# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data__Ni_thio_bpy _shelx_refln_list_code 4 _shelx_F_calc_maximum 225.43 _exptl_crystal_F_000 864.00 _reflns_d_resolution_high 0.7694 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' _cell_length_a 12.3770 _cell_length_b 6.9740 _cell_length_c 19.8220 _cell_angle_alpha 90.000 _cell_angle_beta 102.820 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 -25 125.82 98.69 10.45 o 2 1 -25 38.03 45.81 6.48 o 3 1 -25 44.99 27.40 15.15 o 4 1 -25 68.92 46.19 8.87 o 5 1 -25 162.78 140.40 11.47 o 6 1 -25 84.67 74.08 9.32 o 2 2 -25 96.61 82.48 9.09 o 3 2 -25 4.55 6.29 7.22 o 4 2 -25 28.40 37.79 6.81 o 5 2 -25 164.46 124.05 11.36 o 0 0 -24 1116.31 969.98 49.87 o 1 0 -24 228.61 173.73 11.81 o 2 0 -24 739.99 679.04 41.10 o 3 0 -24 0.26 2.08 11.02 o 4 0 -24 123.54 108.99 9.76 o 5 0 -24 537.74 485.64 25.56 o 6 0 -24 35.22 25.99 15.59 o 7 0 -24 1493.06 1355.71 58.05 o 8 0 -24 0.78 -2.80 13.03 o 9 0 -24 802.00 725.72 43.53 o 0 1 -24 142.70 125.87 10.06 o 1 1 -24 31.66 28.26 7.29 o 2 1 -24 254.67 227.21 14.77 o 3 1 -24 39.67 42.55 6.81 o 4 1 -24 646.85 546.93 36.93 o 5 1 -24 173.34 151.38 11.04 o 6 1 -24 144.26 141.14 10.40 o 7 1 -24 102.58 57.26 8.68 o 8 1 -24 12.02 16.98 14.75 o 0 2 -24 62.38 74.59 9.33 o 1 2 -24 296.14 287.19 17.72 o 2 2 -24 93.99 81.43 8.94 o 3 2 -24 79.22 71.77 8.72 o 4 2 -24 17.32 25.15 13.51 o 5 2 -24 131.43 117.40 10.85 o 6 2 -24 3.77 -9.23 12.31 o 7 2 -24 69.54 63.73 7.63 o 1 3 -24 74.24 68.80 9.28 o 2 3 -24 55.91 1.43 17.98 o 3 3 -24 19.96 12.36 18.60 o 4 3 -24 86.43 69.11 9.61 o 5 3 -24 39.90 35.98 8.11 o 0 1 -23 73.05 55.73 8.66 o 1 1 -23 114.81 93.62 9.40 o 2 1 -23 88.05 81.54 8.20 o 3 1 -23 70.07 63.04 7.91 o 4 1 -23 174.83 143.82 11.00 o 5 1 -23 11.31 14.03 10.35 o 6 1 -23 289.73 271.55 17.93 o 7 1 -23 77.88 64.43 8.75 o 8 1 -23 385.48 383.08 22.37 o 9 1 -23 173.70 148.75 10.80 o 10 1 -23 70.67 75.18 8.90 o 0 2 -23 11.67 -14.63 15.47 o 1 2 -23 380.86 329.72 21.04 o 2 2 -23 12.85 -3.32 13.87 o 3 2 -23 449.56 418.51 22.31 o 4 2 -23 29.70 16.52 15.25 o 5 2 -23 193.84 168.66 11.88 o 6 2 -23 9.87 -1.00 13.46 o 7 2 -23 101.95 88.98 9.59 o 8 2 -23 87.72 86.04 8.94 o 9 2 -23 147.08 143.15 11.35 o 0 3 -23 372.38 332.56 21.95 o 1 3 -23 142.67 119.75 10.71 o 2 3 -23 817.39 762.08 42.94 o 3 3 -23 36.31 7.82 17.29 o 4 3 -23 536.34 593.05 36.63 o 5 3 -23 46.29 39.90 7.48 o 6 3 -23 542.52 525.01 25.94 o 7 3 -23 192.66 176.90 12.77 o 2 4 -23 73.99 67.37 9.25 o 3 4 -23 191.13 167.18 12.17 o 4 4 -23 34.82 47.17 7.34 o 0 0 -22 320.22 280.09 18.24 o 1 0 -22 3822.98 3579.73 92.61 o 2 0 -22 165.83 167.51 11.02 o 3 0 -22 2998.70 2857.53 79.89 o 4 0 -22 175.12 154.82 10.09 o 5 0 -22 319.52 326.42 19.32 o 6 0 -22 312.18 257.40 14.42 o 7 0 -22 81.76 89.24 7.89 o 8 0 -22 1316.60 1207.10 52.19 o 9 0 -22 24.14 37.10 7.07 o 10 0 -22 1271.29 1241.27 56.46 o 11 0 -22 184.05 185.90 11.55 o 0 1 -22 337.20 377.39 20.66 o 1 1 -22 77.44 67.72 9.21 o 2 1 -22 57.56 46.66 7.43 o 3 1 -22 744.23 685.97 37.58 o 4 1 -22 150.37 153.09 10.06 o 5 1 -22 705.88 620.39 36.89 o 6 1 -22 680.82 676.05 37.82 o 7 1 -22 40.15 18.91 16.52 o 8 1 -22 469.23 431.18 24.15 o 9 1 -22 36.04 44.94 8.18 o 10 1 -22 237.01 222.59 13.19 o 11 1 -22 48.64 39.42 8.29 o 0 2 -22 61.17 69.19 7.87 o 1 2 -22 169.85 150.73 10.50 o 2 2 -22 441.32 436.41 23.26 o 3 2 -22 450.15 442.36 22.57 o 4 2 -22 172.74 163.45 10.49 o 5 2 -22 177.32 158.78 10.88 o 6 2 -22 104.56 94.46 9.71 o 7 2 -22 169.62 134.61 11.02 o 8 2 -22 141.39 106.34 11.04 o 9 2 -22 105.55 88.59 9.18 o 10 2 -22 153.20 139.83 10.81 o 0 3 -22 148.42 151.09 11.50 o 1 3 -22 425.55 379.42 22.69 o 2 3 -22 167.50 149.66 10.80 o 3 3 -22 111.38 107.62 9.44 o 4 3 -22 46.93 48.36 8.27 o 5 3 -22 93.15 68.61 9.27 o 6 3 -22 144.39 124.75 10.07 o 7 3 -22 123.46 121.04 10.26 o 8 3 -22 84.12 87.18 9.76 o 9 3 -22 91.13 69.97 10.11 o 0 4 -22 173.83 173.01 11.60 o 1 4 -22 24.06 9.46 14.77 o 2 4 -22 5.05 13.13 11.21 o 3 4 -22 521.97 531.44 26.13 o 4 4 -22 130.79 118.10 10.83 o 5 4 -22 300.62 303.71 20.30 o 6 4 -22 178.73 151.93 11.83 o 7 4 -22 99.95 86.38 9.88 o 0 1 -21 174.31 167.06 11.40 o 1 1 -21 29.33 20.10 7.27 o 2 1 -21 460.57 442.25 28.86 o 3 1 -21 394.01 349.49 18.76 o 4 1 -21 56.53 48.07 7.24 o 5 1 -21 267.99 229.52 13.79 o 6 1 -21 63.63 52.43 7.01 o 7 1 -21 687.51 636.56 37.24 o 8 1 -21 109.80 94.76 8.85 o 9 1 -21 375.74 327.37 21.35 o 10 1 -21 133.44 125.13 10.19 o 11 1 -21 66.86 58.09 9.23 o 0 2 -21 95.09 83.05 8.72 o 1 2 -21 125.18 117.29 9.11 o 2 2 -21 733.80 688.53 39.11 o 3 2 -21 94.33 109.76 9.06 o 4 2 -21 436.42 427.81 22.80 o 5 2 -21 192.55 172.82 11.31 o 6 2 -21 372.36 323.64 19.56 o 7 2 -21 65.42 61.05 7.68 o 8 2 -21 533.45 507.79 33.09 o 9 2 -21 30.47 20.51 16.81 o 10 2 -21 319.32 308.20 20.84 o 11 2 -21 20.93 25.31 13.03 o 0 3 -21 586.05 617.33 37.49 o 1 3 -21 641.09 608.41 35.98 o 2 3 -21 510.71 552.76 33.52 o 3 3 -21 889.77 838.28 41.16 o 4 3 -21 144.11 142.62 10.02 o 5 3 -21 760.91 763.09 41.53 o 6 3 -21 38.05 38.90 6.72 o 7 3 -21 587.23 566.30 28.26 o 8 3 -21 155.30 159.26 11.57 o 9 3 -21 646.14 634.11 42.15 o 10 3 -21 117.59 115.09 10.26 o 0 4 -21 2.30 9.20 14.17 o 1 4 -21 128.86 133.33 10.49 o 2 4 -21 27.08 20.61 15.63 o 3 4 -21 6.49 -3.92 10.38 o 4 4 -21 40.84 29.26 7.65 o 5 4 -21 36.18 43.58 8.01 o 6 4 -21 166.20 151.26 11.45 o 7 4 -21 191.62 231.87 14.97 o 8 4 -21 200.83 191.11 13.13 o 1 5 -21 406.32 413.36 24.63 o 2 5 -21 72.58 88.91 8.94 o 3 5 -21 101.31 104.23 10.21 o 4 5 -21 161.19 167.37 11.41 o 5 5 -21 7.43 17.52 6.26 o 0 0 -20 2547.22 2444.18 68.66 o 1 0 -20 16.34 19.49 5.62 o 2 0 -20 6405.78 6101.20 119.39 o 3 0 -20 48.30 34.28 6.41 o 4 0 -20 4951.55 4815.72 102.22 o 5 0 -20 42.50 72.10 6.81 o 6 0 -20 1468.56 1327.64 50.56 o 7 0 -20 196.34 209.27 12.17 o 8 0 -20 81.16 67.25 8.11 o 9 0 -20 1951.08 1900.07 65.62 o 10 0 -20 218.40 191.58 12.82 o 11 0 -20 992.73 946.78 49.63 o 12 0 -20 97.05 75.73 8.48 o 0 1 -20 346.17 358.17 19.51 o 1 1 -20 214.02 245.07 13.37 o 2 1 -20 181.00 224.57 12.50 o 3 1 -20 609.52 588.31 32.75 o 4 1 -20 122.38 118.70 8.41 o 5 1 -20 1224.55 1055.63 45.80 o 6 1 -20 13.37 6.19 11.11 o 7 1 -20 1804.61 1689.22 59.00 o 8 1 -20 238.07 220.37 12.89 o 9 1 -20 1263.90 1300.10 53.07 o 10 1 -20 9.20 7.98 11.26 o 11 1 -20 437.55 416.78 23.78 o 12 1 -20 18.50 22.86 12.74 o 0 2 -20 370.99 307.67 18.64 o 1 2 -20 199.34 217.17 12.69 o 2 2 -20 730.25 645.06 35.41 o 3 2 -20 226.35 206.52 13.08 o 4 2 -20 524.66 490.65 31.51 o 5 2 -20 120.19 114.30 8.54 o 6 2 -20 752.63 723.31 37.79 o 7 2 -20 132.53 128.26 9.09 o 8 2 -20 455.97 349.85 21.09 o 9 2 -20 130.14 116.07 9.25 o 10 2 -20 324.93 297.42 16.97 o 11 2 -20 121.49 123.93 10.80 o 12 2 -20 165.15 139.90 11.67 o 0 3 -20 397.35 403.95 21.08 o 1 3 -20 259.45 251.56 13.96 o 2 3 -20 161.81 154.72 10.73 o 3 3 -20 379.70 362.49 20.77 o 4 3 -20 357.12 358.52 19.25 o 5 3 -20 375.66 325.82 20.20 o 6 3 -20 42.20 40.97 6.64 o 7 3 -20 119.17 118.19 9.59 o 8 3 -20 151.98 169.92 10.56 o 9 3 -20 356.09 330.86 20.66 o 10 3 -20 63.97 55.53 8.39 o 11 3 -20 152.94 167.06 11.57 o 0 4 -20 303.02 350.58 20.06 o 1 4 -20 97.76 94.31 9.33 o 2 4 -20 24.50 26.46 6.00 o 3 4 -20 48.41 53.38 7.22 o 4 4 -20 103.58 111.74 9.37 o 5 4 -20 586.89 644.09 38.32 o 6 4 -20 259.15 281.78 16.31 o 7 4 -20 199.88 207.29 12.34 o 8 4 -20 49.20 58.74 8.22 o 9 4 -20 43.11 40.04 8.01 o 0 5 -20 35.63 34.93 7.03 o 1 5 -20 134.62 153.65 10.64 o 2 5 -20 13.42 2.63 15.01 o 3 5 -20 142.45 156.03 10.92 o 4 5 -20 59.72 72.79 8.75 o 5 5 -20 86.41 94.02 9.37 o 6 5 -20 69.08 77.29 8.41 o 7 5 -20 7.33 7.05 16.49 o 0 1 -19 47.02 38.71 6.76 o 1 1 -19 1432.13 1438.01 49.89 o 2 1 -19 319.01 312.86 16.37 o 3 1 -19 296.50 287.57 16.88 o 4 1 -19 459.93 429.05 27.21 o 5 1 -19 182.87 184.20 11.26 o 6 1 -19 149.68 134.07 8.77 o 7 1 -19 303.47 258.12 15.99 o 8 1 -19 404.51 391.46 20.82 o 9 1 -19 205.97 216.23 13.36 o 10 1 -19 430.67 408.27 22.88 o 11 1 -19 262.04 233.13 15.28 o 12 1 -19 31.38 34.74 7.13 o 13 1 -19 1.13 8.63 7.70 o 0 2 -19 540.79 581.57 32.04 o 1 2 -19 34.70 21.09 11.41 o 2 2 -19 1020.75 972.77 41.58 o 3 2 -19 364.39 328.24 18.48 o 4 2 -19 328.05 330.77 17.38 o 5 2 -19 220.27 197.08 11.79 o 6 2 -19 649.79 587.23 34.14 o 7 2 -19 542.43 514.41 32.63 o 8 2 -19 313.70 312.72 17.95 o 9 2 -19 1112.69 1011.17 46.33 o 10 2 -19 359.79 343.80 20.56 o 11 2 -19 499.08 468.11 24.72 o 12 2 -19 57.75 50.82 7.77 o 0 3 -19 114.13 116.83 9.21 o 1 3 -19 1206.21 1144.33 47.96 o 2 3 -19 1049.73 1040.29 46.26 o 3 3 -19 906.14 864.89 40.43 o 4 3 -19 618.62 563.92 32.42 o 5 3 -19 251.22 239.97 15.97 o 6 3 -19 452.20 447.52 22.38 o 7 3 -19 117.16 113.68 8.99 o 8 3 -19 576.32 547.14 33.83 o 9 3 -19 20.65 -14.47 14.47 o 10 3 -19 334.59 336.74 17.95 o 11 3 -19 19.77 36.82 7.31 o 0 4 -19 332.00 365.03 20.42 o 1 4 -19 349.38 395.27 20.30 o 2 4 -19 49.62 62.40 7.01 o 3 4 -19 10.46 16.97 8.66 o 4 4 -19 63.64 72.01 8.10 o 5 4 -19 3.39 7.87 9.27 o 6 4 -19 222.18 246.60 14.63 o 7 4 -19 119.43 102.51 9.09 o 8 4 -19 314.74 314.16 20.59 o 9 4 -19 114.87 94.19 10.06 o 10 4 -19 560.40 566.68 28.47 o 0 5 -19 28.36 20.15 12.62 o 1 5 -19 156.44 166.31 10.73 o 2 5 -19 299.02 331.96 20.99 o 3 5 -19 417.21 398.47 22.81 o 4 5 -19 71.42 86.11 7.87 o 5 5 -19 174.17 193.12 11.67 o 6 5 -19 36.55 46.91 7.87 o 7 5 -19 120.77 119.89 10.18 o 8 5 -19 19.76 38.47 7.39 o 1 6 -19 34.52 40.55 8.89 o 2 6 -19 212.53 224.27 13.60 o 3 6 -19 147.63 172.32 12.05 o 4 6 -19 21.92 31.96 16.95 o 0 0 -18 522.04 528.74 29.17 o 1 0 -18 707.70 682.57 33.97 o 2 0 -18 87.08 93.30 6.84 o 3 0 -18 8369.97 8317.47 139.30 o 4 0 -18 380.03 425.03 24.94 o 5 0 -18 962.38 1068.97 40.88 o 6 0 -18 349.89 335.26 16.68 o 7 0 -18 1249.05 1220.20 45.83 o 8 0 -18 15.62 15.94 9.66 o 9 0 -18 98.43 111.64 8.25 o 10 0 -18 405.76 404.16 21.27 o 11 0 -18 577.89 639.61 37.01 o 12 0 -18 754.48 834.54 44.30 o 13 0 -18 464.06 469.02 26.10 o 0 1 -18 144.09 137.46 8.54 o 1 1 -18 3525.03 3689.28 82.24 o 2 1 -18 732.61 684.48 33.47 o 3 1 -18 263.54 303.52 15.78 o 4 1 -18 228.97 212.60 13.31 o 5 1 -18 476.15 395.27 25.67 o 6 1 -18 603.03 655.39 34.14 o 7 1 -18 521.59 437.32 29.29 o 8 1 -18 2200.34 2105.64 63.97 o 9 1 -18 83.26 88.12 7.99 o 10 1 -18 2478.43 2450.26 74.04 o 11 1 -18 167.88 192.75 12.79 o 12 1 -18 569.99 529.60 25.98 o 13 1 -18 30.11 16.54 8.58 o 0 2 -18 362.04 325.06 17.33 o 1 2 -18 989.08 1003.06 40.36 o 2 2 -18 1049.38 995.98 40.61 o 3 2 -18 1156.56 1094.89 42.77 o 4 2 -18 332.36 311.62 16.52 o 5 2 -18 420.01 388.64 18.38 o 6 2 -18 317.15 279.66 16.54 o 7 2 -18 924.37 874.62 40.71 o 8 2 -18 312.89 286.88 17.67 o 9 2 -18 1082.66 972.24 44.66 o 10 2 -18 442.81 426.99 23.22 o 11 2 -18 820.18 716.93 40.71 o 12 2 -18 21.24 15.25 8.20 o 13 2 -18 205.59 196.56 13.55 o 0 3 -18 388.34 376.28 19.56 o 1 3 -18 533.38 469.73 30.70 o 2 3 -18 368.59 341.60 18.62 o 3 3 -18 511.19 509.21 31.65 o 4 3 -18 1206.71 1200.00 45.87 o 5 3 -18 38.79 44.35 6.36 o 6 3 -18 435.21 387.43 20.04 o 7 3 -18 50.81 52.54 6.95 o 8 3 -18 111.63 96.87 8.48 o 9 3 -18 52.28 59.50 7.37 o 10 3 -18 197.45 204.90 13.75 o 11 3 -18 54.79 43.42 8.51 o 12 3 -18 109.56 101.94 9.80 o 0 4 -18 218.44 249.72 14.03 o 1 4 -18 533.25 546.21 34.09 o 2 4 -18 10.08 11.86 8.58 o 3 4 -18 13.67 -9.47 11.91 o 4 4 -18 116.50 116.02 8.60 o 5 4 -18 11.94 6.40 11.83 o 6 4 -18 191.85 201.55 12.24 o 7 4 -18 50.41 65.02 7.68 o 8 4 -18 282.92 293.52 19.55 o 9 4 -18 0.85 -14.23 14.23 o 10 4 -18 249.27 243.77 15.49 o 11 4 -18 113.30 115.56 10.90 o 0 5 -18 103.34 130.69 8.96 o 1 5 -18 35.60 23.74 17.24 o 2 5 -18 107.93 114.35 9.54 o 3 5 -18 46.14 54.94 7.77 o 4 5 -18 425.09 467.70 30.96 o 5 5 -18 159.01 174.68 11.57 o 6 5 -18 581.12 634.12 28.47 o 7 5 -18 153.03 151.68 10.88 o 8 5 -18 185.24 181.86 11.88 o 9 5 -18 309.07 362.23 21.47 o 0 6 -18 209.06 264.33 16.02 o 1 6 -18 216.98 245.35 15.45 o 2 6 -18 334.13 405.69 24.36 o 3 6 -18 47.02 50.42 7.84 o 4 6 -18 168.94 209.35 13.80 o 5 6 -18 87.10 112.12 9.59 o 6 6 -18 113.71 136.39 10.90 o 0 1 -17 18.11 10.09 8.85 o 1 1 -17 508.06 442.70 26.84 o 2 1 -17 844.05 854.80 34.71 o 3 1 -17 412.15 448.60 25.17 o 4 1 -17 733.47 705.55 32.03 o 5 1 -17 514.39 536.99 27.69 o 6 1 -17 48.68 46.50 5.83 o 7 1 -17 13.06 3.85 10.09 o 8 1 -17 481.75 452.21 27.99 o 9 1 -17 144.64 137.87 9.61 o 10 1 -17 446.40 459.33 22.52 o 11 1 -17 250.52 240.59 14.72 o 12 1 -17 92.24 81.19 9.35 o 13 1 -17 25.33 16.30 15.56 o 14 1 -17 50.22 48.94 8.30 o 0 2 -17 63.78 56.15 6.57 o 1 2 -17 1526.26 1598.02 50.20 o 2 2 -17 154.34 147.65 9.61 o 3 2 -17 2643.64 2490.32 64.36 o 4 2 -17 23.99 -0.76 10.38 o 5 2 -17 746.65 721.47 33.88 o 6 2 -17 77.14 69.02 6.10 o 7 2 -17 979.25 910.79 39.93 o 8 2 -17 493.18 480.64 29.14 o 9 2 -17 738.91 735.69 37.46 o 10 2 -17 919.87 887.23 44.03 o 11 2 -17 670.55 671.20 39.75 o 12 2 -17 385.41 436.34 22.74 o 13 2 -17 226.48 225.08 13.99 o 0 3 -17 653.73 679.23 33.99 o 1 3 -17 0.95 1.25 9.42 o 2 3 -17 2888.06 2946.05 73.22 o 3 3 -17 818.21 841.41 37.49 o 4 3 -17 1295.68 1257.16 45.88 o 5 3 -17 99.95 94.77 7.60 o 6 3 -17 566.14 566.87 31.24 o 7 3 -17 32.86 37.42 6.12 o 8 3 -17 398.94 347.27 19.05 o 9 3 -17 170.63 158.14 9.73 o 10 3 -17 32.64 36.07 7.27 o 11 3 -17 79.31 71.03 7.98 o 12 3 -17 29.48 8.05 21.80 o 0 4 -17 444.28 483.01 30.84 o 1 4 -17 855.99 925.96 41.16 o 2 4 -17 721.96 737.54 35.50 o 3 4 -17 528.34 547.70 32.53 o 4 4 -17 80.52 88.88 8.10 o 5 4 -17 136.07 155.48 9.23 o 6 4 -17 13.31 9.13 7.58 o 7 4 -17 1447.38 1460.61 55.13 o 8 4 -17 30.85 39.28 6.26 o 9 4 -17 987.60 990.17 46.21 o 10 4 -17 48.50 50.37 8.41 o 11 4 -17 665.11 591.44 29.90 o 0 5 -17 184.88 181.79 11.35 o 1 5 -17 30.11 42.65 6.91 o 2 5 -17 404.25 441.83 22.11 o 3 5 -17 140.74 156.30 10.64 o 4 5 -17 740.80 810.61 41.77 o 5 5 -17 102.29 126.97 9.03 o 6 5 -17 840.10 990.73 46.45 o 7 5 -17 123.63 136.58 9.95 o 8 5 -17 374.89 369.64 23.64 o 9 5 -17 108.66 119.05 10.47 o 10 5 -17 12.60 -10.90 15.42 o 0 6 -17 23.72 23.59 15.25 o 1 6 -17 550.47 580.88 27.92 o 2 6 -17 191.19 223.88 12.93 o 3 6 -17 168.35 201.79 12.31 o 4 6 -17 241.24 260.44 15.27 o 5 6 -17 23.43 24.86 6.22 o 6 6 -17 214.42 226.90 15.28 o 7 6 -17 23.05 19.00 14.75 o 0 0 -16 66.82 65.96 5.50 o 1 0 -16 45.51 47.72 5.33 o 2 0 -16 1242.06 1216.35 40.04 o 3 0 -16 22.85 31.89 4.88 o 4 0 -16 2262.61 2134.16 55.35 o 5 0 -16 11.70 8.41 8.27 o 6 0 -16 1093.34 1092.40 40.00 o 7 0 -16 812.00 790.15 33.69 o 8 0 -16 345.28 308.73 16.93 o 9 0 -16 4.47 -1.72 9.64 o 10 0 -16 106.83 102.05 7.98 o 11 0 -16 39.86 22.90 12.31 o 12 0 -16 120.77 116.31 9.49 o 13 0 -16 1.49 -10.30 15.23 o 14 0 -16 897.83 958.16 50.39 o 0 1 -16 46.32 43.53 5.16 o 1 1 -16 681.92 578.99 28.24 o 2 1 -16 3369.32 3457.89 74.32 o 3 1 -16 266.00 256.33 13.68 o 4 1 -16 1928.59 1998.59 53.82 o 5 1 -16 20.28 11.64 10.26 o 6 1 -16 443.49 501.44 27.26 o 7 1 -16 653.00 639.97 31.24 o 8 1 -16 799.51 739.04 35.53 o 9 1 -16 2198.70 2046.34 62.40 o 10 1 -16 1106.94 1173.95 47.22 o 11 1 -16 1045.65 1094.88 47.84 o 12 1 -16 331.39 315.21 19.92 o 13 1 -16 378.03 400.62 23.74 o 14 1 -16 79.23 72.80 9.99 o 0 2 -16 205.78 212.17 13.07 o 1 2 -16 708.07 711.96 32.23 o 2 2 -16 538.47 560.89 29.60 o 3 2 -16 2227.25 2072.01 56.49 o 4 2 -16 444.09 431.92 26.39 o 5 2 -16 1188.88 1171.07 41.79 o 6 2 -16 25.52 33.38 5.23 o 7 2 -16 715.49 676.38 32.68 o 8 2 -16 567.05 523.62 31.13 o 9 2 -16 1267.63 1319.91 49.18 o 10 2 -16 841.00 932.75 43.42 o 11 2 -16 490.98 514.11 34.38 o 12 2 -16 695.89 737.46 42.70 o 13 2 -16 103.22 117.17 10.19 o 14 2 -16 282.95 316.42 17.95 o 0 3 -16 316.02 295.43 15.99 o 1 3 -16 790.87 783.72 35.41 o 2 3 -16 454.68 458.14 27.35 o 3 3 -16 813.85 797.01 35.40 o 4 3 -16 482.15 563.93 28.92 o 5 3 -16 483.24 517.55 29.07 o 6 3 -16 58.39 70.28 6.33 o 7 3 -16 364.25 375.64 25.22 o 8 3 -16 110.87 106.86 8.63 o 9 3 -16 48.17 41.60 6.96 o 10 3 -16 7.12 6.33 5.98 o 11 3 -16 47.85 3.28 16.83 o 12 3 -16 43.26 54.60 6.91 o 13 3 -16 14.89 25.56 13.15 o 0 4 -16 840.74 845.37 39.37 o 1 4 -16 88.59 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32.90 o 1 4 -1 19.12 25.84 3.16 o 2 4 -1 1233.74 1008.47 31.65 o 3 4 -1 747.18 771.27 28.19 o 4 4 -1 1325.29 1199.83 37.24 o 5 4 -1 511.75 461.51 23.43 o 6 4 -1 1975.69 1747.69 49.30 o 7 4 -1 1164.06 1081.79 39.47 o 8 4 -1 57.00 54.39 5.81 o 9 4 -1 149.78 158.78 10.16 o 10 4 -1 189.26 188.19 12.14 o 11 4 -1 20.74 24.24 13.25 o 12 4 -1 869.56 817.38 44.04 o 13 4 -1 110.02 106.77 10.09 o 14 4 -1 752.86 825.37 46.42 o 0 5 -1 2362.55 2647.44 58.59 o 1 5 -1 6.83 -2.44 8.23 o 2 5 -1 332.41 351.35 21.09 o 3 5 -1 29.16 40.48 4.47 o 4 5 -1 77.64 100.00 6.45 o 5 5 -1 99.90 95.01 6.77 o 6 5 -1 367.77 294.84 15.75 o 7 5 -1 851.89 762.81 35.76 o 8 5 -1 346.88 330.50 18.60 o 9 5 -1 1718.31 1751.38 58.88 o 10 5 -1 55.32 48.84 7.44 o 11 5 -1 411.47 371.05 21.97 o 12 5 -1 13.38 15.68 11.67 o 13 5 -1 56.45 33.56 17.81 o 0 6 -1 601.96 682.26 30.15 o 1 6 -1 418.45 434.59 25.15 o 2 6 -1 2295.54 2290.82 62.32 o 3 6 -1 12.17 11.43 9.13 o 4 6 -1 1355.93 1283.39 47.26 o 5 6 -1 316.38 293.36 17.35 o 6 6 -1 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2530.58 63.86 o 11 0 0 12.20 11.95 4.56 o 12 0 0 723.34 764.02 36.91 o 13 0 0 47.52 39.78 6.81 o 14 0 0 38.55 38.85 6.77 o 15 0 0 10.90 18.88 6.60 o 0 1 0 939.10 940.96 16.92 o 1 1 0 7698.10 7428.61 91.27 o 2 1 0 8296.53 8088.66 101.55 o 3 1 0 11198.03 10750.87 134.81 o 4 1 0 465.28 446.04 16.14 o 5 1 0 17217.64 17209.67 215.11 o 6 1 0 2744.17 2932.13 57.01 o 7 1 0 9112.96 8838.80 130.89 o 8 1 0 735.53 793.52 30.14 o 9 1 0 1229.68 1233.43 40.69 o 10 1 0 106.27 86.95 6.55 o 11 1 0 164.98 154.55 10.28 o 12 1 0 1281.07 1251.31 49.54 o 13 1 0 758.93 809.16 41.91 o 14 1 0 401.01 411.16 22.11 o 15 1 0 189.93 191.87 13.13 o 0 2 0 21316.11 20044.74 236.24 o 1 2 0 4541.43 4685.62 67.80 o 2 2 0 1524.57 1516.95 31.53 o 3 2 0 149.65 148.38 7.25 o 4 2 0 994.70 954.51 26.85 o 5 2 0 227.26 190.84 9.21 o 6 2 0 3866.38 3746.34 69.59 o 7 2 0 1172.25 1167.64 36.32 o 8 2 0 876.86 897.02 33.06 o 9 2 0 651.78 635.46 30.46 o 10 2 0 394.31 411.26 26.53 o 11 2 0 396.12 444.01 28.62 o 12 2 0 1119.87 1244.59 49.63 o 13 2 0 497.91 518.29 33.26 o 14 2 0 191.26 177.15 12.09 o 15 2 0 202.74 249.15 16.30 o 0 3 0 7330.73 7332.43 103.35 o 1 3 0 5161.41 5334.20 82.26 o 2 3 0 1778.31 1588.02 37.06 o 3 3 0 1096.90 1078.80 30.55 o 4 3 0 711.68 679.87 24.74 o 5 3 0 1176.57 1121.69 33.92 o 6 3 0 1771.38 1609.73 43.53 o 7 3 0 250.70 240.91 12.72 o 8 3 0 329.25 334.55 21.51 o 9 3 0 412.37 368.64 23.55 o 10 3 0 382.31 402.56 25.87 o 11 3 0 34.92 21.57 14.27 o 12 3 0 31.52 38.39 6.84 o 13 3 0 105.16 91.46 9.06 o 14 3 0 38.77 56.80 7.31 o 0 4 0 4.77 13.51 3.11 o 1 4 0 2756.92 3032.07 60.86 o 2 4 0 2919.00 2818.22 58.81 o 3 4 0 442.15 352.09 19.56 o 4 4 0 738.77 633.18 26.97 o 5 4 0 42.54 39.69 4.50 o 6 4 0 542.84 488.38 25.32 o 7 4 0 558.42 526.52 27.85 o 8 4 0 274.07 276.64 14.84 o 9 4 0 380.62 412.34 26.39 o 10 4 0 202.11 218.81 12.09 o 11 4 0 154.15 169.25 10.42 o 12 4 0 358.41 395.34 21.32 o 13 4 0 40.27 35.12 17.72 o 14 4 0 14.89 -1.34 15.47 o 0 5 0 277.05 332.18 19.94 o 1 5 0 453.01 486.66 24.55 o 2 5 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0 15.04 26.49 5.79 o 4 8 0 121.52 54.58 7.41 o 5 8 0 4.07 8.89 7.37 o 6 8 0 11.62 0.53 10.80 o 7 8 0 39.30 18.86 10.26 o 0 9 0 27.33 23.52 7.07 o 1 9 0 5.42 15.61 11.12 o 0 1 1 1964.28 1949.51 28.81 o 1 1 1 2080.70 2014.88 30.86 o 2 1 1 5365.92 5237.47 70.16 o 3 1 1 1174.18 1169.12 25.68 o 4 1 1 3210.80 3145.14 53.26 o 5 1 1 1810.05 1837.96 39.93 o 6 1 1 2550.14 2669.47 53.91 o 7 1 1 1666.46 1709.14 43.91 o 8 1 1 2129.88 2230.60 54.03 o 9 1 1 572.97 561.58 27.06 o 10 1 1 260.21 276.21 14.60 o 11 1 1 101.78 87.33 7.03 o 12 1 1 320.87 357.43 19.13 o 13 1 1 288.77 310.45 18.60 o 14 1 1 171.36 197.39 12.60 o 15 1 1 84.64 88.64 9.76 o 0 2 1 25759.92 25217.09 292.81 o 1 2 1 9349.49 9089.04 116.43 o 2 2 1 359.36 299.86 13.03 o 3 2 1 1315.14 1294.33 30.20 o 4 2 1 753.19 692.09 22.54 o 5 2 1 2741.40 2665.44 53.17 o 6 2 1 1695.53 1726.04 43.20 o 7 2 1 2576.11 2648.11 58.55 o 8 2 1 457.21 463.42 24.60 o 9 2 1 1563.52 1516.90 46.93 o 10 2 1 85.97 97.44 6.91 o 11 2 1 983.00 1075.59 43.39 o 12 2 1 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678.54 793.67 39.37 o 2 7 5 105.15 119.98 8.80 o 3 7 5 82.03 80.02 7.32 o 4 7 5 58.02 49.97 7.37 o 5 7 5 227.94 178.68 10.88 o 6 7 5 17.52 -14.11 15.15 o 7 7 5 71.40 52.28 8.84 o 8 7 5 299.10 234.73 15.70 o 0 8 5 0.12 15.90 10.49 o 1 8 5 31.38 40.57 7.29 o 2 8 5 310.34 205.93 12.19 o 3 8 5 702.97 442.74 24.05 o 4 8 5 299.23 174.32 11.93 o 5 8 5 439.50 255.87 16.81 o 6 8 5 124.60 75.67 9.75 o 0 0 6 80.91 103.13 5.16 o 1 0 6 1714.20 1781.59 34.02 o 2 0 6 3670.09 3933.22 61.63 o 3 0 6 202.61 151.23 10.14 o 4 0 6 1615.39 1462.52 35.24 o 5 0 6 1176.11 1122.86 32.32 o 6 0 6 6247.92 6330.38 102.41 o 7 0 6 484.57 517.98 24.72 o 8 0 6 1190.77 1220.06 40.35 o 9 0 6 2125.96 2144.09 58.52 o 10 0 6 849.30 834.55 38.13 o 11 0 6 27.35 29.21 5.29 o 12 0 6 311.61 284.80 18.33 o 13 0 6 214.22 224.07 12.88 o 14 0 6 169.02 178.53 11.74 o 0 1 6 6875.83 6882.64 93.24 o 1 1 6 4308.41 4218.58 64.40 o 2 1 6 274.78 238.87 11.81 o 3 1 6 3146.07 3069.24 54.67 o 4 1 6 2870.95 3043.73 56.92 o 5 1 6 4951.93 4879.16 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11 3 6 84.54 85.01 8.94 o 12 3 6 61.67 60.67 7.25 o 13 3 6 61.78 71.45 9.13 o 0 4 6 20.48 30.72 4.35 o 1 4 6 76.99 56.04 4.83 o 2 4 6 15.00 3.71 7.10 o 3 4 6 429.41 434.81 21.94 o 4 4 6 2.99 -8.18 8.18 o 5 4 6 43.06 43.84 5.24 o 6 4 6 342.75 312.48 15.73 o 7 4 6 3.21 5.78 8.66 o 8 4 6 15.36 14.34 13.10 o 9 4 6 341.53 366.55 19.25 o 10 4 6 37.81 30.22 15.94 o 11 4 6 653.87 763.00 41.60 o 12 4 6 28.38 30.53 15.80 o 0 5 6 733.95 803.49 31.58 o 1 5 6 344.09 445.90 23.07 o 2 5 6 1055.20 1164.10 39.54 o 3 5 6 193.74 197.44 10.74 o 4 5 6 2246.86 2059.99 57.07 o 5 5 6 659.57 622.71 30.62 o 6 5 6 1157.75 1038.75 42.91 o 7 5 6 181.43 166.37 9.99 o 8 5 6 1049.94 1103.45 48.20 o 9 5 6 261.82 240.62 14.46 o 10 5 6 261.26 239.59 15.45 o 11 5 6 228.01 202.97 13.37 o 0 6 6 1188.17 1297.28 45.64 o 1 6 6 531.42 558.67 29.07 o 2 6 6 846.53 897.83 37.92 o 3 6 6 77.09 78.73 7.50 o 4 6 6 232.18 222.61 12.26 o 5 6 6 322.93 346.24 18.48 o 6 6 6 0.69 5.45 9.70 o 7 6 6 233.10 179.30 11.17 o 8 6 6 199.71 168.83 10.69 o 9 6 6 22.54 3.82 13.39 o 10 6 6 131.82 112.69 10.66 o 0 7 6 356.20 461.13 21.57 o 1 7 6 923.02 1069.07 45.75 o 2 7 6 211.34 219.12 12.94 o 3 7 6 357.79 300.24 19.51 o 4 7 6 10.21 7.12 11.47 o 5 7 6 784.90 631.24 40.30 o 6 7 6 27.47 1.13 13.58 o 7 7 6 258.41 207.39 12.82 o 8 7 6 36.39 4.38 17.91 o 0 8 6 63.43 64.40 8.44 o 1 8 6 2.11 -14.18 15.11 o 2 8 6 195.06 142.22 10.86 o 3 8 6 1.82 14.54 12.48 o 4 8 6 135.05 86.26 8.90 o 5 8 6 2.92 2.73 10.88 o 0 1 7 1607.70 1603.56 33.59 o 1 1 7 2596.16 2643.37 47.46 o 2 1 7 1226.53 1174.21 29.53 o 3 1 7 1194.50 1103.73 30.05 o 4 1 7 1122.03 1154.82 32.54 o 5 1 7 1447.82 1438.21 38.75 o 6 1 7 260.41 257.95 17.38 o 7 1 7 297.06 289.41 14.32 o 8 1 7 715.75 688.82 31.55 o 9 1 7 567.79 573.15 29.59 o 10 1 7 296.66 315.18 17.86 o 11 1 7 96.96 105.04 8.89 o 12 1 7 144.63 162.83 11.43 o 13 1 7 6.32 4.31 12.03 o 14 1 7 3.38 5.83 9.76 o 0 2 7 1674.88 1696.27 37.24 o 1 2 7 2285.92 2189.87 44.25 o 2 2 7 1465.47 1411.33 35.05 o 3 2 7 1662.62 1560.17 38.51 o 4 2 7 2252.30 2285.50 50.46 o 5 2 7 1949.89 1886.97 47.28 o 6 2 7 2843.90 2907.97 64.24 o 7 2 7 1020.72 974.33 36.32 o 8 2 7 1237.03 1185.76 43.56 o 9 2 7 74.51 80.85 7.19 o 10 2 7 347.77 336.10 19.05 o 11 2 7 741.55 777.27 40.05 o 12 2 7 145.14 150.40 10.50 o 13 2 7 123.28 143.27 10.21 o 0 3 7 54.93 61.06 4.21 o 1 3 7 117.10 111.09 7.34 o 2 3 7 1507.15 1670.03 41.50 o 3 3 7 454.85 425.98 20.35 o 4 3 7 412.50 388.55 20.15 o 5 3 7 1914.64 1962.50 50.76 o 6 3 7 581.34 560.89 27.57 o 7 3 7 247.76 243.18 13.92 o 8 3 7 21.63 21.70 13.03 o 9 3 7 652.05 701.94 35.43 o 10 3 7 49.24 49.29 6.88 o 11 3 7 281.28 273.49 16.00 o 12 3 7 210.59 193.26 12.77 o 13 3 7 80.52 77.10 9.23 o 0 4 7 10790.75 11709.90 165.12 o 1 4 7 128.71 149.54 9.59 o 2 4 7 4413.94 4583.58 84.22 o 3 4 7 6.43 9.66 6.81 o 4 4 7 2552.35 2448.56 59.36 o 5 4 7 271.64 282.45 14.65 o 6 4 7 328.02 283.87 14.94 o 7 4 7 1419.01 1319.92 47.74 o 8 4 7 80.50 86.13 7.56 o 9 4 7 1543.12 1548.27 56.09 o 10 4 7 446.00 495.37 25.06 o 11 4 7 1012.43 1058.05 51.47 o 12 4 7 3.49 -9.23 16.86 o 0 5 7 209.81 220.18 12.60 o 1 5 7 635.50 661.53 30.24 o 2 5 7 567.64 554.91 27.08 o 3 5 7 480.35 500.15 28.06 o 4 5 7 900.98 923.69 37.06 o 5 5 7 977.10 934.81 38.54 o 6 5 7 2165.82 2152.22 62.95 o 7 5 7 879.70 841.39 39.87 o 8 5 7 165.03 135.62 10.19 o 9 5 7 248.55 242.70 13.75 o 10 5 7 49.31 19.61 12.02 o 11 5 7 58.21 56.68 8.48 o 0 6 7 156.40 187.47 10.88 o 1 6 7 727.88 885.20 37.61 o 2 6 7 344.04 412.21 27.52 o 3 6 7 53.54 63.62 6.53 o 4 6 7 519.86 564.77 32.30 o 5 6 7 147.58 134.78 9.33 o 6 6 7 30.59 15.87 11.91 o 7 6 7 164.34 145.44 10.37 o 8 6 7 77.54 57.80 8.73 o 9 6 7 55.09 35.19 7.58 o 0 7 7 303.08 376.41 20.87 o 1 7 7 147.20 203.85 12.22 o 2 7 7 455.23 452.81 21.80 o 3 7 7 87.93 72.55 7.53 o 4 7 7 178.97 144.27 10.31 o 5 7 7 94.25 82.53 9.68 o 6 7 7 51.67 49.29 7.17 o 7 7 7 61.05 43.96 8.30 o 8 7 7 39.49 34.04 7.43 o 0 8 7 44.61 25.61 14.03 o 1 8 7 245.68 219.67 12.38 o 2 8 7 92.56 76.33 8.17 o 3 8 7 286.66 212.31 14.18 o 4 8 7 332.59 236.31 15.64 o 5 8 7 346.12 267.65 16.86 o 0 0 8 15294.81 15914.01 197.20 o 1 0 8 290.65 261.97 13.31 o 2 0 8 2407.62 2600.15 49.44 o 3 0 8 2195.77 2691.90 52.66 o 4 0 8 257.10 220.03 14.23 o 5 0 8 73.53 59.36 4.33 o 6 0 8 1142.95 1040.71 34.97 o 7 0 8 1045.81 1158.76 38.89 o 8 0 8 63.72 65.55 5.97 o 9 0 8 147.65 162.63 10.18 o 10 0 8 500.25 613.00 33.14 o 11 0 8 115.71 140.00 9.23 o 12 0 8 59.37 63.04 8.08 o 13 0 8 116.95 104.71 9.80 o 0 1 8 1761.93 1778.53 37.51 o 1 1 8 2206.19 2100.41 42.55 o 2 1 8 7952.60 8047.08 114.29 o 3 1 8 2851.54 2549.94 51.52 o 4 1 8 2664.90 2500.65 53.00 o 5 1 8 3367.71 3465.42 68.13 o 6 1 8 1498.72 1432.85 41.81 o 7 1 8 297.43 319.17 20.84 o 8 1 8 240.41 249.72 13.86 o 9 1 8 32.05 40.19 5.72 o 10 1 8 1899.62 1844.20 59.55 o 11 1 8 12.36 -2.68 12.62 o 12 1 8 729.67 813.89 44.97 o 13 1 8 7.91 -0.62 13.39 o 0 2 8 4854.11 4996.04 79.27 o 1 2 8 2336.16 2460.10 49.36 o 2 2 8 1335.00 1258.89 33.83 o 3 2 8 1123.35 1056.44 31.51 o 4 2 8 816.01 781.90 28.59 o 5 2 8 3292.79 3273.78 67.42 o 6 2 8 1122.56 1070.36 36.74 o 7 2 8 1558.24 1472.65 46.62 o 8 2 8 772.94 714.32 33.11 o 9 2 8 1278.99 1289.29 47.91 o 10 2 8 155.89 163.76 10.49 o 11 2 8 491.06 488.83 23.47 o 12 2 8 67.44 68.20 8.48 o 13 2 8 62.28 59.12 8.08 o 0 3 8 56.69 80.78 5.33 o 1 3 8 1096.45 1183.46 34.57 o 2 3 8 2196.27 2331.77 52.05 o 3 3 8 703.52 730.74 28.71 o 4 3 8 1435.90 1464.46 42.63 o 5 3 8 1261.60 1202.46 39.38 o 6 3 8 255.60 242.10 13.07 o 7 3 8 95.15 89.67 7.29 o 8 3 8 269.79 281.54 16.42 o 9 3 8 138.78 145.13 9.42 o 10 3 8 65.77 60.22 8.39 o 11 3 8 16.05 6.24 15.52 o 12 3 8 45.67 41.71 8.18 o 0 4 8 1564.55 1765.22 45.87 o 1 4 8 237.06 237.51 12.12 o 2 4 8 679.99 669.64 27.92 o 3 4 8 17.25 28.85 4.42 o 4 4 8 9.96 15.06 9.04 o 5 4 8 289.25 278.79 14.53 o 6 4 8 168.56 166.89 9.61 o 7 4 8 42.12 55.03 5.83 o 8 4 8 300.61 330.69 18.21 o 9 4 8 239.81 229.22 14.17 o 10 4 8 107.15 113.36 9.03 o 11 4 8 186.97 175.38 12.14 o 12 4 8 203.85 204.35 13.03 o 0 5 8 485.15 518.45 26.63 o 1 5 8 1255.71 1415.87 45.02 o 2 5 8 817.57 893.47 36.05 o 3 5 8 1491.12 1654.70 50.73 o 4 5 8 118.10 120.37 7.84 o 5 5 8 1257.85 1276.52 48.19 o 6 5 8 690.48 716.90 36.20 o 7 5 8 698.72 726.27 39.97 o 8 5 8 109.19 105.21 9.71 o 9 5 8 409.00 399.11 21.78 o 10 5 8 37.02 44.39 7.56 o 11 5 8 162.69 163.92 12.27 o 0 6 8 34.35 33.30 5.26 o 1 6 8 418.50 454.87 20.41 o 2 6 8 50.14 60.63 7.01 o 3 6 8 318.50 314.42 17.33 o 4 6 8 292.25 329.53 17.74 o 5 6 8 107.62 130.39 8.97 o 6 6 8 93.68 75.88 8.05 o 7 6 8 56.22 40.55 7.80 o 8 6 8 112.07 86.14 9.51 o 9 6 8 78.97 61.22 9.16 o 0 7 8 116.70 133.33 9.04 o 1 7 8 400.05 438.23 21.95 o 2 7 8 200.01 214.41 13.96 o 3 7 8 219.34 224.39 14.29 o 4 7 8 278.81 228.19 14.82 o 5 7 8 14.89 27.42 6.29 o 6 7 8 455.63 356.61 22.33 o 7 7 8 8.74 -13.67 16.31 o 0 8 8 48.47 74.20 8.53 o 1 8 8 1.77 10.28 12.02 o 2 8 8 5.94 3.70 13.00 o 3 8 8 5.51 -11.86 11.86 o 4 8 8 2.67 8.20 14.15 o 0 1 9 2417.31 2396.11 47.07 o 1 1 9 16.73 19.39 3.15 o 2 1 9 1265.43 1153.27 31.85 o 3 1 9 658.66 652.36 24.84 o 4 1 9 2247.72 2361.06 52.85 o 5 1 9 92.58 105.38 6.84 o 6 1 9 435.40 418.84 22.86 o 7 1 9 231.48 218.17 12.67 o 8 1 9 21.74 0.83 10.09 o 9 1 9 133.31 147.48 9.39 o 10 1 9 456.96 431.92 29.12 o 11 1 9 208.99 212.55 13.12 o 12 1 9 248.28 238.08 15.82 o 13 1 9 13.48 22.80 14.34 o 0 2 9 2658.00 2725.15 53.72 o 1 2 9 4450.44 4571.58 77.17 o 2 2 9 3046.76 3159.77 61.39 o 3 2 9 1907.88 1901.89 46.26 o 4 2 9 1171.05 1113.65 35.59 o 5 2 9 3205.64 3055.56 66.29 o 6 2 9 145.21 124.77 7.36 o 7 2 9 1122.64 1055.90 39.83 o 8 2 9 8.47 13.37 4.50 o 9 2 9 1453.79 1517.05 52.43 o 10 2 9 28.80 39.18 5.67 o 11 2 9 434.37 444.64 24.17 o 12 2 9 16.52 7.56 14.82 o 13 2 9 40.71 40.26 7.55 o 0 3 9 566.58 572.41 23.60 o 1 3 9 384.75 387.54 19.44 o 2 3 9 161.61 141.09 9.04 o 3 3 9 86.19 78.12 5.43 o 4 3 9 626.71 643.18 28.35 o 5 3 9 60.00 53.69 6.34 o 6 3 9 1392.85 1322.33 45.02 o 7 3 9 84.17 85.85 7.55 o 8 3 9 495.94 541.58 31.92 o 9 3 9 209.78 242.17 16.06 o 10 3 9 829.15 789.99 41.31 o 11 3 9 6.65 5.81 13.00 o 12 3 9 290.34 292.85 17.26 o 0 4 9 119.65 108.75 7.31 o 1 4 9 2131.57 2453.49 57.71 o 2 4 9 37.03 37.56 5.07 o 3 4 9 5070.67 5277.68 97.54 o 4 4 9 1093.15 1116.09 40.18 o 5 4 9 1541.65 1429.10 47.05 o 6 4 9 52.20 55.72 6.46 o 7 4 9 263.77 257.38 15.83 o 8 4 9 663.47 777.31 39.09 o 9 4 9 84.50 91.65 8.80 o 10 4 9 233.46 242.77 15.16 o 11 4 9 222.06 212.48 13.10 o 0 5 9 1268.64 1335.76 43.84 o 1 5 9 805.48 938.25 36.72 o 2 5 9 253.69 262.54 14.97 o 3 5 9 342.97 365.48 17.36 o 4 5 9 122.37 134.93 8.30 o 5 5 9 415.50 405.57 20.22 o 6 5 9 1396.22 1404.55 52.19 o 7 5 9 51.86 53.27 7.63 o 8 5 9 594.32 646.33 37.53 o 9 5 9 8.87 12.55 12.29 o 10 5 9 334.07 297.35 17.00 o 0 6 9 51.78 59.53 6.27 o 1 6 9 48.77 53.03 5.98 o 2 6 9 13.56 18.86 5.76 o 3 6 9 133.39 150.64 9.04 o 4 6 9 83.46 83.69 7.91 o 5 6 9 185.68 173.56 11.24 o 6 6 9 127.81 122.67 10.23 o 7 6 9 95.25 77.48 8.99 o 8 6 9 220.85 190.29 12.55 o 9 6 9 37.62 18.94 12.70 o 0 7 9 49.25 70.00 7.41 o 1 7 9 105.39 137.49 9.18 o 2 7 9 50.81 57.42 8.06 o 3 7 9 432.42 477.19 23.62 o 4 7 9 144.85 145.25 10.69 o 5 7 9 63.02 53.29 7.41 o 6 7 9 227.38 168.82 12.02 o 7 7 9 22.62 9.04 13.24 o 0 8 9 308.86 371.12 22.16 o 1 8 9 307.78 337.54 21.95 o 2 8 9 168.82 178.56 11.64 o 3 8 9 0.30 -0.69 13.32 o 0 0 10 28.75 24.72 2.92 o 1 0 10 4614.11 4913.39 80.11 o 2 0 10 123.97 135.98 7.79 o 3 0 10 3267.79 3215.47 62.94 o 4 0 10 301.05 299.52 17.72 o 5 0 10 409.44 386.14 21.28 o 6 0 10 1163.48 1193.35 39.64 o 7 0 10 907.88 817.60 34.67 o 8 0 10 2.29 7.15 8.78 o 9 0 10 2158.45 2205.09 64.93 o 10 0 10 763.98 767.75 39.02 o 11 0 10 1194.75 1201.65 52.17 o 12 0 10 150.77 164.91 11.55 o 13 0 10 136.04 158.86 10.76 o 0 1 10 9321.67 9674.29 134.45 o 1 1 10 596.99 642.31 23.31 o 2 1 10 2097.34 1975.26 45.47 o 3 1 10 3574.80 3630.44 68.87 o 4 1 10 10416.07 10556.59 153.02 o 5 1 10 461.86 490.25 23.84 o 6 1 10 1950.87 1983.56 53.24 o 7 1 10 805.34 680.21 32.75 o 8 1 10 19.91 29.09 4.93 o 9 1 10 807.65 850.80 39.45 o 10 1 10 182.69 167.84 10.76 o 11 1 10 379.47 383.70 21.92 o 12 1 10 28.50 29.34 6.27 o 0 2 10 86.45 94.48 5.52 o 1 2 10 5669.31 5845.43 94.29 o 2 2 10 1217.10 1277.86 36.89 o 3 2 10 4239.52 4536.35 82.36 o 4 2 10 1753.82 1741.27 46.88 o 5 2 10 1603.01 1558.67 45.26 o 6 2 10 610.98 578.48 28.76 o 7 2 10 373.15 392.81 24.69 o 8 2 10 456.66 465.14 29.10 o 9 2 10 530.67 584.96 33.47 o 10 2 10 315.84 335.65 19.51 o 11 2 10 223.74 236.60 14.39 o 12 2 10 56.65 55.85 9.03 o 0 3 10 1436.55 1453.32 40.04 o 1 3 10 50.52 47.91 4.59 o 2 3 10 523.66 509.54 23.50 o 3 3 10 431.67 435.57 22.92 o 4 3 10 202.30 186.56 10.02 o 5 3 10 925.19 926.66 35.89 o 6 3 10 1129.16 1137.58 42.62 o 7 3 10 291.83 305.69 16.09 o 8 3 10 760.70 772.51 38.16 o 9 3 10 14.10 -0.09 10.54 o 10 3 10 167.61 173.20 11.38 o 11 3 10 117.05 109.28 10.11 o 12 3 10 75.84 72.36 10.40 o 0 4 10 23.18 20.89 4.25 o 1 4 10 112.94 112.81 7.50 o 2 4 10 221.85 270.02 14.01 o 3 4 10 1146.22 1310.12 42.99 o 4 4 10 541.67 578.53 29.55 o 5 4 10 111.53 114.15 8.17 o 6 4 10 139.05 150.09 9.28 o 7 4 10 193.87 212.89 12.27 o 8 4 10 3.38 3.82 9.80 o 9 4 10 142.91 144.75 10.02 o 10 4 10 38.22 32.71 7.74 o 11 4 10 42.55 39.99 7.87 o 0 5 10 558.21 618.46 30.05 o 1 5 10 944.99 1027.45 39.26 o 2 5 10 556.14 576.74 29.74 o 3 5 10 906.20 1045.02 41.40 o 4 5 10 736.69 741.10 35.83 o 5 5 10 393.86 391.47 19.63 o 6 5 10 165.71 173.87 11.33 o 7 5 10 100.25 98.37 9.11 o 8 5 10 499.38 481.43 24.00 o 9 5 10 34.51 17.66 16.47 o 10 5 10 125.77 134.31 12.27 o 0 6 10 99.44 122.07 7.91 o 1 6 10 1.69 -4.61 8.77 o 2 6 10 88.89 101.34 8.05 o 3 6 10 45.72 46.57 6.62 o 4 6 10 12.42 4.40 12.57 o 5 6 10 319.66 295.67 19.58 o 6 6 10 70.61 68.56 6.98 o 7 6 10 211.72 191.32 11.79 o 8 6 10 123.24 116.78 10.56 o 0 7 10 206.99 257.74 16.97 o 1 7 10 13.52 22.09 11.67 o 2 7 10 298.79 332.78 20.65 o 3 7 10 62.78 65.58 8.03 o 4 7 10 13.43 15.32 14.49 o 5 7 10 142.46 137.15 11.14 o 6 7 10 69.39 65.29 8.68 o 0 8 10 21.74 54.84 7.94 o 1 8 10 20.28 21.99 12.22 o 2 8 10 35.12 32.78 18.91 o 0 1 11 931.15 962.13 29.67 o 1 1 11 556.00 542.87 23.04 o 2 1 11 205.56 175.88 9.83 o 3 1 11 1371.98 1357.69 39.47 o 4 1 11 816.30 880.66 32.75 o 5 1 11 703.79 704.61 30.20 o 6 1 11 184.57 190.75 12.55 o 7 1 11 156.22 167.51 10.13 o 8 1 11 240.45 245.57 15.23 o 9 1 11 303.93 327.83 18.65 o 10 1 11 94.13 96.82 8.99 o 11 1 11 166.75 169.98 11.59 o 12 1 11 22.77 13.37 18.07 o 0 2 11 2551.43 2558.65 54.79 o 1 2 11 3092.23 3217.32 64.35 o 2 2 11 1296.28 1245.09 37.44 o 3 2 11 4102.77 4141.77 79.65 o 4 2 11 1560.36 1563.48 45.81 o 5 2 11 923.88 914.53 35.48 o 6 2 11 1058.46 1058.77 40.11 o 7 2 11 5.41 11.21 9.99 o 8 2 11 816.03 816.18 38.28 o 9 2 11 187.64 185.65 10.92 o 10 2 11 430.75 440.74 23.41 o 11 2 11 39.17 35.77 7.46 o 12 2 11 108.30 116.49 10.40 o 0 3 11 1333.60 1343.22 39.71 o 1 3 11 281.89 303.70 18.86 o 2 3 11 991.90 1063.24 35.81 o 3 3 11 3.50 -0.58 9.18 o 4 3 11 1228.26 1205.26 42.15 o 5 3 11 256.48 247.64 14.11 o 6 3 11 382.12 388.88 24.58 o 7 3 11 802.29 775.66 36.74 o 8 3 11 338.27 380.88 20.89 o 9 3 11 526.77 522.12 34.19 o 10 3 11 300.98 347.46 22.11 o 11 3 11 632.76 559.45 29.45 o 0 4 11 467.92 479.35 25.08 o 1 4 11 201.88 221.47 12.86 o 2 4 11 2079.10 2369.83 60.50 o 3 4 11 45.43 67.11 6.46 o 4 4 11 1834.00 1847.53 55.61 o 5 4 11 404.89 416.26 26.82 o 6 4 11 553.87 574.52 32.56 o 7 4 11 132.88 140.11 9.25 o 8 4 11 34.56 39.87 6.55 o 9 4 11 46.71 43.10 6.45 o 10 4 11 262.83 248.82 16.09 o 0 5 11 925.50 1082.34 41.09 o 1 5 11 200.25 205.60 13.70 o 2 5 11 855.24 918.22 38.40 o 3 5 11 25.00 36.69 5.91 o 4 5 11 173.06 171.60 10.18 o 5 5 11 46.29 54.29 6.12 o 6 5 11 25.16 34.90 6.05 o 7 5 11 450.44 380.40 22.19 o 8 5 11 44.01 35.96 7.17 o 9 5 11 86.09 90.37 9.44 o 0 6 11 229.43 264.02 15.47 o 1 6 11 66.43 86.73 8.22 o 2 6 11 246.49 272.24 17.35 o 3 6 11 22.68 28.14 5.55 o 4 6 11 2.09 -4.56 12.43 o 5 6 11 251.79 251.56 14.58 o 6 6 11 20.30 9.71 12.98 o 7 6 11 234.88 215.18 12.77 o 8 6 11 41.76 35.40 8.11 o 0 7 11 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4 4 14 24.44 40.05 6.03 o 5 4 14 399.07 411.48 20.94 o 6 4 14 230.74 238.47 14.46 o 7 4 14 234.20 224.22 14.87 o 8 4 14 232.98 266.60 15.37 o 9 4 14 204.68 203.95 12.88 o 0 5 14 295.96 318.98 17.64 o 1 5 14 401.85 430.51 28.14 o 2 5 14 267.32 285.06 17.43 o 3 5 14 429.84 482.16 29.98 o 4 5 14 2.85 7.43 10.28 o 5 5 14 41.89 57.62 7.10 o 6 5 14 11.00 12.62 7.41 o 7 5 14 26.61 16.09 15.49 o 0 6 14 245.92 256.08 14.75 o 1 6 14 119.27 161.01 10.95 o 2 6 14 286.10 361.72 20.75 o 3 6 14 131.51 148.60 11.16 o 4 6 14 115.16 115.54 9.68 o 5 6 14 210.77 211.24 12.52 o 6 6 14 245.34 229.22 13.75 o 0 7 14 227.01 269.33 15.97 o 1 7 14 118.06 121.73 10.52 o 2 7 14 69.05 81.64 9.11 o 3 7 14 26.18 18.48 11.81 o 0 1 15 193.44 214.65 11.93 o 1 1 15 377.91 390.68 22.06 o 2 1 15 1625.31 1624.60 48.63 o 3 1 15 153.50 197.32 12.15 o 4 1 15 1076.83 1054.73 40.64 o 5 1 15 53.23 57.47 6.84 o 6 1 15 262.32 279.20 16.54 o 7 1 15 2.46 6.74 10.71 o 8 1 15 166.47 171.41 11.35 o 9 1 15 36.45 24.82 7.00 o 10 1 15 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2 19 24.24 24.00 13.17 o 4 2 19 239.41 238.97 14.03 o 5 2 19 0.27 -13.58 13.58 o 6 2 19 142.79 174.61 11.35 o 7 2 19 26.02 15.35 18.03 o 0 3 19 128.42 126.35 9.37 o 1 3 19 554.80 596.94 33.21 o 2 3 19 20.25 6.77 15.42 o 3 3 19 706.16 707.84 39.01 o 4 3 19 83.05 88.16 8.34 o 5 3 19 504.90 608.15 37.77 o 6 3 19 176.12 171.60 11.88 o 0 4 19 335.38 401.72 20.17 o 1 4 19 2.44 5.24 11.54 o 2 4 19 236.98 236.93 14.73 o 3 4 19 34.03 20.04 7.12 o 4 4 19 195.39 173.58 11.83 o 5 4 19 1.97 -4.52 11.59 o 0 5 19 31.75 40.74 7.58 o 1 5 19 65.31 60.55 8.80 o 2 5 19 11.54 13.25 11.29 o 3 5 19 172.80 177.98 11.83 o 0 0 20 2566.19 2529.55 70.48 o 1 0 20 1.20 14.82 9.87 o 2 0 20 928.82 821.30 41.67 o 3 0 20 836.35 750.45 40.36 o 4 0 20 383.68 342.58 19.44 o 5 0 20 835.24 801.36 44.68 o 6 0 20 443.07 408.08 22.19 o 7 0 20 627.96 624.57 41.45 o 0 1 20 344.12 348.89 18.60 o 1 1 20 1646.44 1613.11 56.68 o 2 1 20 30.26 29.69 6.55 o 3 1 20 1306.21 1241.58 51.76 o 4 1 20 7.53 -8.30 11.79 o 5 1 20 331.71 367.53 22.30 o 6 1 20 0.74 4.78 10.52 o 0 2 20 298.63 297.20 18.14 o 1 2 20 15.86 13.51 11.29 o 2 2 20 354.57 338.25 20.11 o 3 2 20 64.71 63.26 7.62 o 4 2 20 208.99 201.80 13.49 o 5 2 20 59.94 29.64 16.81 o 6 2 20 181.76 228.49 13.62 o 0 3 20 395.06 381.36 20.68 o 1 3 20 147.47 144.04 10.01 o 2 3 20 45.31 45.90 7.63 o 3 3 20 86.95 92.16 8.46 o 4 3 20 59.76 50.64 8.82 o 5 3 20 164.47 152.47 11.38 o 0 4 20 302.18 274.68 16.23 o 1 4 20 202.23 224.38 13.37 o 2 4 20 327.92 332.51 20.77 o 3 4 20 128.14 119.74 10.25 o 4 4 20 33.93 23.59 19.44 o 0 5 20 22.16 19.19 10.50 o 1 5 20 75.76 70.28 8.65 o 2 5 20 8.66 -9.61 12.72 o 0 1 21 159.44 146.12 10.68 o 1 1 21 66.19 55.35 7.94 o 2 1 21 111.53 70.71 11.79 o 3 1 21 119.27 87.81 10.83 o 4 1 21 185.75 114.41 14.51 o 5 1 21 50.40 41.43 8.13 o 6 1 21 183.35 140.30 12.79 o 0 2 21 79.22 85.16 7.98 o 1 2 21 156.80 142.53 10.23 o 2 2 21 249.37 244.06 14.37 o 3 2 21 121.66 118.26 10.37 o 4 2 21 31.31 34.36 6.65 o 5 2 21 106.11 106.74 9.88 o 0 3 21 583.91 564.43 37.42 o 1 3 21 514.70 567.41 35.88 o 2 3 21 525.48 473.65 24.75 o 3 3 21 63.35 71.39 8.85 o 4 3 21 560.68 553.60 26.89 o 0 4 21 6.99 15.28 6.17 o 1 4 21 131.57 125.37 11.11 o 2 4 21 159.59 137.89 11.38 o 0 0 22 318.19 264.95 17.66 o 1 0 22 1501.86 1504.93 57.09 o 2 0 22 106.54 99.33 8.78 o 3 0 22 673.52 647.96 40.04 o 4 0 22 105.20 106.52 9.88 o 5 0 22 100.45 84.36 9.58 o 0 1 22 349.50 322.73 19.92 o 1 1 22 9.76 7.63 10.74 o 2 1 22 855.14 730.27 41.84 o 3 1 22 13.34 1.05 13.63 o 4 1 22 732.64 775.16 43.68 o 0 2 22 80.10 68.02 8.42 o 1 2 22 224.01 215.54 12.50 o 2 2 22 116.88 108.75 8.97 o 3 2 22 164.98 144.47 11.29 o 4 2 22 39.88 33.47 6.93 o 0 3 22 154.10 152.02 10.76 o 1 3 22 159.47 159.81 11.23 o 2 3 22 114.94 113.46 10.25 o 3 3 22 40.49 36.27 9.11 o 0 4 22 173.90 193.45 11.91 o 1 4 22 3.81 8.96 8.49 o 0 1 23 93.00 68.59 9.32 o 1 1 23 151.10 154.19 10.85 o 2 1 23 110.65 107.17 10.35 o 3 1 23 29.35 -7.94 21.63 o 0 2 23 14.39 12.77 5.86 o 1 2 23 236.89 232.56 15.28 o 2 2 23 22.34 19.79 12.00 o 0 3 23 362.44 351.18 21.11 o 1 3 23 96.91 95.12 10.14 o 0 0 24 1108.03 1082.95 50.32 o 1 0 24 620.52 543.75 26.97 o 2 0 24 405.00 359.64 22.90 o 0 1 24 117.35 127.37 10.09 o 1 1 24 19.10 16.50 14.25 o 2 1 24 234.27 226.97 13.55 o 0 2 24 75.04 68.13 8.66 o 1 2 24 219.71 222.69 14.56 o ############################################################################# # # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data__Ni_thio_phen _shelx_refln_list_code 4 _shelx_F_calc_maximum 209.52 _exptl_crystal_F_000 436.00 _reflns_d_resolution_high 0.7698 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.4340 _cell_length_b 8.7820 _cell_length_c 11.3440 _cell_angle_alpha 90.469 _cell_angle_beta 91.275 _cell_angle_gamma 104.230 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 849.76 840.22 8.92 o 2 0 0 10332.06 10175.85 105.72 o 3 0 0 7.91 13.92 0.55 o 4 0 0 252.85 216.15 3.20 o 5 0 0 1272.69 1225.69 14.05 o 6 0 0 126.73 118.87 2.78 o 7 0 0 442.67 448.70 6.50 o 8 0 0 285.62 290.61 5.08 o 9 0 0 3.29 6.83 2.27 o 10 0 0 5.11 5.34 0.71 o -10 1 0 45.65 48.03 3.11 o -9 1 0 188.58 200.79 6.08 o -8 1 0 44.18 45.05 2.46 o -7 1 0 185.43 191.08 5.05 o -6 1 0 46.69 50.88 2.20 o -5 1 0 253.11 276.91 5.70 o -4 1 0 9.29 10.10 0.65 o -3 1 0 4.76 5.44 0.39 o -2 1 0 1242.83 1235.15 18.77 o -1 1 0 4024.96 3819.10 56.31 o 0 1 0 36.69 47.77 1.04 o 1 1 0 3876.09 3388.01 50.10 o 2 1 0 18.34 49.58 1.42 o 3 1 0 5377.65 5317.69 79.10 o 4 1 0 1505.00 1362.79 21.62 o 5 1 0 191.92 187.06 4.53 o 6 1 0 22.19 21.23 1.42 o 7 1 0 448.47 453.10 9.45 o 8 1 0 217.32 219.56 6.08 o 9 1 0 106.18 93.60 4.14 o 10 1 0 156.50 158.20 5.70 o -10 2 0 532.91 546.70 12.17 o -9 2 0 522.78 556.66 11.78 o -8 2 0 52.36 47.64 2.59 o -7 2 0 440.98 475.88 9.58 o -6 2 0 694.81 685.60 12.30 o -5 2 0 2564.88 2673.67 41.04 o -4 2 0 712.51 760.17 12.69 o -3 2 0 1159.08 1173.14 18.38 o -2 2 0 28.07 41.30 1.29 o -1 2 0 181.13 186.16 3.37 o 0 2 0 753.39 744.25 11.65 o 1 2 0 68.52 82.08 1.94 o 2 2 0 1342.17 1240.84 19.29 o 3 2 0 1220.18 1149.96 18.38 o 4 2 0 6.64 5.44 0.39 o 5 2 0 121.30 123.37 3.50 o 6 2 0 42.72 38.97 2.07 o 7 2 0 99.33 102.92 3.62 o 8 2 0 28.35 43.89 2.59 o 9 2 0 1.28 2.72 0.65 o -10 3 0 25.07 25.50 1.68 o -9 3 0 2.75 2.85 0.65 o -8 3 0 400.71 422.42 9.19 o -7 3 0 25.23 27.32 1.81 o -6 3 0 6313.94 6553.61 98.39 o -5 3 0 157.61 167.65 4.14 o -4 3 0 2218.64 2280.64 35.08 o -3 3 0 619.48 615.31 10.36 o -2 3 0 3602.97 3463.09 51.78 o -1 3 0 3250.63 3128.32 46.86 o 0 3 0 408.75 373.09 6.47 o 1 3 0 3537.05 3297.65 49.45 o 2 3 0 2557.40 2383.94 36.38 o 3 3 0 824.42 726.90 12.43 o 4 3 0 39.07 41.43 1.81 o 5 3 0 586.05 563.78 10.74 o 6 3 0 648.44 626.05 12.04 o 7 3 0 10.78 10.10 0.78 o 8 3 0 7.88 8.93 0.78 o 9 3 0 20.48 21.36 1.42 o -10 4 0 30.88 29.00 1.81 o -9 4 0 9.02 10.49 0.78 o -8 4 0 96.45 101.11 3.75 o -7 4 0 122.54 130.23 4.01 o -6 4 0 637.19 669.16 12.30 o -5 4 0 75.89 75.86 2.59 o -4 4 0 440.68 471.48 8.67 o -3 4 0 4132.05 4265.72 64.08 o -2 4 0 848.72 858.56 13.98 o -1 4 0 96.26 103.82 2.72 o 0 4 0 473.54 416.07 7.51 o 1 4 0 2739.77 2748.23 41.81 o 2 4 0 435.33 377.50 7.38 o 3 4 0 384.68 357.30 7.12 o 4 4 0 118.79 99.16 3.24 o 5 4 0 1368.71 1298.71 22.01 o 6 4 0 90.37 92.82 3.62 o 7 4 0 235.62 230.95 6.47 o 8 4 0 9.73 10.36 0.91 o -10 5 0 2.37 4.27 0.65 o -9 5 0 337.07 332.70 8.41 o -8 5 0 0.83 1.42 1.29 o -7 5 0 822.16 829.17 15.28 o -6 5 0 4.19 5.44 0.52 o -5 5 0 1176.70 1142.20 19.16 o -4 5 0 1916.48 1909.74 30.16 o -3 5 0 719.62 748.00 12.82 o -2 5 0 453.37 461.25 8.54 o -1 5 0 271.81 272.89 5.57 o 0 5 0 1578.29 1567.72 24.86 o 1 5 0 1802.76 1831.55 28.87 o 2 5 0 345.75 340.47 6.99 o 3 5 0 109.36 107.32 3.50 o 4 5 0 1634.95 1510.24 25.11 o 5 5 0 135.12 124.41 4.14 o 6 5 0 40.26 40.65 2.59 o 7 5 0 2.86 2.59 0.65 o 8 5 0 96.50 90.23 4.14 o -10 6 0 176.10 165.57 5.96 o -9 6 0 175.14 167.65 5.70 o -8 6 0 361.91 360.28 8.54 o -7 6 0 228.36 223.57 5.96 o -6 6 0 4.73 5.44 0.65 o -5 6 0 33.02 36.25 1.94 o -4 6 0 118.33 118.58 3.50 o -3 6 0 569.66 590.97 10.87 o -2 6 0 54.97 60.97 2.33 o -1 6 0 1281.36 1241.88 20.45 o 0 6 0 2580.73 2609.84 40.52 o 1 6 0 5.72 6.34 0.52 o 2 6 0 769.36 802.50 14.37 o 3 6 0 57.13 49.58 2.46 o 4 6 0 310.85 297.10 7.12 o 5 6 0 3.31 3.75 0.65 o 6 6 0 55.55 46.09 2.85 o 7 6 0 25.26 25.50 1.42 o -10 7 0 0.05 1.68 0.91 o -9 7 0 307.08 309.79 8.41 o -8 7 0 63.25 64.47 3.37 o -7 7 0 9.25 9.58 0.78 o -6 7 0 119.55 141.50 4.53 o -5 7 0 974.68 1003.55 17.74 o -4 7 0 6.52 4.92 0.65 o -3 7 0 486.80 476.27 9.45 o -2 7 0 184.28 184.48 4.79 o -1 7 0 2166.95 2183.80 34.69 o 0 7 0 23.10 17.87 1.17 o 1 7 0 617.92 622.30 11.91 o 2 7 0 0.75 5.31 0.52 o 3 7 0 553.83 494.91 10.49 o 4 7 0 366.96 332.44 8.41 o 5 7 0 202.31 177.23 5.83 o 6 7 0 80.18 76.90 3.88 o -9 8 0 27.44 27.32 1.68 o -8 8 0 34.87 31.46 1.81 o -7 8 0 5.38 5.83 0.65 o -6 8 0 486.22 468.37 10.23 o -5 8 0 265.60 259.69 6.73 o -4 8 0 7.90 9.19 0.65 o -3 8 0 407.24 415.04 8.93 o -2 8 0 995.11 973.64 17.35 o -1 8 0 82.93 84.54 3.37 o 0 8 0 30.76 31.59 2.20 o 1 8 0 42.67 41.17 2.46 o 2 8 0 340.23 330.89 8.03 o 3 8 0 533.44 511.87 11.26 o 4 8 0 1.68 4.27 0.78 o 5 8 0 52.41 57.61 3.24 o -8 9 0 1.65 0.91 1.55 o -7 9 0 256.23 247.91 7.12 o -6 9 0 520.34 492.97 11.00 o -5 9 0 3.04 3.75 0.65 o -4 9 0 161.83 162.86 5.31 o -3 9 0 2.48 2.59 1.29 o -2 9 0 471.57 455.43 9.97 o -1 9 0 64.63 68.22 3.24 o 0 9 0 329.45 341.64 8.29 o 1 9 0 271.72 298.14 7.77 o 2 9 0 2.67 2.20 1.29 o 3 9 0 16.44 15.79 1.04 o 4 9 0 10.30 11.26 1.04 o -7 10 0 258.02 258.78 7.64 o -6 10 0 0.84 0.00 1.29 o -5 10 0 10.06 8.29 0.78 o -4 10 0 0.09 1.29 0.65 o -3 10 0 422.95 415.94 9.84 o -2 10 0 421.28 398.73 9.58 o -1 10 0 271.86 281.57 7.64 o 0 10 0 358.76 373.87 9.32 o 1 10 0 0.37 1.04 1.29 o 2 10 0 175.33 188.23 6.34 o -5 11 0 8.48 9.97 0.91 o -4 11 0 31.60 30.42 1.94 o -3 11 0 14.19 13.20 0.91 o -2 11 0 1.85 4.01 0.65 o -1 11 0 0.97 1.42 0.65 o 0 11 0 1.74 1.29 0.91 o 0 -11 1 366.67 379.44 9.97 o 1 -11 1 244.09 268.23 7.90 o 2 -11 1 2.11 3.62 0.78 o 3 -11 1 127.53 124.15 5.05 o 4 -11 1 2.35 3.24 0.78 o 5 -11 1 133.61 144.09 5.57 o -2 -10 1 22.31 23.56 1.42 o -1 -10 1 187.64 189.78 6.21 o 0 -10 1 241.75 245.45 7.12 o 1 -10 1 31.22 34.31 1.81 o 2 -10 1 73.02 73.53 3.75 o 3 -10 1 18.15 18.38 1.17 o 4 -10 1 231.76 234.70 6.86 o 5 -10 1 134.94 134.12 5.05 o 6 -10 1 23.03 17.61 1.17 o 7 -10 1 165.27 149.13 5.57 o -4 -9 1 61.69 69.13 3.62 o -3 -9 1 19.74 23.30 1.55 o -2 -9 1 158.22 159.88 5.44 o -1 -9 1 49.82 48.42 2.85 o 0 -9 1 178.85 185.77 5.57 o 1 -9 1 51.50 55.80 2.85 o 2 -9 1 373.29 360.80 8.54 o 3 -9 1 229.81 224.22 6.34 o 4 -9 1 104.89 105.64 4.01 o 5 -9 1 9.79 8.16 0.78 o 6 -9 1 27.20 23.69 1.29 o 7 -9 1 39.49 43.24 2.85 o 8 -9 1 67.93 60.59 3.50 o -5 -8 1 226.55 233.41 7.12 o -4 -8 1 2.17 2.20 0.65 o -3 -8 1 533.99 541.91 11.78 o -2 -8 1 4.84 4.79 0.65 o -1 -8 1 606.95 612.33 12.30 o 0 -8 1 11.43 13.98 0.91 o 1 -8 1 1104.72 1104.14 19.42 o 2 -8 1 391.70 396.27 8.67 o 3 -8 1 289.49 287.26 6.86 o 4 -8 1 292.54 296.33 7.25 o 5 -8 1 21.38 23.56 1.29 o 6 -8 1 516.41 508.25 10.87 o 7 -8 1 133.23 126.87 4.79 o 8 -8 1 32.15 31.33 1.81 o 9 -8 1 103.05 96.45 4.53 o -6 -7 1 199.51 186.42 6.34 o -5 -7 1 32.49 32.23 1.81 o -4 -7 1 75.53 80.52 3.88 o -3 -7 1 46.32 52.04 2.72 o -2 -7 1 303.94 320.53 7.51 o -1 -7 1 542.65 536.99 10.62 o 0 -7 1 225.39 234.06 5.70 o 1 -7 1 341.06 340.99 7.38 o 2 -7 1 130.83 126.22 3.88 o 3 -7 1 581.95 563.40 10.87 o 4 -7 1 9.03 9.06 0.65 o 5 -7 1 1120.00 1116.43 19.42 o 6 -7 1 614.33 624.89 12.43 o 7 -7 1 327.05 325.19 8.03 o 8 -7 1 207.12 206.48 6.21 o 9 -7 1 31.73 32.49 1.94 o -7 -6 1 0.07 0.13 1.55 o -6 -6 1 341.76 319.76 8.29 o -5 -6 1 5.51 4.14 0.65 o -4 -6 1 1484.28 1451.86 24.73 o -3 -6 1 759.95 779.46 14.24 o -2 -6 1 102.23 111.20 3.62 o -1 -6 1 267.59 263.44 5.96 o 0 -6 1 2.50 4.40 0.52 o 1 -6 1 480.76 494.52 9.32 o 2 -6 1 210.80 210.63 4.92 o 3 -6 1 270.63 255.81 5.83 o 4 -6 1 402.70 413.74 8.41 o 5 -6 1 1099.51 1100.90 18.90 o 6 -6 1 168.87 172.82 4.92 o 7 -6 1 248.70 259.82 6.60 o 8 -6 1 136.61 149.78 4.92 o 9 -6 1 1082.91 1072.68 20.07 o 10 -6 1 93.71 95.54 4.53 o -8 -5 1 0.03 2.33 1.17 o -7 -5 1 201.18 183.31 5.83 o -6 -5 1 29.15 27.19 1.55 o -5 -5 1 887.49 876.29 16.05 o -4 -5 1 981.70 942.57 16.70 o -3 -5 1 197.17 237.42 5.96 o -2 -5 1 1042.82 1034.23 17.35 o -1 -5 1 49.88 58.64 2.20 o 0 -5 1 2423.03 2355.98 36.38 o 1 -5 1 962.48 937.14 15.53 o 2 -5 1 244.74 241.82 5.18 o 3 -5 1 455.01 482.87 8.93 o 4 -5 1 208.75 224.09 5.18 o 5 -5 1 110.92 114.57 3.50 o 6 -5 1 22.41 21.23 1.17 o 7 -5 1 114.64 124.80 4.14 o 8 -5 1 272.14 283.90 7.25 o 9 -5 1 122.49 118.06 4.53 o 10 -5 1 14.95 16.57 1.04 o -8 -4 1 11.05 10.62 0.91 o -7 -4 1 163.55 159.49 5.31 o -6 -4 1 118.67 123.11 4.14 o -5 -4 1 236.93 233.28 5.83 o -4 -4 1 1.66 3.37 0.39 o -3 -4 1 116.54 145.38 3.88 o -2 -4 1 65.55 68.48 2.33 o -1 -4 1 4705.55 4648.79 69.65 o 0 -4 1 1597.08 1500.01 23.43 o 1 -4 1 451.96 434.46 7.77 o 2 -4 1 1075.89 1094.81 17.48 o 3 -4 1 332.83 353.68 6.73 o 4 -4 1 2851.10 3014.14 46.09 o 5 -4 1 26.79 24.34 1.42 o 6 -4 1 1604.31 1621.44 26.28 o 7 -4 1 625.95 644.18 12.30 o 8 -4 1 117.77 119.23 4.14 o 9 -4 1 130.67 124.67 4.66 o 10 -4 1 99.20 100.46 4.40 o -9 -3 1 79.20 77.80 3.75 o -8 -3 1 12.87 13.20 0.91 o -7 -3 1 84.64 74.05 3.37 o -6 -3 1 126.39 129.59 4.14 o -5 -3 1 262.39 294.51 6.60 o -4 -3 1 382.20 367.01 7.38 o -3 -3 1 854.81 870.85 14.50 o -2 -3 1 3829.80 3927.45 59.29 o -1 -3 1 0.21 0.78 0.52 o 0 -3 1 1246.07 1247.96 19.42 o 1 -3 1 1953.23 2022.24 30.68 o 2 -3 1 601.40 703.21 11.52 o 3 -3 1 3599.86 3652.10 54.89 o 4 -3 1 95.66 143.70 3.50 o 5 -3 1 195.12 221.11 4.92 o 6 -3 1 986.01 985.42 16.83 o 7 -3 1 225.72 252.31 6.08 o 8 -3 1 704.26 729.36 13.85 o 9 -3 1 21.60 22.27 1.42 o 10 -3 1 702.26 736.35 15.15 o -9 -2 1 0.39 -1.04 1.29 o -8 -2 1 101.47 101.88 4.01 o -7 -2 1 352.24 336.85 7.77 o -6 -2 1 868.87 829.43 14.89 o -5 -2 1 1200.79 1255.73 20.71 o -4 -2 1 9.56 19.03 1.29 o -3 -2 1 5451.48 5312.90 79.23 o -2 -2 1 4.84 20.58 1.04 o -1 -2 1 460.29 463.58 7.77 o 0 -2 1 1469.16 1499.62 22.65 o 1 -2 1 2515.82 2499.03 37.28 o 2 -2 1 502.71 496.47 8.16 o 3 -2 1 430.28 498.93 8.54 o 4 -2 1 613.08 670.46 11.39 o 5 -2 1 987.63 1042.00 17.22 o 6 -2 1 80.09 68.74 2.59 o 7 -2 1 165.66 183.05 4.92 o 8 -2 1 6.67 7.38 0.65 o 9 -2 1 272.69 275.10 7.25 o 10 -2 1 147.38 151.46 5.44 o -10 -1 1 0.77 0.52 1.55 o -9 -1 1 0.90 0.13 1.04 o -8 -1 1 64.11 62.92 2.98 o -7 -1 1 570.56 532.33 10.62 o -6 -1 1 226.99 219.56 5.31 o -5 -1 1 3.79 44.92 1.94 o -4 -1 1 3049.42 3173.50 48.16 o -3 -1 1 2411.69 2442.98 37.02 o -2 -1 1 43898.67 40312.13 590.19 o -1 -1 1 1299.79 1317.09 20.07 o 0 -1 1 17342.00 14139.76 210.50 o 1 -1 1 4799.37 4607.23 67.84 o 2 -1 1 1381.02 1367.45 20.84 o 3 -1 1 172.35 149.39 3.24 o 4 -1 1 1333.17 1356.96 21.36 o 5 -1 1 2631.41 2608.16 40.13 o 6 -1 1 467.44 487.66 9.32 o 7 -1 1 197.20 187.06 5.05 o 8 -1 1 125.80 126.48 4.27 o 9 -1 1 159.70 166.87 5.31 o 10 -1 1 169.10 167.91 5.83 o -10 0 1 18.84 20.51 1.94 o -9 0 1 218.61 230.68 4.71 o -8 0 1 145.52 151.82 5.50 o -7 0 1 119.38 119.20 2.72 o -6 0 1 93.04 100.01 2.29 o -5 0 1 45.26 51.55 1.42 o -4 0 1 1719.22 1811.66 26.41 o -3 0 1 1342.60 1432.69 17.41 o -2 0 1 3277.56 3569.92 43.43 o -1 0 1 2112.79 2090.14 24.86 o 1 0 1 1512.41 1396.26 14.78 o 2 0 1 1590.15 1543.34 16.52 o 3 0 1 511.24 480.84 5.81 o 4 0 1 2658.81 2561.89 38.06 o 5 0 1 757.98 733.52 14.43 o 6 0 1 42.77 47.92 1.46 o 7 0 1 184.74 185.03 3.57 o 8 0 1 80.16 85.13 2.42 o 9 0 1 1153.65 1137.78 18.38 o 10 0 1 0.01 -0.14 0.96 o -10 1 1 7.99 10.87 0.91 o -9 1 1 587.31 601.20 12.56 o -8 1 1 2.80 2.33 1.29 o -7 1 1 760.78 793.83 14.37 o -6 1 1 605.38 626.70 11.39 o -5 1 1 4053.31 4137.69 62.53 o -4 1 1 13.60 12.04 0.65 o -3 1 1 7.01 13.20 0.78 o -2 1 1 285.86 281.57 4.92 o -1 1 1 2483.80 2666.16 39.48 o 0 1 1 196.28 196.90 3.37 o 1 1 1 3570.93 3153.69 46.73 o 2 1 1 782.71 762.63 12.17 o 3 1 1 2843.71 2776.07 41.94 o 4 1 1 1.28 1.68 0.26 o 5 1 1 58.11 60.07 2.20 o 6 1 1 619.86 598.87 11.26 o 7 1 1 107.91 103.82 3.62 o 8 1 1 415.26 408.31 9.19 o 9 1 1 47.84 53.34 2.98 o 10 1 1 57.23 59.16 3.24 o -10 2 1 20.99 25.76 1.68 o -9 2 1 34.79 36.12 2.46 o -8 2 1 936.80 986.98 17.74 o -7 2 1 130.86 145.51 4.27 o -6 2 1 3565.37 3756.05 57.35 o -5 2 1 1598.47 1623.90 25.76 o -4 2 1 2353.03 2521.94 38.45 o -3 2 1 1135.97 1135.59 17.87 o -2 2 1 4315.80 4417.19 65.51 o -1 2 1 13734.59 11426.10 167.78 o 0 2 1 2038.13 1908.84 28.74 o 1 2 1 1483.29 1337.93 20.71 o 2 2 1 1112.23 1032.68 16.31 o 3 2 1 1151.76 994.36 16.05 o 4 2 1 771.79 728.71 12.56 o 5 2 1 119.17 115.60 3.37 o 6 2 1 974.07 928.98 16.31 o 7 2 1 204.03 209.33 5.70 o 8 2 1 40.18 40.13 2.59 o 9 2 1 13.56 16.44 1.04 o -10 3 1 295.06 284.93 7.90 o -9 3 1 24.99 26.15 1.55 o -8 3 1 60.56 56.18 2.72 o -7 3 1 2.13 3.75 0.52 o -6 3 1 112.89 121.69 3.62 o -5 3 1 323.40 345.00 6.86 o -4 3 1 484.60 510.45 9.06 o -3 3 1 528.10 543.85 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