Acta Crystallographica Section C

Crystal Structure Communications

Volume 54, Part 8 (August 1998)

Cover illustration: 3,4-Bis(1-adamantyl)-1,2-dithiete: the First Structurally Characterized Dithiete Unsupported by a Ring or Benzenoid Frame, see Donahue & Holm, pages 1175-1178. One of the two independent molecules in the unit cell is shown with displacement ellipsoids plotted at the 50% probability level and H atoms omitted for clarity.

• cif-access (inorganic compounds)
• cif-access (metal-organic compounds)
• cif-access (organic compounds)
• inorganic compounds
• metal-organic compounds
• organic compounds
• addenda and errata

cif-access (inorganic compounds)

 

A Sanidine Feldspar Analogue: KFeGe₃O₈

D. Lévy and J. Barbier

Synopsis: The crystal structure of the sanidine feldspar analogue potassium iron germanate, quenched from 873 K, has been determined in the C2/m space group using a flux-grown single crystal. A partial ordering of Fe is observed on the two tetrahedral sites, with a preferential occupancy for the T1 site (32%) over the T2 site (18%). This ordering is also reflected by the difference in the size of the tetrahedral sites [mean <<span class="it">T1-O> 1.765 (2) Å versus <<span class="it">T2-O> 1.749 (2) Å].

Formula: KFeGe₃O₈

cif-access (metal-organic compounds)

 

Redetermination of Bis(1,2-ethanediammonium) Dichloride Tetrachloromercurate(II)

R. Spengler, R. Zouari, A. Ben Salah, H. Zimmermann and H. Burzlaff

Synopsis: The structure of bis(1,2-ethanediammonium) dichloride tetrachloromercurate, originally determined at 153 K [Wen et al. (1992). Inorg. Chim. Acta, 193, 77-85], has been redetermined with room-temperature data carefully corrected for absorption effects.

Formula: (C₂H₁₀N₂)₂Cl₂[HgCl₄]

 

[N,N'-Bis(trimethylsilyl)-o-phenylenediamido](1,4-butanediyl)(phenylimido)tungsten(VI), a Deactivation Product from Olefin Metathesis Polymerization

S.-Y. S. Wang, J. M. Boncella and K. A. Abboud

Synopsis: This compound was isolated as a deactivation product from olefin metathesis polymerization and its crystal structure was determined. The W atom has a square-pyramidal coordination geometry with the phenylimido ligand occupying the apical position. A relatively short W-N(imido) bond, 1.736 (3) Å, is interpreted as arising from the interaction of the lone pair of N(imido) and the W metal center.

Formula: [W(C₄H₈)(C₆H₅N)(C₁₂H₂₂N₂Si₂)]

 

Dimethanolbis(N-nitroso-N-phenylhydroxylaminato-O,O')cobalt(II)

A. Deák, L. Párkányi, A. Kálmán, M. Venter and I. Haiduc

Synopsis: This complex is isostructural with the analogous nickel complex but has slightly longer metal-oxygen bonds. The crystal is built up from infinite one-dimensional chains of hydrogen-bonded molecules.

Formula: [Co(C₆H₅N₂O₂)₂(CH₄O)₂]

 

[N,N'-Bis(2-pyridylmethyl)ethylenediaminediacetato]cobalt(III) Perchlorate Monohydrate

P. Caravan, C. Orvig and S. J. Rettig

Synopsis: The structure of [Co(C₁₈H₂₀N₄O₄)]ClO₄.H₂O is isomorphous with that of the corresponding tetrafluoroborate monohydrate [Mandel & Douglas (1989). Inorg. Chim. Acta, 155, 55-69]. The cobalt(III) atom has distorted octahedral coordination with trans carboxylato groups.

Formula: [Co(C₁₈H₂₀N₄O₄)]ClO₄.H₂O

 

Tetraphenylphosphonium Tetrachloroaluminate

N. Burford, D. J. LeBlanc and A. J. Lough

Synopsis: The crystal structure of tetraphenylphosphonium tetrachloroaluminate was determined at 150 K. Bond lengths and angles are normal.

Formula: (C₂₄H₂₀P)[AlCl₄]

 

A New Polymorph of Bis(di-n-propyldithiocarbamato-S,S')nickel(II)

F.-F. Jian, Z.-X. Wang, H.-K. Fun, Z.-P. Bai, X.-Z. You, I. A. Razak and K. Chinnakali

Synopsis: The structure of bis(di-n-propyldithiocarbamato-S,S^')nickel(II) has been reported previously in the rhombohedral space group R-3. The new triclinic polymorph shows similar structural features with a square-planar environment for the Ni atoms.

Formula: [Ni(C₇H₁₄NS₂)₂]

cif-access (organic compounds)

 

(2S,3S,5R)-2-Benzyl-N-(tert-butoxycarbonyl)-3-hydroxy-5-methylpyrrolidine at 158K

J. W. Bats, T. Heinrich and M. Reggelin

Synopsis: The pyrrolidine ring has an envelope conformation. The crystal packing is stabilized by an intermolecular hydrogen bond.

Formula: C₁₇H₂₅NO₃

 

(2S,3R,5S)-2-Benzyl-N-(tert-butoxycarbonyl)-3-hydroxy-5-methylpyrrolidine at 158K

J. W. Bats, T. Heinrich and M. Reggelin

Synopsis: The pyrrolidine ring has a conformation intermediate between a twist and an envelope. The crystal packing is stabilized by an intermolecular hydrogen bond.

Formula: C₁₇H₂₅NO₃

 

Disorder in Tris(2-methyl-1,2-propanediammonium) cyclo-Hexaphosphate Trihydrate

M. Charfi, A. Jouini and M. Pierrot

Synopsis: 3C₄H₁₄N₂²⁺.P₆O₁₈^6-.3H₂O contains tetragonal channels parallel to the a direction of the unit cell built up by four rows of P₆O₁₈ rings and completed by organic groups. The condensed phosphoric groups are centrosymmetric, while the three independent organic cations have no internal symmetry.

Formula: 3C₄H₁₄N₂²⁺.P₆O₁₈^6-.3H₂O

 

Piperazine-1,4-diium Dihydrogendiphosphate

M. Charfi, A. Jouini and M. Pierrot

Synopsis: C₄H₁₂N₂²⁺.H₂P₂O₇^2- has a typical layer structure composed of organic and inorganic groups centred on planes parallel to (100). The formula unit consists of one acidic anion and two crystallographically independent organic half cations. The H₂P₂O₇^2- anions have no internal symmetry whereas the piperazinium cations are centrosymmetric.

Formula: C₄H₁₂N₂²⁺.H₂P₂O₇^2-

inorganic compounds

 

The Layered Perovskite K₂Nd₂Ti₃O₁₀

G. Amow and J. E. Greedan

Synopsis: The preparation of single crystals of the layered perovskite K₂Nd₂Ti₃O₁₀ and the characterization of its structure are described.

Formula: K₂Nd₂Ti₃O₁₀

 

Na₃Mn₄Te₂O₁₂

C. R. Feger and J. W. Kolis

Synopsis: Na₃Mn₄Te₂O₁₂ has a superstructure of the CaFe₂O₄ structure type. A tripling of the b axis arises because of significant differences in the oxidation states of tellurium and manganese within their respective octahedra.

Formula: Na₃Mn₄Te₂O₁₂

 

A Neodymium-Substituted Britholite Compound

L. Boyer, J.-M. Savariault, J. Carpena and J.-L. Lacout

Synopsis: Ca₉Nd(PO₄)₅(SiO₄)F_1.5O_0.25 belongs to the britholite family and is isostructural with apatite. The neodymium ions are distributed over the two calcium sites but are mainly localized in calcium site II.

Formula: (Ca_9.02.Nd_0.98)[(PO₄)_5.1.(SiO₄)_0.9]F_1.53O_0.27

 

A Mixed Zinc-Cobalt Diphosphate, ZnCoP₂O₇

M. Bettach, K. Benkhouja, M. Zahir, K. Rissouli, A. Sadel, M. Giorgi and M. Pierrot

Synopsis: The structure of the mixed zinc cobalt diphosphate ZnCoP₂O₇ presents a low-dimensional system not previously observed in the diphosphates of 3d transition elements.

Formula: ZnCoP₂O₇

 

Pb₅O₄MoO₄

P. Vassilev and D. Nihtianova

Synopsis: The crystal structure of pentalead molybdenum octaoxide is a 4:3:2 superstructure of tetragonal -PbO (litharge).

Formula: Pb₅MoO₈

 

Neutron Powder Diffraction Study on Highly Deuterated Ca(IO₃)₂.D₂O

S. Peter, E. Suchanek, T. Roisnel and H. D. Lutz

Synopsis: Neutron powder diffraction studies confirm the results of a previous X-ray single-crystal study of the protonated compound. The water molecules form hydrogen bonds of different strengths. Deviation from a random distribution of the H atoms (H/D enrichment effect) has been established.

Formula: Ca(IO₃)₂.D₂O

metal-organic compounds

 

(Diethylenetriamine)bis(isothiocyanato)zinc(II)

T.-H. Lu, J.-M. Lo, B.-H. Chen, M.-Y. Yeh, S.-F. Tung, W.-T. Huang and H.-H. Yao

Formula: [Zn(NCS)₂(C₄H₁₃N₃)]

 

[7-Methyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene-⁴N](nitrato-O)copper(II) Nitrate Hydrate

T.-H. Lu, S.-F. Tung, T.-Y. Chi and C.-S. Chung

Formula: [Cu(NO₃)(C₁₄H₂₄N₄)]NO₃.H₂O

 

(Isothiocyanato-N)(1,4,8,11-tetramethyl-1,4,8,11-tetraazacyclotetradecane-⁴N)copper(II) Perchlorate

T.-H. Lu, W.-Z. Shui, S.-F. Tung, T.-Y. Chi, F.-L. Liao and C.-S. Chung

Formula: [Cu(NCS)(C₁₄H₃₂N₄)]ClO₄

 

Bis[N-(2-bromo-4-methylphenyl)naphthaldiminato]copper(II)

Y. Elerman, A. Elmali and S. Özbey

Formula: [Cu(C₁₈H₁₃BrNO)₂]

 

Rerefinement of {1-[(2-Hydroxybenzylidene)aminomethyl]naphthalen-2-olato(2 -)-N,O,O'}(piperidine-N)nickel(II)

H. Paulus, I. Svoboda and H. Fuess

Formula: [Ni(C₁₈H₁₃NO₂)(C₅H₁₁N)]

 

Bis(N-n-butyl-2-hydroxy-1-naphthaldiminato)nickel(II)

Y. Elerman, A. Elmali, I. Svoboda and H. Fuess

Formula: [Ni(C₁₅H₁₆NO)₂]

 

A Silver(I) Complex of a Tube-Shaped Hydrocarbon

S. Kammermeier, P. G. Jones, I. Dix and R. Herges

Formula: [Ag₂(C₅₆H₃₂)(C₇H₈)₂(H₂O)₂](CF₃SO₃)₂

 

Manganese(II) Triphenylacetate Hydrate, a Manganese(II) Complex with a Chain Structure

T. S. Yaukey, O. W. Steward and S.-C. Chang

Formula: [Mn₂(C₂₀H₁₅O₂)₄(H₂O)₄]

 

Absolute Configuration of (+)₅₈₉-(4,4'-Dimethoxy-2,2'-bipyridine 1,1'-dioxide-O,O')bis(ethylene-diamine-N,N')cobalt(III) Triperchlorate

H. Kanno, S. Utsuno, J. Fujita and K. Iijima

Formula: [Co(C₂H₈N₂)₂(C₁₂H₁₂N₂O₄)](ClO₄)₃

 

Carbonyl(1,3-diphenyl-1,3-propanedionato-O,O')(4-methyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane-P)rhodium(I)

J. J. C. Erasmus, G. J. Lamprecht, T. Kohzuma and Y. Nakano

Formula: [Rh(C₁₅H₁₁O₂)(C₅H₉O₃P)(CO)]

 

Iodo(1,10-phenanthroline-N,N')(triphenylphosphine)copper(I)

Q.-H. Jin, X.-L. Xin, C.-J. Dong and H.-J. Zhu

Formula: [CuI(C₁₂H₈N₂)(C₁₈H₁₅P)]

 

Exopolyhedral Cyclized Platinaundecaboranes: [(PPh₃)(PhCOS)PtB₁₀H₁₁].0.5CH₂Cl₂

C.-H. Hu, J.-M. Dou, J. Sun, H.-J. Yao, J.-D. Wei, R.-S. Jin and P.-J. Zheng

Formula: C₂₅H₃₁B₁₀OPPtS.0.5CH₂Cl₂

 

1-Bromomercurio-2-(2,5,8,11,14-pentaoxapentadecyl)benzene

M. Lutz, A. L. Spek, P. R. Markies, O. S. Akkerman and F. Bickelhaupt

Formula: [HgBr(C₁₆H₂₅O₅)]

 

Organization of the Cavity in a Bipyridyl Crown Ether Through Coordination with PdCl₂

S. V. Luis, J. C. Frías, M. I. Burguete and M. Bolte

Formula: [PdCl₂(C₂₂H₃₀N₂O₆)]

 

[(1,2,5,6-)-Cyclooctatetraene](⁵-cyclopentadienyl)cobalt

H. Wadepohl, R. Merkel and H. Pritzkow

Formula: [Co(C₅H₅)(C₈H₈)]

 

6,6-Bis[3-(dimethylamino)-1,1-dimethylpropyl]-2,2,4,4-tetramethyl-1,3,5-trioxa-2,4-disila-6-stannacyclohexane

N. Pieper, M. Schürmann and K. Jurkschat

Formula: [Sn(C₄H₁₂O₃Si₂)(C₇H₁₆N)₂]

 

Aqua(1,10-phenanthroline-N,N')(₃-thiosulfato-S:S:O)cadmium(II) Hydrate

S. Baggio, R. Baggio and M. T. Garland

Formula: [Cd(S₂O₃)(C₁₂H₈N₂)(H₂O)].H₂O

 

Di--phenylthio-bis[bis(triethylphosphine-P)platinum(II)] Bis(hexafluorophosphate), [Pt₂(-SPh)₂(PEt₃)₄](PF₆)₂

C. Bruhn, S. Becke and D. Steinborn

Formula: [Pt₂(C₆H₅S)₂(C₆H₁₅P)₄](PF₆)₂

 

Hexaaquacobalt(II) Bis(hydrogen cyclopropane-1,1-dicarboxylate)

T. Schwarz, A. Petri, J. Schilling and A. Lentz

Formula: [Co(H₂O)₆](C₅H₅O₄)₂

organic compounds

 

(2R,3S)-3-Phenyl-2-[(2S,4S)-4-phenyl-3-tosyl-1,3-oxazolidin-2-yl]cyclopentanone

B. Berger and M. Bolte

Formula: C₂₇H₂₇NO₄S

 

2,3,4,5-Tetrahydrocyclohepta[b]pyrido[2,1-a]benzimidazole-7-carbonitrile

G. E. H. Elgemeie, N. M. Fathy, H. Hopf, I. Dix and P. G. Jones

Formula: C₁₇H₁₅N₃

 

1,2,3,4-Tetrahydrobenzimidazo[2,1-b]quinazoline

G. E. H. Elgemeie, N. M. Fathy, H. Hopf and P. G. Jones

Formula: C₁₄H₁₃N₃

 

A Triclinic Polymorph of Hexaphenylcyclotrisiloxane

B. Ziemer, M. Backer and N. Auner

Formula: C₃₆H₃₀O₃Si₃

 

2,6-Dibromo-4-nitroaniline

R. Bryant, S. C. James, N. C. Norman and A. G. Orpen

Formula: C₆H₄Br₂N₂O₂

 

17-Hydroxymethyl-3-methoxy-19,21-dinorestra-1,3,5(10)-trieno-18,20-lactone

A. Kuhl, A. Kornath, H. Preut and W. Kreiser

Formula: C₂₀H₂₄O₃

 

(9-Anthrylmethyl)bis(2-pyridylmethyl)amine

S. A. de Silva, M. A. Whitener, D. E. Baron, A. Zavaleta, E. V. Isidor and O. Allam

Formula: C₂₇H₂₃N₃

 

3-[(2-Aminoethyl)iminomethyl]-4-hydroxybenzoic Acid 0.28-Hydrate

M. A. Whitener, C. Bolt de Freitas and A. Zavaleta

Formula: C₁₀H₁₂N₂O₃.0.28H₂O

 

N-HS and N-HPh Hydrogen Bonding in 1-(2-Fluorophenyl)thiourea

T. Steiner

Formula: C₇H₇FN₂S

 

2',4'-Dihydroxy-2-[3-(4-methylphenyl)isoxazol-5-yl]acetophenone

N. Kumar, S. Roy, V. S. Parmar and W. Errington

Formula: C₁₈H₁₅NO₄

 

9,10-Dihydro-1,4-dimethoxy-5,8-dimethyl-cis-9,10-diphenyl-9,10-anthracenediol, a Crowded Planar 9,10-Dihydroanthracene

C. Krieger, A. R. Wartini and F. A. Neugebauer

Formula: C₃₀H₂₈O₄

 

Characterization of Quinoline Derivatives. II. 7-(4-Methyl-1-piperazinyl)-6H-[1]benzopyrano[3,4-c]quinoline

G. Giorgi, A. Cappelli, M. Anzini and S. Vomero

Formula: C₂₁H₂₁N₃O

 

N,N'-Bis(2-pyridylmethyl)dithiooxamide

E. Bermejo, R. Carballo, A. Castiñeiras and C. Maichle-Mössmer

Formula: C₁₄H₁₄N₄S₂

 

1,4-Bis(3-pyridyloxy)benzene

D. A. McMorran and P. J. Steel

Formula: C₁₆H₁₂N₂O₂

 

(-)-(2S)-Tifluadom Hydrochloride and Two of its (-)-(2S)-2-(Acylaminomethyl)benzodiazepine Hydrochloride Analogues

O. M. Peeters, R. L. Meurisse, N. M. Blaton and C. J. De Ranter

Formula: C₂₂H₂₁FN₃OS⁺.Cl^-, C₂₃H₂₄N₃OS⁺.Cl^- and C₂₆H₂₇FN₃O⁺.Cl^-.0.5C₆H₁₂O

 

N-(2-Bromo-4-methylphenyl)naphthaldimine

A. Elmali, Y. Elerman and E. Kendi

Formula: C₁₈H₁₄BrNO

 

3-Bikhaconine Acetone Solvate

M. Parvez, W. Gul and S. Anwar

Formula: C₂₅H₄₁NO₈.C₃H₆O

 

(1'S,5'S,6'R,8'S)-1-[(6'-Acetoxy-8'-hydroxy-2'-oxabicyclo[3.2.1]oct-5'-yl)oxymethyl]-N⁴-benzoylcytosine

C. Epple, C. Leumann and H. Stoeckli-Evans

Formula: C₂₁H₂₃N₃O₇

 

(1,3,5)-1,3,5-Trimethyl-1,3,5-cyclohexanetricarboxylic Acid Acetonitrile Solvate

T. Hirose, B. W. Baldwin, Z.-H. Wang and C. H. L. Kennard

Formula: C₁₂H₁₈O₆.C₂H₃N

 

3-tert-Butyl-2'-chloro-2-hydroxy-5-methylazobenzene

S. Isik, M. Aygün, H. Kocaokutgen and M. N. Tahir

Formula: C₁₇H₁₉ClN₂O

 

N-(2-Dimethoxymethyl-3-hydroxy-2-methyl-6-nitro-3,4-dihydro-2H-1-benzopyran-4-yl)acetamide

T.-S. Yoon, S. E. Yoo and W. Shin

Formula: C₁₅H₂₀N₂O₇

 

-Naphthyl Phenyl Pinacols

T. C. W. Mak, B. O. Patrick, S. J. Rettig, J. R. Scheffer, J. Trotter, P. Ukpabi, B.-M. Wu and V. C. Yee

Formula: C₃₄H₂₆O₂ and C₃₄H₂₆O₂

 

10-Ethyl-3-nitrophenothiazine

F. Hdii, J.-P. Reboul, J. Barbe, D. Siri and G. Pèpe

Formula: C₁₄H₁₂N₂O₂S

 

(Z)-5-(1-Methoxy-2-naphthylmethylene)-4-oxo-2-thioxo-1,3-thiazolidine-3-acetic Acid Dimethyl Sulfoxide Solvate

D. TranQui, P. Fresneau and M. Cussac

Formula: C₁₇H₁₃NO₄S₂.C₂H₆OS

 

2,2'-Biphenol

J. J. Byrne, P. Y. Chavant, M.-T. Averbuch-Pouchot and Y. Vallée

Formula: C₁₂H₁₀O₂

 

(20S)-3-Hydroxyholosta-7,9-diene

S. G. Ilyin, A. S. Antonov, V. A. Stonik, M. Yu. Antipin and G. B. Elyakov

Formula: C₃₀H₄₆O₃.1/3C₃H₆O.1/3H₂O

 

D-Secoestrone Derivatives. IV. 3-Hydroxy-18-methyl-17-oxaestra-1,3,5(10)-trien-16-one

S. Stankovic, D. Lazar, V. Pejanovic, J. Petrovic and C. Courseille

Formula: C₁₈H₂₂O₃

 

1H-Tetrazol-5(4H)-one

Y. Ohno, Y. Akutsu, M. Arai, M. Tamura, T. Matsunaga and M. Iida

Formula: CH₂N₄O

 

(7R,8S,10bR)-7,8-Dihydroxy-1,5,6,7,8,9,10,10b-octahydro-3H-1,3-oxazolo[4,3-a]isoquinolin-3-one

K. A. Abboud, G. Butora, S. P. Fearnley, A. G. Gum, M. R. Stabile and T. Hudlicky

Formula: C₁₁H₁₅NO₄

 

N-Benzyl-N-(tert-butyloxycarbonyl)glycine, an N-Substituted Glycine (Peptoid) Monomer

M. Doi, K. Kinoshita, A. Asano, R. Yoneda, T. Kurihara and T. Ishida

Formula: C₁₄H₁₉NO₄

 

9-Deoxy-15-hydroxy- and 9-Deoxy-19-hydroxycotylenol

N. Kato, F. Li, A. Mori, H. Takeshita and T. Sassa

Formula: Two isomers of C₂₁H₃₄O₄

 

5,5-Diphenyl-2-thiohydantoin

A. W. Roszak and D. F. Weaver

Formula: C₁₅H₁₂N₂OS

 

Racemic 2-Hydroxy-2-phenylpropanamidinium Chloride and (S)-2-Hydroxy-2-phenylbutanamidinium (R)-2-Hydroxy-2-phenylethanoate

J. C. Barnes and T. J. R. Weakley

Formula: C₉H₁₃N₂O⁺.Cl^- and C₁₀H₁₅N₂O⁺.C₈H₇O₃^-

 

sp-9-[o-(-Chloro-,-dimethylethyl)phenyl]fluorene: an Unanticipated Exclusive Product from the Reaction of sp-9-(o-tert-Butylphenyl)-9-fluorenol with Thionyl Chloride

P. D. Robinson, Y. Hou and C. Y. Meyers

Formula: C₂₃H₂₁Cl

 

3,4-Bis(1-adamantyl)-1,2-dithiete: the First Structurally Characterized Dithiete Unsupported by a Ring or Benzenoid Frame

J. P. Donahue and R. H. Holm

Formula: C₂₂H₃₀S₂

 

8-Aminoquinolinium Chloride Dihydrate

B. J. Prince and M. M. Turnbull

Formula: C₉H₉N₂⁺.Cl^-.2H₂O

 

(±)-4-Oxo-1,2,3,4-tetrahydronaphthalene-1-carboxylic Acid: Hydrogen Bonding and Carboxyl Disordering in a -Keto Acid

H. W. Thompson, R. A. Lalancette and A. P. J. Brunskill

Formula: C₁₁H₁₀O₃

 

-Dihydroentandrophragmin-Ethyl Acetate (1/0.355)

R. L. Baxter, F. J. J. Dijksma, R. O. Gould and S. Parsons

Formula: C₄₃H₅₈O₁₇.0.355C₄H₈O₂

 

ortho-(1-Naphthoyl)benzoic Acid

R. E. Gerkin

Formula: C₁₈H₁₂O₃

 

1-Phenethylguanidinium Chloride

M. A. Soriano-Lesh, E. M. Holt, F. A. García and M. Soriano-García

Formula: C₁₀H₁₆N₅⁺.Cl^-

 

Cyclopropylcarboxamidinium Chloride

J. Barker and H. R. Powell

Formula: C₄H₉N₂⁺.Cl^-

 

myo-Inositol 1,3,5-Bicyclic Phosphate

S. Neidle, P. R. J. Gaffney and C. B. Reese

Formula: C₆H₉O₇P

addenda and errata

 

Comment on Interwoven Hydrogen-Bonding Networks in Benzene-1,3,5-triacetic Acid by Fitzgerald & Gerkin (1997)

S. R. Batten

Synopsis: A re-examination of the structure of benzene-1,3,5-triacetic acid reported by Fitzgerald & Gerkin [Acta Cryst. (1997), C53, 967-969].

 

Response to Batten's (1998) Comment on Interwoven Hydrogen-Bonding Networks in Benzene-1,3,5-triacetic Acid

L. J. Fitzgerald and R. E. Gerkin

Synopsis: A response to the comment by Batten [Acta Cryst. (1998), C54, 1193].

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