Acta Crystallographica Section C

Crystal Structure Communications

Volume 54, Part 11 (November 1998)


Cover illustration Cover illustration: An Oxomolybdenum(V) Cluster, \[Mo8O16(OCH3)8(C5H5N)4\], see Modec et al., pages 1573-1575. Displacement ellipsoids are shown at the 30% probability level and H atoms have been omitted for clarity.

cif-access (inorganic compounds)



Acta Cryst. (1998). C54, IUC9800059    [ doi:10.1107/S0108270198099284 ]

Redetermination of Tetrakis(methylammonium) Hexachloroindate Chloride

W. Rothammel, R. Spengler, H. Burzlaff, S. Jarraya and A. Ben Salah

Synopsis: The structure of tetrakis(methylammonium) hexachloroindate chloride, originally determined by Schlimper & Ziegler [Z. Naturforsch. Teil B (1972), 27, 377-379], has been redetermined and compared with the redetermination of Knop et al. [Can. J. Chem. (1987), 65, 1527-1555].

Formula: (CH6N)4[InCl6]Cl



Acta Cryst. (1998). C54, IUC9800061    [ doi:10.1107/S0108270198099272 ]

A New Ammonium Manganese(II) Gallium Phosphate Hydrate: NH4[MnGa2(PO4)3(H2 O)2]

A. M. Chippindale, A. R. Cowley and A. D. Bond

Synopsis: The title compound, ammonium manganese(II) digallium tris(phosphate) dihydrate, consists of GaO5, MnO6 and PO4 polyhedra linked to form a three-dimensional framework containing channels in which the NH4+ cations reside.

Formula: NH4[MnGa2(PO4)3(H2O)2]


cif-access (metal-organic compounds)



Acta Cryst. (1998). C54, IUC9800054    [ doi:10.1107/S0108270198099260 ]

Pentacarbonyl(1,2,3,4-tetracyclohexylcyclotetraphosphane-P)chromium(0), [Cr(CO)5(chexP)4]

A. Deeg and H. Wunderlich

Synopsis: The Cr octahedron is slightly distorted with the bond Cr-C opposite the P atom shortened to 1.845 (2) Å. The geometry of the P4 ring is not influenced by the addition of Cr(CO)5 and the cyclohexyl residues reveal an all-trans configuration.

Formula: [Cr(C24H44P4)(CO)5]



Acta Cryst. (1998). C54, IUC9800058    [ doi:10.1107/S0108270198099259 ]

Chloro[5,10,15,20-tetrakis(pentafluorophenyl)porphinato]iron(III) 0.57-Toluene Solvate

B. Song, D. C. Swenson and H. M. Goff

Synopsis: The title compound was structurally characterized in an attempt to relate molecular structure properties with oxidative catalytic and high-affinity ligand-binding properties.

Formula: [FeCl(C44H8F20N4)].0.57C7H8


cif-access (organic compounds)



Acta Cryst. (1998). C54, IUC9800055    [ doi:10.1107/S0108270198099247 ]

(E)-3,4-Diisopropyl-2,5-dimethylhex-3-ene at 125K

R. Boese, W. R. Roth, D. Bläser, R. Latz and A. Bäumen

Synopsis: The title compound belongs to the family of sterically crowded alkenes. The molecule has a normal C3-C4 double-bond length of 1.3686 (14) Å and the torsion angles around this bond are in good agreement with the results of force-field calculations.

Formula: C16H32



Acta Cryst. (1998). C54, IUC9800056    [ doi:10.1107/S0108270198099235 ]

(±)-(1S)-2-(2-Methyl-1,3-dioxolan-2-yl)-1-[(1S)-2-methylenecyclopropyl]-1-ethyl 4-Nitrobenzoate

R. J. Boffey, J. D. Kilburn and M. Webster

Synopsis: The structure of the p-nitrobenzoate title compound was required for stereochemical assignments of the precursor alcohol which was used in the stereoselective synthesis of the natural product paeonilactone B.

Formula: C17H19NO6



Acta Cryst. (1998). C54, IUC9800057    [ doi:10.1107/S0108270198099223 ]

(1-Methylimidazole-N3)triphenylboron

S. Bélanger and A. L. Beauchamp

Synopsis: The addition compound of 1-methylimidazole with triphenylboron contains an approximately tetrahedrally coordinated B atom, with a B-N distance of 1.628 (5) Å and B-C bond lengths averaging 1.628 Å.

Formula: C22H21BN2



Acta Cryst. (1998). C54, IUC9800060    [ doi:10.1107/S0108270198099211 ]

(3S,4S,4aR,10aS)-5-Acetyl-3,4,4a,5,6,7,10,10a-octahydro-8-methoxy-7-methyl-6-oxo-2H-pyrano[3,2-g]pteridine-3,4-diyl Diacetate

J. N. Low, G. Ferguson, L. M. Dolores, Q. M. Luisa, A. Sánchez, M. Nogueras and J. Cobo

Synopsis: The structure and stereochemistry of the title compound, the enantiomer of the compound reported previously by Low et al. [Acta Cryst. (1995), C51, 2141-2143], are reported.

Formula: C17H22N4O8


inorganic compounds



Acta Cryst. (1998). C54, 1551-1553    [ doi:10.1107/S0108270198007021 ]

Copper-Zinc Oxide Catalysts. VII. Zn(NH3)0.7(H2 O)0.3Cu(CN)3

J. Cernák

Synopsis: The structure of a new Cu-Zn bimetallic compound, poly[ammineaqua-di-[bold mu]2-cyano-[bold mu]3-cyano-copper(I)zinc(II)], is built up of infinite double sheets. Each sheet corresponds to a hexagonal network, with Zn and Cu atoms occupying alternate corners of the hexagons and cyano groups forming the edges. The sheets are connected into pairs by weaker Cu-C bonds completing the trigonal pyramidal coordination geometry of copper(I).

Formula: [ZnCu(CN)3(NH3)0.7(H2O)0.3]



Acta Cryst. (1998). C54, 1554-1556    [ doi:10.1107/S010827019800794X ]

Barium Cobalt Phosphate, BaCo2(PO4)2

Z. Bircsak and W. T. A. Harrison

Synopsis: BaCo2(PO4)2 contains BaO12 polyhedra, CoO6 octahedra and PO4 tetrahedra. Edge-sharing octahedra are a feature of its layered crystal structure which is isostructural with that of BaNi2(AsO4)2.

Formula: BaCo2(PO4)2



Acta Cryst. (1998). C54, 1556-1558    [ doi:10.1107/S0108270198005629 ]

K6[As6V15O42(H2O)].6H2O

G.-Y. Yang, L.-S. Chen, J.-Q. Xu, Y.-F. Li, H.-R. Sun, Z.-W. Pei, Q. Su, Y.-H. Lin, Y. Xing and H.-Q. Jia

Synopsis: The structure determination of K6[As6V15O42(H2O)].6H2O shows the heteropolyanion to have D3 symmetry.

Formula: K6[As6V15O42(H2O)].6H2O



Acta Cryst. (1998). C54, 1558-1561    [ doi:10.1107/S0108270198004855 ]

Inversion Symmetry in the Spin-Peierls Compound [alpha]'-NaV2O5

A. Meetsma, J. L. de Boer, A. Damascelli, J. Jegoudez, A. Revcolevschi and T. T. M. Palstra

Synopsis: Single crystals of NaV2O5 are found to be centrosymmetric. The structure consists of edge- and corner-sharing V2O5 square pyramids. This structure allows only one V position in the asymmetric unit and V is therefore non-integer valent.

Formula: NaV2O5



Acta Cryst. (1998). C54, 1561-1563    [ doi:10.1107/S0108270198007458 ]

Cobalt Lithium Orthoborate, LiCoBO3

Y. Piffard, K. K. Rangan, Y. An, D. Guyomard and M. Tournoux

Synopsis: The structure of cobalt lithium orthoborate, LiCoBO3, is isotypic with those of LiMgBO3, LiMnBO3 and LiZnBO3. It is built up from CoO5 trigonal bipyramids, LiO4 tetrahedra and BO3 planar groups.

Formula: LiCoBO3


metal-organic compounds



Acta Cryst. (1998). C54, 1564-1566    [ doi:10.1107/S0108270198006842 ]

A Cobalt Aluminophosphate with Encapsulated Ethylenediamine: Co0.65Al0.35PO4.0.5NH2.65CH2CH2NH2.65

G. J. Gainsford, K. R. Morgan and A. D. Rae

Synopsis: A cobalt-substituted aluminophosphate, Co0.65Al0.35PO4, with the zeolite gismondine topology encapsulating hydrogen-bonded (O...N) ethylenediamine is reported.

Formula: Co0.65Al0.35PO4.0.5C2H9.3N2



Acta Cryst. (1998). C54, 1566-1569    [ doi:10.1107/S010827019800643X ]

A Linear-Chain Copper(I) Coordination Polymer with Hexakis(methylthio)benzene

Y. Suenaga, T. Kuroda-Sowa, M. Munakata, M. Maekawa and H. Morimoto

Formula: [Cu(C12H18S6)]PF6



Acta Cryst. (1998). C54, 1569-1571    [ doi:10.1107/S0108270198007422 ]

cis-syn-cis-Dicyclohexano-18-crown-6 Sodium Perrhenate

J. C. Bryan

Formula: [NaReO4(C20H36O6)]



Acta Cryst. (1998). C54, 1571-1573    [ doi:10.1107/S0108270198006039 ]

Racemic Phase of Diaquabis(5-oxoprolinato)zinc(II)

A. M. Loireau-Lozach, R. Céolin, X. Solans and M. Font-Bardia

Formula: [Zn(C5H6NO3)2(H2O)2]



Acta Cryst. (1998). C54, 1573-1575    [ doi:10.1107/S0108270198006106 ]

An Oxomolybdenum(V) Cluster, [Mo8O16(OCH3)8(C5H5N)4]

B. Modec, J. V. Brencic, R. Rotar, L. Golic and K. Prout

Formula: [Mo8O16(CH3O)8(C5H5N)4]



Acta Cryst. (1998). C54, 1575-1578    [ doi:10.1107/S0108270198007215 ]

Ferrocenium Tetrachloroferrate Revisited, and Ferrocenium Tetrachloroaluminate

F. A. Cotton, L. M. Daniels and I. Pascual

Formula: [Fe(C5H5)2][FeCl4] and [Fe(C5H5)2][AlCl4]



Acta Cryst. (1998). C54, 1578-1580    [ doi:10.1107/S0108270198006507 ]

Aqua(4,4'-dicarbomethoxy-2,2'-bipyridine-N,N')(3,6-dichloro-4,5-dihydroxy-1,2-benzoquinonato-O4,O5)copper(II) Acetonitrile Hemisolvate

L.-M. Zheng, H. W. Schmalle, S. Ferlay and S. Decurtins

Formula: [Cu(C6Cl2O4)(C14H12N2O4)(H2O)].0.5C2H3N



Acta Cryst. (1998). C54, 1580-1582    [ doi:10.1107/S010827019800571X ]

A New Dinuclear Molybdenum Compound, (Bu4 N)[Mo2(CO)6(SPh)2(CH2CCH3COO)]

G. Pan, B. Zhuang and J. Chen

Formula: (C16H36N)[Mo2(C4H5O2)(C6H5S)2(CO)6]



Acta Cryst. (1998). C54, 1582-1584    [ doi:10.1107/S0108270198005617 ]

(-)-Sparteine Copper(II) Dinitrite

Y.-M. Lee, S.-N. Choi, I.-H. Suh and R. D. Bereman

Formula: [Cu(NO2)2(C15H26N2)]



Acta Cryst. (1998). C54, 1584-1586    [ doi:10.1107/S0108270198006428 ]

cis-(2,2'-Bipyridyl-N,N')carbonyl(methanoato-C)([bold eta]2-2,2':6',2''-terpyridyl-N,N')ruthenium(II) Hexafluorophosphate

D. H. Gibson, B. A. Sleadd, M. S. Mashuta and J. F. Richardson

Formula: [Ru(CHO2)(C10H8N2)(C15H11N3)(CO)]PF6



Acta Cryst. (1998). C54, 1586-1588    [ doi:10.1107/S0108270198006441 ]

Bis(acetato-[bold kappa]2O,O')(di-2-pyridyl-[bold kappa]N-amine)copper(II) Dihydrate

S. Youngme, C. Pakawatchai, H.-K. Fun and K. Chinnakali

Formula: [Cu(C2H3O2)2(C10H9N3)].2H2O



Acta Cryst. (1998). C54, 1588-1590    [ doi:10.1107/S0108270198006921 ]

Metal Alkoxycarboxylate Complexes. I. Poly[aquabis(methoxyacetato)(nitrato)neodymium(III)]

J. T. Mague, A. W. Apblett and E. H. Walker

Formula: [Nd(C3H5O3)2(NO3)(H2O)]



Acta Cryst. (1998). C54, 1590-1592    [ doi:10.1107/S010827019800612X ]

Dichloro(tetrahydrofuran-O)[tris(1-pyrazolyl-N2)borato]vanadium(III)

D. Rehder, H. Gailus and H. Schmidt

Formula: [VCl2(C9H10BN6)(C4H8O)]



Acta Cryst. (1998). C54, 1592-1594    [ doi:10.1107/S010827019800691X ]

Bromotricarbonyl(3,3'-dimethyl-2,2'-biquinoline-N,N')rhenium(I)

J. Guerrero, S. A. Moya, M. T. Garland and R. F. Baggio

Formula: [ReBr(C20H16N2)(CO)3]



Acta Cryst. (1998). C54, 1594-1596    [ doi:10.1107/S0108270198006829 ]

Bis(1-ethyl-3-methylimidazolium) Tetrachloropalladate(II)

M. F. Ortwerth, M. J. Wyzlic and R. G. Baughman

Formula: (C6H11N2)2[PdCl4]



Acta Cryst. (1998). C54, 1596-1600    [ doi:10.1107/S0108270198006398 ]

fac-Tricarbonylchlorobis(pyridine-N)rhenium and fac-Tricarbonylchlorobis(4,4'-bipyridine-N)rhenium

S. Bélanger, J. T. Hupp and C. L. Stern

Formula: [ReCl(C5H5N)2(CO)3] and [ReCl(C10H8N2)2(CO)3]



Acta Cryst. (1998). C54, 1600-1602    [ doi:10.1107/S0108270198004831 ]

An Ethanol-Solvated Copper(II) Complex of 1,3-Bis(2-hydroxybenzylimino)pentane

T.-H. Lu, H.-H. Yao, J.-M. Lo and S.-F. Tung

Formula: 2[Cu(C19H20N2O2)].C2H6O



Acta Cryst. (1998). C54, 1602-1604    [ doi:10.1107/S0108270198002637 ]

A Copper(II) Complex of a Structurally Reinforced Chiral 14-Membered Aza-Macrocycle

Y. Kojima, Y. Seki, S. Yasuda, K. Hirotsu and H. Miyake

Formula: [CuCl(C20H42N4)]ClO4.H2O



Acta Cryst. (1998). C54, 1604-1605    [ doi:10.1107/S0108270198006313 ]

Bis(methyl 3-pyridyl-[bold kappa]N1-carbamate)bis(propionato-[bold kappa]O)copper(II)-Water (4/1)

M. Koman, M. Melník and T. Glowiak

Formula: [Cu(C3H5O2)2(C7H8N2O2)2].0.25H2O



Acta Cryst. (1998). C54, 1605-1607    [ doi:10.1107/S0108270198007240 ]

Dichlorobis(quinoline-N)zinc(II)

Y. Cui, D. Long, W. Chen and J. Huang

Formula: [ZnCl2(C9H7N)2]



Acta Cryst. (1998). C54, 1607-1608    [ doi:10.1107/S010827019800818X ]

Trichlorooxo(triphenylphosphine)(triphenylphosphine oxide)rhenium(V)

J. C. Bryan, M. C. Perry and J. B. Arterburn

Formula: [ReCl3O(C18H15OP)(C18H15P)]



Acta Cryst. (1998). C54, 1609-1612    [ doi:10.1107/S0108270198006945 ]

A [{TiCl2(isodiCp)}2([bold mu]-O)] Dimer and a Twinned Cyclic [TiCl(isodiCp)([bold mu]-O)]4 Tetramer

J. C. Gallucci, N. Kozmina and L. A. Paquette

Formula: [Ti2Cl4O(C10H11)2] and [Ti4Cl4O4(C10H11)4]



Acta Cryst. (1998). C54, 1612-1615    [ doi:10.1107/S010827019800482X ]

A Trinuclear Molybdenum Cluster Coordinated by o-Nitrobenzoate

J.-B. Xia, Y.-G. Yao, L. Wu, X.-Y. Huang and J.-X. Lu

Formula: [Mo3S4(C7H4NO4)(C4H10PS2)3(C5H5N)]



Acta Cryst. (1998). C54, 1615-1616    [ doi:10.1107/S0108270198006519 ]

Hexapotassium [bold mu]-Oxo-bis[(citrato)dioxomolybdenum] Dihydrate

Y.-H. Xing, J.-Q. Xu, H.-R. Sun, D.-M. Li, R.-Z. Wang, T.-G. Wang, W.-M. Bu, L. Ye, G.-D. Yang and Y.-G. Fan

Formula: K6[Mo2O5(C6H4O7)2].2H2O



Acta Cryst. (1998). C54, 1617-1618    [ doi:10.1107/S0108270198005368 ]

Di-[bold mu]-chloro-bis[chloro([bold eta]5-indenyl)methylhafnium(IV)]

R. J. Morris, S. L. Shaw, J. C. Huffman and J. C. Bollinger

Formula: [Hf2Cl4(CH3)2(C9H7)2]



Acta Cryst. (1998). C54, 1618-1622    [ doi:10.1107/S0108270198006209 ]

2:1 Adducts of Halotris(p-tolyl)tin(IV) with 1,9-Bis(4-oxopent-2-en-2-ylamino)-3,7-dithianonane

S. A. Bajue, F. B. Bramwell, C. P. Brock and J. Bontemps

Formula: [Sn2Br2(C7H7)6(C17H30N2O2S2)] and[Sn2I2(C7H7)6(C17H30N2O2S2)]



Acta Cryst. (1998). C54, 1622-1624    [ doi:10.1107/S0108270198006465 ]

(1,1-Dimercaptoethene-2,2-dicarbonitrilato-S,S')bis(triphenylphosphine)palladium(II) Diacetonitrile Solvate

M. Bao, R. Cao, W. Su and M. Hong

Formula: [Pd(C4N2S2)(C18H15P)2].2C2H3N



Acta Cryst. (1998). C54, 1624-1626    [ doi:10.1107/S0108270198008300 ]

Dicyclopentadienyl Complexes of Samarium(III): [Sm([bold eta]5-C5H4SiMe3)2([bold mu]-Cl)]2

M.-R. Spirlet and J. Goffart

Formula: [SmCl2(C8H13Si)4]



Acta Cryst. (1998). C54, 1626-1628    [ doi:10.1107/S0108270198008294 ]

Heavy-Metal [bold pi] Complexes. 13. Trichloro(1,2,3-trimethylbenzene)bismuth(III)

W. Frank and V. Reiland

Formula: [BiCl3(C9H12)]



Acta Cryst. (1998). C54, 1628-1631    [ doi:10.1107/S0108270198008282 ]

1,3-Propanediammonium Tetrachloromercurate

R. Spengler, R. Zouari, H. Zimmermann, A. Ben Salah and H. Burzlaff

Formula: (C3H12N2)[HgCl4]


organic compounds



Acta Cryst. (1998). C54, 1632-1634    [ doi:10.1107/S0108270198007045 ]

5-Ammoniosalicylic Acid Chloride Monohydrate

A. J. Dobson and R. E. Gerkin

Formula: C7H8NO3+.Cl-.H2O



Acta Cryst. (1998). C54, 1634-1637    [ doi:10.1107/S0108270198006416 ]

(4R)-(-)-2-Thioxothiazolidine-4-carboxylic Acid (Raphanusamic Acid)

A. J. Dobson and R. E. Gerkin

Formula: C4H5NO2S2



Acta Cryst. (1998). C54, 1637-1639    [ doi:10.1107/S0108270198007483 ]

1,3,5-Trihydroxybenzene-2,2'-Bipyridyl (1/2): a Hydrogen-Bonded Structure Based on a Stem-and-Leaves Motif

E. S. Lavender, C. Glidewell and G. Ferguson

Formula: C6H6O3.2C10H8N2



Acta Cryst. (1998). C54, 1639-1642    [ doi:10.1107/S0108270198007471 ]

Pairwise-Interlocked Chains in 4,4'-Sulfonyldiphenol-2,2'-Bipyridyl (1/1)

E. S. Lavender, C. Glidewell and G. Ferguson

Formula: C12H10O4S.C10H8N2



Acta Cryst. (1998). C54, 1642-1644    [ doi:10.1107/S0108270197017988 ]

5-Oxo-4-phenyl-1,2,3,4,5,7-hexahydrofuro[3,4-b]-2(1H)-pyridone

J. D. Rodríguez, R. P. Hernández, G. Punte, G. Hechevarría, M. S. Navarro, Y. V. Reyes, E. O. Rodríguez and B. P. Mieres

Formula: C13H11NO3



Acta Cryst. (1998). C54, 1644-1645    [ doi:10.1107/S010827019701799X ]

5-Methoxycarbonyl-6-methyl-4-phenyl-3,4-dihydro-2(1H)-pyridone

J. D. Rodríguez, R. P. Hernández, A. G. González, M. S. Navarro, Y. V. Reyes, E. O. Rodríguez and Y. Mascarenhas

Formula: C14H15NO3



Acta Cryst. (1998). C54, 1645-1647    [ doi:10.1107/S0108270198007410 ]

N-Borane-N-(trimethylsilyl)morpholine

R. Huertas, J. R. Medina, J. A. Soderquist and S. D. Huang

Formula: C7H20BNOSi



Acta Cryst. (1998). C54, 1647-1649    [ doi:10.1107/S0108270198006751 ]

o-Phenylenediamine Pyrocatechol Hemihydrate Complex

S. Goswami, R. Mukherjee, G. D. Nigam, K. Chinnakali and H.-K. Fun

Formula: C6H8N2.C6H6O2.0.5H2O



Acta Cryst. (1998). C54, 1649-1651    [ doi:10.1107/S0108270198007069 ]

Fibleucin from Fibraurea chloroleuca Miers

N. A. Bakhari, S. T. Wah, K. Chinnakali, H.-K. Fun and I. A. Razak

Formula: C20H20O6



Acta Cryst. (1998). C54, 1651-1653    [ doi:10.1107/S0108270198007495 ]

(±)-cis-10-Carboxymethyl-2-decalone: Catemeric Hydrogen Bonding in an [bold epsilon]-Keto Acid

D. Zewge, A. P. J. Brunskill, R. A. Lalancette and H. W. Thompson

Formula: C12H18O3



Acta Cryst. (1998). C54, 1653-1659    [ doi:10.1107/S0108270198006933 ]

Amaryllidaceae Alkaloids: (+)-Tazettine, (+)-3-O-Demethylcriwelline and (+)-3-Epimacronine at 173 K

A. Linden, G. Akineri, S. Noyan, T. Gözler and M. Hesse

Formula: C18H21NO5, C17H19NO5 and C18H19NO5.0.066H2O



Acta Cryst. (1998). C54, 1659-1662    [ doi:10.1107/S0108270198008476 ]

3-(Dimethylamino)-5,6,7,8,9,10-hexahydro-12,13-dimethoxy-4H-spiro[benzo-1-thia-2,5-diazacyclododecene-4,1'-cyclobutan]-6-one 1,1-Dioxide Dichloromethane Solvate (1/1) at 173K

A. Linden, T. R. Mihova and H. Heimgartner

Formula: C20H29N3O5S.CH2Cl2



Acta Cryst. (1998). C54, 1662-1666    [ doi:10.1107/S0108270198006490 ]

Highly Rigid Crown Ether Fragments: Phenyl and Cyclohexyl Catechol Ethers

J. C. Bryan, J. L. Lavis and R. A. Sachleben

Formula: C18H12N2O6, C18H16N2O2 and C18H26O4



Acta Cryst. (1998). C54, 1666-1668    [ doi:10.1107/S0108270198004806 ]

1,4-Bis(imidazol-1-ylmethyl)benzene Dihydrate

B. F. Abrahams, B. F. Hoskins, R. Robson and D. A. Slizys

Formula: C14H14N4.2H2O



Acta Cryst. (1998). C54, 1668-1670    [ doi:10.1107/S0108270198003485 ]

Bis(4-chlorophenyl)(5-pyrimidinyl)methanol

F. Caruso and M. Rossi

Formula: C17H12Cl2N2O



Acta Cryst. (1998). C54, 1670-1672    [ doi:10.1107/S0108270198007306 ]

[beta]-1-N-Benzamido-D-glucopyranose

D. Sriram, S. Srinivasan, K. Priya, V. Aruna and D. Loganathan

Formula: C13H17NO6



Acta Cryst. (1998). C54, 1672-1673    [ doi:10.1107/S0108270198008269 ]

12,12-Ethylenedioxy-8[alpha],9[alpha]-epoxypodocarpan-19-oic Acid

R. C. Cambie, L. H. Mitchell, C. E. F. Rickard and P. S. Rutledge

Formula: C19H28O5



Acta Cryst. (1998). C54, 1673-1675    [ doi:10.1107/S0108270198007811 ]

Intermediates in the Synthesis of (+)-Grandisol. III. (1S,5R)-2,5-Dimethyl-1-(phenylsulfonyl)bicyclo[3.2.0]hept-2-ene

J. Zukerman-Schpector and H. J. Monteiro

Formula: C15H18O2S



Acta Cryst. (1998). C54, 1675-1677    [ doi:10.1107/S0108270198006386 ]

The Antifungal Drug Clotrimazole

H. Song and H.-S. Shin

Formula: C22H17ClN2



Acta Cryst. (1998). C54, 1677-1679    [ doi:10.1107/S0108270198006453 ]

(4S,5R,2'R)-3,4-Dimethyl-1-[2'-(1-naphthyl)-2'-phenylacetyl]-5-phenylimidazolidin-2-one

R. Baggio, G. Lotz, S. Palacios and R. A. Mariezcurrena

Formula: C29H26N2O2



Acta Cryst. (1998). C54, 1679-1681    [ doi:10.1107/S010827019800780X ]

2-(7-Ethylidene-6-methyl-1-oxa-4-thiaspiro[4.5]dec-7-yl)ethanol

M. Parvez, V. K. Yadav and D. A. Jeyaraj

Formula: C13H22O2S



Acta Cryst. (1998). C54, 1681-1683    [ doi:10.1107/S0108270198005460 ]

Methyl N-(tert-Butoxycarbonyl)glycyl-L-valyl-L-tryptophanate

S. Banumathi, D. Velmurugan, E. Subramanian, S. B. Katti and W. Haq

Formula: C24H34N4O6



Acta Cryst. (1998). C54, 1683-1685    [ doi:10.1107/S010827019800403X ]

4-(Dimethylaminomethylene)-2-(2-nitrophenyl)oxazol-5(4H)-one

L. Vijayalakshmi, V. Parthasarathi, P. T. Perumal and V. J. Majo

Formula: C12H11N3O4



Acta Cryst. (1998). C54, 1685-1687    [ doi:10.1107/S010827019800568X ]

Ethyl 5-Ethoxy-3-methyl-1H-indole-2-carboxylate

T. N. Chandrakantha, Puttaraja. Puttaraja, M. K. Kokila and N. C. Shivaprakash

Formula: C14H17NO3



Acta Cryst. (1998). C54, 1687-1689    [ doi:10.1107/S0108270198007434 ]

1,5-Dinitro-1H-indazole

J. Zaleski, Z. Daszkiewicz and J. Kyziol

Formula: C7H4N4O4



Acta Cryst. (1998). C54, 1689-1690    [ doi:10.1107/S0108270198006738 ]

2,3-Dihydrodioxin[2,3-b]acridin-11(6H)-one

J. Karolak-Wojciechowska, A. Mrozek, B. Trzezwinska, S. Morel, J.-P. Galy and J. Barbe

Formula: C15H11NO3



Acta Cryst. (1998). C54, 1691-1693    [ doi:10.1107/S010827019800701X ]

2-(1,2-Dihydro-1-oxophthalazin-2-yl)-4,5-dihydroimidazolium Iodide and 2-(1,2-Dihydro-1-oxophthalazin-2-yl)-4,5,6,7-tetrahydro-1,3-diazepinium Iodide

M. L. Glówka and W. Ksiazek

Formula: C11H11N4O+.I- and C13H15N4O+.I-



Acta Cryst. (1998). C54, 1694-1695    [ doi:10.1107/S0108270198007951 ]

A Bicyclic Cyclopropane Carboxylic Acid Lactone from a Solid-Liquid PTC Reaction

Z. Böcskei, Z. Hell, Z. Finta, L. Toke and K. Simon

Formula: C11H13Cl3O4



Acta Cryst. (1998). C54, 1695-1698    [ doi:10.1107/S0108270198009305 ]

A Triclinic Modification of Triphenylphosphine

H. Kooijman, A. L. Spek, K. J. C. van Bommel, W. Verboom and D. N. Reinhoudt

Formula: C18H15P



Acta Cryst. (1998). C54, 1698-1701    [ doi:10.1107/S0108270198004399 ]

Quininium Hydrogen (S,S)-Tartrate Hemihydrate, a Salt with a Unique Conformation of the Hydrogen Tartrate Ion

C. Ryttersgaard and S. Larsen

Formula: 2C20H25N2O2+.2C4H5O6-.H2O



Acta Cryst. (1998). C54, 1701-1703    [ doi:10.1107/S0108270198005046 ]

N,N'-Bis(5-bromo-2-hydroxybenzylidene)-1,3-propanediamine

Y. Elerman, A. Elmali, M. Kabak and I. Svoboda

Formula: C17H16Br2N2O2



Acta Cryst. (1998). C54, 1703-1705    [ doi:10.1107/S0108270198005666 ]

2,4-Cl2-6,9-exo,endo-(PMe2Ph)2-arachno-B10H10

U. Dörfler, T. D. McGrath, P. A. Cooke, J. D. Kennedy and M. Thornton-Pett

Formula: C16H32B10Cl2P2



Acta Cryst. (1998). C54, 1705-1707    [ doi:10.1107/S0108270198005939 ]

(1R,7S,8aS)-1,7-Dihydroxyindolizidine Hydrate

L. Garofano, A. Guerri and P. Orioli

Formula: C8H15NO2.H2O



Acta Cryst. (1998). C54, 1707-1710    [ doi:10.1107/S0108270198007203 ]

Polysulfonylamines. CVI. 1,4,7,10,13,16-Hexaoxacyclooctadecane-Dimethyl Sulfoxide-Bis(4-fluorophenylsulfonyl)amine (1/2/2)

K. Wijaya, O. Moers, A. Blaschette and P. G. Jones

Formula: C12H24O6.2C2H6OS.2C12H9F2NO4S2



Acta Cryst. (1998). C54, 1710-1712    [ doi:10.1107/S0108270198006957 ]

L'Anhydride cis-1,2,3,6-Tétrahydrophtalique

A. Ben Fredj, S. Ben Redjeb, F. Ben Amor et A. Driss

Formula: C8H8O3



Acta Cryst. (1998). C54, 1712-1714    [ doi:10.1107/S0108270198005216 ]

N-tert-Butyl-N-(1-dibenzylphosphono-2,2-dimethylpropyl)nitroxide

S. Grimaldi, D. Siri, J.-P. Finet and P. Tordo

Formula: C23H33NO4P



Acta Cryst. (1998). C54, 1714-1716    [ doi:10.1107/S0108270198005472 ]

13,13-Ethylenedithio-3-mesyloxy-18-nor-13,17-secoestra-1,3,5(10)-triene-17-nitrile

A. Kuhl, M. Schürmann, H. Preut and W. Kreiser

Formula: C20H25NO3S3



Acta Cryst. (1998). C54, 1716-1718    [ doi:10.1107/S0108270198007264 ]

1-(2-Mercaptoethyl)-2-methyl-1,2-dicarba-closo-dodecaborane(12)

R. Kivekäs, J. Pedrajas, F. Teixidor and R. Sillanpää

Formula: C5H18B10S



Acta Cryst. (1998). C54, 1718-1720    [ doi:10.1107/S010827019800729X ]

(S)-N-Triphenylmethylpyroglutamyl Fluoride

V. Nastopoulos, G. Karigiannis, P. Mamos, D. Papaioannou and C. Kavounis

Formula: C24H20FNO2



Acta Cryst. (1998). C54, 1720-1722    [ doi:10.1107/S0108270198004727 ]

Photochromic Properties of Spiro[fluorene-chromenes]

S. Aldoshin, I. Chuev, O. Filipenko, J. L. Pozzo, V. Lokshin and G. Pèpe

Formula: C25H16O and C28H22O2



Acta Cryst. (1998). C54, 1722-1724    [ doi:10.1107/S0108270198007252 ]

A Water Adduct of Tris(pentafluorophenyl)borane: (C6F5)3B(OH2)-Dioxane-CH2Cl2 (1/1/1)

C. Janiak, L. Braun, T. G. Scharmann and F. Girgsdies

Formula: [B(C6H5)3(H2O)].C4H8O2.CH2Cl2



Acta Cryst. (1998). C54, 1724-1727    [ doi:10.1107/S010827019800849X ]

1,5-Diphenylbicyclo[2.2.1]hept-5-ene-endo-2,endo-3-dicarboxylic Anhydride and 1,5-diphenylbicyclo[2.2.1]hept-5-ene-exo-2,exo-3-dicarboxylic Anhydride

A. Pajunen and M. Kokko

Formula: C21H16O3


addenda and errata



Acta Cryst. (1998). C54, 1728    [ doi:10.1107/S0108270198018538 ]

Three Intermediates in the Synthesis of Chrysanthemic Acid. Erratum

G. Baudoux, B. Norberg, L. Provins, A. Froidbise, A. Krief and G. Evrard

Synopsis: Erratum to Acta Cryst. (1998), C54, 834-837.

Formula: C14H23NO8



Acta Cryst. (1998). C54, 1728    [ doi:10.1107/S010827019801854X ]

[alpha]-Naphthyl Phenyl Pinacols. Erratum

T. C. W. Mak, B. O. Patrick, S. J. Rettig, J. R. Scheffer, J. Trotter, P. Ukpabi, B.-M. Wu and V. C. Yee

Synopsis: Erratum to Acta Cryst. (1998), C54, 1148-1151.

Formula: C34H26O2



Acta Cryst. (1998). C54, 1728    [ doi:10.1107/S010827019809920X ]

Cover Illustration. Vol. C54, Part 9. Erratum

S.R. Hall

Synopsis: Erratum to Cover Illustration Acta Cryst. C54, Part 9.


Copyright © International Union of Crystallography
IUCr Webmaster