![]() |
Cover illustration: Tetraethylammonium (1-Pyrrolidinecarbodithioato-S,S')(tetrathiotungstenio-S,S')nickelate(1-), see Long, Wang & Huang, pages 1251-1253. Displacement ellipsoids are shown at the 30% probability level and H atoms have been omitted for clarity. |
Acta Cryst. (1998). C54, IUC9800046 [ doi:10.1107/S0108270198099375 ]
Synopsis: The structure of strontium nitrate, originally determined with neutron radiation at room temperature [Nowotny & Heger (1983). Acta Cryst. C39, 952-956], has been redetermined using X-ray analysis at 173 K.
Formula: Sr(NO3)2
Acta Cryst. (1998). C54, IUC9800047 [ doi:10.1107/S0108270198099363 ]
Synopsis: Better data have enabled eight Na+ cations per [Ce(W5O18)2]8- anion to be identified, in contrast to the six found earlier [Iball et al. (1974). J. Chem. Soc. Dalton Trans. pp. 2021-2024]. The two W5O186- ligands, related by a crystallographic twofold axis through the square antiprismatic CeO8 group, are therefore unprotonated.
Formula: Na8[Ce(W5O18)2].30H2O
Acta Cryst. (1998). C54, IUC9800045 [ doi:10.1107/S0108270198099351 ]
Synopsis: The structure is isomorphous with that of the bis(thioselenato) analog, with the Ni atom lying on a center of symmetry.
Formula: (C16H36N)2[Ni(C4N2S2)2]
Acta Cryst. (1998). C54, IUC9800048 [ doi:10.1107/S010827019809934X ]
Synopsis: The title compound consists of discrete neutral complexes with crystallographic C2 symmetry. The Fe-O bond distances are 2.0556 (12) and 2.0937 (13) Å, and the Fe-N bond distance is 2.2290 (16) Å.
Formula: [Fe(C5HF6O2)2(C6H16N2)]
Acta Cryst. (1998). C54, 1195-1197 [ doi:10.1107/S0108270198002856 ]
-Ammonium Vanadium Hydrogen Phosphate,
-(NH4)V(HPO4)2Synopsis:
-(NH4)V(HPO4)2 is a new ammonium vanadium(III) phosphate, built up from a three-dimensional framework of VO6 octahedra and HPO4 tetrahedra.
Formula: (NH4)3V3(HPO4)6
Acta Cryst. (1998). C54, 1197-1200 [ doi:10.1107/S0108270198003667 ]
Synopsis: Triammonium dizinc vanadium bis(phosphate) bis(hydrogen phosphate) is built up from a three-dimensional network of VO6 octahedra and ZnO4, PO4 and HPO4 tetrahedra. NH4+ cations occupy two different interstices in the framework.
Formula: (NH4)3Zn2V(PO4)2(HPO4)2
Acta Cryst. (1998). C54, 1200-1202 [ doi:10.1107/S010827019701994X ]
Synopsis: Tetrasodium titanium nonaoxodiarsenate, Na4TiAs2O9, is built up from infinite [TiO(AsO4)2]n chains linked together by Na+ cations.
Formula: Na4TiAs2O9
Acta Cryst. (1998). C54, 1202-1204 [ doi:10.1107/S0108270197007415 ]
Synopsis: The three-dimensional network structure of this compound comprises VO5 pyramids and (As,V)2O7 groups sharing corners to form puckered layers. The layers are linked to each other by chains of VO6 octahedra. Cs2V3(As0,635V0,365)4O17 is isostructural with Cs2V3P4O17.
Formula: Cs2V3(As0,635V0,365)4O17
Acta Cryst. (1998). C54, 1204-1206 [ doi:10.1107/S0108270198004211 ]
Synopsis: Li3V6O13 is found to be the composition of the phase formed (at 2.45 V versus Li/Li+) on electrochemical lithiation of V6O13; this phase retains the C2/m space group of V6O13.
Formula: Li3V6O13
Acta Cryst. (1998). C54, 1206-1209 [ doi:10.1107/S0108270198003837 ]
Synopsis: In the novel title rubidium antimonate, Sb has both octahedral and trigonal-bipyramidal coordination. These polyhedra build up a network with channels containing Rb, forming a structure similar to that of pyrochlore.
Formula: Rb5Sb7TiO22
Acta Cryst. (1998). C54, 1209-1211 [ doi:10.1107/S0108270198003886 ]
Synopsis: ZnNiP4O12 is composed of cyclic [P4O12] groups forming sheets parallel to the crystallographic (100) plane. These sheets are separated by zigzag chains of alternating NiO6 or ZnO6 octahedra that share a common edge, the cations being statistically disordered.
Formula: ZnNiP4O12
Acta Cryst. (1998). C54, 1211-1214 [ doi:10.1107/S0108270198003035 ]
Synopsis: ErRh2B2C is the end member of the rhodium-based quaternary borocarbides. The structure of ErRh2B2C can be viewed as a layered structure of tetrahedrally coordinated Rh2B2 layers and ErC NaCl-type layers.
Formula: ErRh2B2C
Acta Cryst. (1998). C54, 1214-1217 [ doi:10.1107/S0108270198004223 ]
Synopsis: The tetracalcium dialuminium hydroxide carbonate pentahydrate Ca4Al2(OH)12CO3.5H2O is a layered compound encountered in the chemistry of cement paste. It is composed of positively charged [Ca4Al2(OH)12]2+ main layers and negatively charged [CO3.5H2O]2- interlayers. The Al3+ and Ca2+ ions are six- and sevenfold coordinated, respectively, by O atoms. The planar CO32- groups are directly connected to the main layers and tilted by 21.8 (9)° from the planes formed by these layers.
Formula: Ca4Al2(OH)12CO3.5H2O
Acta Cryst. (1998). C54, 1217-1219 [ doi:10.1107/S010827019800448X ]
Synopsis: V2MnTeO7 is an MnII/VIV tellurite compound which contains slabs of TeO3+1 units, MnO6 octahedra, VO5 square pyramids, and distorted VO6 octahedra.
Formula: V2MnTeO7
Acta Cryst. (1998). C54, 1219-1220 [ doi:10.1107/S010827019800331X ]
Synopsis: CsSbO2 crystallizes in the monoclinic space group C2/c, is isotypic with
NaBiO2 and CsBiO2, and contains infinite
1[SbO2/2O'2/2] chains running parallel to
[001].
Formula: CsSbO2
Acta Cryst. (1998). C54, 1221-1223 [ doi:10.1107/S0108270198003618 ]
Formula: [Cu(C10H9N3)2(C3H5O2)]Cl.H2O
Acta Cryst. (1998). C54, 1223-1225 [ doi:10.1107/S0108270198001917 ]
Formula: [Ni(C5H10NS2)(C28H28P2)]ClO4
Acta Cryst. (1998). C54, 1225-1229 [ doi:10.1107/S0108270198004314 ]
Formula: [CdCl2(CH4N2S)2], [CdBr2(CH4N2S)2] and [CdI2(CH4N2S)2]
Acta Cryst. (1998). C54, 1229-1233 [ doi:10.1107/S0108270198004491 ]
Formula: C16H36N+.CN3O6- and Cs+.CN3O6-
Acta Cryst. (1998). C54, 1233-1236 [ doi:10.1107/S0108270198003898 ]
Formula: [Ce(C5H7O2)3(C12H8N2)] and [Pr(C5H7O2)3(C12H8N2)]
Acta Cryst. (1998). C54, 1236-1238 [ doi:10.1107/S0108270198004673 ]
Formula: [Cu(C9H7NO3)(C7H9N)(H2O)]
Acta Cryst. (1998). C54, 1238-1240 [ doi:10.1107/S0108270198003655 ]
Formula: [MgBr2(C6H15N)(C4H10O)]
Acta Cryst. (1998). C54, 1240-1242 [ doi:10.1107/S0108270198003710 ]
4N]copper(II)Formula: [Cu(ClO4)2(C14H32N4)]
Acta Cryst. (1998). C54, 1242-1244 [ doi:10.1107/S0108270198004533 ]
Formula: [Co(C7H4NO4)2(C6H6N2O)2(H2O)2]
Acta Cryst. (1998). C54, 1244-1247 [ doi:10.1107/S0108270198004521 ]
-methylenebis(dicyclohexylphosphine)-P:P']bis[chloropalladium(I)](Pd-Pd) Diacetonitrile SolvateFormula: [Pd2Cl2(C25H46P2)2].2C2H3N
Acta Cryst. (1998). C54, 1247-1249 [ doi:10.1107/S0108270198004752 ]
5-cyclopentadienyl)bis(1,4-tetraselenido-Se1,Se4)tungstate(IV)Formula: [K(C12H24O6)][W(C5H5)(Se4)2]
Acta Cryst. (1998). C54, 1249-1251 [ doi:10.1107/S0108270198003424 ]
Formula: (C16H36N)2[V2O4(C4H6O3)2].2H2O
Acta Cryst. (1998). C54, 1251-1253 [ doi:10.1107/S0108270198004296 ]
Formula: (C8H20N)[NiWS4(C5H8NS2)]
Acta Cryst. (1998). C54, 1253-1255 [ doi:10.1107/S0108270198003473 ]
Formula: (C4H14N2)[PdBr4]
Acta Cryst. (1998). C54, 1255-1257 [ doi:10.1107/S0108270198004594 ]
-acetato-O:O'] TetrafluoroborateFormula: [Cu(C2H3O2)(NH3)2]BF4
Acta Cryst. (1998). C54, 1257-1259 [ doi:10.1107/S0108270198004065 ]
Formula: 2K+.C3H2O52- and 2NH4+.C3H2O52-
Acta Cryst. (1998). C54, 1259-1261 [ doi:10.1107/S0108270198004375 ]
-Acetato-
-aqua-
-hydroxo-bis[(1,4-dimethyl-1,4,7-triazacyclononane-
3N)copper(II)] DiperchlorateFormula: [Cu2(OH)(C2H3O2)(C8H19N3)2(H2O)](ClO4)2
Acta Cryst. (1998). C54, 1261-1263 [ doi:10.1107/S0108270198003461 ]
-OiPr)2]Formula: [Ti2(C3H7O)6(C9H11O)2]
Acta Cryst. (1998). C54, 1263-1265 [ doi:10.1107/S0108270198003990 ]
Formula: [VO(C26H34N2O2)]
Acta Cryst. (1998). C54, 1265-1268 [ doi:10.1107/S0108270198003163 ]
-N,N'-C10H12N2O8)(
-O)(
-S)Mo2O2].2H2OFormula: Na2[Mo2O3S(C10H12N2O8)].2H2O
Acta Cryst. (1998). C54, 1268-1270 [ doi:10.1107/S0108270198003679 ]
-Acetato Bridge: Bis{(
-acetato)[
-bis(salicylidene)-1,3-propanediaminato](N,N-dimethylformamide)nickel(II)}manganese(II)Formula: [MnNi2(C2H3O2)2(C3H7NO)2(C17H16N2O2)2]
Acta Cryst. (1998). C54, 1270-1273 [ doi:10.1107/S0108270198000183 ]
Formula: [Fe(C7H3NO4)(H2O)3][Fe(C7H3NO4)2].6H2O
Acta Cryst. (1998). C54, 1273-1275 [ doi:10.1107/S0108270198003643 ]
2-
2-disulfido)(
3-sulfido)trimolybdenum(IV)(3 Mo-Mo)DiethyldithiocarbamateFormula: [Mo3S7(C5H10NS2)3](C5H10NS2)
Acta Cryst. (1998). C54, 1275-1277 [ doi:10.1107/S0108270198004545 ]
Formula: [Gd(C2H6OS)8][Fe(CN)6]
Acta Cryst. (1998). C54, 1277-1279 [ doi:10.1107/S0108270198003631 ]
-[2,3,5,6-Tetra-(2-pyridyl)pyrazine]-bis-[bis(acetato)aquanickel(II)]-Formaldehyde (1/1)Formula: [Ni2(C2H3O2)4(C24H16N6)(H2O)2].CH2O
Acta Cryst. (1998). C54, 1279-1280 [ doi:10.1107/S0108270198004739 ]
Formula: [Fe(C10H6NO2)2(H2O)2].2C2H6O.2H2O
Acta Cryst. (1998). C54, 1281-1282 [ doi:10.1107/S0108270198000584 ]
-Chloro-16
-cyano-3-methoxy-14,17
-ethenoestra-1,3,5(10)-trien-17
-yl AcetateFormula: C24H26ClNO3
Acta Cryst. (1998). C54, 1282-1285 [ doi:10.1107/S0108270198004740 ]
-Keto AcidFormula: C7H8O3
Acta Cryst. (1998). C54, 1285-1287 [ doi:10.1107/S0108270198003849 ]
Formula: C14H22O3
Acta Cryst. (1998). C54, 1287-1289 [ doi:10.1107/S010827019800393X ]
Formula: C30H40O12
Acta Cryst. (1998). C54, 1289-1291 [ doi:10.1107/S0108270197017721 ]
Formula: C14H14O7
Acta Cryst. (1998). C54, 1291-1292 [ doi:10.1107/S010827019800314X ]
Formula: C21H23N2O+.I-
Acta Cryst. (1998). C54, 1293-1295 [ doi:10.1107/S0108270198003783 ]
Formula: C10H16O2.0.12C4H10O
Acta Cryst. (1998). C54, 1295-1297 [ doi:10.1107/S0108270198004260 ]
5, 4
5, 6
5, 8
5-tetraphosphazatetraeneFormula: C28H60N12O6P4
Acta Cryst. (1998). C54, 1297-1299 [ doi:10.1107/S0108270198005083 ]
Formula: C14H13NOS2
Acta Cryst. (1998). C54, 1299-1301 [ doi:10.1107/S0108270198003874 ]
Formula: C21H18BrNO2
Acta Cryst. (1998). C54, 1301-1302 [ doi:10.1107/S010827019800479X ]
Formula: C13H13NO3S
Acta Cryst. (1998). C54, 1302-1304 [ doi:10.1107/S0108270198003308 ]
Formula: C10H20O
Acta Cryst. (1998). C54, 1304-1306 [ doi:10.1107/S0108270198003989 ]
Formula: C16H15BrN2O3
Acta Cryst. (1998). C54, 1306-1309 [ doi:10.1107/S0108270196011985 ]
-Hydroxy-
-enamino KetonesFormula: C23H27NO2 and C24H31NO2.H2O
Acta Cryst. (1998). C54, 1309-1312 [ doi:10.1107/S0108270198003540 ]
Formula: C29H44O5.H2O und C29H42O4
Acta Cryst. (1998). C54, 1312-1314 [ doi:10.1107/S010827019800362X ]
Formula: C6H13N2Si+.Br-
Acta Cryst. (1998). C54, 1314-1316 [ doi:10.1107/S0108270198003813 ]
Formula: C20H14ClN3
Acta Cryst. (1998). C54, 1316-1318 [ doi:10.1107/S010827019800345X ]
Formula: C9H9ClN4O2
Acta Cryst. (1998). C54, 1318-1320 [ doi:10.1107/S0108270198003333 ]
Formula: C22H18N2O2
Acta Cryst. (1998). C54, 1320-1322 [ doi:10.1107/S0108270198003436 ]
Formula:
Acta Cryst. (1998). C54, 1322-1324 [ doi:10.1107/S0108270198003977 ]
Formula: C9H10N22+.2Cl-
Acta Cryst. (1998). C54, 1324-1327 [ doi:10.1107/S0108270197004332 ]
Formula: C11H12BF2NO and two forms of C22H24B2F4N2O2
Acta Cryst. (1998). C54, 1327-1329 [ doi:10.1107/S0108270198004387 ]
Formula: C14H24N4
Acta Cryst. (1998). C54, 1330-1331 [ doi:10.1107/S0108270198003175 ]
Formula: C11H9NO3
Acta Cryst. (1998). C54, 1331-1335 [ doi:10.1107/S0108270198004089 ]
N Hydrogen Bonding in the Four Independent Molecules of (2S,4S,5R)-(-)-2-(1H-Imidazol-2-yl)-3,4-dimethyl-5-phenyl-1,3-oxazolidine, with C-H
arene, C-H
O and C-H
C=C InteractionsSynopsis: The title compound is cubic (space group Pa3) and not orthorhombic (space group Pbca) as reported [Azumaya, Kagechika, Yamaguchi & Shudo (1995). Tetrahedron, 51, 5277-5290].
Formula: C14H17N3O
Acta Cryst. (1998). C54, 1335-1341 [ doi:10.1107/S0108270198004508 ]
Formula:
Acta Cryst. (1998). C54, 1341-1343 [ doi:10.1107/S0108270198002881 ]
Formula: C27H33NO2
Acta Cryst. (1998). C54, 1343-1345 [ doi:10.1107/S0108270198003825 ]
Formula: C27H24Cl2N4O2S
Acta Cryst. (1998). C54, 1345-1347 [ doi:10.1107/S0108270198003291 ]
Formula: C16H18ClO2PS
Acta Cryst. (1998). C54, 1347-1351 [ doi:10.1107/S0108270198003734 ]
Formula: C2H10N22+.2C2HO4-.H2O, C3H12N22+.2C2HO4-.H2O and C3H12N22+.2C2HO4-.H2O
Acta Cryst. (1998). C54, 1351-1353 [ doi:10.1107/S0108270198004351 ]
Formula: C15H9Cl5N2O3
Acta Cryst. (1998). C54, 1353-1355 [ doi:10.1107/S0108270198004090 ]
Formula: C22H24N2O6
Acta Cryst. (1998). C54, 1355-1357 [ doi:10.1107/S0108270198003795 ]
Formula: C24H22N3O2P and C24H22N3OPS
Acta Cryst. (1998). C54, 1357-1360 [ doi:10.1107/S010827019800451X ]
Formula: C18H20O2
Acta Cryst. (1998). C54, 1360-1362 [ doi:10.1107/S0108270198004302 ]
Formula: C14H13NO and C19H15NO
Acta Cryst. (1998). C54, 1362-1364 [ doi:10.1107/S010827019800287X ]
Formula: C14H18O7
Acta Cryst. (1998). C54, 1364-1367 [ doi:10.1107/S0108270198000602 ]
Formula: C20H14O2S2 and C22H16O2S2
Acta Cryst. (1998). C54, 1367-1369 [ doi:10.1107/S0108270197019227 ]
Formula: C18H36O2.C6H6N2O
Acta Cryst. (1998). C54, 1369-1372 [ doi:10.1107/S0108270198005204 ]
Formula: C16H14O4
Copyright © International Union of Crystallography
IUCr Webmaster