# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' (CH3)2SnSC(S)N(CH2CH2OH)2 in Pnma' _shelx_refln_list_code 4 _shelx_F_calc_maximum 375.26 _exptl_crystal_F_000 1032.00 _reflns_d_resolution_high 0.7107 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' _cell_length_a 7.2510 _cell_length_b 28.7610 _cell_length_c 9.6350 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6646.67 6429.21 79.76 o 4 0 0 31923.20 30914.67 258.75 o 6 0 0 100.48 115.16 11.46 o 8 0 0 226.19 208.21 16.24 o 10 0 0 10.20 14.04 18.06 o 2 1 0 17444.31 16452.54 92.09 o 4 1 0 3890.02 3312.18 59.91 o 6 1 0 8.72 4.85 7.53 o 8 1 0 1173.77 1285.76 40.47 o 10 1 0 420.92 391.57 17.25 o 2 2 0 14.61 18.68 5.51 o 4 2 0 11305.34 10494.56 146.63 o 6 2 0 2625.22 2544.79 98.84 o 8 2 0 44.30 47.64 14.70 o 10 2 0 128.72 138.56 19.99 o 2 3 0 438.35 395.27 17.89 o 4 3 0 24231.71 23176.96 223.56 o 6 3 0 61.99 45.41 12.29 o 8 3 0 2153.01 2468.47 116.95 o 10 3 0 91.95 81.15 19.16 o 0 4 0 8757.22 8701.29 68.67 o 2 4 0 23827.36 23501.52 167.04 o 4 4 0 6.83 30.00 8.84 o 6 4 0 9315.68 9018.19 176.54 o 8 4 0 7.81 2.71 14.48 o 10 4 0 535.57 533.12 31.06 o 2 5 0 14709.59 15076.25 133.57 o 4 5 0 19112.31 18057.49 197.98 o 6 5 0 176.46 201.16 14.22 o 8 5 0 1530.60 1550.56 71.21 o 10 5 0 6.23 15.00 17.80 o 0 6 0 24341.48 23436.16 145.87 o 2 6 0 3125.01 3076.41 64.04 o 4 6 0 5601.14 5754.43 112.21 o 6 6 0 8360.29 8118.05 170.04 o 8 6 0 16.40 -4.02 14.17 o 10 6 0 270.83 267.08 21.75 o 2 7 0 27140.70 27238.68 197.51 o 4 7 0 9180.55 9167.16 142.16 o 6 7 0 1119.06 1064.67 60.37 o 8 7 0 841.48 845.30 31.27 o 10 7 0 14.18 25.11 18.28 o 0 8 0 25878.51 24617.26 169.93 o 2 8 0 7840.03 8215.10 107.04 o 4 8 0 240.09 264.57 13.31 o 6 8 0 2353.80 2271.23 98.86 o 8 8 0 280.08 244.54 16.90 o 10 8 0 170.80 200.23 20.61 o 2 9 0 62086.57 61226.77 338.65 o 4 9 0 633.09 768.35 35.59 o 6 9 0 1082.19 1112.81 47.71 o 8 9 0 243.01 217.10 16.85 o 0 10 0 38049.69 36466.13 235.32 o 2 10 0 2581.64 2812.13 70.61 o 4 10 0 367.71 379.33 26.56 o 6 10 0 3269.25 3245.61 113.42 o 8 10 0 1693.40 1748.99 85.13 o 2 11 0 32838.45 33770.67 249.97 o 4 11 0 224.72 230.10 10.55 o 6 11 0 586.07 607.06 29.77 o 8 11 0 103.20 113.36 16.01 o 0 12 0 9425.94 9309.99 118.69 o 2 12 0 4275.15 4445.45 90.33 o 4 12 0 1226.30 1333.55 62.80 o 6 12 0 3054.86 3050.53 113.77 o 8 12 0 70.72 63.43 15.79 o 2 13 0 7335.02 7727.88 120.86 o 4 13 0 13682.63 13791.46 196.27 o 6 13 0 188.06 178.84 14.18 o 8 13 0 1500.60 1425.22 76.46 o 0 14 0 24064.23 23745.41 215.02 o 2 14 0 2372.29 2176.55 69.45 o 4 14 0 4653.51 4793.48 124.22 o 6 14 0 2719.86 3001.39 114.83 o 8 14 0 48.45 59.14 16.62 o 2 15 0 1236.81 1485.00 61.01 o 4 15 0 14720.33 14623.09 211.47 o 6 15 0 168.26 156.06 14.66 o 8 15 0 1334.80 1234.97 72.90 o 0 16 0 13266.02 12984.47 165.89 o 2 16 0 1411.76 1392.35 60.57 o 4 16 0 3922.23 3985.42 118.42 o 6 16 0 3079.54 3093.91 120.60 o 8 16 0 2.44 36.43 17.71 o 2 17 0 16.36 24.10 9.01 o 4 17 0 4515.52 4708.63 130.79 o 6 17 0 7.41 4.02 13.17 o 8 17 0 1328.68 1251.85 69.25 o 0 18 0 28608.41 26565.78 261.92 o 2 18 0 3012.01 3106.41 95.78 o 4 18 0 2387.66 2572.41 103.38 o 6 18 0 837.41 801.02 38.38 o 8 18 0 66.40 63.65 18.20 o 2 19 0 8470.04 8669.45 153.89 o 4 19 0 2719.65 2899.75 111.41 o 6 19 0 32.67 20.60 12.73 o 8 19 0 523.64 520.35 27.60 o 0 20 0 44492.14 43601.36 367.21 o 2 20 0 112.04 77.45 11.86 o 4 20 0 8363.13 8475.43 180.65 o 6 20 0 10.91 5.25 12.77 o 8 20 0 83.22 88.11 18.29 o 2 21 0 4426.23 4794.75 121.19 o 4 21 0 310.95 359.47 17.12 o 6 21 0 85.03 72.75 14.44 o 8 21 0 328.27 358.46 20.88 o 0 22 0 9282.47 8959.59 175.90 o 2 22 0 1874.71 1845.27 88.54 o 4 22 0 767.17 751.71 35.88 o 6 22 0 936.53 872.90 50.76 o 8 22 0 22.24 20.82 17.10 o 2 23 0 3224.51 3186.00 106.83 o 4 23 0 4986.19 4999.04 153.93 o 6 23 0 4.32 -16.36 16.36 o 8 23 0 351.46 362.15 21.85 o 0 24 0 1244.38 1398.88 62.96 o 2 24 0 1351.93 1185.16 75.51 o 4 24 0 32.48 28.61 15.62 o 6 24 0 3826.28 3827.48 154.31 o 8 24 0 34.93 28.61 18.81 o 2 25 0 5489.50 5572.30 149.25 o 4 25 0 2415.10 2287.28 107.63 o 6 25 0 358.77 330.36 21.15 o 8 25 0 308.09 301.21 21.84 o 0 26 0 760.18 568.84 38.52 o 2 26 0 1971.14 1996.10 94.65 o 4 26 0 1.59 -0.22 14.17 o 6 26 0 1649.82 1577.69 86.77 o 2 27 0 4207.90 4061.13 136.52 o 4 27 0 395.57 433.04 20.01 o 6 27 0 346.77 297.85 20.75 o 0 28 0 4007.77 3938.90 133.50 o 2 28 0 456.06 405.53 26.90 o 4 28 0 456.15 492.38 19.62 o 6 28 0 616.06 601.08 35.05 o 2 29 0 4900.79 4709.11 154.66 o 4 29 0 154.46 168.25 15.97 o 6 29 0 65.84 49.48 17.89 o 0 30 0 3723.07 3864.40 138.98 o 2 30 0 116.72 95.56 18.86 o 4 30 0 175.01 194.08 16.41 o 6 30 0 57.30 63.69 17.98 o 2 31 0 1533.86 1320.39 85.10 o 4 31 0 201.47 235.97 17.90 o 6 31 0 17.77 3.15 18.37 o 0 32 0 1857.75 1968.19 97.96 o 2 32 0 193.46 194.01 17.55 o 4 32 0 674.50 654.85 28.71 o 6 32 0 591.46 593.66 36.32 o 2 33 0 64.97 57.44 15.27 o 4 33 0 1874.78 1968.54 94.65 o 0 34 0 2053.17 2175.32 99.48 o 2 34 0 200.25 211.90 16.76 o 4 34 0 704.97 643.42 30.81 o 2 35 0 12.13 3.98 15.09 o 4 35 0 1074.47 1249.30 61.77 o 0 36 0 1495.34 1147.82 83.61 o 2 36 0 54.99 67.67 16.62 o 4 36 0 486.23 392.86 24.09 o 2 37 0 81.93 96.90 17.85 o 4 37 0 301.34 353.16 22.81 o 0 38 0 1823.99 2001.69 93.21 o 2 38 0 219.26 240.53 21.01 o 2 39 0 622.62 670.39 32.95 o 0 40 0 546.16 492.35 32.06 o 1 0 1 536.16 523.05 15.36 o 2 0 1 2088.55 2006.18 48.83 o 3 0 1 1990.04 1594.48 38.68 o 4 0 1 138.80 125.41 6.14 o 5 0 1 3251.13 3351.17 69.22 o 6 0 1 15.00 19.86 7.25 o 7 0 1 534.63 482.40 27.26 o 8 0 1 11.76 7.88 9.58 o 9 0 1 2125.45 2209.09 70.24 o 10 0 1 31.72 39.81 12.41 o 0 1 1 5384.78 5722.52 50.51 o 1 1 1 73181.80 73080.70 2409.59 o 2 1 1 1549.16 1692.92 32.48 o 3 1 1 7425.12 7245.02 55.72 o 4 1 1 79.32 66.63 4.09 o 5 1 1 5043.78 5063.21 59.13 o 6 1 1 90.41 87.12 5.89 o 7 1 1 237.47 230.60 7.06 o 8 1 1 186.52 176.83 7.73 o 9 1 1 20.38 26.70 8.94 o 10 1 1 1.25 5.42 8.65 o 1 2 1 10876.29 11355.30 194.19 o 2 2 1 17638.17 17511.50 595.14 o 3 2 1 11286.98 10741.37 294.79 o 4 2 1 6.79 38.75 5.63 o 5 2 1 1119.23 1155.74 48.29 o 6 2 1 114.84 115.43 8.11 o 7 2 1 686.59 713.77 28.72 o 8 2 1 14.17 16.89 9.82 o 9 2 1 883.99 911.09 28.89 o 10 2 1 21.42 35.87 12.66 o 0 3 1 4560.63 4874.69 35.61 o 1 3 1 8219.59 8938.91 120.51 o 2 3 1 885.09 978.13 27.43 o 3 3 1 1942.72 1932.34 40.98 o 4 3 1 65.84 54.08 5.89 o 5 3 1 8637.58 8521.62 108.17 o 6 3 1 273.75 250.11 9.90 o 7 3 1 409.58 364.37 12.55 o 8 3 1 3.92 4.78 9.91 o 9 3 1 195.87 208.22 13.40 o 10 3 1 24.34 19.46 17.80 o 1 4 1 15008.71 15365.01 216.39 o 2 4 1 2412.46 2452.74 39.10 o 3 4 1 28609.72 27435.89 1441.56 o 4 4 1 3620.29 3501.61 88.53 o 5 4 1 1470.35 1466.33 53.48 o 6 4 1 0.07 -0.40 8.75 o 7 4 1 1825.63 1802.48 144.77 o 8 4 1 150.40 149.25 10.83 o 9 4 1 358.99 332.25 22.68 o 10 4 1 11.06 14.14 12.51 o 0 5 1 1829.40 2108.76 28.42 o 1 5 1 13805.27 13945.55 225.59 o 2 5 1 6642.93 6805.03 65.17 o 3 5 1 6487.07 6563.79 145.50 o 4 5 1 0.38 10.53 5.74 o 5 5 1 10363.79 10255.70 215.51 o 6 5 1 2668.17 2597.44 95.56 o 7 5 1 2461.46 2293.27 143.14 o 8 5 1 8.16 12.63 9.85 o 9 5 1 399.25 459.32 19.95 o 10 5 1 37.64 39.46 13.01 o 1 6 1 699.51 685.40 16.04 o 2 6 1 2687.33 2796.77 43.77 o 3 6 1 14298.57 13957.06 109.28 o 4 6 1 2275.12 2317.46 53.07 o 5 6 1 2850.50 2894.48 69.25 o 6 6 1 101.74 100.95 9.04 o 7 6 1 1634.81 1713.29 212.81 o 8 6 1 296.19 279.74 11.76 o 9 6 1 365.65 342.06 15.00 o 10 6 1 0.82 -3.19 12.37 o 0 7 1 7442.58 7776.26 61.40 o 1 7 1 188.34 221.88 7.50 o 2 7 1 1099.68 1111.27 39.24 o 3 7 1 488.62 468.03 23.19 o 4 7 1 185.88 196.06 9.55 o 5 7 1 5648.85 5632.84 305.44 o 6 7 1 54.85 68.56 8.77 o 7 7 1 2165.44 2272.41 91.75 o 8 7 1 0.36 1.05 9.96 o 9 7 1 162.87 207.06 12.96 o 10 7 1 2.72 10.04 12.73 o 1 8 1 25011.87 25167.68 470.46 o 2 8 1 4675.62 5207.18 61.57 o 3 8 1 15853.72 15940.63 480.71 o 4 8 1 225.88 242.88 8.63 o 5 8 1 211.47 182.72 17.01 o 6 8 1 159.01 149.26 9.19 o 7 8 1 979.83 946.26 28.14 o 8 8 1 25.20 29.03 9.85 o 9 8 1 554.29 572.07 23.04 o 0 9 1 9846.75 9985.07 246.06 o 1 9 1 29399.79 29720.23 527.09 o 2 9 1 4.06 12.41 4.87 o 3 9 1 1506.94 1518.09 42.82 o 4 9 1 2519.15 2464.88 57.03 o 5 9 1 1741.57 1624.93 55.84 o 6 9 1 1.99 1.98 8.39 o 7 9 1 2036.94 2054.97 69.79 o 8 9 1 10.37 18.72 9.97 o 9 9 1 1.84 -6.24 11.51 o 1 10 1 51966.55 53283.24 1615.14 o 2 10 1 1834.90 2096.49 43.37 o 3 10 1 17589.33 17975.32 134.82 o 4 10 1 6.99 12.14 6.21 o 5 10 1 3038.47 3056.02 71.81 o 6 10 1 0.03 -0.76 8.41 o 7 10 1 127.25 131.85 10.43 o 8 10 1 1.11 5.26 9.94 o 9 10 1 162.78 146.97 12.75 o 0 11 1 16671.96 16721.59 521.17 o 1 11 1 6413.06 6213.71 83.45 o 2 11 1 2256.28 2310.60 47.11 o 3 11 1 383.57 365.67 13.55 o 4 11 1 403.92 439.86 35.19 o 5 11 1 3967.78 3779.17 81.46 o 6 11 1 28.17 29.99 8.46 o 7 11 1 1821.58 1881.53 60.95 o 8 11 1 6.36 6.83 10.00 o 9 11 1 1.41 11.10 11.64 o 1 12 1 11697.58 11875.88 92.04 o 2 12 1 1924.95 2368.44 66.25 o 3 12 1 8483.98 8561.19 96.78 o 4 12 1 27.66 54.56 6.87 o 5 12 1 33.49 31.79 8.75 o 6 12 1 26.65 27.22 8.68 o 7 12 1 611.94 628.34 41.05 o 8 12 1 14.61 17.50 10.40 o 9 12 1 324.56 295.23 16.20 o 0 13 1 1.22 3.94 4.55 o 1 13 1 8779.38 8605.61 81.14 o 2 13 1 16.21 46.76 5.43 o 3 13 1 524.10 476.44 29.56 o 4 13 1 152.39 174.30 9.04 o 5 13 1 3441.27 3408.78 82.66 o 6 13 1 251.77 251.60 10.20 o 7 13 1 579.00 595.09 21.14 o 8 13 1 6.19 9.67 10.35 o 9 13 1 157.01 192.03 20.54 o 1 14 1 195.56 217.00 6.26 o 2 14 1 8.94 42.15 8.05 o 3 14 1 11199.65 11538.43 215.11 o 4 14 1 2494.32 2613.25 67.47 o 5 14 1 7998.41 8057.97 120.76 o 6 14 1 45.01 37.14 9.12 o 7 14 1 1379.74 1396.01 45.55 o 8 14 1 188.37 183.58 16.24 o 9 14 1 725.05 691.46 20.10 o 0 15 1 539.43 480.91 78.65 o 1 15 1 3848.12 3866.16 52.22 o 2 15 1 3522.73 3160.77 60.94 o 3 15 1 237.12 239.26 10.84 o 4 15 1 280.06 283.74 11.10 o 5 15 1 8399.23 8221.03 123.10 o 6 15 1 1037.67 1022.54 38.52 o 7 15 1 633.97 634.84 22.84 o 8 15 1 7.43 7.60 11.16 o 9 15 1 207.65 228.15 15.69 o 1 16 1 2.20 0.35 5.81 o 2 16 1 249.44 287.75 11.21 o 3 16 1 3747.95 3737.74 126.05 o 4 16 1 599.65 716.59 21.56 o 5 16 1 1999.12 2054.21 70.37 o 6 16 1 104.99 89.68 9.95 o 7 16 1 1004.59 1016.61 83.35 o 8 16 1 70.70 68.95 12.05 o 9 16 1 368.93 341.88 17.27 o 0 17 1 589.95 513.89 92.47 o 1 17 1 18410.00 17811.32 242.50 o 2 17 1 175.36 137.69 7.23 o 3 17 1 903.26 911.48 30.67 o 4 17 1 99.34 105.33 8.97 o 5 17 1 3306.42 3212.47 84.29 o 6 17 1 380.07 382.47 12.92 o 7 17 1 55.93 59.38 13.60 o 8 17 1 18.82 21.85 11.61 o 9 17 1 48.83 48.55 19.16 o 1 18 1 3251.74 3165.74 58.04 o 2 18 1 5161.09 5498.51 86.01 o 3 18 1 3802.73 3724.28 77.92 o 4 18 1 3.88 -2.73 8.27 o 5 18 1 220.00 256.47 10.80 o 6 18 1 30.97 30.31 10.10 o 7 18 1 250.00 251.38 12.56 o 8 18 1 1.32 16.71 11.49 o 9 18 1 532.08 568.31 23.92 o 0 19 1 1466.35 1435.20 49.50 o 1 19 1 12613.09 11796.20 498.33 o 2 19 1 135.74 111.96 7.92 o 3 19 1 3446.67 3265.74 75.88 o 4 19 1 4.60 2.28 8.64 o 5 19 1 1792.51 1882.28 114.61 o 6 19 1 6.05 14.22 9.01 o 7 19 1 154.07 146.29 11.19 o 8 19 1 66.93 60.42 12.24 o 1 20 1 1037.11 782.46 85.86 o 2 20 1 824.58 855.26 73.96 o 3 20 1 2188.02 2280.11 70.29 o 4 20 1 2.73 13.81 8.90 o 5 20 1 607.19 598.54 23.50 o 6 20 1 0.03 2.88 9.01 o 7 20 1 159.32 158.74 11.74 o 8 20 1 3.21 6.95 11.98 o 0 21 1 792.23 797.95 108.35 o 1 21 1 8249.40 8152.08 389.07 o 2 21 1 25.31 25.05 7.58 o 3 21 1 733.84 690.39 25.79 o 4 21 1 190.71 199.78 10.14 o 5 21 1 1372.18 1345.56 45.11 o 6 21 1 46.83 56.81 9.62 o 7 21 1 135.65 131.81 11.71 o 8 21 1 27.84 27.47 11.95 o 1 22 1 1431.55 1171.90 41.45 o 2 22 1 522.26 525.82 26.78 o 3 22 1 2836.35 2911.73 105.09 o 4 22 1 55.85 71.54 9.71 o 5 22 1 147.18 149.58 14.97 o 6 22 1 0.90 -1.76 9.74 o 7 22 1 376.58 357.65 14.25 o 8 22 1 4.30 5.58 12.23 o 0 23 1 995.81 995.87 33.12 o 1 23 1 1272.51 1019.42 483.00 o 2 23 1 257.45 268.90 9.58 o 3 23 1 180.52 180.17 11.20 o 4 23 1 118.34 103.26 13.41 o 5 23 1 2328.56 2407.54 78.93 o 6 23 1 120.34 131.41 13.67 o 7 23 1 667.58 720.09 22.07 o 8 23 1 7.40 9.87 12.59 o 1 24 1 3460.25 3178.72 92.39 o 2 24 1 20.76 24.19 11.98 o 3 24 1 7729.61 7169.02 346.17 o 4 24 1 777.49 789.43 26.19 o 5 24 1 163.01 172.17 11.93 o 6 24 1 0.86 9.77 11.32 o 7 24 1 342.19 311.75 14.95 o 8 24 1 106.11 132.50 13.35 o 0 25 1 68.04 60.81 8.12 o 1 25 1 19.46 -173.86 489.09 o 2 25 1 308.51 289.20 10.70 o 3 25 1 1644.11 1568.21 58.83 o 4 25 1 5.36 5.60 9.70 o 5 25 1 1412.08 1380.72 46.47 o 6 25 1 304.62 305.56 30.29 o 7 25 1 745.12 760.38 25.03 o 1 26 1 1447.95 1408.12 84.95 o 2 26 1 157.03 158.13 9.81 o 3 26 1 2233.41 2179.95 71.96 o 4 26 1 381.26 403.79 12.56 o 5 26 1 26.72 14.16 10.71 o 6 26 1 50.48 45.12 12.16 o 7 26 1 436.49 391.83 16.96 o 0 27 1 1080.67 1051.80 37.27 o 1 27 1 1243.51 850.21 167.13 o 2 27 1 67.81 55.49 9.26 o 3 27 1 402.25 418.65 20.76 o 4 27 1 143.99 130.70 10.41 o 5 27 1 809.25 800.92 29.32 o 6 27 1 37.80 32.38 14.02 o 7 27 1 663.35 703.47 46.93 o 1 28 1 2262.35 1878.26 112.28 o 2 28 1 203.14 185.30 10.77 o 3 28 1 2098.03 1837.46 392.77 o 4 28 1 1.22 0.39 9.60 o 5 28 1 0.13 8.46 10.68 o 6 28 1 3.58 -1.23 11.67 o 7 28 1 111.88 119.66 14.20 o 0 29 1 1365.14 1340.74 178.28 o 1 29 1 1873.37 1430.09 120.22 o 2 29 1 1.19 14.42 9.86 o 3 29 1 52.08 58.70 13.65 o 4 29 1 183.64 170.56 11.05 o 5 29 1 359.25 385.81 22.99 o 6 29 1 7.06 -4.33 11.62 o 7 29 1 229.17 244.21 14.81 o 1 30 1 1971.80 1574.72 114.39 o 2 30 1 561.06 531.43 51.77 o 3 30 1 1237.67 1249.19 61.59 o 4 30 1 15.24 23.40 10.35 o 5 30 1 92.46 89.25 12.23 o 6 30 1 0.86 8.02 12.23 o 0 31 1 105.26 97.31 10.46 o 1 31 1 1341.51 975.48 118.72 o 2 31 1 8.81 4.74 10.51 o 3 31 1 129.13 118.50 11.79 o 4 31 1 30.00 31.07 10.96 o 5 31 1 368.29 380.53 15.11 o 6 31 1 21.62 15.50 12.49 o 1 32 1 269.95 92.97 302.08 o 2 32 1 126.11 114.40 10.87 o 3 32 1 915.91 905.90 34.85 o 4 32 1 8.22 19.74 11.74 o 5 32 1 179.60 212.58 15.25 o 6 32 1 2.35 4.42 12.70 o 0 33 1 7.71 13.35 10.22 o 1 33 1 1026.18 870.77 79.64 o 2 33 1 109.53 115.66 10.93 o 3 33 1 112.76 92.79 12.29 o 4 33 1 10.58 13.69 12.78 o 5 33 1 833.82 770.90 28.66 o 1 34 1 174.80 83.36 244.48 o 2 34 1 34.10 46.55 20.19 o 3 34 1 466.59 460.36 18.43 o 4 34 1 155.10 173.43 15.51 o 5 34 1 886.00 993.84 35.65 o 0 35 1 143.99 136.07 12.27 o 1 35 1 684.05 626.63 16.29 o 2 35 1 29.37 30.66 10.85 o 3 35 1 65.93 55.19 12.68 o 4 35 1 5.70 25.83 13.70 o 5 35 1 452.06 443.10 18.42 o 1 36 1 20.71 -285.12 301.13 o 2 36 1 69.33 56.20 12.88 o 3 36 1 254.10 291.01 15.87 o 4 36 1 55.39 64.63 13.73 o 0 37 1 131.38 153.94 13.46 o 1 37 1 1097.00 1016.93 46.46 o 2 37 1 49.33 52.53 12.31 o 3 37 1 110.38 67.23 17.15 o 4 37 1 0.89 12.99 13.31 o 1 38 1 288.90 190.29 184.84 o 2 38 1 134.44 134.43 14.07 o 3 38 1 237.00 258.63 14.64 o 0 39 1 86.61 82.56 13.33 o 1 39 1 591.34 582.75 14.23 o 2 39 1 0.60 -1.80 12.76 o 1 40 1 307.04 258.56 27.65 o 0 0 2 140823.14 135356.97 2331.03 o 1 0 2 26554.99 27592.02 1328.29 o 2 0 2 4055.26 3840.91 70.51 o 3 0 2 13648.89 14071.64 152.78 o 4 0 2 11540.82 12172.25 163.85 o 5 0 2 877.61 828.52 40.06 o 6 0 2 587.32 603.07 34.33 o 7 0 2 490.36 515.35 23.40 o 8 0 2 85.45 73.10 16.49 o 9 0 2 192.40 177.37 18.60 o 10 0 2 3.28 -0.31 18.19 o 1 1 2 18078.22 18352.09 393.93 o 2 1 2 1235.80 1229.56 31.41 o 3 1 2 5941.45 6367.11 102.06 o 4 1 2 5188.61 4945.48 104.09 o 5 1 2 1194.13 1060.49 41.06 o 6 1 2 0.22 -3.90 7.92 o 7 1 2 63.93 59.67 9.25 o 8 1 2 1823.02 1790.04 66.96 o 9 1 2 70.76 78.52 12.42 o 10 1 2 247.77 240.97 14.92 o 0 2 2 30457.66 32466.62 173.87 o 1 2 2 2776.61 2721.55 50.18 o 2 2 2 178.19 201.71 10.08 o 3 2 2 1481.51 1477.25 53.94 o 4 2 2 8986.61 9099.31 139.31 o 5 2 2 35.90 50.26 10.41 o 6 2 2 1379.81 1362.14 66.77 o 7 2 2 429.31 442.35 21.90 o 8 2 2 14.35 9.62 15.40 o 9 2 2 2.70 19.46 16.97 o 10 2 2 124.39 128.63 19.47 o 1 3 2 7.22 11.50 3.88 o 2 3 2 7854.72 7927.68 100.19 o 3 3 2 6917.65 7263.93 109.93 o 4 3 2 4427.75 4407.74 101.26 o 5 3 2 783.60 855.03 48.77 o 6 3 2 157.41 171.87 13.48 o 7 3 2 747.14 784.18 41.66 o 8 3 2 1241.15 1368.42 55.51 o 9 3 2 155.14 162.60 18.20 o 10 3 2 76.26 73.49 19.12 o 0 4 2 3843.38 3936.81 59.49 o 1 4 2 1379.27 1587.82 79.44 o 2 4 2 5745.53 5996.37 87.80 o 3 4 2 662.95 698.03 37.09 o 4 4 2 1326.48 1200.73 55.97 o 5 4 2 3657.20 3650.58 105.37 o 6 4 2 4877.95 4886.54 135.39 o 7 4 2 1420.70 1351.83 74.30 o 8 4 2 0.90 3.81 14.70 o 9 4 2 141.81 163.64 18.11 o 10 4 2 320.73 337.73 22.46 o 1 5 2 1178.86 1354.65 40.32 o 2 5 2 10142.35 9759.59 115.82 o 3 5 2 4342.47 4463.49 89.81 o 4 5 2 11046.98 11290.20 160.19 o 5 5 2 2686.59 2560.68 93.01 o 6 5 2 185.89 212.55 14.44 o 7 5 2 916.91 911.99 46.12 o 8 5 2 933.59 940.30 43.04 o 9 5 2 67.94 68.86 16.93 o 10 5 2 51.81 50.83 18.72 o 0 6 2 1505.94 1560.57 43.74 o 1 6 2 17745.00 18285.03 105.13 o 2 6 2 489.14 487.53 22.75 o 3 6 2 111.81 119.49 8.36 o 4 6 2 3379.67 3400.90 92.00 o 5 6 2 3273.81 3333.31 102.97 o 6 6 2 3828.05 3862.80 118.40 o 7 6 2 185.68 170.25 15.10 o 8 6 2 22.31 22.18 14.74 o 9 6 2 206.01 232.21 18.82 o 1 7 2 1490.82 1646.47 34.39 o 2 7 2 18529.21 17693.82 165.93 o 3 7 2 2143.86 2015.86 66.53 o 4 7 2 1332.60 1354.74 64.36 o 5 7 2 1538.82 1427.18 69.11 o 6 7 2 816.51 827.54 39.32 o 7 7 2 911.23 913.52 39.18 o 8 7 2 480.74 439.40 25.63 o 9 7 2 348.05 334.71 20.40 o 0 8 2 17329.63 18737.47 154.76 o 1 8 2 4996.71 4940.80 58.01 o 2 8 2 1897.80 2035.36 61.42 o 3 8 2 5156.23 5130.11 100.25 o 4 8 2 1100.03 978.59 56.58 o 5 8 2 1360.18 1305.49 67.60 o 6 8 2 2058.19 1977.98 96.48 o 7 8 2 3.59 12.60 13.60 o 8 8 2 189.30 164.99 16.59 o 9 8 2 0.70 -7.61 16.71 o 1 9 2 3629.29 3546.94 119.05 o 2 9 2 26555.53 25495.97 213.19 o 3 9 2 2558.34 2669.29 75.48 o 4 9 2 836.82 822.94 39.10 o 5 9 2 215.84 225.72 12.39 o 6 9 2 1088.11 1051.54 51.79 o 7 9 2 46.44 42.17 13.60 o 8 9 2 510.42 504.71 29.40 o 9 9 2 320.00 316.47 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1771.88 1779.49 87.59 o 6 13 2 74.99 73.59 13.34 o 7 13 2 622.87 567.54 34.36 o 8 13 2 660.61 677.16 32.78 o 9 13 2 98.18 97.60 18.94 o 0 14 2 14863.33 16074.14 175.54 o 1 14 2 444.05 438.08 54.14 o 2 14 2 683.61 633.84 29.46 o 3 14 2 366.96 349.38 22.83 o 4 14 2 4620.94 4598.50 122.05 o 5 14 2 1730.83 1830.34 81.09 o 6 14 2 1178.62 1067.49 61.67 o 7 14 2 333.11 336.93 17.47 o 8 14 2 0.12 12.77 16.05 o 9 14 2 135.35 142.20 19.21 o 1 15 2 1.96 3.39 5.63 o 2 15 2 1114.70 928.50 47.40 o 3 15 2 3028.17 2824.48 91.59 o 4 15 2 7530.74 7408.39 153.61 o 5 15 2 602.07 669.74 33.23 o 6 15 2 0.45 2.67 13.47 o 7 15 2 1009.34 893.36 40.99 o 8 15 2 855.26 884.47 56.44 o 9 15 2 64.87 63.21 19.12 o 0 16 2 7357.44 7248.32 125.71 o 1 16 2 396.19 413.67 15.38 o 2 16 2 402.12 436.90 26.17 o 3 16 2 1985.86 2120.02 81.29 o 4 16 2 3954.32 3755.62 117.71 o 5 16 2 876.56 951.61 44.72 o 6 16 2 1294.74 1240.43 59.71 o 7 16 2 952.64 842.92 48.57 o 8 16 2 21.07 48.07 17.15 o 9 16 2 58.06 53.15 19.03 o 1 17 2 909.55 853.82 88.48 o 2 17 2 1157.11 1093.31 48.66 o 3 17 2 2236.82 2250.62 87.63 o 4 17 2 2154.26 2291.05 94.76 o 5 17 2 0.18 0.66 12.33 o 6 17 2 40.29 26.90 13.95 o 7 17 2 164.05 166.90 16.50 o 8 17 2 939.62 959.73 45.26 o 9 17 2 9.12 26.64 18.50 o 0 18 2 19280.30 19504.32 222.79 o 1 18 2 170.55 136.60 56.05 o 2 18 2 906.05 868.07 49.03 o 3 18 2 7.04 17.50 11.28 o 4 18 2 2310.63 2327.59 98.86 o 5 18 2 130.63 148.69 14.00 o 6 18 2 768.36 695.02 33.46 o 7 18 2 483.56 493.23 19.10 o 8 18 2 46.84 72.13 18.46 o 9 18 2 7.13 13.21 18.33 o 1 19 2 6631.34 6334.42 96.93 o 2 19 2 1625.49 1633.80 73.55 o 3 19 2 3342.51 3321.65 107.52 o 4 19 2 2025.49 2031.49 97.71 o 5 19 2 513.04 546.47 26.86 o 6 19 2 8.27 2.36 13.38 o 7 19 2 54.12 56.65 15.40 o 8 19 2 762.97 763.16 40.37 o 0 20 2 12120.36 12913.16 191.54 o 1 20 2 5563.35 5364.87 398.42 o 2 20 2 201.95 186.27 15.89 o 3 20 2 1210.40 1171.21 61.06 o 4 20 2 2717.76 2718.50 108.07 o 5 20 2 18.40 31.54 13.25 o 6 20 2 378.45 366.14 17.25 o 7 20 2 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o 8 24 2 20.95 22.26 18.37 o 1 25 2 145.55 157.90 25.08 o 2 25 2 3347.37 3244.30 118.01 o 3 25 2 734.15 650.63 31.27 o 4 25 2 879.59 890.61 52.47 o 5 25 2 804.09 872.39 35.21 o 6 25 2 269.92 229.02 20.49 o 7 25 2 238.04 248.42 19.74 o 0 26 2 60.07 69.86 11.81 o 1 26 2 698.28 699.38 20.86 o 2 26 2 757.82 651.85 39.04 o 3 26 2 236.09 231.78 15.41 o 4 26 2 3.33 10.50 13.86 o 5 26 2 1051.82 1105.98 44.94 o 6 26 2 1030.82 1054.41 40.36 o 7 26 2 39.79 37.22 17.93 o 1 27 2 40.86 45.55 14.06 o 2 27 2 3076.27 2765.74 120.68 o 3 27 2 109.17 112.05 14.88 o 4 27 2 159.57 166.46 15.58 o 5 27 2 179.18 174.39 17.24 o 6 27 2 182.50 169.13 18.64 o 7 27 2 63.33 73.01 18.77 o 0 28 2 2650.31 2818.06 113.22 o 1 28 2 2794.74 2779.97 113.00 o 2 28 2 284.45 246.97 17.21 o 3 28 2 259.44 227.11 16.02 o 4 28 2 301.89 292.62 16.81 o 5 28 2 123.19 96.74 16.58 o 6 28 2 426.72 462.35 27.15 o 7 28 2 2.64 4.85 17.54 o 1 29 2 483.53 471.27 26.68 o 2 29 2 2281.61 2159.01 103.14 o 3 29 2 268.53 301.53 17.38 o 4 29 2 144.30 155.42 16.10 o 5 29 2 0.84 5.29 15.22 o 6 29 2 97.76 121.18 18.55 o 0 30 2 1040.03 1007.96 55.44 o 1 30 2 292.37 280.47 12.82 o 2 30 2 240.84 248.62 17.64 o 3 30 2 578.27 603.16 29.67 o 4 30 2 123.37 115.47 16.50 o 6 30 2 303.91 316.10 20.66 o 1 31 2 570.27 541.92 17.49 o 2 31 2 559.41 564.14 25.19 o 3 31 2 358.00 390.88 18.65 o 4 31 2 291.20 308.49 19.09 o 5 31 2 16.12 16.23 16.88 o 6 31 2 24.82 18.41 18.37 o 0 32 2 944.79 973.78 44.09 o 1 32 2 317.46 292.94 20.53 o 2 32 2 71.39 66.84 15.70 o 3 32 2 71.39 87.89 16.32 o 4 32 2 340.36 347.41 20.66 o 5 32 2 125.08 156.72 19.16 o 6 32 2 297.14 298.22 22.11 o 1 33 2 38.95 37.89 11.21 o 2 33 2 221.54 212.23 17.11 o 3 33 2 433.00 428.57 20.54 o 4 33 2 850.20 917.44 49.98 o 0 34 2 1705.94 1575.46 97.57 o 1 34 2 12.65 21.65 10.87 o 2 34 2 20.13 8.22 15.48 o 3 34 2 137.58 152.70 18.55 o 4 34 2 667.49 700.13 33.83 o 5 34 2 176.01 178.14 21.66 o 1 35 2 27.66 40.94 15.48 o 2 35 2 1.42 -2.32 15.22 o 3 35 2 431.50 396.54 25.22 o 4 35 2 465.67 527.99 24.53 o 0 36 2 1276.97 1252.74 65.99 o 1 36 2 8.86 8.06 11.75 o 2 36 2 31.11 11.37 16.67 o 3 36 2 112.58 141.93 18.73 o 4 36 2 438.98 411.85 24.74 o 1 37 2 90.44 77.77 12.95 o 2 37 2 117.36 119.53 18.38 o 3 37 2 94.83 84.83 18.86 o 0 38 2 869.79 849.26 45.42 o 1 38 2 208.68 206.34 14.76 o 2 38 2 117.44 149.28 19.38 o 3 38 2 3.75 -3.50 18.06 o 1 39 2 229.93 219.70 15.48 o 2 39 2 213.63 193.26 20.74 o 0 40 2 133.25 120.85 19.64 o 1 0 3 167.88 152.45 17.37 o 2 0 3 38895.90 37319.28 253.58 o 3 0 3 6634.80 6058.47 106.77 o 4 0 3 54.82 35.44 8.88 o 5 0 3 3923.57 3678.63 108.65 o 6 0 3 191.45 164.14 13.53 o 7 0 3 1515.92 1385.26 73.04 o 8 0 3 52.11 60.63 15.53 o 9 0 3 772.06 827.55 44.93 o 0 1 3 16335.47 16572.68 165.99 o 1 1 3 20027.91 20568.15 308.01 o 2 1 3 406.89 373.54 13.22 o 3 1 3 936.95 1047.35 34.77 o 4 1 3 1224.92 1410.96 46.01 o 5 1 3 2877.37 2802.25 67.48 o 6 1 3 1068.50 1084.41 47.55 o 7 1 3 262.41 228.41 10.86 o 8 1 3 633.68 599.00 19.20 o 9 1 3 37.45 41.05 12.18 o 1 2 3 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150.48 o 7 5 3 173.65 156.54 15.10 o 9 5 3 1.30 7.70 16.44 o 1 6 3 9398.38 9577.69 104.57 o 2 6 3 22.13 54.77 7.13 o 3 6 3 10559.83 10814.33 148.00 o 4 6 3 5316.26 5398.74 118.05 o 5 6 3 9.22 9.75 11.24 o 6 6 3 0.11 1.57 13.12 o 7 6 3 355.12 362.90 17.12 o 8 6 3 1437.32 1358.67 77.51 o 9 6 3 150.21 135.51 18.64 o 0 7 3 15885.03 16009.78 151.65 o 1 7 3 3715.43 3666.46 105.87 o 2 7 3 2395.43 2481.17 68.45 o 3 7 3 278.34 254.10 11.83 o 4 7 3 3336.88 3360.72 99.02 o 5 7 3 2652.97 2514.06 95.27 o 6 7 3 924.54 982.62 54.96 o 7 7 3 672.61 631.95 31.43 o 8 7 3 78.61 91.74 17.11 o 9 7 3 154.76 169.95 19.03 o 1 8 3 363.30 391.80 13.33 o 2 8 3 2363.42 2255.18 67.15 o 3 8 3 3861.99 3887.38 93.83 o 4 8 3 3011.62 2911.23 95.54 o 5 8 3 101.14 97.88 11.73 o 6 8 3 130.44 118.72 13.13 o 7 8 3 693.12 688.71 27.53 o 8 8 3 873.07 824.04 43.95 o 9 8 3 163.91 163.39 19.56 o 0 9 3 31096.91 31778.18 234.70 o 1 9 3 4049.93 4005.15 58.99 o 2 9 3 90.02 83.67 8.01 o 3 9 3 2555.69 2420.77 79.30 o 4 9 3 8679.43 8401.22 153.84 o 5 9 3 2070.85 1952.98 87.42 o 6 9 3 397.62 425.15 21.03 o 7 9 3 1944.27 1970.17 94.57 o 8 9 3 99.78 107.67 16.58 o 9 9 3 48.73 72.48 18.07 o 1 10 3 9857.28 11134.31 98.13 o 2 10 3 9687.30 9928.85 139.27 o 3 10 3 5770.25 5958.59 118.09 o 4 10 3 31.52 45.58 10.98 o 5 10 3 90.76 110.74 12.21 o 6 10 3 4.02 -4.16 12.16 o 7 10 3 258.12 242.56 16.94 o 8 10 3 257.34 270.07 19.87 o 9 10 3 138.65 123.82 18.90 o 0 11 3 35665.69 36401.92 267.65 o 1 11 3 1574.30 1499.96 41.55 o 2 11 3 1803.79 1905.24 69.16 o 3 11 3 501.14 480.13 19.87 o 4 11 3 2944.21 2953.03 94.68 o 5 11 3 1172.67 1220.97 56.52 o 6 11 3 378.96 357.09 15.68 o 7 11 3 777.57 799.50 29.16 o 8 11 3 45.67 49.39 15.62 o 9 11 3 65.44 76.90 18.07 o 1 12 3 1138.93 1267.45 38.57 o 2 12 3 3143.32 2910.13 83.42 o 3 12 3 4546.23 4520.87 107.18 o 4 12 3 1328.66 1348.51 63.15 o 5 12 3 43.95 53.06 12.34 o 6 12 3 15.97 12.38 13.25 o 7 12 3 491.25 450.18 26.59 o 8 12 3 461.84 448.50 29.78 o 9 12 3 110.07 90.30 18.55 o 0 13 3 21.65 62.99 7.83 o 1 13 3 4509.79 4397.13 67.64 o 2 13 3 206.08 228.70 10.68 o 3 13 3 162.00 166.60 11.25 o 4 13 3 1829.86 1748.05 81.58 o 5 13 3 2430.74 2309.90 97.47 o 6 13 3 2278.89 2299.77 109.19 o 7 13 3 264.12 279.50 21.58 o 8 13 3 0.53 3.59 16.18 o 9 13 3 50.36 44.71 17.63 o 1 14 3 1238.65 1251.93 64.40 o 2 14 3 2239.44 2153.87 77.16 o 3 14 3 4668.26 4995.13 118.77 o 4 14 3 6719.43 6924.16 151.63 o 5 14 3 823.54 945.61 44.63 o 6 14 3 21.40 7.70 14.35 o 7 14 3 215.31 205.97 16.54 o 8 14 3 841.55 906.74 46.30 o 9 14 3 181.65 181.38 19.78 o 0 15 3 857.73 819.37 43.86 o 1 15 3 7856.83 7832.46 146.36 o 2 15 3 4195.46 4134.67 104.70 o 3 15 3 2486.66 2477.59 93.33 o 4 15 3 1.13 -1.14 12.60 o 5 15 3 1035.69 1048.73 54.14 o 6 15 3 2740.96 2499.29 115.43 o 7 15 3 15.28 22.35 14.87 o 8 15 3 1.54 4.59 16.97 o 9 15 3 0.09 8.35 17.71 o 1 16 3 818.89 942.90 64.99 o 2 16 3 4660.34 4626.40 114.25 o 3 16 3 2275.57 2340.87 89.98 o 4 16 3 1052.98 1132.75 53.64 o 5 16 3 285.66 303.21 14.89 o 6 16 3 667.82 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o 0 1 13 14.11 21.16 12.86 o 1 1 13 844.54 865.02 21.51 o 2 1 13 16.30 17.86 13.08 o 1 2 13 114.31 117.25 14.43 o 2 2 13 120.99 124.95 19.60 o 0 3 13 74.63 75.42 18.46 o 1 3 13 150.27 153.91 14.36 o 2 3 13 5.25 4.59 18.33 o 1 4 13 118.24 110.14 14.07 o 2 4 13 98.34 86.10 19.21 o 0 5 13 235.27 205.09 20.92 o 1 5 13 279.81 268.67 20.59 o 2 5 13 12.23 15.00 18.54 o 1 6 13 129.07 129.89 14.43 o 2 6 13 27.74 21.48 18.28 o 0 7 13 200.09 186.03 20.17 o 1 7 13 378.30 402.92 19.13 o 2 7 13 2.04 -8.00 18.50 o 1 8 13 274.95 292.64 15.93 o 2 8 13 0.77 11.50 18.81 o 0 9 13 123.71 114.19 20.13 o 1 9 13 299.95 283.75 16.06 o 1 10 13 162.57 150.86 15.66 o 0 11 13 32.61 36.00 19.25 o