# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_xx13 _shelx_title ' xx13 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 260.62 _exptl_crystal_F_000 804.00 _reflns_d_resolution_high 0.7697 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.1952 _cell_length_b 10.2164 _cell_length_c 19.3172 _cell_angle_alpha 75.501 _cell_angle_beta 74.862 _cell_angle_gamma 64.474 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 13683.86 15099.35 783.43 o 2 0 0 56686.66 57803.74 1696.54 o 3 0 0 6807.98 6905.76 221.56 o 4 0 0 606.09 655.75 42.71 o 5 0 0 15.47 24.06 12.82 o 6 0 0 3507.38 3754.86 135.69 o 7 0 0 2947.42 3078.36 207.40 o 8 0 0 2092.26 2079.96 66.71 o 9 0 0 2263.61 2342.08 74.72 o 10 0 0 3748.04 3978.56 221.16 o 11 0 0 1591.97 1516.44 119.88 o -11 1 0 575.58 507.39 77.60 o -10 1 0 1821.18 1598.00 119.89 o -9 1 0 2477.23 2532.39 156.26 o -8 1 0 2151.72 2199.59 69.51 o -7 1 0 2875.00 2956.88 84.20 o -6 1 0 7583.18 7506.82 178.41 o -5 1 0 2767.57 2790.20 82.79 o -4 1 0 2380.58 2516.10 71.72 o -3 1 0 124.84 136.25 17.55 o -2 1 0 49.66 57.69 18.70 o -1 1 0 1551.03 1781.27 123.47 o 0 1 0 33899.65 37768.49 1536.56 o 1 1 0 39747.77 45939.71 1953.29 o 2 1 0 10088.07 9691.18 440.99 o 3 1 0 3944.91 3893.23 130.00 o 4 1 0 1820.89 1855.84 99.68 o 5 1 0 1953.76 1975.31 79.66 o 6 1 0 12.87 19.66 21.25 o 7 1 0 1863.57 1941.50 85.10 o 8 1 0 980.70 951.21 68.24 o 9 1 0 1601.44 1535.25 56.95 o 10 1 0 2595.61 2701.07 85.12 o 11 1 0 2073.68 2082.39 87.18 o 12 1 0 1451.56 1427.34 119.40 o -10 2 0 1544.12 1437.13 116.56 o -9 2 0 2124.11 2095.38 140.32 o -8 2 0 3895.77 4283.07 226.90 o -7 2 0 1451.58 1385.76 100.66 o -6 2 0 7802.00 7683.28 182.69 o -5 2 0 3397.91 3543.60 183.45 o -4 2 0 1862.44 1918.87 47.41 o -3 2 0 70.09 89.12 11.97 o -2 2 0 421.79 457.10 20.37 o -1 2 0 219.25 241.01 20.81 o 0 2 0 1390.07 1430.07 77.74 o 1 2 0 13369.46 14227.70 426.72 o 2 2 0 8953.60 8829.85 392.88 o 3 2 0 5614.08 5543.21 258.16 o 4 2 0 6746.44 6810.50 275.73 o 5 2 0 3239.12 3167.39 137.54 o 6 2 0 2464.97 2578.78 100.04 o 7 2 0 160.75 150.34 28.42 o 8 2 0 8.03 -1.90 22.12 o 9 2 0 419.31 405.93 31.40 o 10 2 0 1174.31 1212.95 52.75 o 11 2 0 1800.05 1852.65 68.81 o 12 2 0 1506.94 1479.07 74.14 o -10 3 0 101.75 56.95 48.64 o -9 3 0 1068.97 1098.96 99.45 o -8 3 0 1619.42 1717.61 122.74 o -7 3 0 3454.81 3539.03 195.52 o -6 3 0 1580.71 1443.07 102.57 o -5 3 0 10056.30 9588.31 428.49 o -4 3 0 5149.61 5152.92 120.53 o -3 3 0 2891.35 2833.52 79.98 o -2 3 0 805.30 786.78 39.45 o -1 3 0 1040.48 1062.73 69.34 o 0 3 0 43.11 68.81 27.76 o 1 3 0 7698.59 8290.09 275.87 o 2 3 0 15248.44 15368.93 669.28 o 3 3 0 17436.85 17309.08 755.22 o 4 3 0 7388.49 7204.13 331.82 o 5 3 0 20543.86 20969.42 1332.69 o 6 3 0 9575.62 9628.39 236.16 o 7 3 0 2925.42 3072.27 117.73 o 8 3 0 1865.36 1948.80 88.13 o 9 3 0 158.95 208.85 35.68 o 10 3 0 17.64 11.67 19.83 o 11 3 0 2379.90 2399.38 81.81 o 12 3 0 1976.16 2012.08 88.81 o -8 4 0 118.69 153.29 51.02 o -7 4 0 218.56 272.89 55.77 o -6 4 0 2532.09 2651.87 155.80 o -5 4 0 3393.55 3319.48 178.67 o -4 4 0 8256.01 8286.40 250.65 o -3 4 0 7712.83 7334.15 222.37 o -2 4 0 3710.61 3783.04 184.99 o -1 4 0 200.20 188.19 36.07 o 0 4 0 1520.99 1588.43 90.74 o 1 4 0 1926.04 1972.25 73.09 o 2 4 0 1280.43 1297.04 55.00 o 3 4 0 4980.79 4718.46 223.85 o 4 4 0 4202.79 3893.48 193.91 o 5 4 0 20261.24 22905.04 1000.64 o 6 4 0 12437.78 11525.58 643.10 o 7 4 0 9292.90 9403.45 438.64 o 8 4 0 6383.76 6330.79 314.24 o 9 4 0 151.85 129.56 46.98 o 10 4 0 198.15 187.49 31.60 o 11 4 0 311.87 304.39 38.58 o 12 4 0 922.24 972.94 61.03 o -8 5 0 0.00 -4.03 44.13 o -7 5 0 30.88 151.15 55.29 o -6 5 0 793.24 856.33 84.97 o -5 5 0 2832.55 2826.52 161.04 o -4 5 0 6625.47 6746.72 211.76 o -3 5 0 6847.66 6464.41 201.34 o -2 5 0 4420.80 4335.53 211.15 o -1 5 0 3962.97 3993.99 194.98 o 0 5 0 910.12 892.41 66.47 o 1 5 0 40.06 83.27 17.67 o 2 5 0 530.42 563.87 34.37 o 3 5 0 3597.66 3912.70 133.93 o 4 5 0 1347.97 1192.07 80.26 o 5 5 0 7559.17 7893.24 367.58 o 6 5 0 8930.58 9285.94 279.98 o 7 5 0 5684.76 5851.12 289.48 o 8 5 0 2025.00 2062.18 133.46 o 9 5 0 1324.42 1305.19 104.22 o 10 5 0 23.23 -6.41 33.93 o 11 5 0 5.64 8.30 46.98 o 12 5 0 561.27 461.47 44.74 o -8 6 0 365.20 361.42 66.68 o -7 6 0 14.11 31.32 49.59 o -6 6 0 4.97 16.85 38.91 o -5 6 0 1345.28 1232.99 97.57 o -4 6 0 3773.70 3644.75 142.08 o -3 6 0 6701.26 6572.23 207.95 o -2 6 0 10722.41 10546.63 314.52 o -1 6 0 8440.02 8223.22 369.43 o 0 6 0 9934.80 9915.15 434.65 o 1 6 0 2753.38 2656.59 79.13 o 2 6 0 641.41 708.97 39.84 o 3 6 0 78.03 87.08 20.71 o 4 6 0 1090.89 1131.78 55.14 o 5 6 0 864.34 858.36 69.79 o 6 6 0 3261.12 3163.65 111.68 o 7 6 0 6931.85 7231.07 440.09 o 8 6 0 5173.21 5771.20 292.42 o 9 6 0 3088.52 2978.22 178.15 o 10 6 0 2006.04 2141.66 146.50 o 11 6 0 587.94 510.96 82.35 o 12 6 0 90.90 53.92 31.35 o -7 7 0 304.98 397.95 69.29 o -6 7 0 295.62 285.00 57.90 o -5 7 0 21.38 3.56 36.07 o -4 7 0 580.24 439.04 54.82 o -3 7 0 1930.09 1842.64 81.29 o -2 7 0 2812.04 2872.67 108.40 o -1 7 0 5196.70 5302.18 173.54 o 0 7 0 5869.99 5993.78 281.40 o 1 7 0 3893.42 4039.03 199.42 o 2 7 0 2152.11 2247.81 126.36 o 3 7 0 913.47 869.52 69.08 o 4 7 0 51.25 39.35 21.64 o 5 7 0 85.42 90.87 24.09 o 6 7 0 1069.26 1032.58 54.28 o 7 7 0 2816.36 3076.53 112.42 o 8 7 0 5455.16 5937.48 300.27 o 9 7 0 6985.93 7084.72 354.85 o 10 7 0 3759.26 3834.91 132.46 o 11 7 0 2525.05 2936.29 192.34 o 12 7 0 1381.53 1209.71 69.40 o -6 8 0 458.49 455.16 69.77 o -5 8 0 149.33 95.39 47.22 o -3 8 0 345.83 348.11 38.58 o -2 8 0 773.47 784.55 52.36 o -1 8 0 1441.32 1445.79 69.37 o 0 8 0 2032.88 2051.39 85.45 o 1 8 0 2905.02 3160.58 168.66 o 2 8 0 6821.29 7002.37 322.86 o 3 8 0 724.31 701.37 64.56 o 4 8 0 1496.66 1578.34 59.60 o 5 8 0 217.63 199.43 33.46 o 6 8 0 119.06 101.36 20.90 o 7 8 0 520.53 515.00 53.64 o 8 8 0 1423.16 1356.01 105.17 o 9 8 0 3372.58 3362.79 158.44 o 10 8 0 1932.10 1995.93 85.49 o 11 8 0 1912.86 2010.96 108.10 o 12 8 0 1289.52 1356.62 73.65 o -4 9 0 293.43 273.61 61.22 o -3 9 0 5.47 11.85 40.34 o -2 9 0 58.43 18.20 24.86 o -1 9 0 967.90 1053.80 60.75 o 0 9 0 2374.78 2460.14 100.82 o 1 9 0 3624.56 3677.92 132.82 o 2 9 0 5365.31 5449.08 268.64 o 3 9 0 7711.75 7573.49 238.32 o 4 9 0 2284.98 2277.01 92.41 o 5 9 0 1852.47 1917.72 82.56 o 6 9 0 35.08 61.68 18.98 o 7 9 0 60.70 52.91 17.59 o 8 9 0 239.05 243.15 30.14 o 9 9 0 1570.54 1478.80 69.74 o 10 9 0 1937.20 2128.72 91.77 o 11 9 0 1811.93 1694.03 80.54 o -3 10 0 330.64 358.44 42.02 o -2 10 0 64.12 49.06 27.85 o -1 10 0 1.67 12.46 29.42 o 0 10 0 385.57 411.96 41.55 o 1 10 0 1563.98 1567.47 77.18 o 2 10 0 2128.03 2080.20 91.00 o 3 10 0 4556.75 4634.31 160.56 o 4 10 0 4403.09 4537.59 157.94 o 5 10 0 4859.13 5234.96 177.86 o 6 10 0 1258.81 1385.99 70.31 o 7 10 0 803.30 904.27 56.60 o 8 10 0 221.79 244.28 32.16 o 9 10 0 180.43 102.94 31.09 o 10 10 0 512.20 464.64 44.72 o 11 10 0 1207.43 1090.72 65.72 o -1 11 0 147.34 170.83 36.33 o 0 11 0 4.00 -17.90 27.84 o 1 11 0 138.95 137.77 33.46 o 2 11 0 294.73 311.83 39.61 o 3 11 0 1245.64 1304.14 112.75 o 4 11 0 2211.33 2398.22 101.82 o 5 11 0 2219.43 2287.67 98.24 o 6 11 0 1525.61 1553.72 110.15 o 7 11 0 462.03 474.15 60.75 o 8 11 0 187.08 182.24 48.17 o 10 11 0 67.25 19.61 36.17 o 1 12 0 27.98 -19.92 31.80 o 2 12 0 129.43 79.29 32.90 o 3 12 0 661.80 614.91 73.81 o 4 12 0 867.21 847.30 85.44 o 5 12 0 1988.42 2048.90 132.72 o 6 12 0 1738.01 1777.64 121.55 o 7 12 0 1196.53 1293.38 99.45 o 8 12 0 743.49 750.67 77.37 o -7 -12 1 115.52 195.53 58.85 o -6 -12 1 82.90 70.24 51.02 o -5 -12 1 777.17 892.85 88.29 o -4 -12 1 1109.81 1095.39 66.62 o -3 -12 1 1512.50 1566.14 81.84 o -2 -12 1 1369.62 1498.81 81.13 o -1 -12 1 1221.03 1215.31 73.32 o -10 -11 1 1660.57 1594.30 97.13 o -7 -11 1 988.27 934.14 59.83 o -6 -11 1 984.55 942.62 60.18 o -5 -11 1 158.02 135.92 51.37 o -4 -11 1 272.36 284.48 38.91 o -3 -11 1 1190.11 1088.80 64.67 o -2 -11 1 1111.26 1145.05 74.89 o -1 -11 1 2160.94 2153.15 97.46 o 0 -11 1 2020.91 2006.51 107.91 o 1 -11 1 1638.99 1723.41 86.94 o -11 -10 1 821.87 866.62 76.10 o -10 -10 1 2138.79 2388.84 123.57 o -9 -10 1 2166.41 2203.31 89.27 o -8 -10 1 1773.68 2001.15 81.14 o -7 -10 1 1816.32 1896.24 86.31 o -6 -10 1 1703.25 1656.67 78.47 o -5 -10 1 2106.07 2047.89 89.86 o -4 -10 1 64.98 48.05 26.34 o -3 -10 1 767.82 766.29 52.25 o -2 -10 1 512.25 499.80 43.08 o -1 -10 1 2221.53 2220.25 96.29 o 0 -10 1 2337.09 2443.86 106.97 o 1 -10 1 2224.81 2127.09 95.25 o 2 -10 1 1289.85 1310.51 72.54 o 3 -10 1 478.83 492.36 46.87 o -11 -9 1 58.75 88.67 42.11 o -10 -9 1 1236.28 1392.93 70.68 o -9 -9 1 2678.46 2651.70 100.89 o -8 -9 1 2999.01 3163.18 94.07 o -7 -9 1 3692.12 3799.82 91.56 o -6 -9 1 1346.65 1438.50 61.45 o -5 -9 1 4272.88 4377.75 222.43 o -4 -9 1 737.49 829.75 74.29 o -3 -9 1 73.36 62.17 34.17 o -2 -9 1 1082.51 1151.73 89.01 o -1 -9 1 672.39 693.02 70.25 o 0 -9 1 1558.84 1634.88 76.81 o 1 -9 1 2728.09 2601.54 199.49 o 2 -9 1 1958.97 2014.49 90.98 o 3 -9 1 1725.45 1803.14 85.31 o 4 -9 1 649.72 609.45 77.61 o -12 -8 1 169.62 128.12 48.48 o -11 -8 1 13.56 9.72 28.35 o -10 -8 1 62.30 35.52 29.07 o -9 -8 1 1794.42 1916.46 82.90 o -8 -8 1 4081.56 4475.28 144.76 o -7 -8 1 3687.60 3993.50 105.89 o -6 -8 1 3601.63 3730.28 101.67 o -5 -8 1 4209.94 4349.65 112.79 o -4 -8 1 2295.89 2354.08 79.74 o -3 -8 1 2021.22 2276.16 132.75 o -2 -8 1 161.89 158.28 39.39 o -1 -8 1 8.01 14.95 30.37 o 0 -8 1 100.64 172.04 41.29 o 1 -8 1 514.62 579.31 65.26 o 2 -8 1 2398.33 2464.69 99.94 o 3 -8 1 2167.92 2088.95 91.31 o 4 -8 1 1654.67 1766.49 125.35 o 5 -8 1 1292.61 1315.73 107.05 o 6 -8 1 606.64 754.68 85.91 o -12 -7 1 331.43 315.96 57.90 o -11 -7 1 337.84 300.35 42.92 o -10 -7 1 82.95 43.36 35.14 o -9 -7 1 8.26 0.95 37.97 o -8 -7 1 2102.88 2057.60 103.29 o -7 -7 1 1787.69 1952.39 61.76 o -6 -7 1 3136.53 3179.28 135.46 o -5 -7 1 6469.77 6424.26 156.42 o -4 -7 1 4433.03 4735.11 118.87 o -3 -7 1 7676.61 7644.80 207.94 o -2 -7 1 1685.58 1696.64 104.48 o -1 -7 1 1553.00 1546.45 99.96 o 0 -7 1 112.80 122.21 39.15 o 1 -7 1 41.60 54.58 34.41 o 2 -7 1 1125.68 1174.79 90.92 o 3 -7 1 1102.27 1104.20 59.64 o 4 -7 1 2474.45 2423.42 102.71 o 5 -7 1 1930.66 2031.85 134.38 o 6 -7 1 1199.72 1342.76 109.42 o 7 -7 1 1180.45 1175.16 106.10 o -12 -6 1 1241.06 1344.85 92.06 o -11 -6 1 771.44 771.72 53.10 o -10 -6 1 1313.93 1317.73 68.47 o -9 -6 1 1079.76 1077.20 57.64 o -8 -6 1 25.65 3.32 33.46 o -7 -6 1 587.41 600.94 66.69 o -6 -6 1 3926.10 3937.00 207.50 o -5 -6 1 6506.69 6555.16 313.68 o -4 -6 1 10325.00 10258.38 322.91 o -3 -6 1 12387.63 12294.71 277.37 o -2 -6 1 8271.16 8412.10 223.94 o -1 -6 1 1736.01 1792.06 125.75 o 0 -6 1 1861.77 1919.18 111.86 o 1 -6 1 557.68 656.48 62.90 o 2 -6 1 717.13 748.37 70.02 o 3 -6 1 669.85 649.13 43.86 o 4 -6 1 3327.41 3232.51 118.21 o 5 -6 1 3047.13 3130.51 176.00 o 6 -6 1 2122.70 2120.54 139.85 o 7 -6 1 2256.29 2368.66 154.57 o 8 -6 1 708.02 790.54 90.66 o -12 -5 1 1205.13 1234.28 127.94 o -11 -5 1 2895.42 2831.25 108.16 o -10 -5 1 2534.67 2603.75 100.99 o -9 -5 1 3588.82 3559.22 152.17 o -8 -5 1 862.25 821.98 79.52 o -7 -5 1 277.21 269.11 51.73 o -6 -5 1 498.93 448.09 56.96 o -5 -5 1 5412.64 5828.01 281.24 o -4 -5 1 5204.62 5196.48 250.82 o -3 -5 1 10823.68 10773.50 334.58 o -2 -5 1 10975.28 10853.92 244.24 o -1 -5 1 6192.38 5830.13 187.34 o 0 -5 1 5283.30 5550.68 257.03 o 1 -5 1 3377.82 3623.75 180.65 o 2 -5 1 21.60 57.42 32.75 o 3 -5 1 33.43 50.07 35.36 o 4 -5 1 1519.18 1461.89 107.91 o 5 -5 1 2471.87 2336.92 141.31 o 6 -5 1 1673.29 1644.79 115.86 o 7 -5 1 1756.78 1908.05 131.52 o 8 -5 1 1721.14 1762.44 129.86 o -12 -4 1 1636.25 1574.50 98.94 o -11 -4 1 3024.55 2960.54 115.51 o -10 -4 1 2158.10 2224.80 106.58 o -9 -4 1 4273.51 4572.87 205.20 o -8 -4 1 1679.52 1831.11 123.94 o -7 -4 1 209.97 202.18 47.94 o -6 -4 1 597.58 745.28 70.02 o -5 -4 1 431.09 520.01 55.30 o -4 -4 1 1957.61 2065.45 118.07 o -3 -4 1 8554.43 8334.11 378.09 o -2 -4 1 9205.15 9119.79 283.52 o -1 -4 1 9765.32 9598.09 250.08 o 0 -4 1 6857.91 6605.11 293.73 o 1 -4 1 3504.08 3448.90 169.56 o 2 -4 1 3250.56 3270.21 164.97 o 3 -4 1 253.14 221.41 43.43 o 4 -4 1 172.02 118.63 24.85 o 5 -4 1 16.49 -12.10 32.27 o 6 -4 1 752.93 789.65 77.85 o 7 -4 1 724.90 763.04 79.98 o 8 -4 1 1748.68 1793.37 129.39 o 9 -4 1 1160.10 1092.09 100.88 o -12 -3 1 739.06 734.35 53.63 o -11 -3 1 1748.27 1767.30 105.49 o -10 -3 1 1763.93 1828.89 67.02 o -9 -3 1 2993.71 2975.05 89.13 o -8 -3 1 2137.78 2121.65 93.83 o -7 -3 1 1718.91 1681.35 77.83 o -6 -3 1 201.53 206.46 42.24 o -5 -3 1 307.69 358.36 46.99 o -4 -3 1 3868.36 4497.60 219.60 o -3 -3 1 1574.12 1662.63 96.46 o -2 -3 1 22040.05 23908.40 1029.94 o -1 -3 1 10400.48 11113.58 247.03 o 0 -3 1 18841.29 19106.21 793.79 o 1 -3 1 2330.28 2161.37 113.16 o 2 -3 1 11987.91 12118.75 311.94 o 3 -3 1 4240.22 4167.42 144.33 o 4 -3 1 2365.92 2442.81 99.81 o 5 -3 1 17.57 -1.39 20.17 o 6 -3 1 75.37 68.10 41.29 o 7 -3 1 220.31 224.25 51.49 o 8 -3 1 1453.01 1507.20 113.71 o 9 -3 1 2217.79 2160.44 145.79 o 10 -3 1 1548.75 1478.18 120.59 o -12 -2 1 116.69 72.38 43.79 o -11 -2 1 310.81 342.29 38.33 o -10 -2 1 1824.58 1811.64 66.60 o -9 -2 1 3436.09 3507.54 113.36 o -8 -2 1 5599.39 5593.89 142.91 o -7 -2 1 5647.38 5550.23 190.86 o -6 -2 1 5028.00 4665.28 237.29 o -5 -2 1 6514.40 6577.22 259.89 o -4 -2 1 3483.93 3636.92 126.07 o -3 -2 1 4545.65 5148.08 241.86 o -2 -2 1 116.83 145.47 30.61 o -1 -2 1 3699.92 3846.71 93.06 o 0 -2 1 12794.04 12737.05 533.51 o 1 -2 1 15616.62 15604.23 651.38 o 2 -2 1 17271.32 16791.75 534.78 o 3 -2 1 12619.05 11775.08 492.74 o 4 -2 1 8269.74 8247.71 436.60 o 5 -2 1 1317.46 1353.83 53.72 o 6 -2 1 23.72 -10.19 14.40 o 7 -2 1 144.49 136.51 30.82 o 8 -2 1 125.50 179.15 48.88 o 9 -2 1 1458.06 1379.23 109.44 o 10 -2 1 2437.46 2707.85 172.39 o -12 -1 1 25.81 135.73 61.22 o -11 -1 1 4.77 8.21 25.72 o -10 -1 1 974.50 931.99 54.38 o -9 -1 1 955.81 999.02 45.43 o -8 -1 1 4601.01 4733.51 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