# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Bis(dicyclohexylammonium) adipate monohydrate in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 355.33 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.8408 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 10.1550 _cell_length_b 15.6380 _cell_length_c 20.1020 _cell_angle_alpha 90.000 _cell_angle_beta 104.560 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 126258.78 127964.05 380.31 o 4 0 0 860.93 844.05 35.83 o 6 0 0 263.24 237.19 31.99 o 8 0 0 194.31 234.80 39.13 o 10 0 0 14.37 -28.36 40.20 o 1 1 0 603.55 574.64 13.21 o 3 1 0 4127.36 4131.67 59.19 o 5 1 0 2670.10 2832.41 67.51 o 7 1 0 34.01 20.65 31.67 o 9 1 0 358.55 276.05 42.75 o 11 1 0 121.75 78.78 49.03 o 0 2 0 16917.37 20265.14 82.21 o 2 2 0 4147.14 3788.22 48.29 o 4 2 0 11999.25 11955.37 123.07 o 6 2 0 206.25 243.43 32.53 o 8 2 0 46.69 53.42 35.80 o 10 2 0 68.62 91.43 33.87 o 1 3 0 644.75 703.69 19.51 o 3 3 0 940.48 946.49 34.23 o 5 3 0 688.45 773.03 44.28 o 7 3 0 219.42 170.35 46.03 o 9 3 0 117.72 118.17 40.77 o 11 3 0 47.72 66.36 35.25 o 0 4 0 57026.09 61674.57 221.21 o 2 4 0 14063.94 14959.92 116.23 o 4 4 0 4142.35 4232.02 76.70 o 6 4 0 579.35 525.58 42.28 o 8 4 0 2596.26 2691.15 85.63 o 10 4 0 16.12 27.53 42.40 o 1 5 0 1522.23 1346.04 33.66 o 3 5 0 3714.17 3864.61 70.08 o 5 5 0 6854.10 7240.97 120.53 o 7 5 0 956.45 931.85 62.55 o 9 5 0 0.15 -2.48 34.69 o 11 5 0 122.43 103.01 49.30 o 0 6 0 3878.64 3557.64 52.47 o 2 6 0 2735.86 3070.00 60.46 o 4 6 0 2120.49 2525.65 67.97 o 6 6 0 62.89 94.74 31.67 o 8 6 0 332.04 331.45 42.47 o 10 6 0 69.06 80.69 39.65 o 1 7 0 1933.71 1875.58 47.91 o 3 7 0 1208.33 1346.94 47.24 o 5 7 0 500.29 438.28 39.22 o 7 7 0 1842.34 2036.85 76.43 o 9 7 0 5.90 -29.73 46.53 o 0 8 0 8996.23 9575.98 102.68 o 2 8 0 3749.38 4063.90 77.30 o 4 8 0 4.88 -31.66 31.66 o 6 8 0 865.71 847.77 50.89 o 8 8 0 926.71 833.57 58.34 o 10 8 0 29.64 -49.84 52.59 o 1 9 0 659.71 587.82 37.62 o 3 9 0 135.51 74.67 32.51 o 5 9 0 19.56 -2.20 35.24 o 7 9 0 0.66 12.39 39.09 o 9 9 0 231.55 177.19 59.25 o 0 10 0 710.43 774.49 37.89 o 2 10 0 24.19 66.91 27.81 o 4 10 0 254.44 220.29 36.39 o 6 10 0 406.94 405.23 46.90 o 8 10 0 70.92 4.96 42.41 o 1 11 0 661.91 694.60 38.97 o 3 11 0 51.05 11.84 35.25 o 5 11 0 185.61 165.61 37.20 o 7 11 0 0.01 -31.11 41.02 o 9 11 0 261.02 263.46 54.29 o 0 12 0 3791.68 3711.34 86.02 o 2 12 0 1038.66 950.18 58.42 o 4 12 0 24.75 89.21 35.52 o 6 12 0 112.69 109.08 44.90 o 8 12 0 70.33 58.66 50.12 o 1 13 0 447.28 387.15 44.15 o 3 13 0 1582.82 1644.17 77.41 o 5 13 0 314.07 304.37 48.25 o 7 13 0 0.07 -20.37 48.45 o 0 14 0 373.84 371.79 35.85 o 2 14 0 155.40 115.16 41.33 o 4 14 0 276.31 229.34 52.37 o 6 14 0 7.24 18.45 46.53 o 1 15 0 66.17 92.81 33.60 o 3 15 0 47.24 83.16 43.78 o 5 15 0 8.34 28.63 50.11 o 0 16 0 44.87 124.46 26.16 o 2 16 0 1.41 14.32 41.02 o 4 16 0 0.58 16.52 44.87 o 1 17 0 0.01 -8.53 46.80 o 3 17 0 69.14 19.55 55.08 o 0 18 0 43.91 34.69 40.75 o 2 18 0 1.14 114.53 35.79 o -11 1 1 53.49 56.17 41.30 o -9 1 1 766.46 665.66 51.95 o -7 1 1 2157.38 2041.84 73.91 o -5 1 1 351.48 312.56 31.48 o -3 1 1 6169.75 6078.44 71.17 o -1 1 1 7460.71 6940.21 45.43 o 1 1 1 10.37 6.61 5.78 o 3 1 1 8916.13 9178.09 91.20 o 5 1 1 4304.30 4617.52 84.54 o 7 1 1 60.51 26.71 29.19 o 9 1 1 1093.16 1035.77 63.92 o 11 1 1 10.70 -22.03 47.35 o -10 2 1 50.91 54.52 33.87 o -8 2 1 2.77 -37.72 37.72 o -6 2 1 21.26 17.62 25.33 o -4 2 1 5828.34 5892.59 85.27 o -2 2 1 2001.18 1822.08 33.62 o 0 2 1 13.93 22.16 4.09 o 2 2 1 383.73 358.18 16.90 o 4 2 1 79.13 70.81 20.11 o 6 2 1 931.82 997.25 47.65 o 8 2 1 382.53 262.33 45.24 o 10 2 1 417.77 297.03 55.99 o -11 3 1 0.00 38.27 33.59 o -9 3 1 245.41 203.96 39.97 o -7 3 1 428.34 420.62 40.85 o -5 3 1 387.36 434.38 32.31 o -3 3 1 2125.28 2115.36 45.15 o -1 3 1 15149.73 14476.57 91.76 o 1 3 1 45495.08 47248.24 191.20 o 3 3 1 313.19 454.46 25.42 o 5 3 1 1242.27 1341.38 50.30 o 7 3 1 804.43 942.00 58.91 o 9 3 1 82.65 13.50 43.51 o 11 3 1 124.52 107.15 51.78 o -10 4 1 0.12 63.59 29.46 o -8 4 1 843.79 951.44 59.45 o -6 4 1 1235.13 999.36 52.45 o -4 4 1 50.88 87.59 22.03 o -2 4 1 8541.02 8653.58 85.80 o 0 4 1 949.90 944.07 16.79 o 2 4 1 4068.46 4367.53 60.94 o 4 4 1 58.59 59.22 22.59 o 6 4 1 1149.90 1091.18 56.29 o 8 4 1 67.12 87.30 35.25 o 10 4 1 54.43 83.44 36.62 o -11 5 1 15.74 -11.29 43.23 o -9 5 1 549.84 475.00 50.78 o -7 5 1 139.77 134.18 42.98 o -5 5 1 254.39 306.70 33.65 o -3 5 1 180.17 182.29 20.96 o -1 5 1 2012.14 1928.08 39.22 o 1 5 1 29521.79 30999.07 172.25 o 3 5 1 9778.76 9551.28 110.13 o 5 5 1 1854.54 2007.53 64.69 o 7 5 1 344.18 362.98 43.86 o 9 5 1 123.09 125.88 40.77 o 11 5 1 115.98 154.24 46.27 o -10 6 1 44.27 30.84 40.48 o -8 6 1 321.28 304.41 52.11 o -6 6 1 46.10 38.00 29.47 o -4 6 1 2050.62 2199.36 60.67 o -2 6 1 128.44 186.61 19.57 o 0 6 1 21.05 28.18 9.60 o 2 6 1 756.16 679.60 33.55 o 4 6 1 998.57 1185.35 45.48 o 6 6 1 14.68 -3.85 33.04 o 8 6 1 755.02 947.44 53.60 o 10 6 1 0.31 7.98 44.60 o -9 7 1 49.78 34.15 47.64 o -7 7 1 147.99 166.69 45.46 o -5 7 1 310.76 292.68 34.48 o -3 7 1 113.46 134.19 26.73 o -1 7 1 147.19 141.42 18.19 o 1 7 1 17128.61 17523.44 143.09 o 3 7 1 7547.49 7782.32 111.39 o 5 7 1 8931.06 8615.14 135.81 o 7 7 1 207.92 257.13 48.78 o 9 7 1 224.20 209.98 48.22 o -10 8 1 7.69 62.77 38.82 o -8 8 1 1.17 52.03 30.83 o -6 8 1 423.84 456.69 44.43 o -4 8 1 1937.29 2189.13 67.75 o -2 8 1 1386.20 1201.99 45.35 o 0 8 1 2819.41 2697.67 77.73 o 2 8 1 3573.66 3775.00 76.33 o 4 8 1 307.84 364.40 41.93 o 6 8 1 1614.99 1568.62 70.53 o 8 8 1 66.74 125.85 32.50 o 10 8 1 64.99 78.48 42.41 o -9 9 1 237.84 172.51 57.32 o -7 9 1 168.54 135.83 45.19 o -5 9 1 276.88 228.86 39.15 o -3 9 1 3.63 3.03 26.15 o -1 9 1 214.31 217.28 24.54 o 1 9 1 2362.39 2265.14 57.11 o 3 9 1 54.11 75.46 28.64 o 5 9 1 664.12 704.33 48.36 o 7 9 1 2.35 -15.14 43.50 o 9 9 1 79.63 160.83 40.48 o -8 10 1 59.08 84.81 44.34 o -6 10 1 9.32 72.68 33.31 o -4 10 1 228.14 224.94 41.35 o -2 10 1 539.69 515.49 40.61 o 0 10 1 138.78 113.67 17.76 o 2 10 1 36.12 45.16 25.33 o 4 10 1 91.14 111.28 34.71 o 6 10 1 206.67 191.53 42.99 o 8 10 1 4.09 -45.98 47.35 o -9 11 1 7.87 52.58 37.17 o -7 11 1 72.07 30.84 45.44 o -5 11 1 1.44 39.92 36.06 o -3 11 1 6.46 7.71 31.66 o -1 11 1 95.38 43.25 29.75 o 1 11 1 184.77 164.81 28.11 o 3 11 1 122.13 104.69 37.19 o 5 11 1 295.46 378.00 38.60 o 7 11 1 8.64 -5.23 46.80 o 9 11 1 7.17 -45.43 51.21 o -8 12 1 1.52 -44.60 44.60 o -6 12 1 53.67 63.89 41.31 o -4 12 1 95.05 93.65 42.69 o -2 12 1 3619.26 3729.93 95.72 o 0 12 1 6149.51 5757.32 74.57 o 2 12 1 668.20 673.06 48.90 o 4 12 1 194.35 143.57 39.13 o 6 12 1 6.01 -31.11 44.60 o 8 12 1 0.15 -31.11 46.25 o -7 13 1 7.86 2.75 51.76 o -5 13 1 50.48 90.04 39.93 o -3 13 1 327.94 294.50 46.88 o -1 13 1 295.23 343.55 38.33 o 1 13 1 195.01 114.92 39.41 o 3 13 1 3.49 42.40 36.34 o 5 13 1 31.14 44.33 42.40 o 7 13 1 162.21 303.86 49.59 o -6 14 1 34.92 64.43 41.30 o -4 14 1 2.62 73.23 38.54 o -2 14 1 136.00 119.56 39.94 o 0 14 1 131.57 138.52 26.58 o 2 14 1 1064.66 1181.50 69.17 o 4 14 1 174.92 105.52 54.00 o 6 14 1 4.22 21.75 47.08 o -7 15 1 0.63 65.25 46.25 o -5 15 1 15.76 53.69 36.89 o -3 15 1 0.09 -25.05 43.77 o -1 15 1 96.39 14.32 39.94 o 1 15 1 92.79 54.81 31.95 o 3 15 1 15.21 55.61 37.17 o 5 15 1 2.06 -47.90 52.03 o -6 16 1 38.21 77.10 54.52 o -4 16 1 15.87 0.00 52.86 o -2 16 1 144.45 192.28 48.48 o 0 16 1 66.49 75.97 25.01 o 2 16 1 0.03 25.88 39.64 o 4 16 1 7.71 10.19 44.88 o -3 17 1 21.50 35.79 47.08 o -1 17 1 35.21 8.54 47.36 o 1 17 1 46.58 28.36 42.68 o 3 17 1 0.06 68.55 43.77 o -2 18 1 12.17 26.98 55.34 o 0 18 1 0.01 21.47 25.89 o 2 18 1 0.45 -16.79 49.55 o -10 0 2 385.71 265.02 49.09 o -8 0 2 302.28 276.03 42.74 o -6 0 2 61.37 97.50 30.85 o -4 0 2 814.08 870.25 33.88 o -2 0 2 19467.67 20765.54 111.83 o 0 0 2 1743.23 2211.77 58.82 o 2 0 2 6782.13 6799.06 66.16 o 4 0 2 7846.06 7899.97 100.32 o 6 0 2 814.27 834.23 42.62 o 8 0 2 46.50 20.93 34.70 o 10 0 2 74.82 54.53 41.58 o -11 1 2 91.87 52.60 45.72 o -9 1 2 18.34 41.85 26.43 o -7 1 2 11.36 21.48 26.16 o -5 1 2 1730.51 2020.61 55.58 o -3 1 2 17727.98 18316.45 129.66 o -1 1 2 192.69 163.08 9.14 o 1 1 2 254.78 225.74 11.63 o 3 1 2 2406.42 2524.31 50.11 o 5 1 2 993.66 1074.97 46.88 o 7 1 2 0.42 -13.49 31.38 o 9 1 2 21.99 49.83 32.21 o 11 1 2 1.12 64.97 40.19 o -10 2 2 54.61 4.68 39.38 o -8 2 2 103.96 113.21 39.39 o -6 2 2 439.16 452.33 39.77 o -4 2 2 489.64 533.69 28.22 o -2 2 2 1363.68 1141.06 27.61 o 0 2 2 1879.24 2011.75 30.54 o 2 2 2 747.11 810.54 26.16 o 4 2 2 1204.77 1267.43 42.86 o 6 2 2 266.09 419.74 33.37 o 8 2 2 345.81 307.78 44.13 o 10 2 2 5.63 39.92 36.89 o -11 3 2 109.91 99.43 46.55 o -9 3 2 88.34 21.48 36.63 o -7 3 2 106.38 95.59 31.96 o -5 3 2 780.01 742.12 40.17 o -3 3 2 702.03 727.00 29.98 o -1 3 2 1299.67 1299.97 27.89 o 1 3 2 2782.75 2711.88 40.00 o 3 3 2 29.83 40.76 17.62 o 5 3 2 121.38 87.35 27.28 o 7 3 2 537.98 524.65 50.81 o 9 3 2 38.51 -30.29 45.98 o 11 3 2 50.49 51.77 46.26 o -10 4 2 7.08 14.32 36.07 o -8 4 2 0.78 26.98 30.28 o -6 4 2 3060.03 3039.03 78.91 o -4 4 2 208.52 175.70 25.10 o -2 4 2 2180.24 2344.54 45.83 o 0 4 2 129.78 118.03 8.72 o 2 4 2 991.72 1122.29 33.42 o 4 4 2 47.05 34.98 24.24 o 6 4 2 762.45 776.14 48.40 o 8 4 2 369.37 345.31 42.20 o 10 4 2 150.25 121.21 42.15 o -11 5 2 28.41 58.65 43.23 o -9 5 2 73.91 70.50 35.80 o -7 5 2 789.87 802.21 54.20 o -5 5 2 501.74 479.93 38.68 o -3 5 2 1306.06 1436.40 42.65 o -1 5 2 24.82 22.58 12.39 o 1 5 2 7361.44 7083.60 77.20 o 3 5 2 2502.22 2486.77 57.97 o 5 5 2 2537.65 2388.86 70.00 o 7 5 2 632.70 669.87 50.83 o 9 5 2 530.06 570.12 56.29 o -10 6 2 3.08 -45.98 45.98 o -8 6 2 241.64 213.89 47.68 o -6 6 2 14.10 0.00 30.29 o -4 6 2 3020.58 2890.48 71.54 o -2 6 2 261.31 302.49 23.18 o 0 6 2 248.75 220.05 25.67 o 2 6 2 3193.60 3292.25 64.59 o 4 6 2 1688.55 1720.94 57.40 o 6 6 2 940.91 878.81 59.23 o 8 6 2 108.29 97.51 43.80 o 10 6 2 41.46 26.98 45.98 o -11 7 2 2.93 5.78 43.77 o -9 7 2 232.99 267.04 44.09 o -7 7 2 121.15 156.47 40.22 o -5 7 2 419.87 428.97 40.03 o -3 7 2 0.18 0.00 20.92 o -1 7 2 201.04 178.17 19.03 o 1 7 2 3843.05 4078.67 68.29 o 3 7 2 1737.00 1827.98 55.49 o 5 7 2 707.29 690.67 48.11 o 7 7 2 595.48 563.85 51.64 o 9 7 2 133.13 141.86 42.70 o -10 8 2 32.79 86.46 39.37 o -8 8 2 716.31 652.71 54.69 o -6 8 2 193.73 199.81 39.96 o -4 8 2 1340.04 1398.38 54.99 o -2 8 2 186.91 181.13 25.64 o 0 8 2 172.07 203.29 22.33 o 2 8 2 0.14 5.23 23.13 o 4 8 2 2.84 -34.14 34.14 o 6 8 2 202.94 188.78 40.51 o 8 8 2 138.85 76.03 44.63 o 10 8 2 0.21 17.07 42.95 o -9 9 2 16.59 21.20 39.65 o -7 9 2 11.08 -31.94 41.57 o -5 9 2 28.74 6.06 37.45 o -3 9 2 34.67 80.96 23.41 o -1 9 2 784.62 830.30 39.04 o 1 9 2 35.38 25.33 20.93 o 3 9 2 18.81 66.63 24.78 o 5 9 2 824.09 722.33 49.22 o 7 9 2 181.58 154.85 50.15 o 9 9 2 1.56 77.64 35.79 o -10 10 2 46.05 3.03 48.74 o -8 10 2 34.02 12.39 44.61 o -6 10 2 0.44 -16.79 36.89 o -4 10 2 693.59 666.12 53.07 o -2 10 2 509.55 481.41 38.67 o 0 10 2 181.65 184.11 28.94 o 2 10 2 889.30 842.38 47.89 o 4 10 2 3.90 4.13 33.31 o 6 10 2 0.51 -20.10 38.54 o 8 10 2 175.87 168.89 46.84 o -9 11 2 4.11 24.78 39.64 o -7 11 2 381.07 367.61 57.36 o -5 11 2 138.81 149.87 36.64 o -3 11 2 157.07 150.72 36.10 o -1 11 2 578.69 487.87 40.61 o 1 11 2 37.94 7.99 27.54 o 3 11 2 581.36 560.66 50.82 o 5 11 2 11.14 -2.20 35.79 o 7 11 2 2.88 23.95 40.19 o 9 11 2 33.86 -2.75 44.60 o -8 12 2 13.35 11.01 41.30 o -6 12 2 23.88 63.60 41.30 o -4 12 2 204.34 256.57 47.40 o -2 12 2 446.90 468.60 50.50 o 0 12 2 330.98 360.04 27.31 o 2 12 2 48.55 93.08 28.64 o 4 12 2 7.32 61.67 31.66 o 6 12 2 58.54 -14.32 57.00 o 8 12 2 44.72 63.33 38.82 o -7 13 2 0.65 -25.88 49.28 o -5 13 2 17.32 2.48 44.05 o -3 13 2 416.38 370.49 48.00 o -1 13 2 530.64 432.58 49.41 o 1 13 2 366.04 461.45 44.13 o 3 13 2 8.90 -26.15 45.70 o 5 13 2 64.05 55.90 48.47 o 7 13 2 0.03 -38.82 46.80 o -6 14 2 78.80 -126.13 126.13 o -4 14 2 27.35 -39.37 49.29 o -2 14 2 19.42 32.76 34.42 o 0 14 2 0.74 14.98 19.87 o 2 14 2 37.63 39.10 37.45 o 4 14 2 37.12 60.58 41.03 o 6 14 2 139.07 94.76 55.64 o -7 15 2 6.17 19.55 53.13 o -5 15 2 5.06 -52.86 52.86 o -3 15 2 0.01 36.06 38.54 o -1 15 2 418.38 349.48 48.27 o 1 15 2 285.01 283.65 43.00 o 3 15 2 24.87 72.96 33.87 o 5 15 2 10.72 19.27 48.46 o -6 16 2 1.92 66.62 46.80 o -4 16 2 72.13 16.52 53.70 o -2 16 2 8.50 -25.88 41.85 o 0 16 2 10.23 24.62 21.01 o 2 16 2 47.46 69.39 41.30 o 4 16 2 0.01 33.59 43.77 o -3 17 2 40.48 110.41 42.68 o -1 17 2 52.69 36.90 45.16 o 1 17 2 156.65 104.41 53.44 o 3 17 2 81.05 39.66 54.25 o -2 18 2 33.50 152.26 43.50 o 0 18 2 0.03 -3.96 27.96 o 2 18 2 52.77 44.33 53.97 o -11 1 3 13.27 36.62 36.34 o -9 1 3 475.61 405.09 44.43 o -7 1 3 418.83 478.61 36.99 o -5 1 3 2110.54 2229.80 59.68 o -3 1 3 13407.11 14341.52 113.31 o -1 1 3 7854.62 6370.07 50.70 o 1 1 3 10105.26 9240.88 66.92 o 3 1 3 2491.87 2521.45 51.46 o 5 1 3 787.03 656.00 42.92 o 7 1 3 80.87 127.80 34.15 o 9 1 3 549.37 549.78 47.47 o 11 1 3 77.21 95.28 45.99 o -10 2 3 70.32 -30.02 46.82 o -8 2 3 7.06 25.60 27.53 o -6 2 3 242.01 280.18 34.47 o -4 2 3 181.33 230.02 22.62 o -2 2 3 7180.84 6723.91 66.97 o 0 2 3 300.51 268.82 9.30 o 2 2 3 136.47 125.77 15.72 o 4 2 3 11.25 23.68 18.45 o 6 2 3 56.48 79.87 28.37 o 8 2 3 10.21 31.11 30.84 o 10 2 3 11.84 38.27 42.67 o -11 3 3 3.53 -23.95 42.12 o -9 3 3 10.99 10.74 33.59 o -7 3 3 1.81 0.00 31.11 o -5 3 3 4.56 15.14 21.20 o -3 3 3 648.92 789.68 29.96 o -1 3 3 28922.81 25862.86 141.13 o 1 3 3 2666.37 2518.97 40.61 o 3 3 3 152.68 147.51 21.51 o 5 3 3 1941.29 1769.05 60.56 o 7 3 3 65.26 37.73 38.56 o 9 3 3 893.88 921.55 61.92 o 11 3 3 218.13 308.87 46.01 o -10 4 3 1.57 4.68 30.56 o -8 4 3 723.79 771.28 50.29 o -6 4 3 253.12 209.86 33.37 o -4 4 3 338.12 330.53 30.37 o -2 4 3 1692.67 1723.67 39.34 o 0 4 3 27.94 28.09 9.35 o 2 4 3 32.96 69.95 14.60 o 4 4 3 0.39 -8.26 23.40 o 6 4 3 779.24 702.82 48.13 o 8 4 3 31.10 -9.09 40.75 o 10 4 3 0.45 84.52 34.69 o -11 5 3 22.09 69.11 35.52 o -9 5 3 10.02 65.53 30.84 o -7 5 3 8.92 12.11 33.86 o -5 5 3 630.78 645.21 46.18 o -3 5 3 16.56 -20.93 20.93 o -1 5 3 2728.46 2587.65 46.57 o 1 5 3 547.59 620.95 27.97 o 3 5 3 336.90 320.55 28.71 o 5 5 3 427.17 453.04 38.10 o 7 5 3 648.21 590.59 58.29 o 9 5 3 913.19 924.84 64.68 o -10 6 3 2.05 12.39 34.14 o -8 6 3 37.53 48.74 38.27 o -6 6 3 2.46 -31.66 31.66 o -4 6 3 632.30 668.08 38.45 o -2 6 3 346.27 364.59 25.96 o 0 6 3 437.38 385.81 20.88 o 2 6 3 11281.43 12254.92 125.12 o 4 6 3 381.54 508.46 39.47 o 6 6 3 179.57 181.06 33.90 o 8 6 3 3.91 36.62 35.51 o 10 6 3 2.61 -13.77 44.05 o -11 7 3 67.40 37.73 48.19 o -9 7 3 91.83 103.83 37.73 o -7 7 3 3012.88 3321.44 92.57 o -5 7 3 3541.06 3492.53 86.42 o -3 7 3 69.52 59.22 27.27 o -1 7 3 175.67 161.58 21.78 o 1 7 3 199.62 214.55 24.27 o 3 7 3 245.75 302.55 30.89 o 5 7 3 2077.57 1915.13 72.74 o 7 7 3 121.13 64.73 49.58 o 9 7 3 1057.66 1138.74 69.41 o -10 8 3 24.32 45.43 44.60 o -8 8 3 778.41 846.88 57.47 o -6 8 3 1500.62 1360.70 66.06 o -4 8 3 52.58 87.30 26.44 o -2 8 3 19.73 53.69 19.55 o 0 8 3 74.90 95.60 13.37 o 2 8 3 617.69 623.03 35.95 o 4 8 3 1018.85 1108.95 54.02 o 6 8 3 2.99 -18.45 37.72 o 8 8 3 23.93 -14.59 47.08 o 10 8 3 4.25 3.03 45.15 o -9 9 3 0.59 -46.80 46.80 o -7 9 3 27.87 53.69 39.37 o -5 9 3 0.19 -38.27 38.27 o -3 9 3 1.28 11.56 19.82 o -1 9 3 96.58 88.16 21.76 o 1 9 3 236.51 238.53 28.40 o 3 9 3 257.55 270.51 37.50 o 5 9 3 0.11 28.08 26.70 o 7 9 3 152.49 229.49 41.60 o 9 9 3 263.49 209.73 61.73 o -10 10 3 30.06 46.26 46.26 o -8 10 3 96.00 44.34 41.31 o -6 10 3 149.56 179.08 41.33 o -4 10 3 33.14 63.88 33.04 o -2 10 3 5.43 -9.91 25.88 o 0 10 3 21.93 27.69 15.85 o 2 10 3 173.02 210.28 28.39 o 4 10 3 6.00 63.05 27.26 o 6 10 3 2.94 7.71 32.76 o 8 10 3 70.47 45.16 41.03 o -9 11 3 0.11 -19.27 41.85 o -7 11 3 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