# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' tbcr in C 2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 708.82 _exptl_crystal_F_000 3704.00 _reflns_d_resolution_high 0.7097 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 17.6320 _cell_length_b 18.2840 _cell_length_c 22.9980 _cell_angle_alpha 90.000 _cell_angle_beta 91.270 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 31167.37 27749.98 1596.36 o 6 0 0 21131.79 18601.33 1078.31 o 8 0 0 7480.63 10233.41 421.59 o 10 0 0 444.39 392.27 113.46 o 12 0 0 7422.32 7486.03 376.15 o 14 0 0 1218.47 958.11 163.89 o 16 0 0 2609.93 2672.33 252.13 o 18 0 0 126.80 206.10 272.66 o 20 0 0 397.72 341.85 334.81 o 22 0 0 4214.11 4289.79 466.45 o 24 0 0 169.57 -197.60 454.13 o 1 1 0 17739.45 -19.35 19.35 o 3 1 0 56397.95 56187.75 2967.26 o 5 1 0 22578.17 26632.38 1255.10 o 7 1 0 812.96 1880.74 117.56 o 9 1 0 15805.57 14736.05 812.69 o 11 1 0 24494.85 24938.10 1434.82 o 13 1 0 2245.33 1766.11 170.34 o 15 1 0 3221.38 3886.38 277.05 o 17 1 0 13.08 -27.85 243.05 o 19 1 0 0.52 60.69 282.62 o 21 1 0 322.06 357.09 317.22 o 23 1 0 852.72 780.15 443.87 o 0 2 0 20428.89 23805.54 1586.68 o 2 2 0 7890.98 6861.56 308.42 o 4 2 0 126442.38 119874.73 5719.63 o 6 2 0 1517.72 2453.91 126.07 o 8 2 0 3457.81 3750.35 158.32 o 10 2 0 380.06 688.97 112.58 o 12 2 0 2911.01 2944.69 186.76 o 14 2 0 10732.97 10977.21 581.08 o 16 2 0 1015.77 995.64 211.97 o 18 2 0 5673.11 5681.81 440.35 o 20 2 0 79.49 -147.76 322.79 o 22 2 0 39.81 25.80 373.80 o 24 2 0 4.44 3.52 451.50 o 1 3 0 83565.70 84809.34 4167.54 o 3 3 0 10464.65 10293.81 510.13 o 5 3 0 9197.17 7800.61 358.85 o 7 3 0 23551.11 25183.19 1125.81 o 9 3 0 3879.62 3061.67 171.51 o 11 3 0 2507.74 2158.97 145.42 o 13 3 0 6255.71 6417.69 352.11 o 15 3 0 10418.41 9525.38 587.24 o 17 3 0 337.70 157.44 241.87 o 19 3 0 78.65 174.44 270.60 o 21 3 0 839.45 837.32 345.66 o 23 3 0 169.77 -69.78 424.82 o 0 4 0 26223.38 26212.84 1177.11 o 2 4 0 71116.40 76231.52 3469.19 o 4 4 0 17514.68 18257.13 815.62 o 6 4 0 74781.93 79410.46 3500.85 o 8 4 0 29.42 231.90 99.97 o 10 4 0 8687.17 9860.49 395.50 o 12 4 0 3597.30 3515.80 220.47 o 14 4 0 1724.25 1635.65 187.05 o 16 4 0 1240.79 755.23 198.78 o 18 4 0 610.59 849.05 243.34 o 20 4 0 1389.68 1237.80 292.01 o 22 4 0 23.41 -132.81 401.36 o 24 4 0 601.14 678.12 465.86 o 1 5 0 7.94 914.43 103.49 o 3 5 0 293.31 438.01 83.56 o 5 5 0 2850.66 5288.66 243.05 o 7 5 0 12151.66 12264.26 460.00 o 9 5 0 13779.52 15873.59 681.35 o 11 5 0 640.63 337.45 136.04 o 13 5 0 320.45 265.03 152.75 o 15 5 0 1840.93 1722.72 200.83 o 17 5 0 363.58 598.38 240.41 o 19 5 0 460.19 579.32 287.02 o 21 5 0 43.98 151.28 342.73 o 23 5 0 98.34 -118.74 430.09 o 0 6 0 2012.49 1557.37 114.05 o 2 6 0 6488.50 6788.56 281.16 o 4 6 0 285.53 1133.14 104.96 o 6 6 0 32025.37 32439.67 1431.01 o 8 6 0 2001.82 2541.57 156.56 o 10 6 0 26257.21 27412.82 1199.98 o 12 6 0 4521.17 3531.05 221.35 o 14 6 0 1078.84 1666.43 171.22 o 16 6 0 2160.45 1879.57 236.60 o 18 6 0 6.10 35.18 260.34 o 20 6 0 9.72 97.34 313.99 o 22 6 0 40.92 -121.67 395.21 o 24 6 0 18.66 230.15 481.11 o 1 7 0 2401.25 2045.22 124.01 o 3 7 0 6465.62 8743.77 376.15 o 5 7 0 16.72 131.93 103.49 o 7 7 0 5085.62 3864.98 197.02 o 9 7 0 700.13 1066.00 132.81 o 11 7 0 5667.93 5154.97 258.58 o 13 7 0 424.58 969.54 175.91 o 15 7 0 916.59 1325.46 202.29 o 17 7 0 74.79 113.46 236.60 o 19 7 0 1291.69 1632.71 309.01 o 21 7 0 27.69 -245.10 387.58 o 23 7 0 134.89 -14.07 442.99 o 0 8 0 12328.23 9790.71 433.90 o 2 8 0 6.39 84.14 110.53 o 4 8 0 106.27 292.30 109.65 o 6 8 0 1056.00 848.75 123.14 o 8 8 0 516.81 523.32 136.91 o 10 8 0 5478.87 7069.72 401.07 o 12 8 0 1411.14 1646.79 178.25 o 14 8 0 1062.89 1100.89 195.55 o 16 8 0 29.91 95.87 201.71 o 18 8 0 1451.81 1324.00 252.72 o 20 8 0 63.05 108.48 328.95 o 22 8 0 6.65 -191.74 407.81 o 1 9 0 116.80 301.09 117.56 o 3 9 0 3519.31 4230.57 220.18 o 5 9 0 8238.47 7546.72 335.10 o 7 9 0 7275.48 6150.90 330.71 o 9 9 0 3501.14 3180.70 223.40 o 11 9 0 4955.04 4166.95 253.89 o 13 9 0 41.09 73.59 169.75 o 15 9 0 2466.55 2904.82 221.06 o 17 9 0 396.80 436.54 243.05 o 19 9 0 6.22 116.39 309.89 o 21 9 0 35.03 118.44 376.73 o 23 9 0 0.46 127.53 479.35 o 0 10 0 1.39 194.96 127.24 o 2 10 0 561.81 966.32 143.07 o 4 10 0 5855.24 5050.01 261.22 o 6 10 0 1146.21 1791.03 156.85 o 8 10 0 813.75 1265.07 164.47 o 10 10 0 1157.50 879.83 161.54 o 12 10 0 15450.54 14741.04 940.22 o 14 10 0 1772.42 1722.72 205.23 o 16 10 0 1110.25 1294.97 212.55 o 18 10 0 95.89 86.19 284.97 o 20 10 0 6.59 184.41 348.30 o 22 10 0 34.96 -122.55 428.63 o 1 11 0 21626.31 21376.27 1043.13 o 3 11 0 7515.86 9386.71 496.65 o 5 11 0 1668.12 1662.32 171.51 o 7 11 0 2279.92 1766.70 177.37 o 9 11 0 369.90 267.38 164.47 o 11 11 0 4943.99 4419.67 315.46 o 13 11 0 86.48 236.60 181.48 o 15 11 0 80.15 107.60 201.41 o 17 11 0 248.68 236.01 245.68 o 19 11 0 159.89 -28.15 360.02 o 21 11 0 219.58 19.06 399.31 o 0 12 0 22288.13 22241.73 1320.77 o 2 12 0 9305.92 10637.71 657.89 o 4 12 0 337.62 335.69 163.30 o 6 12 0 246.36 172.39 172.68 o 8 12 0 3001.79 2630.70 222.82 o 10 12 0 1697.41 1644.44 211.09 o 12 12 0 957.51 1109.39 192.03 o 14 12 0 139.22 196.14 190.86 o 16 12 0 6.35 125.19 239.23 o 18 12 0 3.26 98.21 291.42 o 20 12 0 182.77 308.13 327.77 o 1 13 0 228.91 365.01 172.39 o 3 13 0 5521.07 4691.16 289.07 o 5 13 0 474.98 464.69 186.76 o 7 13 0 996.12 1014.69 192.91 o 9 13 0 24.56 221.06 210.50 o 11 13 0 3063.56 2431.63 236.30 o 13 13 0 2751.43 3005.96 256.53 o 15 13 0 1647.84 1048.11 243.92 o 17 13 0 1475.22 1348.04 294.64 o 19 13 0 0.28 177.37 360.32 o 21 13 0 22.14 269.14 452.38 o 0 14 0 192.96 125.48 188.81 o 2 14 0 4011.91 4672.39 292.30 o 4 14 0 1408.30 1329.86 199.36 o 6 14 0 595.47 824.42 195.26 o 8 14 0 191.44 44.27 194.08 o 10 14 0 657.58 561.44 224.28 o 12 14 0 604.45 819.14 217.54 o 14 14 0 2639.02 2783.44 284.38 o 16 14 0 25.70 -51.60 285.26 o 18 14 0 277.53 428.63 382.89 o 20 14 0 345.25 14.07 458.53 o 1 15 0 552.36 1024.37 218.42 o 3 15 0 10661.10 8154.19 513.36 o 5 15 0 211.76 547.66 206.10 o 7 15 0 1166.39 1250.12 221.64 o 9 15 0 1097.03 1608.38 210.21 o 11 15 0 139.76 128.71 224.28 o 13 15 0 1282.35 1243.96 269.43 o 15 15 0 19.48 -14.07 269.72 o 17 15 0 7.62 -52.77 372.34 o 19 15 0 9.24 -211.68 437.13 o 0 16 0 2753.34 2443.65 272.66 o 2 16 0 960.76 1137.53 237.77 o 4 16 0 169.61 395.79 223.40 o 6 16 0 163.96 229.85 227.80 o 8 16 0 6.40 114.05 221.06 o 10 16 0 291.14 287.02 240.11 o 12 16 0 65.21 95.87 246.56 o 14 16 0 614.76 620.07 282.04 o 16 16 0 401.63 374.98 321.91 o 18 16 0 53.81 165.65 429.80 o 1 17 0 279.82 1370.90 234.84 o 3 17 0 335.78 371.16 231.61 o 5 17 0 2201.42 2309.37 257.41 o 7 17 0 964.10 1067.76 241.87 o 9 17 0 1355.17 1322.24 255.95 o 11 17 0 1942.07 1415.17 287.90 o 13 17 0 332.55 260.34 297.58 o 15 17 0 396.65 813.28 321.91 o 17 17 0 5.52 -105.54 428.63 o 0 18 0 2729.93 3745.07 314.87 o 2 18 0 547.99 740.86 250.08 o 4 18 0 4493.82 4956.78 367.94 o 6 18 0 338.29 246.86 248.03 o 8 18 0 9.84 -53.07 242.75 o 10 18 0 36.61 -19.06 280.87 o 12 18 0 630.82 842.30 299.63 o 14 18 0 244.87 570.23 331.29 o 16 18 0 233.01 14.07 423.94 o 1 19 0 7.42 68.02 267.67 o 3 19 0 750.10 525.38 266.21 o 5 19 0 211.99 255.95 265.33 o 7 19 0 1163.73 1137.24 292.30 o 9 19 0 1379.20 1711.58 294.94 o 11 19 0 2153.92 2332.53 351.52 o 13 19 0 352.61 497.82 355.33 o 15 19 0 50.65 380.25 425.40 o 0 20 0 30.81 -52.77 291.71 o 2 20 0 4.80 486.09 294.06 o 4 20 0 1.73 132.22 289.07 o 6 20 0 550.31 630.33 288.78 o 8 20 0 13.61 116.69 325.14 o 10 20 0 203.57 9.97 316.34 o 12 20 0 296.69 543.85 370.87 o 14 20 0 497.19 880.12 406.35 o 1 21 0 152.99 341.26 318.10 o 3 21 0 815.77 727.96 322.79 o 5 21 0 690.39 676.07 345.07 o 7 21 0 797.20 311.65 322.50 o 9 21 0 274.39 590.76 337.45 o 11 21 0 100.31 124.89 359.14 o 13 21 0 131.60 -40.46 391.10 o 0 22 0 1365.69 1811.85 366.47 o 2 22 0 762.97 1000.62 543.26 o 4 22 0 9.21 -134.57 353.57 o 6 22 0 0.92 82.97 350.94 o 8 22 0 0.43 137.50 357.09 o 10 22 0 37.99 66.55 378.20 o 12 22 0 30.05 -62.15 396.96 o 1 23 0 227.37 232.49 384.06 o 3 23 0 286.33 209.62 383.77 o 5 23 0 717.53 1068.05 389.93 o 7 23 0 6.50 -222.23 396.08 o 9 23 0 14.83 231.32 406.35 o 11 23 0 8.87 -75.05 418.37 o 0 24 0 14.42 201.12 409.28 o 2 24 0 117.84 65.67 421.59 o 4 24 0 200.86 230.15 420.71 o 6 24 0 36.86 -86.49 425.40 o 8 24 0 168.11 297.87 557.63 o 1 25 0 3.32 -57.17 462.05 o 3 25 0 4.24 -8.50 462.34 o 5 25 0 59.37 -91.77 462.64 o -23 1 1 41.85 9.09 425.11 o -21 1 1 148.36 15.25 359.14 o -19 1 1 1973.33 1479.97 286.14 o -17 1 1 460.58 113.46 225.16 o -15 1 1 0.32 0.59 184.41 o -13 1 1 128.92 9.09 152.16 o -11 1 1 5092.34 5045.90 374.10 o -9 1 1 21119.49 23325.90 1119.36 o -7 1 1 2132.13 2153.69 124.31 o -5 1 1 17182.54 19407.28 1045.77 o -3 1 1 321.50 411.92 47.20 o -1 1 1 124.40 89.42 18.76 o 1 1 1 6588.00 -28.73 28.73 o 3 1 1 59276.08 73003.32 3917.16 o 5 1 1 8472.28 8900.33 384.94 o 7 1 1 14197.76 14019.53 708.61 o 9 1 1 12180.26 11146.66 477.30 o 11 1 1 1900.67 1952.87 150.11 o 13 1 1 2155.25 2758.23 194.67 o 15 1 1 546.32 339.21 172.10 o 17 1 1 5211.48 5912.25 453.84 o 19 1 1 1889.85 1833.83 318.39 o 21 1 1 46.67 85.32 373.80 o 23 1 1 150.23 -27.56 376.15 o -24 2 1 152.35 -72.71 450.91 o -22 2 1 5.01 40.75 355.63 o -20 2 1 76.52 71.83 293.18 o -18 2 1 187.52 287.02 252.13 o -16 2 1 2663.81 2437.49 220.18 o -14 2 1 2702.07 2189.75 191.15 o -12 2 1 4447.77 4161.68 240.70 o -10 2 1 5343.69 5858.60 287.02 o -8 2 1 21195.78 22642.51 1072.74 o -6 2 1 41324.66 39876.45 1966.06 o -4 2 1 135928.13 138866.27 7109.00 o -2 2 1 44184.04 41757.19 2194.44 o 0 2 1 38.81 647.93 62.15 o 2 2 1 7865.11 5112.16 226.33 o 4 2 1 406.61 275.00 65.97 o 6 2 1 109.22 778.98 90.59 o 8 2 1 2849.67 3026.78 158.90 o 10 2 1 4826.65 6056.49 353.57 o 12 2 1 34.05 9.38 152.16 o 14 2 1 2226.98 2043.46 192.91 o 16 2 1 2.73 -27.85 224.58 o 18 2 1 63.10 66.84 269.43 o 20 2 1 1095.39 1114.67 337.45 o 22 2 1 22.80 -122.84 380.84 o 24 2 1 48.58 191.15 469.38 o -23 3 1 9.95 -19.06 416.90 o -21 3 1 250.91 478.76 327.77 o -19 3 1 191.28 58.05 281.45 o -17 3 1 6093.59 7224.81 518.34 o -15 3 1 4636.99 5156.43 315.46 o -13 3 1 506.92 447.98 155.68 o -11 3 1 283.68 301.39 132.52 o -9 3 1 1.55 53.36 104.66 o -7 3 1 11387.18 10777.55 490.49 o -5 3 1 69906.41 76824.03 3763.83 o -3 3 1 203585.97 206743.94 10108.22 o -1 3 1 42738.24 35925.57 1784.29 o 1 3 1 673.10 778.98 61.27 o 3 3 1 59.55 2980.46 223.99 o 5 3 1 208169.06 209952.22 9082.68 o 7 3 1 8263.22 11062.23 498.11 o 9 3 1 27381.51 25896.79 1142.52 o 11 3 1 589.60 533.88 155.68 o 13 3 1 4.53 84.14 145.12 o 15 3 1 199.26 205.81 212.26 o 17 3 1 265.51 355.04 235.42 o 19 3 1 62.84 53.65 267.97 o 21 3 1 2.68 53.07 336.57 o 23 3 1 152.59 76.23 373.80 o -24 4 1 260.97 159.78 455.01 o -22 4 1 42.52 -131.34 367.94 o -20 4 1 935.85 959.28 307.84 o -18 4 1 4.38 164.47 261.81 o -16 4 1 214.41 217.54 205.52 o -14 4 1 333.85 720.34 172.98 o -12 4 1 6038.46 7025.15 356.80 o -10 4 1 6409.53 6629.66 283.50 o -8 4 1 7199.82 7168.52 324.84 o -6 4 1 330.59 -0.29 78.87 o -4 4 1 25032.35 26369.69 1338.36 o -2 4 1 7431.38 3701.68 165.94 o 0 4 1 3848.37 7087.31 319.86 o 2 4 1 285588.44 276003.38 12816.03 o 4 4 1 35792.03 43927.30 2021.76 o 6 4 1 27126.98 26559.67 1277.09 o 8 4 1 999.68 639.72 103.20 o 10 4 1 3665.53 3811.62 189.10 o 12 4 1 4311.05 4209.46 243.05 o 14 4 1 3860.54 3188.61 242.17 o 16 4 1 346.77 294.94 216.07 o 18 4 1 1266.86 1290.28 264.45 o 20 4 1 6.54 19.35 294.35 o 22 4 1 609.14 581.67 377.61 o 24 4 1 164.13 623.01 473.48 o -23 5 1 151.72 314.58 422.47 o -21 5 1 1348.52 1648.25 377.32 o -19 5 1 253.31 54.82 294.64 o -17 5 1 8989.06 9851.11 674.31 o -15 5 1 113.45 138.09 190.57 o -13 5 1 134.84 153.63 153.63 o -11 5 1 3679.26 3879.64 220.76 o -9 5 1 16855.97 16576.34 716.53 o -7 5 1 12477.14 13224.13 570.53 o -5 5 1 31436.02 32736.07 1550.92 o -3 5 1 3370.23 4517.01 206.98 o -1 5 1 1259.01 481.11 91.47 o 1 5 1 5602.01 7823.77 337.16 o 3 5 1 58.47 83.26 88.25 o 5 5 1 17128.69 16077.94 693.95 o 7 5 1 23875.26 29036.45 1201.74 o 9 5 1 3890.91 3750.05 195.55 o 11 5 1 4613.03 5011.89 270.02 o 13 5 1 18264.61 20056.96 1037.56 o 15 5 1 5245.39 5174.90 320.15 o 17 5 1 629.65 558.80 243.34 o 19 5 1 528.76 561.14 287.02 o 21 5 1 209.09 254.48 331.88 o 23 5 1 103.95 -167.41 376.44 o -24 6 1 175.13 268.26 470.26 o -22 6 1 90.63 163.30 387.58 o -20 6 1 43.55 23.16 306.96 o -18 6 1 43.95 29.61 234.84 o -16 6 1 10346.44 11968.15 688.09 o -14 6 1 1744.81 1485.24 179.43 o -12 6 1 1289.92 1249.24 157.14 o -10 6 1 2508.46 2623.95 169.46 o -8 6 1 3799.30 3302.07 175.03 o -6 6 1 1104.86 1171.84 108.48 o -4 6 1 1624.31 1710.11 120.50 o -2 6 1 55827.81 58742.52 2467.39 o 0 6 1 11065.44 8677.51 393.15 o 2 6 1 1967.83 1510.75 111.70 o 4 6 1 20130.02 26772.81 1142.81 o 6 6 1 73787.66 72585.55 2954.66 o 8 6 1 17387.29 17034.58 705.97 o 10 6 1 4960.00 4256.37 221.94 o 12 6 1 570.29 838.49 158.32 o 14 6 1 13478.87 13554.25 720.63 o 16 6 1 3460.77 3091.28 276.47 o 18 6 1 2897.67 2849.41 304.91 o 20 6 1 4.04 -31.96 325.14 o 22 6 1 97.36 120.50 350.06 o 24 6 1 755.56 662.88 491.95 o -23 7 1 140.58 283.80 440.65 o -21 7 1 183.89 217.83 381.13 o -19 7 1 343.22 354.75 285.26 o -17 7 1 1069.52 1290.57 252.43 o -15 7 1 3833.22 3881.10 262.69 o -13 7 1 6686.51 6934.56 379.67 o -11 7 1 76.72 146.59 139.55 o -9 7 1 19016.21 19823.30 888.04 o -7 7 1 18684.88 18642.66 794.81 o -5 7 1 5636.55 6031.28 283.50 o -3 7 1 30232.21 25376.40 1040.49 o -1 7 1 14154.78 12278.63 524.50 o 1 7 1 4550.31 4762.11 204.93 o 3 7 1 43190.08 50977.38 1956.97 o 5 7 1 24876.21 24966.24 1263.89 o 7 7 1 5022.03 5872.38 292.59 o 9 7 1 17656.44 19704.85 954.88 o 11 7 1 26885.43 29303.24 1421.62 o 13 7 1 4960.49 5123.01 295.52 o 15 7 1 7118.33 6363.74 366.47 o 17 7 1 8.26 3.52 241.87 o 19 7 1 525.09 507.49 299.34 o 21 7 1 215.82 135.16 393.74 o 23 7 1 6.35 -113.46 447.10 o -22 8 1 566.13 684.57 407.52 o -20 8 1 27.61 -63.03 351.23 o -18 8 1 2051.09 1955.50 284.97 o -16 8 1 1185.88 1282.07 200.24 o -14 8 1 1436.69 1822.40 193.20 o -12 8 1 1616.69 1985.99 169.16 o -10 8 1 9167.73 9073.30 457.65 o -8 8 1 219.17 474.95 124.31 o -6 8 1 4148.75 4152.29 215.49 o -4 8 1 8877.16 8000.56 355.04 o -2 8 1 21751.23 23549.89 928.20 o 0 8 1 4814.78 3275.10 168.58 o 2 8 1 35263.08 35194.67 1586.39 o 4 8 1 46286.89 46541.57 1897.75 o 6 8 1 1484.73 1439.22 138.97 o 8 8 1 4675.81 5395.08 291.42 o 10 8 1 10399.73 12359.55 641.48 o 12 8 1 6006.61 4594.99 282.33 o 14 8 1 248.10 355.63 193.79 o 16 8 1 408.72 394.62 209.33 o 18 8 1 1049.68 1076.55 288.19 o 20 8 1 1149.65 858.43 313.12 o 22 8 1 198.51 336.86 418.95 o -23 9 1 659.43 711.55 414.56 o -21 9 1 6.37 184.70 364.13 o -19 9 1 1072.29 839.96 308.42 o -17 9 1 300.57 174.73 225.16 o -15 9 1 1035.76 1295.85 193.50 o -13 9 1 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