

Formula: [Ag2(C56H32)(C7H8)2(H2O)2](CF3SO3)2

Acta Cryst. (1998). C54, 1081-1083    [ doi:10.1107/S0108270198003126 ]

Manganese(II) Triphenylacetate Hydrate, a Manganese(II) Complex with a Chain Structure

T. S. Yaukey, O. W. Steward and S.-C. Chang

Formula: [Mn2(C20H15O2)4(H2O)4]

Acta Cryst. (1998). C54, 1083-1085    [ doi:10.1107/S0108270198002959 ]

Absolute Configuration of (+)589-(4,4'-Dimethoxy-2,2'-bipyridine 1,1'-dioxide-O,O')bis(ethylene-diamine-N,N')cobalt(III) Triperchlorate

H. Kanno, S. Utsuno, J. Fujita and K. Iijima

Formula: [Co(C2H8N2)2(C12H12N2O4)](ClO4)3

Acta Cryst. (1998). C54, 1085-1087    [ doi:10.1107/S0108270198002388 ]


J. J. C. Erasmus, G. J. Lamprecht, T. Kohzuma and Y. Nakano

Formula: [Rh(C15H11O2)(C5H9O3P)(CO)]

Acta Cryst. (1998). C54, 1087-1089    [ doi:10.1107/S0108270198001991 ]


Q.-H. Jin, X.-L. Xin, C.-J. Dong and H.-J. Zhu

Formula: [CuI(C12H8N2)(C18H15P)]

Acta Cryst. (1998). C54, 1089-1091    [ doi:10.1107/S010827019800290X ]

Exopolyhedral Cyclized Platinaundecaboranes: [(PPh3)(PhCOS)PtB10H11].0.5CH2Cl2

C.-H. Hu, J.-M. Dou, J. Sun, H.-J. Yao, J.-D. Wei, R.-S. Jin and P.-J. Zheng

Formula: C25H31B10OPPtS.0.5CH2Cl2

Acta Cryst. (1998). C54, 1091-1093    [ doi:10.1107/S0108270198002418 ]


M. Lutz, A. L. Spek, P. R. Markies, O. S. Akkerman and F. Bickelhaupt

Formula: [HgBr(C16H25O5)]

Acta Cryst. (1998). C54, 1093-1095    [ doi:10.1107/S0108270198002558 ]

Organization of the Cavity in a Bipyridyl Crown Ether Through Coordination with PdCl2

S. V. Luis, J. C. Frías, M. I. Burguete and M. Bolte

Formula: [PdCl2(C22H30N2O6)]

Acta Cryst. (1998). C54, 1095-1097    [ doi:10.1107/S0108270198002078 ]

[(1,2,5,6-[bold eta])-Cyclooctatetraene]([bold eta]5-cyclopentadienyl)cobalt

H. Wadepohl, R. Merkel and H. Pritzkow

Formula: [Co(C5H5)(C8H8)]

Acta Cryst. (1998). C54, 1097-1099    [ doi:10.1107/S0108270198003199 ]


N. Pieper, M. Schürmann and K. Jurkschat

Formula: [Sn(C4H12O3Si2)(C7H16N)2]

Acta Cryst. (1998). C54, 1099-1102    [ doi:10.1107/S0108270198003138 ]

Aqua(1,10-phenanthroline-N,N')([bold mu]3-thiosulfato-S:S:O)cadmium(II) Hydrate

S. Baggio, R. Baggio and M. T. Garland

Formula: [Cd(S2O3)(C12H8N2)(H2O)].H2O

Acta Cryst. (1998). C54, 1102-1103    [ doi:10.1107/S0108270198001097 ]

Di-[bold mu]-phenylthio-bis[bis(triethylphosphine-P)platinum(II)] Bis(hexafluorophosphate), [Pt2([bold mu]-SPh)2(PEt3)4](PF6)2

C. Bruhn, S. Becke and D. Steinborn

Formula: [Pt2(C6H5S)2(C6H15P)4](PF6)2

Acta Cryst. (1998). C54, 1104-1105    [ doi:10.1107/S0108270198002960 ]

Hexaaquacobalt(II) Bis(hydrogen cyclopropane-1,1-dicarboxylate)

T. Schwarz, A. Petri, J. Schilling and A. Lentz

Formula: [Co(H2O)6](C5H5O4)2

organic compounds

Acta Cryst. (1998). C54, 1106-1107    [ doi:10.1107/S0108270198002169 ]


B. Berger and M. Bolte

Formula: C27H27NO4S

Acta Cryst. (1998). C54, 1107-1108    [ doi:10.1107/S010827019800328X ]


G. E. H. Elgemeie, N. M. Fathy, H. Hopf, I. Dix and P. G. Jones

Formula: C17H15N3

Acta Cryst. (1998). C54, 1109-1111    [ doi:10.1107/S0108270198003278 ]


G. E. H. Elgemeie, N. M. Fathy, H. Hopf and P. G. Jones

Formula: C14H13N3

Acta Cryst. (1998). C54, 1111-1113    [ doi:10.1107/S0108270198003205 ]

A Triclinic Polymorph of Hexaphenylcyclotrisiloxane

B. Ziemer, M. Backer and N. Auner

Formula: C36H30O3Si3

Acta Cryst. (1998). C54, 1113-1115    [ doi:10.1107/S0108270198001814 ]


R. Bryant, S. C. James, N. C. Norman and A. G. Orpen

Formula: C6H4Br2N2O2

Acta Cryst. (1998). C54, 1115-1117    [ doi:10.1107/S0108270198003047 ]


A. Kuhl, A. Kornath, H. Preut and W. Kreiser

Formula: C20H24O3

Acta Cryst. (1998). C54, 1117-1119    [ doi:10.1107/S0108270198002728 ]


S. A. de Silva, M. A. Whitener, D. E. Baron, A. Zavaleta, E. V. Isidor and O. Allam

Formula: C27H23N3

Acta Cryst. (1998). C54, 1119-1121    [ doi:10.1107/S010827019800273X ]

3-[(2-Aminoethyl)iminomethyl]-4-hydroxybenzoic Acid 0.28-Hydrate

M. A. Whitener, C. Bolt de Freitas and A. Zavaleta

Formula: C10H12N2O3.0.28H2O

Acta Cryst. (1998). C54, 1121-1123    [ doi:10.1107/S010827019800242X ]

N-H...S and N-H...Ph Hydrogen Bonding in 1-(2-Fluorophenyl)thiourea

T. Steiner

Formula: C7H7FN2S

Acta Cryst. (1998). C54, 1123-1125    [ doi:10.1107/S0108270198003102 ]


N. Kumar, S. Roy, V. S. Parmar and W. Errington

Formula: C18H15NO4

Acta Cryst. (1998). C54, 1125-1127    [ doi:10.1107/S0108270198003187 ]

9,10-Dihydro-1,4-dimethoxy-5,8-dimethyl-cis-9,10-diphenyl-9,10-anthracenediol, a Crowded Planar 9,10-Dihydroanthracene

C. Krieger, A. R. Wartini and F. A. Neugebauer

Formula: C30H28O4

Acta Cryst. (1998). C54, 1127-1130    [ doi:10.1107/S0108270198003941 ]

Characterization of Quinoline Derivatives. II. 7-(4-Methyl-1-piperazinyl)-6H-[1]benzopyrano[3,4-c]quinoline

G. Giorgi, A. Cappelli, M. Anzini and S. Vomero

Formula: C21H21N3O

Acta Cryst. (1998). C54, 1130-1131    [ doi:10.1107/S0108270198002510 ]


E. Bermejo, R. Carballo, A. Castiñeiras and C. Maichle-Mössmer

Formula: C14H14N4S2

Acta Cryst. (1998). C54, 1132-1133    [ doi:10.1107/S0108270198003059 ]


D. A. McMorran and P. J. Steel

Formula: C16H12N2O2

Acta Cryst. (1998). C54, 1133-1137    [ doi:10.1107/S0108270198003412 ]

(-)-(2S)-Tifluadom Hydrochloride and Two of its (-)-(2S)-2-(Acylaminomethyl)benzodiazepine Hydrochloride Analogues

O. M. Peeters, R. L. Meurisse, N. M. Blaton and C. J. De Ranter

Formula: C22H21FN3OS+.Cl-, C23H24N3OS+.Cl- and C26H27FN3O+.Cl-.0.5C6H12O

Acta Cryst. (1998). C54, 1137-1139    [ doi:10.1107/S0108270198002893 ]


A. Elmali, Y. Elerman and E. Kendi

Formula: C18H14BrNO

Acta Cryst. (1998). C54, 1139-1141    [ doi:10.1107/S0108270198002546 ]

3[alpha]-Bikhaconine Acetone Solvate

M. Parvez, W. Gul and S. Anwar

Formula: C25H41NO8.C3H6O

Acta Cryst. (1998). C54, 1141-1143    [ doi:10.1107/S010827019800184X ]


C. Epple, C. Leumann and H. Stoeckli-Evans

Formula: C21H23N3O7

Acta Cryst. (1998). C54, 1143-1144    [ doi:10.1107/S0108270198001024 ]

(1[alpha],3[alpha],5[alpha])-1,3,5-Trimethyl-1,3,5-cyclohexanetricarboxylic Acid Acetonitrile Solvate

T. Hirose, B. W. Baldwin, Z.-H. Wang and C. H. L. Kennard

Formula: C12H18O6.C2H3N

Acta Cryst. (1998). C54, 1145-1146    [ doi:10.1107/S0108270198002923 ]


S. Isik, M. Aygün, H. Kocaokutgen and M. N. Tahir

Formula: C17H19ClN2O

Acta Cryst. (1998). C54, 1146-1148    [ doi:10.1107/S0108270198000250 ]


T.-S. Yoon, S. E. Yoo and W. Shin

Formula: C15H20N2O7

Acta Cryst. (1998). C54, 1148-1151    [ doi:10.1107/S0108270198002777 ]

[alpha]-Naphthyl Phenyl Pinacols

T. C. W. Mak, B. O. Patrick, S. J. Rettig, J. R. Scheffer, J. Trotter, P. Ukpabi, B.-M. Wu and V. C. Yee

Formula: C34H26O2 and C34H26O2

Acta Cryst. (1998). C54, 1151-1152    [ doi:10.1107/S0108270198002522 ]


F. Hdii, J.-P. Reboul, J. Barbe, D. Siri and G. Pèpe

Formula: C14H12N2O2S

Acta Cryst. (1998). C54, 1152-1154    [ doi:10.1107/S0108270198003096 ]

(Z)-5-(1-Methoxy-2-naphthylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine-3-acetic Acid Dimethyl Sulfoxide Solvate

D. TranQui, P. Fresneau and M. Cussac

Formula: C17H13NO4S2.C2H6OS

Acta Cryst. (1998). C54, 1154-1156    [ doi:10.1107/S0108270198002431 ]


J. J. Byrne, P. Y. Chavant, M.-T. Averbuch-Pouchot and Y. Vallée

Formula: C12H10O2

Acta Cryst. (1998). C54, 1156-1158    [ doi:10.1107/S0108270198001966 ]


S. G. Ilyin, A. S. Antonov, V. A. Stonik, M. Yu. Antipin and G. B. Elyakov

Formula: C30H46O3.1/3C3H6O.1/3H2O

Acta Cryst. (1998). C54, 1158-1160    [ doi:10.1107/S0108270197019161 ]

D-Secoestrone Derivatives. IV. 3-Hydroxy-18-methyl-17-oxaestra-1,3,5(10)-trien-16-one

S. Stankovic, D. Lazar, V. Pejanovic, J. Petrovic and C. Courseille

Formula: C18H22O3

Acta Cryst. (1998). C54, 1160-1162    [ doi:10.1107/S0108270198002108 ]


Y. Ohno, Y. Akutsu, M. Arai, M. Tamura, T. Matsunaga and M. Iida

Formula: CH2N4O

Acta Cryst. (1998). C54, 1162-1164    [ doi:10.1107/S0108270197019586 ]


K. A. Abboud, G. Butora, S. P. Fearnley, A. G. Gum, M. R. Stabile and T. Hudlicky

Formula: C11H15NO4

Acta Cryst. (1998). C54, 1164-1165    [ doi:10.1107/S0108270198002741 ]

N-Benzyl-N-(tert-butyloxycarbonyl)glycine, an N-Substituted Glycine (Peptoid) Monomer

M. Doi, K. Kinoshita, A. Asano, R. Yoneda, T. Kurihara and T. Ishida

Formula: C14H19NO4

Acta Cryst. (1998). C54, 1165-1168    [ doi:10.1107/S010827019800256X ]

9-Deoxy-15-hydroxy- and 9-Deoxy-19-hydroxycotylenol

N. Kato, F. Li, A. Mori, H. Takeshita and T. Sassa

Formula: Two isomers of C21H34O4

Acta Cryst. (1998). C54, 1168-1170    [ doi:10.1107/S0108270197019963 ]


A. W. Roszak and D. F. Weaver

Formula: C15H12N2OS

Acta Cryst. (1998). C54, 1170-1173    [ doi:10.1107/S010827019800239X ]

Racemic 2-Hydroxy-2-phenylpropanamidinium Chloride and (S)-2-Hydroxy-2-phenylbutanamidinium (R)-2-Hydroxy-2-phenylethanoate

J. C. Barnes and T. J. R. Weakley

Formula: C9H13N2O+.Cl- and C10H15N2O+.C8H7O3-

Acta Cryst. (1998). C54, 1173-1175    [ doi:10.1107/S0108270198002911 ]

sp-9-[o-([beta]-Chloro-[alpha],[alpha]-dimethylethyl)phenyl]fluorene: an Unanticipated Exclusive Product from the Reaction of sp-9-(o-tert-Butylphenyl)-9-fluorenol with Thionyl Chloride

P. D. Robinson, Y. Hou and C. Y. Meyers

Formula: C23H21Cl

Acta Cryst. (1998). C54, 1175-1178    [ doi:10.1107/S0108270198002935 ]

3,4-Bis(1-adamantyl)-1,2-dithiete: the First Structurally Characterized Dithiete Unsupported by a Ring or Benzenoid Frame

J. P. Donahue and R. H. Holm

Formula: C22H30S2

Acta Cryst. (1998). C54, 1178-1180    [ doi:10.1107/S0108270198002133 ]

8-Aminoquinolinium Chloride Dihydrate

B. J. Prince and M. M. Turnbull

Formula: C9H9N2+.Cl-.2H2O

Acta Cryst. (1998). C54, 1180-1182    [ doi:10.1107/S0108270198002765 ]

(±)-4-Oxo-1,2,3,4-tetrahydronaphthalene-1-carboxylic Acid: Hydrogen Bonding and Carboxyl Disordering in a [bold delta]-Keto Acid

H. W. Thompson, R. A. Lalancette and A. P. J. Brunskill

Formula: C11H10O3

Acta Cryst. (1998). C54, 1182-1184    [ doi:10.1107/S0108270198006076 ]

[beta]-Dihydroentandrophragmin-Ethyl Acetate (1/0.355)

R. L. Baxter, F. J. J. Dijksma, R. O. Gould and S. Parsons

Formula: C43H58O17.0.355C4H8O2

Acta Cryst. (1998). C54, 1184-1186    [ doi:10.1107/S0108270198002868 ]

ortho-(1-Naphthoyl)benzoic Acid

R. E. Gerkin

Formula: C18H12O3

Acta Cryst. (1998). C54, 1187-1189    [ doi:10.1107/S0108270198003321 ]

1-Phenethylguanidinium Chloride

M. A. Soriano-Lesh, E. M. Holt, F. A. García and M. Soriano-García

Formula: C10H16N5+.Cl-

Acta Cryst. (1998). C54, 1189-1191    [ doi:10.1107/S0108270197018829 ]

Cyclopropylcarboxamidinium Chloride

J. Barker and H. R. Powell

Formula: C4H9N2+.Cl-

Acta Cryst. (1998). C54, 1191-1192    [ doi:10.1107/S0108270197017435 ]

myo-Inositol 1,3,5-Bicyclic Phosphate

S. Neidle, P. R. J. Gaffney and C. B. Reese

Formula: C6H9O7P

addenda and errata

Acta Cryst. (1998). C54, 1193    [ doi:10.1107/S0108270198003850 ]

Comment on Interwoven Hydrogen-Bonding Networks in Benzene-1,3,5-triacetic Acid by Fitzgerald & Gerkin (1997)

S. R. Batten

Synopsis: A re-examination of the structure of benzene-1,3,5-triacetic acid reported by Fitzgerald & Gerkin [Acta Cryst. (1997), C53, 967-969].

Acta Cryst. (1998). C54, 1193-1194    [ doi:10.1107/S0108270198006040 ]

Response to Batten's (1998) Comment on Interwoven Hydrogen-Bonding Networks in Benzene-1,3,5-triacetic Acid

L. J. Fitzgerald and R. E. Gerkin

Synopsis: A response to the comment by Batten [Acta Cryst. (1998), C54, 1193].

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