Acta Crystallographica Section C

Crystal Structure Communications

Volume 55, Part 5 (May 1999)


Cover illustration Cover illustration: The highly solvated structure of theonellapeptolide Id, a tridecapeptide lactone from the Okinawa marine sponge Theonella swinhoei, see Doi, Ishida, Kobayashi, Deschamps & Flippen-Anderson, pages 796-798. Displacement ellipsoids are shown at the 30% probability level.

cif-access (metal-organic compounds)



Acta Cryst. (1999). C55, IUC9900038    [ doi:10.1107/S0108270199099539 ]

Tris(1,3-diaminopropane-N,N')nickel(II) diperchlorate

O. Kristiansson

Synopsis: The nickel octahedron of the title compound is slightly distorted, with an average Ni-N distance of 2.146(13)Å.

Formula: [Ni(C3H10N2)3](ClO4)2



Acta Cryst. (1999). C55, IUC9900045    [ doi:10.1107/S0108270199099527 ]

[bold mu]-1,3-Imidazolyl-[bold kappa]N:[bold kappa]N'-bis[(diethylenetriaminato-[bold kappa]3N)copper] triperchlorate hydrate

W. Bu, L. Ye, H. Zhu, G. Yang, Y. Fan and W. Tang

Synopsis: The title compound consists of two identical [Cu(dien)]+ cations [dien is diethylenetriaminate(1-)] bridged by an imidazolyl ligand, three ClO4- anions and one water molecule. In the cation, the two Cu atoms are six-coordinate, being also bonded in a (4+2') fashion to perchlorate O atoms. The distance between the two Cu atoms is 5.889(2)Å.

Formula: [Cu2(C4H12N3)2(C3H3N2)](ClO4)3H2O



Acta Cryst. (1999). C55, IUC9900044    [ doi:10.1107/S0108270199099515 ]

Bis([bold mu]-azido-[bold kappa]N1:[bold kappa]N1)bis{[2-(1,5-diazacyclooct-1-yl-[bold kappa]2N,N'-methyl)phenolato-[bold kappa]O]copper(II)

W. Bu, L. Ye, Q. Xu, X. Bu, G. Yang and Y. Fan

Synopsis: The title compound has centrosymmetric Cu dimers linked by two end-on azido bridges. Each Cu atom has the five-coordinated geometry of a distorted trigonal bipyramid. The bridging azide anions are bound asymmetrically to copper at distances of 2.174(3) and 2.215(3)Å. The Cu...Cu distance is 3.129 (2) Å.

Formula: [Cu2(C13H19N2O)2(N3)2]



Acta Cryst. (1999). C55, IUC9900051    [ doi:10.1107/S0108270199099503 ]

Sodium hydrogen bis[dichloro(dihydrogen ethylenediaminetetraacetato-O,N,N',O')ruthenium(III)] nonahydrate

E. Stadler, C. C. Stadler, C. R. deM. Peixoto and I. Vencato

Synopsis: The asymmetric unit of the title compound contains two independent molecules, one Na atom and nine water molecules. The RuIII atom is tetracoordinated by the ethylenediaminetetraacetate (edta) ligand through two N and two carboxylate O atoms. The other two carboxylate groups of edta are free. The remaining two coordination positions of ruthenium(III) are occupied by Cl atoms.

Formula: NaH[RuCl2(C10H14N2O8)]29H2O



Acta Cryst. (1999). C55, IUC9900050    [ doi:10.1107/S0108270199099497 ]

(S,S)-Ferrocenyl[methyl(1-phenylethyl)amino]acetonitrile

J. A. S. Howell, K. Humphries, P. McArdle, D. Cunningham, M. Walsh and P. Daly

Synopsis: The cyano and dialkylamino substituents in the title compound lie endo and exo with respect to the substituted ring plane. Data were collected using synchrotron radiation due to the small size of the only good quality crystal available.

Formula: [Fe(C5H5)(C16H17N2)]



Acta Cryst. (1999). C55, IUC9900049    [ doi:10.1107/S0108270199099485 ]

A redetermination of bis(2-aminomethylpyridine)diperchloratocopper(II)

H.-M. Hu, D.-L. Long, H.-Y. Zeng, W.-D. Cheng and J.-S. Huang

Synopsis: The crystal structure of the title compound has been redetermined. It crystallizes in space group P1, which is the main difference from the previous determination [O'Connor, Eduok, Owens & Stevens (1986). Inorg. Chim. Acta, 117, 175-181].

Formula: [Cu(ClO4)2(C6H8N2)2]


cif-access (organic compounds)



Acta Cryst. (1999). C55, IUC9900047    [ doi:10.1107/S0108270199099473 ]

5-Ethyl-2-phenyl-1-(2,4,6-trichlorophenyl)-3-trifluoromethyl-1H-1,2,4-triazolium hexachloroantimonate

X.-J. Liu, Y.-B. Fan, Y. Liu and Q.-R. Wang

Synopsis: The title compound has interesting biological activity. The three rings in the molecule are planar, with dihedral angles between their least-squares planes of 74.17, 65.15 and 90.69°. In the triazolium ring, the C-N bond lengths are almost equal, with values ranging between 1.315 and 1.340Å; this is due to [bold pi] interaction.

Formula: (C17H12Cl3F3N3)[SbCl6]



Acta Cryst. (1999). C55, IUC9900048    [ doi:10.1107/S0108270199099461 ]

7-Amino-2,3-dihydro-5H-thiazolo[3,2-a]pyrimidin-5-one

J. N. Low, G. Ferguson, M. Melguizo and A. Sánchez

Synopsis: The molecules of the title compound form a two-dimensional network linked by 8 and 24 hydrogen-bonded rings.

Formula: C6H7N3OS



Acta Cryst. (1999). C55, IUC9900046    [ doi:10.1107/S010827019909945X ]

N,N'-Dibenzenesulfonylputrescine

A. Linden and S. Bienz

Synopsis: The title compound, N-4-[(benzenesulfonyl)amino]butylbenzenesulfonamide, is useful in the synthesis of natural or unnatural polyamine derivatives. The molecule is centrosymmetric with a straight-chain alkane core, and N-H...O intermolecular hydrogen bonds link the molecules into an infinite two-dimensional network.

Formula: C16H20N2O4S2



Acta Cryst. (1999). C55, IUC9900043    [ doi:10.1107/S0108270199099448 ]

3[beta],4[beta]-Epoxy-7-oxo-7a-oxa-7a-homo-5[beta]-cholan-24-oic acid

A. D. Morales, S. García-Granda, R. P. Gil and F. Coll-Manchado

Synopsis: In the title compound, the epoxy O atom is [beta]-oriented. The presence of the epoxy group disturbs the chair conformation in ring A of the steroidal nucleus. Ring A has a half-chair conformation. The seven-membered B-ring conformation is midway between chair and twist-chair. The A/B junction is cis, and the B/C and C/D junctions are both trans. The molecules are held together by intermolecular O-H...O hydrogen bonding, forming a zigzag chain along the [010] direction.

Formula: C24H36O5



Acta Cryst. (1999). C55, IUC9900042    [ doi:10.1107/S0108270199099436 ]

(25R)-3[beta]-Bromo-5[alpha]-spirostan-6,23-dione

A. D. Morales, S. García-Granda, M. A. Iglesias-Arteaga and F. Coll-Manchado

Synopsis: In the title compound, the Br atom is [beta]-equatorially oriented. The six-membered rings (A, B, C and F) have the expected chair conformations. The D-ring conformation is midway between a 14[alpha]-envelope and a 13[beta],14[alpha]-half-chair, and the E-ring conformation is midway between an O2[alpha]-envelope and a C21[beta],O2[alpha]-half-chair. The packing of the molecules is assumed to be mainly dictated by van der Waals forces. The closest intermolecular contact between non-H atoms is 3.300(9)Å.

Formula: C27H39BrO4



Acta Cryst. (1999). C55, IUC9900041    [ doi:10.1107/S0108270199099424 ]

(E)-2-[2-(4-Chloromethylphenyl)vinyl]-1-methyl-5-nitro-1H-imidazole

K. Benakli, M. P. Crozet, P. Vanelle and M. Giorgi

Synopsis: In the crystal structure of the title compound, the five- and six-membered rings, together with the nitro substituent, are almost in the same plane. The torsion angle around the bond linking the aromatic ring and the Cl atom is 128.1(3)°.

Formula: C13H12ClN3O2



Acta Cryst. (1999). C55, IUC9900039    [ doi:10.1107/S0108270199099412 ]

cis-4,4-Dimethyltricyclo[6.3.0.01,7]undecane-2,6-dione

M. Umehara, H. Hosomi and S. Ohba

Synopsis: The title compound was obtained as a by-product in the chlorination of a C5-C8 fused-ring compound. The formation of a cyclopropane ring, expected from 1H NMR spectroscopic analysis, was confirmed. The junction at the C-C bond between the seven- and three-membered rings is cis.

Formula: C13H18O2



Acta Cryst. (1999). C55, IUC9900040    [ doi:10.1107/S0108270199099400 ]

3-Bromo-4-methylbicyclo[6.3.0]undecane-2,6-dione, (I), 5-bromo-4-methylbicyclo[6.3.0]undecane-2,6-dione, (II), 3,5-dibromo-4-methylbicyclo[6.3.0]undecane-2,6-dione, (III), and 1,7-dibromo-4-methylbicyclo[6.3.0]undecane-2,6-dione, (IV)

M. Umehara, H. Hosomi and S. Ohba

Synopsis: The structures of the four title compounds, C12H17BrO2, (I), C12H17BrO2, (II), C12H16Br2O2, (III), and C12H16Br2O2, (IV), which were obtained from the bromination of trans-4-methylbicyclo[6.3.0]undecane-2,6-dione, have been determined. The eight-membered rings in compounds (I)-(IV) take the boat-chair form.

Formula: C12H17BrO2, C12H17BrO2, C12H16Br2O2and C12H16Br2O2


inorganic compounds



Acta Cryst. (1999). C55, 701-702    [ doi:10.1107/S0108270199000499 ]

BaNi2(PO4)2

B. El-Bali, M. Bolte, A. Boukhari, J. Aride and M. Taibe

Synopsis: The crystal structure of the title compound, barium dinickel(II) bis(phosphate), is isostructural with BaNi2(AsO4)2, BaNi2(VO4)2 and BaCo2(PO4)2. It is made up of dodecacoordinated barium ions, NiO6 octahedra and PO4 tetrahedra.

Formula: BaNi2(PO4)2



Acta Cryst. (1999). C55, 703-705    [ doi:10.1107/S0108270198018058 ]

Tieftemperaturstruktur von diaquahydrogen(1+) hexachloroantimonat, H5O2+.SbCl6-

R. Minkwitz und C. Hirsch

Synopsis: The cations and anions in the title compound are linked by hydrogen bonds to form 12-membered rings. The O...O distance [2.400 (3) Å] in the H5O2+ cation indicates a strong hydrogen bond. The anion, with formal inversion symmetry, has an almost regular octahedral structure.

Formula: (H5O2)[SbCl6]


metal-organic compounds



Acta Cryst. (1999). C55, 706-707    [ doi:10.1107/S0108270198018010 ]

Dichloro(2,3,6,8,11,12,15,17-octamethyl-5,9,14,18-tetraazadibenzo[a,h]cyclotetradecene-[bold kappa]4N)zirconium(IV) tetrahydrofuran hemisolvate

J. P. Corden, W. Errington, P. Moore and M. G. H. Wallbridge

Formula: [ZrCl2(C26H30N4)]0.5C4H8O



Acta Cryst. (1999). C55, 707-710    [ doi:10.1107/S0108270199000438 ]

Bis[N-benzoyl-N'-(2-pyridylmethylene)hydrazine]trinitratocerium(III) acetone dihydrate

P. C. Christidis, I. A. Tossidis and D. G. Paschalidis

Formula: [Ce(C13H11N3O)2(NO3)3]C3H6O2H2O



Acta Cryst. (1999). C55, 710-712    [ doi:10.1107/S0108270199000542 ]

Polymeric aqua-1[bold kappa]O-bis[[bold mu]-(R,R)-tartrato-1[bold kappa]2O1,O2:2[bold kappa]2O3,O4]dicadmium(II) trihydrate

C. González-Silgo, J. González-Platas, C. Ruiz-Pérez, T. López and M. E. Torres

Formula: [Cd2(C4H4O6)2(H2O)]3H2O



Acta Cryst. (1999). C55, 712-714    [ doi:10.1107/S010827019801693X ]

Bis[iodo(N,N,N',N'',N''-pentamethyldiethylenetriamine-[bold kappa]3N)platinum(II)] di-[bold mu]-iodo-bis[diiodoplatinate(II)]

F. P. Fanizzi, F. P. Intini, L. Maresca, G. Natile and C. Pacifico

Formula: 2[PtI(C9H23N3)][Pt2I6]



Acta Cryst. (1999). C55, 715-717    [ doi:10.1107/S0108270198018095 ]

(2,2'-Bipyridine-N,N')(7-oxabicyclo[2.2.1]heptane-2-exo,3-exo-dicarboxylato-[bold kappa]3O2,3,7)manganese(II)-7-oxabicyclo[2.2.1]heptane-2-exo,3-exo-dicarboxylic acid-water (1/1/1)

U. Baumeister, H. Hartung and R. Kaplonek

Formula: [Mn(C8H8O5)(C10H8N2)]C8H10O5H2O



Acta Cryst. (1999). C55, 717-719    [ doi:10.1107/S010827019801823X ]

Cadmium isopropylxanthate

D. W. Tomlin, T. M. Cooper, D. E. Zelmon, Z. Gebeyehu and J. M. Hughes

Formula: [Cd(C4H7OS2)2]



Acta Cryst. (1999). C55, 719-722    [ doi:10.1107/S0108270198016412 ]

[1,3-Bis(pyridine-2-carboxamido)propane]palladium(II) monohydrate and its nickel(II) analogue

M. Tamura, Y. Kajikawa, N. Azuma, H. Tani, K. Tajima, K. Kanaori, K. Makino and T. Takayama

Formula: [Pd(C15H14N4O2)]H2O and [Ni(C15H14N4O2)]H2O



Acta Cryst. (1999). C55, 722-724    [ doi:10.1107/S0108270198014693 ]

Dichloro(2,6-diisopropylaniline-N)([bold eta]5-pentamethylcyclopentadienyl)rhodium(III)

S. W. Lee and J.-G. Lee

Formula: [RhCl2(C10H15)(C12H19N)]



Acta Cryst. (1999). C55, 724-726    [ doi:10.1107/S0108270198014449 ]

cis-(Nitrato-O,O')[(1RS,4SR,5SR,8RS,11SR,12SR)-C-rac-1,5,8,12-tetramethyl-1,4,8,11-tetraazacyclotetradecane-[bold kappa]4N]nickel(II) nitrate

K. Panneerselvam, T.-H. Lu, T.-Y. Chi, F.-L. Liao and C.-S. Chung

Formula: [Ni(NO3)(C14H32N4)]NO3



Acta Cryst. (1999). C55, 726-728    [ doi:10.1107/S0108270199000207 ]

A W-Ag-Se cluster compound: ([bold mu]3-bromo)([bold mu]3-tetraselenidotungstide)tris(triphenylphosphinesilver) ethanol solvate, [([bold mu]3-Br)([bold mu]3-WSe4)(AgPPh3)3].EtOH

Q. Zhang, X. Xin, M. Hong, R. Cao, S. Shanmuga Sundara Raj and H.-K. Fun

Formula: [Ag3WBrSe4(C18H15P)3]C2H6O



Acta Cryst. (1999). C55, 728-730    [ doi:10.1107/S0108270198015479 ]

Dichloro{2-[([bold eta]5-cyclopentadienyl)phenylmethyl]phenolato-O}titanium

W. Bu, J. Wang, L. Ye, Y. Mu, G. Yang and Y. Fan

Formula: [TiCl2(C18H14O)]



Acta Cryst. (1999). C55, 730-733    [ doi:10.1107/S0108270199000530 ]

A copper(II) dimer: aqua([bold mu]-2,2'-bipyrimidine-N,N')(perchlorato)bis{[2,6-bis(2-pyridyl)pyridine-N,N',N'']copper(II)} triperchlorate

G. Francese, H. W. Schmalle and S. Decurtins

Formula: [Cu2(ClO4)(C8H6N4)(C15H11N3)2(H2O)](ClO4)3



Acta Cryst. (1999). C55, 733-739    [ doi:10.1107/S0108270199000323 ]

Salts of the bis(catecholato)borate anion with rhodium- and iridium-phosphine complex cations

W. Clegg, M. R. J. Elsegood, A. J. Scott, T. B. Marder, C. Dai, N. C. Norman, N. L. Pickett and E. G. Robins

Formula: Five C12H8BO4- complex salts



Acta Cryst. (1999). C55, 740-742    [ doi:10.1107/S0108270198016709 ]

Barium L-tartrate

C. González-Silgo, J. González-Platas, C. Ruiz-Pérez, T. López and M. Torres

Formula: Ba2+C4H4O62-



Acta Cryst. (1999). C55, 742-744    [ doi:10.1107/S0108270198017624 ]

[Tris(2-pyridyl-[bold kappa]N-methyleneamino-[bold kappa]N-ethyl)amine-[bold kappa]N]manganese(II) diperchlorate

M. Qian, S.-H. Gou, L. He, Y.-M. Zhou and C.-Y. Duan

Formula: [Mn(C24H27N7)](ClO4)2



Acta Cryst. (1999). C55, 744-748    [ doi:10.1107/S0108270199002954 ]

catena-Poly[triphenyltin-[bold mu]-(N,N-diethylthiocarbamoylthioacetato-O:O')], catena-poly[triphenyltin-[bold mu]-(N-methyl-N-phenylthiocarbamoylthioacetato-O:O')] and triphenyl(N,N-tetramethylenethiocarbamoylthioacetato-O)tin

K. M. Lo, V. G. Kumar Das, S. W. Ng and J. M. Hook

Formula: [Sn(C6H5)3(C7H12NO2S2)], [Sn(C6H5)3(C10H10NO2S2)]and [Sn(C6H5)3(C7H10NO2S2)]


organic compounds



Acta Cryst. (1999). C55, 749-751    [ doi:10.1107/S0108270198018290 ]

6-Acetylamino-5-(diacetylamino)pyrimidine-2,4(1H,3H)-dione

J. N. Low, G. Ferguson, M. Nogueras, A. Sánchez and J. Cobo

Formula: C10H12N4O5



Acta Cryst. (1999). C55, 751-754    [ doi:10.1107/S0108270199002942 ]

2,2'-Biphenol-1,10-phenanthroline (1/1): a two-dimensional structure built up from three types of hydrogen bond and [bold pi]-[bold pi] stacking interactions

E. S. Lavender, R. M. Gregson, G. Ferguson and C. Glidewell

Formula: C12H10O2C12H8N2



Acta Cryst. (1999). C55, 754-756    [ doi:10.1107/S0108270199000426 ]

Polysulfonylamines. CIX. 1,2,4-Triazolium di(methanesulfonyl)amidate

O. Moers, K. Wijaya, P. G. Jones and A. Blaschette

Formula: C2H4N3+C2H6NO4S2-



Acta Cryst. (1999). C55, 756-759    [ doi:10.1107/S0108270199001808 ]

Heterocycle-substituted [2.2]paracyclophanes

I. Dix, H. Hopf and P. G. Jones

Formula: C20H18O and C20H18S



Acta Cryst. (1999). C55, 759-761    [ doi:10.1107/S0108270199001341 ]

A racemic strigol analogue at 100K

J. K. Rugutt, F. R. Fronczek, H. H. Yarabe, S. A. Shamsi, C. W. Henry III, E. J. Billiot and I. M. Warner

Formula: C13H12O5



Acta Cryst. (1999). C55, 761-764    [ doi:10.1107/S0108270199000475 ]

Two novel 3,4-disubstituted 1,2,4-oxadiazole-5(4H)-thiones

D. R. Billodeaux, F. R. Fronczek and Y. Dürü

Formula: C14H11N3OS and C10H11N3OS



Acta Cryst. (1999). C55, 764-766    [ doi:10.1107/S010827019801806X ]

N-Methyl-2'-nitrocinnamanilide

E. Subramanian, S. Renganayaki, S. Shanmuga Sundara Raj and H.-K. Fun

Formula: C16H14N2O3



Acta Cryst. (1999). C55, 766-768    [ doi:10.1107/S0108270198018277 ]

Pipemidic acid hydrochloride

H.-K. Fun, K. Chinnakali, I. A. Razak, S.-Z. Zhan, C.-J. Hu and Q. Meng

Formula: C14H18N5O3+Cl-



Acta Cryst. (1999). C55, 768-770    [ doi:10.1107/S0108270198018071 ]

2,2-Bis(2-methoxyphenyl)-4-methyl-8,9-epoxy-7,8,9,10-tetrahydro-2H-benzo[h]chromene

K. Chinnakali, H.-K. Fun, K. Sriraghavan and V. T. Ramakrishnan

Formula: C28H26O4



Acta Cryst. (1999). C55, 770-772    [ doi:10.1107/S0108270199001821 ]

4-(p-Methoxyphenyl)-3,5-bis(2-pyridyl)-4H-1,2,4-triazole

H.-K. Fun, K. Chinnakali, S. Shao, D. Zhu and X. Z. You

Formula: C19H15N5O



Acta Cryst. (1999). C55, 772-774    [ doi:10.1107/S0108270198018289 ]

2-Ethyl-2-(3-oxobutyl)cycloheptane-1,3-dione

K. Chinnakali, H.-K. Fun, D. Rajagopal and S. Swaminathan

Formula: C13H20O3



Acta Cryst. (1999). C55, 774-776    [ doi:10.1107/S0108270199001596 ]

5a,6,9,9a-Tetrahydro-4-hydroxy-6,9-methano-5H-fluoreno[2,3-b]furan-5-one and 5a,6,9,9a-tetrahydro-6,9-methano-4-methoxy-5H-fluoreno[2,3-b]furan-5-ol

K. Chinnakali, H.-K. Fun, D. Mal, M. Bandopadhyay, K. Datta and G. D. Nigam

Formula: C16H12O3 and C17H16O3



Acta Cryst. (1999). C55, 776-778    [ doi:10.1107/S0108270199000657 ]

6,11-Dihydroxy-1,4-methano-1,4,4a,12a-tetrahydronaphthacene-5,12-dione

K. Chinnakali, H.-K. Fun, D. Mal, S. K. Ghorai, N. K. Hazra and G. D. Nigam

Formula: C19H14O4



Acta Cryst. (1999). C55, 778-781    [ doi:10.1107/S0108270199000141 ]

5-Benzyloxy-1-phenyltetrazole: catalytic transfer hydrogenolysis of benzyl ethers

A. F. Brigas, W. Clegg, R. A. W. Johnstone and R. F. Mendonca

Formula: C14H12N4O



Acta Cryst. (1999). C55, 781-783    [ doi:10.1107/S010827019801782X ]

12-Formyl-9,10-dimethyl-9,10-dihydro-11-thia-9,10-ethanoanthracene

F. Minassian, N. Pelloux-Léon, A. Durif and Y. Vallée

Formula: C18H16OS



Acta Cryst. (1999). C55, 783-785    [ doi:10.1107/S0108270198016941 ]

2,4,4,6,6-Pentachloro-2-(2,6-di-tert-butyl-4-methylphenoxy)cyclo-2[bold lambda]5,4[bold lambda]5,6[bold lambda]5-triphosphazatriene

T. Hökelek, A. Kilic, S. Begeç and Z. Kilic

Formula: C15H23Cl5N3OP3



Acta Cryst. (1999). C55, 786-787    [ doi:10.1107/S0108270198017296 ]

10[beta]-Hydroxy-6[alpha]-(3,4,5-trimethoxyphenyl)-2,3,6,6a[alpha],7,9,9a[beta],10-octahydroisobenzofuro[5,6-g][1,4]benzodioxin-7-one

A. S. Capilla, M. D. Pujol, X. Solans and M. Font-Bardia

Formula: C23H24O8



Acta Cryst. (1999). C55, 787-789    [ doi:10.1107/S0108270199000517 ]

Androst-4-ene-3,6,17-trione

A. Anthony, M. Jaskólski and A. Nangia

Formula: C19H24O3



Acta Cryst. (1999). C55, 789-791    [ doi:10.1107/S0108270198018253 ]

1,11-Undecanediol

N. Nakamura, S. Setodoi and T. Ikeya

Formula: C11H24O2



Acta Cryst. (1999). C55, 791-794    [ doi:10.1107/S0108270198017922 ]

Tautomerism in a 2,4-dichlorobenzenesulfonamide derived from 2-amino-4-(2,5-dimethoxyphenyl)thiazole

P. Beuchet, J.-M. Léger, M. Varache-Lembége and A. Nuhrich

Formula: C17H14Cl2N2O4S2



Acta Cryst. (1999). C55, 794-796    [ doi:10.1107/S0108270199000219 ]

(+)-(2R-cis)-Dimethyl(10-bromo-2,3,3a,8-tetrahydrodibenz[c,f]isoxazolo[2,3-a]azepin-2-ylmethyl)amine

O. M. Peeters, N. M. Blaton, C. J. De Ranter and H. L. De Winter

Formula: C19H21BrN2O



Acta Cryst. (1999). C55, 796-798    [ doi:10.1107/S0108270198014383 ]

The highly solvated structure of theonellapeptolide Id, a tridecapeptide lactone from the Okinawa marine sponge Theonella swinhoei

M. Doi, T. Ishida, M. Kobayashi, J. R. Deschamps and J. L. Flippen-Anderson

Formula: C70H125N13O1612H2O



Acta Cryst. (1999). C55, 798-801    [ doi:10.1107/S0108270199000128 ]

3-[2-(1,3-Dioxolan-2-yl)ethyl]-2-methylbenzoic acid

R. E. Gerkin

Formula: C13H16O4



Acta Cryst. (1999). C55, 801-806    [ doi:10.1107/S0108270198018034 ]

Capped-porphyrin precursors

P. G. Jene, D. S. Chan, B. L. Cooke and J. A. Ibers

Formula: C17H18O5S, C16H16O5S, C16H16O5S0.5H2Oand C50H54O16



Acta Cryst. (1999). C55, 806-808    [ doi:10.1107/S0108270199000402 ]

(1'R,2'R)-3-[(cis-2'-Cyclohexylmethylcyclopentyl)imino]-2-azabicyclo[2.2.2]octane hydrobromide, a hypoglycaemic semicyclic amidine

S. Hartmann, E. Weckert and A. W. Frahm

Formula: C19H33N2+Br-



Acta Cryst. (1999). C55, 808-811    [ doi:10.1107/S0108270198018241 ]

Imide and tribenzyl ester derivatives of Kemp's triacid

P. Thuéry, M. Nierlich, Z.-H. Wang and T. Hirose

Formula: C22H29NO4, C22H29NO4CH3OH and C33H36O6



Acta Cryst. (1999). C55, 811-813    [ doi:10.1107/S0108270198018083 ]

3-Phenyl-1-(2-pyridyl)thiourea

D. X. West, A. K. Hermetet, L. J. Ackerman, J. Valdés-Martínez and S. Hernández-Ortega

Formula: C12H11N3S



Acta Cryst. (1999). C55, 813-815    [ doi:10.1107/S0108270198016072 ]

7-Hydroxy-4-(4-methoxyphenyl)-3,4-dihydrocoumarin

K. Rajalakshmi, N. Jain, S. Deepthi, H. G. Krishnamurthy and V. Pattabhi

Formula: C16H14O4



Acta Cryst. (1999). C55, 815-817    [ doi:10.1107/S0108270199001833 ]

A chain of fused R22(10) and R46(12) rings in the hydrogen-bonded structure of 1,4,8,11-tetraazacyclotetradecane-2,2'-biphenol (1/2)

G. Ferguson, R. M. Gregson and C. Glidewell

Formula: C10H26N42+2C12H9O2-



Acta Cryst. (1999). C55, 818-819    [ doi:10.1107/S0108270198018393 ]

(E)-3-(Benzoylmethylene)-N-methylisoindolin-1-one

S. Guha, A. K. Mukherjee, M. W. Khan and N. G. Kundu

Formula: C17H13NO2



Acta Cryst. (1999). C55, 819-821    [ doi:10.1107/S0108270198016357 ]

2H-Dibenzo[b,f]azepin-2-one

P. H. Ruane, R. A. McClelland and A. J. Lough

Formula: C14H9NO



Acta Cryst. (1999). C55, 821-823    [ doi:10.1107/S0108270199001961 ]

2-Amino-4-phenylthiazole

O. Au-Alvarez, R. C. Peterson, A. Acosta Crespo, Y. Rodríguez Esteva, H. Marquez Alvarez, A. M. Plutín Stiven and R. Pomés Hernández

Formula: C9H8N2S



Acta Cryst. (1999). C55, 823-825    [ doi:10.1107/S0108270199000852 ]

A functionalized dimethyl maleate (maleic acid dimethyl ester)

D. Zellmer, R. Niewa and R. P. Kreher

Formula: C18H21NO4



Acta Cryst. (1999). C55, 825-827    [ doi:10.1107/S0108270199001456 ]

4-Chloro-N-(p-fluorobenzyl)-2-nitroaniline

M. M. Candan, E. Kendi and H. Göker

Formula: C13H10ClFN2O2



Acta Cryst. (1999). C55, 827-829    [ doi:10.1107/S0108270199000529 ]

A new 14:15-seco-15-norpregnane derivative from Mandevilla illustris Woodson (Apocynaceae)

I. Vencato, R. Niero, J. L. Montanari, J. B. Calixto, A. E. G. Sant'Ana and R. A. Yunes

Formula: C22H30O5



Acta Cryst. (1999). C55, 830-832    [ doi:10.1107/S0108270199002243 ]

4-Nitramino-1,2,4-triazole

A. D. Vasiliev, A. M. Astachov, R. S. Stepanov and S. D. Kirik

Formula: C2H3N5O2


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