# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_98kcm5 _shelx_title ' 98KCM5' _shelx_refln_list_code 4 _shelx_F_calc_maximum 259.36 _exptl_crystal_F_000 864.00 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5240.07 5166.48 59.90 o 2 0 0 6901.21 6746.26 84.53 o 3 0 0 5.41 8.96 34.71 o 4 0 0 227.58 207.69 21.83 o 5 0 0 42.79 106.36 25.19 o 6 0 0 5803.96 5659.11 81.17 o 7 0 0 1650.81 1604.41 47.02 o 8 0 0 1966.41 1907.83 54.30 o 9 0 0 2025.09 2069.61 56.54 o 10 0 0 799.26 751.82 48.14 o 11 0 0 534.15 577.16 49.82 o -11 1 0 295.31 148.35 78.93 o -10 1 0 2819.23 2745.30 67.74 o -9 1 0 546.47 581.08 44.22 o -8 1 0 2000.68 2027.07 55.98 o -7 1 0 5357.83 5313.71 80.61 o -6 1 0 819.98 710.40 35.83 o -5 1 0 4052.77 4155.46 61.02 o -4 1 0 197.46 148.35 21.83 o -3 1 0 4030.48 4312.21 59.90 o -2 1 0 13.92 6.72 27.43 o -1 1 0 10872.48 11541.02 127.64 o 1 1 0 8009.87 7674.42 86.21 o 2 1 0 4518.67 4462.24 62.14 o 3 1 0 4394.44 4335.72 61.58 o 4 1 0 5187.29 5209.58 72.78 o 5 1 0 1897.04 1795.31 38.07 o 6 1 0 6173.15 6221.72 89.01 o 7 1 0 81.32 69.98 57.10 o 8 1 0 1094.76 1058.60 47.02 o 9 1 0 417.07 503.27 42.55 o 10 1 0 444.39 458.48 46.46 o 11 1 0 213.87 278.78 47.58 o -11 2 0 423.84 380.67 51.50 o -10 2 0 20.23 18.47 73.89 o -9 2 0 2256.68 2234.20 60.46 o -8 2 0 320.94 296.14 41.43 o -7 2 0 4891.54 4819.96 77.81 o -6 2 0 10029.11 9929.33 142.75 o -5 2 0 1873.06 1838.97 40.31 o -4 2 0 1300.77 1326.75 33.59 o -3 2 0 3928.28 4009.35 55.98 o -2 2 0 1668.21 1715.25 27.99 o -1 2 0 145.29 137.15 12.88 o 0 2 0 171.13 190.11 7.13 o 1 2 0 40.93 5.04 19.59 o 2 2 0 4572.15 4610.59 62.70 o 3 2 0 2825.11 2705.56 39.75 o 4 2 0 363.49 323.57 22.39 o 5 2 0 81.11 44.22 43.11 o 6 2 0 714.87 703.12 33.59 o 7 2 0 2252.33 2258.83 51.50 o 8 2 0 66.55 75.01 63.26 o 9 2 0 2745.72 2722.91 62.70 o 10 2 0 4489.49 4563.56 85.09 o 11 2 0 221.19 77.25 80.61 o 12 2 0 44.08 117.00 78.93 o -10 3 0 688.36 676.25 50.38 o -9 3 0 10.37 16.79 67.18 o -8 3 0 772.42 777.57 45.90 o -7 3 0 7389.02 7278.64 103.56 o -6 3 0 50.89 54.30 58.22 o -5 3 0 1419.46 1421.35 40.31 o -4 3 0 1481.43 1404.00 38.07 o -3 3 0 0.01 10.64 41.99 o -2 3 0 2273.95 2406.06 35.27 o -1 3 0 17460.95 18454.10 208.81 o 0 3 0 54.71 67.62 26.31 o 1 3 0 230.55 272.07 16.79 o 2 3 0 10804.34 11110.53 136.59 o 3 3 0 1033.05 885.62 26.31 o 4 3 0 265.97 208.81 21.83 o 5 3 0 324.45 249.11 29.11 o 6 3 0 658.93 682.41 33.59 o 7 3 0 176.13 261.99 35.83 o 8 3 0 4010.21 3924.82 71.66 o 9 3 0 330.27 306.22 42.55 o 10 3 0 383.88 408.10 45.34 o 11 3 0 2583.40 2463.16 69.42 o 12 3 0 149.22 138.27 49.26 o -10 4 0 130.61 131.56 79.49 o -9 4 0 332.62 406.42 44.78 o -8 4 0 1035.25 1067.00 48.70 o -7 4 0 0.94 98.53 66.06 o -6 4 0 117.07 82.29 62.14 o -5 4 0 1361.01 1363.13 43.67 o -4 4 0 17.07 11.76 47.02 o -3 4 0 4655.30 5003.57 70.54 o -2 4 0 2523.82 2696.04 39.19 o -1 4 0 1183.83 1363.13 26.87 o 0 4 0 79.48 77.30 14.05 o 1 4 0 7183.49 7117.97 94.61 o 2 4 0 1403.68 1593.22 28.55 o 3 4 0 23890.82 24292.91 273.19 o 4 4 0 8316.25 8135.70 111.40 o 5 4 0 1509.12 1514.28 38.63 o 6 4 0 1810.36 1813.22 44.78 o 7 4 0 362.98 327.49 37.51 o 8 4 0 1148.18 1163.28 47.58 o 9 4 0 4413.49 4435.93 80.05 o 10 4 0 2443.67 2551.05 64.38 o 11 4 0 130.97 18.47 73.89 o 12 4 0 1490.40 1634.64 64.38 o -10 5 0 16.43 19.59 78.93 o -9 5 0 1.51 87.33 72.22 o -8 5 0 206.34 157.87 43.67 o -7 5 0 758.78 863.23 47.02 o -6 5 0 1529.07 1585.94 51.50 o -5 5 0 147.67 241.84 38.07 o -4 5 0 3295.41 3365.57 58.78 o -3 5 0 24.28 11.76 46.46 o -2 5 0 157.15 143.31 22.39 o -1 5 0 8870.38 9716.60 134.35 o 0 5 0 9747.67 10618.86 136.31 o 1 5 0 62.83 45.34 40.31 o 2 5 0 16587.53 18079.59 214.97 o 3 5 0 8856.58 8608.74 114.76 o 4 5 0 2145.41 2407.74 46.46 o 5 5 0 2294.24 2046.66 43.67 o 6 5 0 2.39 14.00 54.86 o 7 5 0 115.75 124.84 37.51 o 8 5 0 1748.97 1817.70 53.74 o 9 5 0 2864.66 2964.19 66.06 o 10 5 0 17.83 76.69 68.86 o 11 5 0 677.23 652.74 52.06 o -9 6 0 210.21 238.48 48.14 o -8 6 0 784.00 782.05 49.26 o -7 6 0 107.35 116.44 69.42 o -6 6 0 1.64 16.23 65.50 o -5 6 0 2028.58 2022.03 55.42 o -4 6 0 7.27 40.31 58.78 o -3 6 0 1845.89 1814.34 46.46 o -2 6 0 1688.95 1401.20 32.47 o -1 6 0 1041.66 1153.21 29.11 o 0 6 0 590.96 565.25 17.80 o 1 6 0 3818.88 4170.02 58.78 o 2 6 0 1979.28 2277.30 38.07 o 3 6 0 1152.81 1033.97 35.27 o 4 6 0 5655.95 5750.36 80.61 o 5 6 0 41.27 12.88 52.06 o 6 6 0 3008.97 3104.70 60.46 o 7 6 0 1920.88 1894.39 52.62 o 8 6 0 8.77 16.79 67.18 o 9 6 0 81.39 17.35 68.86 o 10 6 0 211.99 310.69 44.22 o 11 6 0 30.67 19.03 75.57 o -8 7 0 133.75 19.59 78.37 o -7 7 0 2330.45 2531.46 66.06 o -6 7 0 1922.63 1878.72 57.66 o -5 7 0 444.93 476.40 45.34 o -4 7 0 4002.46 3955.05 71.66 o -3 7 0 2450.96 2233.08 54.30 o -2 7 0 562.41 574.92 31.35 o -1 7 0 5389.06 5580.17 78.93 o 0 7 0 62.73 86.46 47.30 o 1 7 0 4330.52 4340.20 60.46 o 2 7 0 6096.32 6174.69 86.21 o 3 7 0 20.69 12.88 50.94 o 4 7 0 98.76 77.25 57.66 o 5 7 0 2941.06 3016.25 58.22 o 6 7 0 1236.86 1259.01 47.02 o 7 7 0 87.45 99.65 66.62 o 8 7 0 807.55 738.39 47.58 o 9 7 0 284.76 297.82 44.22 o 10 7 0 121.31 122.04 73.33 o 11 7 0 48.68 47.02 78.93 o -8 8 0 1616.93 1675.51 66.62 o -7 8 0 171.35 194.81 48.70 o -6 8 0 924.43 828.52 50.94 o -5 8 0 1741.82 1845.13 56.54 o -4 8 0 348.32 281.02 44.22 o -3 8 0 405.17 428.25 44.78 o -2 8 0 5949.00 6268.18 89.01 o -1 8 0 337.23 378.99 31.91 o 0 8 0 1669.75 1692.31 28.07 o 1 8 0 787.34 853.71 33.59 o 2 8 0 228.36 157.31 38.07 o 3 8 0 45.79 80.61 60.46 o 4 8 0 495.27 524.54 40.87 o 5 8 0 43.01 15.67 62.70 o 6 8 0 76.28 37.51 68.86 o 7 8 0 2187.39 2197.81 57.66 o 8 8 0 1217.42 1343.54 52.62 o 9 8 0 0.22 17.91 70.54 o 10 8 0 407.89 386.83 49.26 o 11 8 0 435.87 468.00 53.74 o -7 9 0 180.56 241.84 51.50 o -6 9 0 65.12 38.63 75.01 o -5 9 0 954.65 965.67 50.94 o -4 9 0 199.95 104.68 72.22 o -3 9 0 719.06 639.86 48.14 o -2 9 0 376.88 329.73 37.51 o -1 9 0 243.36 253.59 35.83 o 0 9 0 2024.61 2104.30 32.24 o 1 9 0 75.26 16.79 68.30 o 2 9 0 871.60 815.64 45.34 o 3 9 0 1250.80 1264.05 49.26 o 4 9 0 2214.90 2230.28 56.54 o 5 9 0 4.07 117.56 67.18 o 6 9 0 2186.99 2257.71 59.34 o 7 9 0 345.91 270.39 45.34 o 8 9 0 1637.08 1713.02 56.54 o 9 9 0 910.89 1009.90 52.62 o 10 9 0 12.48 20.15 79.49 o -6 10 0 325.82 353.24 51.50 o -5 10 0 588.68 576.04 51.50 o -4 10 0 26.17 82.29 72.78 o -3 10 0 116.73 216.09 44.22 o -2 10 0 93.04 72.22 71.10 o -1 10 0 808.80 807.24 40.87 o 0 10 0 9.44 18.19 51.66 o 1 10 0 5791.06 5765.47 82.29 o 2 10 0 1435.76 1430.31 54.86 o 3 10 0 3.18 17.91 72.22 o 4 10 0 693.51 764.70 48.14 o 5 10 0 873.89 856.51 49.26 o 6 10 0 27.23 81.73 71.10 o 7 10 0 1982.28 1971.65 59.34 o 8 10 0 1596.36 1670.47 59.90 o 9 10 0 838.57 822.92 55.42 o 10 10 0 411.33 408.10 54.30 o -5 11 0 201.32 85.65 86.21 o -4 11 0 396.66 285.50 50.94 o -3 11 0 1837.49 1805.94 61.58 o -2 11 0 646.24 663.37 41.99 o -1 11 0 139.81 53.18 76.13 o 0 11 0 628.37 721.57 28.70 o 1 11 0 1061.42 1128.57 43.67 o 2 11 0 834.14 820.68 50.94 o 3 11 0 1291.22 1283.64 53.18 o 4 11 0 876.60 874.42 49.26 o 5 11 0 3058.52 2970.91 67.74 o 6 11 0 4263.97 4178.41 81.17 o 7 11 0 306.30 234.56 48.70 o 8 11 0 652.43 628.67 53.74 o 9 11 0 303.18 267.03 52.62 o -4 12 0 910.18 836.91 58.22 o -3 12 0 162.18 53.74 85.65 o -2 12 0 414.49 414.82 44.78 o -1 12 0 622.58 671.77 43.11 o 0 12 0 601.37 593.87 54.86 o 1 12 0 3276.62 3271.52 63.26 o 2 12 0 1022.42 957.83 54.30 o 3 12 0 335.50 335.89 48.70 o 4 12 0 957.63 894.01 54.30 o 5 12 0 604.25 549.17 52.06 o 6 12 0 20.70 19.03 75.57 o 7 12 0 192.69 168.50 49.26 o 8 12 0 220.83 212.73 52.62 o -2 13 0 52.95 21.83 86.77 o -1 13 0 932.10 963.43 51.50 o 0 13 0 2291.76 2330.04 66.06 o 1 13 0 778.08 788.77 47.58 o 2 13 0 105.18 91.81 80.05 o 3 13 0 541.22 559.25 52.06 o 4 13 0 97.23 137.15 50.94 o 5 13 0 88.11 133.23 49.26 o 6 13 0 517.44 507.75 55.98 o 7 13 0 115.46 193.69 50.94 o 0 14 0 119.37 138.32 63.30 o 1 14 0 8.54 22.95 91.81 o 2 14 0 35.84 22.95 90.69 o 3 14 0 46.81 21.83 86.77 o 4 14 0 2455.22 2233.08 73.89 o 5 14 0 632.07 597.32 59.34 o -3 -14 1 780.08 857.07 61.02 o -2 -14 1 365.43 382.35 57.66 o -6 -13 1 2.01 110.28 81.17 o -5 -13 1 411.66 329.73 54.86 o -4 -13 1 1853.54 1682.23 66.62 o -3 -13 1 358.62 415.94 52.62 o -2 -13 1 196.84 162.90 83.97 o -1 -13 1 902.55 878.34 49.82 o 0 -13 1 4.65 20.99 58.96 o 1 -13 1 534.73 638.18 48.14 o 2 -13 1 378.68 333.65 49.82 o -8 -12 1 294.85 288.30 53.74 o -7 -12 1 176.39 75.57 51.50 o -6 -12 1 1396.10 1216.46 60.46 o -5 -12 1 87.22 155.63 47.58 o -4 -12 1 2.77 19.59 78.37 o -3 -12 1 550.06 501.03 50.94 o -2 -12 1 1304.58 1200.79 57.66 o -1 -12 1 200.14 20.15 81.73 o 0 -12 1 3783.40 3857.69 59.34 o 1 -12 1 1778.98 1846.81 53.18 o 2 -12 1 0.76 49.82 82.29 o 3 -12 1 24.75 112.52 82.29 o -9 -11 1 1593.96 1772.91 66.06 o -8 -11 1 377.84 348.20 53.18 o -7 -11 1 1604.59 1470.06 58.78 o -6 -11 1 330.64 387.95 47.58 o -5 -11 1 184.34 19.59 78.37 o -4 -11 1 2369.84 2320.41 63.26 o -3 -11 1 771.99 752.94 49.82 o -2 -11 1 977.20 967.91 52.62 o -1 -11 1 2915.31 2913.25 58.78 o 0 -11 1 117.84 97.89 33.74 o 1 -11 1 1032.31 1000.94 44.22 o 2 -11 1 2061.23 2122.80 54.30 o 3 -11 1 173.24 158.43 47.02 o 4 -11 1 475.27 466.32 51.50 o 5 -11 1 1668.85 1386.09 64.94 o -10 -10 1 129.95 51.50 84.53 o -9 -10 1 23.80 19.59 77.81 o -8 -10 1 1620.04 1655.91 60.46 o -7 -10 1 289.33 338.12 45.90 o -6 -10 1 4752.63 4639.70 84.53 o -5 -10 1 3440.45 3329.74 69.98 o -4 -10 1 32.06 57.66 70.54 o -3 -10 1 409.51 390.19 47.02 o -2 -10 1 784.21 749.02 49.82 o -1 -10 1 21.28 18.47 73.33 o 0 -10 1 2863.61 2829.60 39.78 o 1 -10 1 2509.51 2577.92 54.86 o 2 -10 1 160.58 140.51 36.39 o 3 -10 1 1585.37 1523.24 56.54 o 4 -10 1 137.11 129.88 74.45 o 5 -10 1 84.51 125.40 78.37 o 6 -10 1 0.74 20.15 80.05 o -10 -9 1 351.65 386.83 52.62 o -9 -9 1 240.68 315.17 47.58 o -8 -9 1 808.23 766.38 50.94 o -7 -9 1 3784.77 3685.22 73.89 o -6 -9 1 115.95 120.92 71.10 o -5 -9 1 1047.50 1110.10 48.70 o -4 -9 1 445.60 389.63 44.78 o -3 -9 1 348.88 340.36 44.22 o -2 -9 1 521.92 577.16 45.34 o -1 -9 1 2281.65 2306.97 48.14 o 0 -9 1 2133.02 2167.53 34.41 o 1 -9 1 1543.89 1535.56 45.34 o 2 -9 1 296.75 272.07 36.95 o 3 -9 1 123.05 100.21 70.54 o 4 -9 1 75.94 118.68 42.55 o 5 -9 1 5.75 57.66 73.89 o 6 -9 1 291.23 374.51 47.58 o 7 -9 1 28.28 20.71 83.41 o -11 -8 1 748.06 717.12 57.10 o -10 -8 1 17.45 19.03 75.57 o -9 -8 1 1387.11 1446.55 56.54 o -8 -8 1 2019.12 1934.14 58.22 o -7 -8 1 20.30 16.79 67.18 o -6 -8 1 1326.96 1344.10 50.94 o -5 -8 1 2472.73 2513.54 58.78 o -4 -8 1 421.84 432.73 40.31 o -3 -8 1 870.17 811.72 43.11 o -2 -8 1 1866.13 1916.23 51.50 o -1 -8 1 173.10 85.09 66.06 o 0 -8 1 69.43 36.43 44.86 o 1 -8 1 583.00 602.91 33.59 o 2 -8 1 0.37 16.23 65.50 o 3 -8 1 2066.29 2047.78 56.54 o 4 -8 1 3957.04 3887.87 73.33 o 5 -8 1 837.53 915.29 48.70 o 6 -8 1 201.48 217.21 45.34 o 7 -8 1 209.44 291.66 48.70 o 8 -8 1 26.63 21.27 85.09 o -11 -7 1 217.16 148.91 82.85 o -10 -7 1 7.95 17.91 72.78 o -9 -7 1 0.59 52.62 69.98 o -8 -7 1 492.15 508.87 44.22 o -7 -7 1 702.33 696.40 45.90 o -6 -7 1 4513.90 4557.40 76.13 o -5 -7 1 101.32 117.00 36.39 o -4 -7 1 1689.07 1679.99 47.58 o -3 -7 1 561.89 470.24 35.83 o -2 -7 1 478.45 509.99 28.55 o -1 -7 1 495.35 463.52 27.99 o 0 -7 1 6661.25 7190.37 71.25 o 1 -7 1 154.47 120.36 27.99 o 2 -7 1 3792.72 3768.07 57.10 o 3 -7 1 7645.47 7639.71 108.04 o 4 -7 1 0.41 16.79 67.18 o 5 -7 1 2651.71 2808.00 64.38 o 6 -7 1 374.87 406.42 44.22 o 7 -7 1 16.58 18.47 74.45 o 8 -7 1 2196.88 2205.09 66.62 o -11 -6 1 897.07 871.62 55.98 o -10 -6 1 3.69 17.91 72.22 o -9 -6 1 75.20 17.35 68.86 o -8 -6 1 96.00 126.52 40.87 o -7 -6 1 2319.46 2225.80 56.54 o -6 -6 1 163.51 36.39 61.02 o -5 -6 1 3796.96 3844.77 64.38 o -4 -6 1 1414.15 1421.91 40.87 o -3 -6 1 5089.62 4816.60 68.86 o -2 -6 1 4607.06 4552.37 66.62 o -1 -6 1 619.45 595.08 26.87 o 0 -6 1 90.99 113.37 16.42 o 1 -6 1 4897.29 5055.07 71.10 o 2 -6 1 79.09 83.97 25.19 o 3 -6 1 1064.50 1141.45 41.99 o 4 -6 1 3877.56 3736.72 67.18 o 5 -6 1 430.32 586.68 44.22 o 6 -6 1 1733.03 1782.99 54.86 o 7 -6 1 1084.63 1154.89 52.62 o 8 -6 1 348.97 343.72 47.02 o 9 -6 1 80.10 195.37 48.70 o -11 -5 1 8.62 106.92 75.01 o -10 -5 1 215.43 269.83 44.78 o -9 -5 1 1383.59 1425.83 52.06 o -8 -5 1 287.37 323.57 41.99 o -7 -5 1 214.94 254.71 38.07 o -6 -5 1 3073.83 3178.59 59.34 o -5 -5 1 372.16 391.31 33.03 o -4 -5 1 3093.25 2861.74 50.38 o -3 -5 1 5767.26 5650.15 78.93 o -2 -5 1 4.53 11.76 46.46 o -1 -5 1 3980.39 3781.51 52.62 o 0 -5 1 821.09 840.30 17.81 o 1 -5 1 2627.76 2822.56 41.43 o 2 -5 1 3529.16 3681.86 51.50 o 3 -5 1 7255.50 7621.24 106.36 o 4 -5 1 545.71 598.44 36.95 o 5 -5 1 480.81 540.78 40.31 o 6 -5 1 35.79 36.39 67.18 o 7 -5 1 261.78 242.96 43.11 o 8 -5 1 103.40 122.04 43.11 o 9 -5 1 45.72 88.45 75.57 o 10 -5 1 254.23 147.23 86.21 o -12 -4 1 3.47 19.59 77.81 o -11 -4 1 647.68 695.28 50.94 o -10 -4 1 113.73 17.35 70.54 o -9 -4 1 1391.40 1415.76 52.62 o -8 -4 1 4820.02 4770.13 80.05 o -7 -4 1 1721.33 1785.79 49.26 o -6 -4 1 875.22 852.59 38.63 o -5 -4 1 1572.20 1482.37 38.07 o -4 -4 1 1193.46 1121.86 34.71 o -3 -4 1 799.07 679.61 25.75 o -2 -4 1 11935.54 12819.06 160.11 o -1 -4 1 168.90 239.04 19.59 o 0 -4 1 1410.03 1537.52 20.19 o 1 -4 1 2309.40 2337.20 34.15 o 2 -4 1 4520.52 5222.46 74.45 o 3 -4 1 1420.83 1590.42 39.75 o 4 -4 1 468.44 452.33 32.47 o 5 -4 1 185.19 105.24 60.46 o 6 -4 1 101.76 153.95 37.51 o 7 -4 1 3568.77 3484.25 70.54 o 8 -4 1 5.29 64.94 64.38 o 9 -4 1 35.07 17.35 69.42 o 10 -4 1 3.16 72.22 75.57 o -12 -3 1 1091.20 1085.47 59.90 o -11 -3 1 81.09 151.71 77.81 o -10 -3 1 2544.54 2628.30 65.50 o -9 -3 1 4066.44 3946.65 75.01 o -8 -3 1 22.10 16.23 64.38 o -7 -3 1 1407.92 1426.39 45.34 o -6 -3 1 2259.99 2460.36 49.82 o -5 -3 1 0.47 27.99 45.90 o -4 -3 1 6542.33 6423.81 89.01 o -3 -3 1 9463.18 9734.52 128.20 o -2 -3 1 1018.53 1055.80 23.51 o -1 -3 1 2496.02 2406.06 34.71 o 0 -3 1 3666.05 3655.59 36.02 o 1 -3 1 562.15 485.91 20.15 o 2 -3 1 452.43 462.40 20.71 o 3 -3 1 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