# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' au in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 419.81 _exptl_crystal_F_000 1242.00 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 112.19 -0.68 2.37 o 2 0 0 19821.16 19201.91 197.12 o 3 0 0 7861.82 7687.08 133.34 o 4 0 0 16295.51 16605.06 229.01 o 5 0 0 5387.57 6894.18 159.80 o 6 0 0 13516.97 15009.09 263.96 o 7 0 0 6395.75 6451.68 130.45 o 8 0 0 3205.21 4024.87 122.31 o 9 0 0 4205.67 4441.27 123.43 o 10 0 0 4847.35 5844.47 155.58 o 11 0 0 37.88 50.86 39.88 o 12 0 0 4211.51 3684.35 137.11 o 13 0 0 354.30 416.05 65.06 o 14 0 0 503.97 578.12 81.18 o 15 0 0 318.28 345.83 87.36 o 16 0 0 452.37 552.35 126.55 o 17 0 0 290.32 262.94 99.75 o -17 1 0 66.78 21.37 86.86 o -16 1 0 142.90 157.43 97.03 o -15 1 0 294.48 361.33 105.18 o -14 1 0 226.05 292.46 98.05 o -13 1 0 562.99 488.22 99.75 o -12 1 0 1962.90 2017.31 109.93 o -11 1 0 1573.35 1720.75 95.48 o -10 1 0 1899.76 2275.84 99.90 o -9 1 0 3267.67 3536.13 131.81 o -8 1 0 4084.99 4862.15 125.08 o -7 1 0 1059.64 772.61 53.86 o -6 1 0 80.09 57.43 21.83 o -5 1 0 46612.78 57134.64 377.49 o -4 1 0 1617.62 2354.84 62.38 o -3 1 0 176241.27 164202.39 772.37 o -2 1 0 216.62 492.97 32.57 o -1 1 0 45383.26 41044.11 382.03 o 0 1 0 428.81 95.64 82.61 o 1 1 0 58581.44 47800.55 966.44 o 2 1 0 5.11 20.47 7.77 o 3 1 0 4323.91 5020.23 74.47 o 4 1 0 2290.24 2807.12 64.99 o 5 1 0 8443.65 10159.59 306.88 o 6 1 0 7737.36 8407.55 135.14 o 7 1 0 13452.63 12698.93 263.28 o 8 1 0 163.45 86.18 41.73 o 9 1 0 9594.88 8913.92 252.76 o 10 1 0 20.62 5.33 32.98 o 11 1 0 4418.60 3855.47 126.50 o 12 1 0 448.84 458.79 67.79 o 13 1 0 2737.48 2826.08 129.43 o 14 1 0 691.45 643.22 83.80 o 15 1 0 581.58 596.95 83.95 o 16 1 0 237.95 248.39 71.77 o 17 1 0 1090.67 1246.86 173.03 o -17 2 0 604.77 709.44 146.23 o -16 2 0 47.58 9.16 86.86 o -15 2 0 352.48 338.60 104.16 o -14 2 0 33.22 75.32 70.57 o -13 2 0 2862.15 2914.76 189.66 o -12 2 0 847.28 977.81 118.41 o -11 2 0 4229.53 4308.52 205.60 o -10 2 0 744.29 587.63 88.21 o -9 2 0 1307.20 1344.57 108.57 o -8 2 0 6218.18 6814.45 208.66 o -7 2 0 142.77 115.36 39.70 o -6 2 0 7994.23 7140.50 182.19 o -5 2 0 198.02 74.64 30.20 o -4 2 0 18043.95 18965.78 256.16 o -3 2 0 1427.51 1266.19 59.71 o -2 2 0 1286.76 1022.93 47.84 o -1 2 0 677.97 832.00 28.68 o 0 2 0 14545.46 17214.95 706.72 o 1 2 0 73.56 118.52 25.28 o 2 2 0 10001.47 11082.75 111.04 o 3 2 0 3081.22 3715.82 142.67 o 4 2 0 11074.79 12362.00 138.91 o 5 2 0 618.17 494.87 37.76 o 6 2 0 7124.93 7650.84 162.68 o 7 2 0 480.08 298.48 55.47 o 8 2 0 11927.94 13684.76 204.57 o 9 2 0 1138.72 1524.73 118.75 o 10 2 0 5435.83 5914.68 220.53 o 11 2 0 5.40 -5.84 30.37 o 12 2 0 5354.59 5247.65 160.77 o 13 2 0 609.87 593.66 75.68 o 14 2 0 1511.26 1427.13 103.68 o 15 2 0 506.18 470.76 76.51 o 16 2 0 935.54 973.04 102.68 o 17 2 0 33.51 41.01 54.34 o -17 3 0 0.66 -83.80 80.75 o -16 3 0 1058.97 1241.09 168.28 o -15 3 0 107.97 105.52 89.91 o -14 3 0 1798.09 1997.00 177.78 o -13 3 0 10.83 11.87 64.12 o -12 3 0 3410.51 3876.96 209.00 o -11 3 0 1652.54 1471.12 135.37 o -10 3 0 3590.38 3639.12 180.16 o -9 3 0 631.00 620.20 86.52 o -8 3 0 2008.36 1845.69 118.07 o -7 3 0 176.46 416.64 63.45 o -6 3 0 1447.02 1068.39 82.11 o -5 3 0 8303.26 8326.28 176.43 o -4 3 0 2109.87 2146.29 89.57 o -3 3 0 2615.14 2539.17 88.55 o -2 3 0 10793.08 12703.00 460.91 o -1 3 0 5247.82 6186.16 263.79 o 0 3 0 41552.41 46014.34 998.67 o 1 3 0 8393.46 8882.11 156.58 o 2 3 0 9064.82 8864.67 434.62 o 3 3 0 740.84 778.02 64.46 o 4 3 0 30.85 36.56 16.75 o 5 3 0 14137.30 14237.30 170.45 o 6 3 0 712.64 857.74 50.61 o 7 3 0 16563.13 14715.70 325.37 o 8 3 0 22.61 2.50 23.26 o 9 3 0 5310.03 5726.76 140.78 o 10 3 0 696.18 753.45 70.78 o 11 3 0 4791.98 4314.97 202.21 o 12 3 0 117.84 147.25 72.27 o 13 3 0 2665.55 2452.05 118.11 o 14 3 0 429.01 426.46 70.52 o 15 3 0 1131.51 1138.28 102.76 o 16 3 0 235.56 245.38 69.69 o 17 3 0 967.86 1041.87 109.16 o -17 4 0 860.92 1249.23 191.35 o -16 4 0 57.51 123.16 97.37 o -15 4 0 1101.72 1330.66 164.21 o -14 4 0 126.30 192.37 92.96 o -13 4 0 2381.29 2845.21 201.53 o -12 4 0 28.16 -3.73 55.30 o -11 4 0 5108.19 4630.50 209.00 o -10 4 0 65.68 150.98 62.43 o -9 4 0 3251.49 3875.94 177.10 o -8 4 0 462.08 630.04 88.55 o -7 4 0 6434.22 6109.08 182.53 o -6 4 0 1048.80 699.60 73.96 o -5 4 0 9209.22 9428.94 202.21 o -4 4 0 7768.77 8046.04 177.44 o -3 4 0 15287.26 14648.22 159.11 o -2 4 0 2093.08 2225.71 127.57 o -1 4 0 46902.57 46945.20 1044.30 o 0 4 0 247.05 315.35 30.85 o 1 4 0 8556.57 9014.40 367.44 o 2 4 0 1995.40 2176.20 61.88 o 3 4 0 7380.45 9364.86 198.14 o 4 4 0 7947.24 7107.89 116.51 o 5 4 0 1162.95 1301.23 57.81 o 6 4 0 5841.05 5207.66 162.68 o 7 4 0 3458.52 3192.42 97.46 o 8 4 0 12361.34 12978.27 299.58 o 9 4 0 646.29 808.60 65.96 o 10 4 0 1459.18 1543.60 85.09 o 11 4 0 405.81 400.17 99.92 o 12 4 0 4078.23 4121.24 213.41 o 13 4 0 6.42 15.61 61.75 o 14 4 0 2446.36 2472.58 267.35 o 15 4 0 237.77 131.97 52.77 o 16 4 0 345.21 439.10 78.93 o 17 4 0 1.19 -12.26 47.97 o -16 5 0 1206.81 1558.99 202.55 o -15 5 0 44.38 25.79 82.11 o -14 5 0 1048.73 1474.51 164.55 o -13 5 0 92.68 103.82 81.09 o -12 5 0 2771.62 3056.24 196.78 o -11 5 0 175.04 214.09 82.11 o -10 5 0 5450.51 5873.62 234.44 o -9 5 0 408.58 355.91 74.64 o -8 5 0 3703.54 3981.79 172.69 o -7 5 0 2002.05 1670.28 110.61 o -6 5 0 10780.58 9132.41 222.23 o -5 5 0 3543.43 2857.08 120.78 o -4 5 0 19854.08 16945.28 596.62 o -3 5 0 1799.54 1424.25 71.59 o -2 5 0 18410.74 19100.07 200.30 o -1 5 0 195.74 136.12 26.49 o 0 5 0 16253.85 18334.63 299.58 o 1 5 0 710.50 1070.58 52.71 o 2 5 0 8031.80 9357.85 413.24 o 3 5 0 4414.11 4108.65 101.61 o 4 5 0 3953.39 3641.46 148.94 o 5 5 0 9016.16 8617.73 269.56 o 6 5 0 3310.77 3002.86 90.54 o 7 5 0 8433.16 8746.07 160.02 o 8 5 0 3345.50 3886.86 235.46 o 9 5 0 4999.89 4991.29 137.25 o 10 5 0 17.67 25.45 30.77 o 11 5 0 849.07 775.76 73.72 o 12 5 0 207.99 145.64 49.89 o 13 5 0 1736.47 1611.24 154.37 o 14 5 0 28.93 1.70 70.57 o 15 5 0 939.28 945.86 96.02 o 16 5 0 13.11 -11.75 47.14 o 17 5 0 264.14 181.68 61.86 o -16 6 0 39.06 -16.62 104.50 o -15 6 0 1163.73 1321.50 178.46 o -14 6 0 9.54 -3.73 75.32 o -13 6 0 778.93 793.92 133.00 o -12 6 0 183.10 245.30 86.52 o -11 6 0 2448.00 2452.32 169.64 o -10 6 0 254.45 303.66 86.52 o -9 6 0 4543.35 4542.29 200.85 o -8 6 0 1345.24 1393.76 115.02 o -7 6 0 6821.46 6711.65 213.07 o -6 6 0 112.22 96.02 44.45 o -5 6 0 16486.08 13305.69 432.41 o -4 6 0 1576.23 1185.58 67.69 o -3 6 0 21076.70 20289.45 816.14 o -2 6 0 30.19 37.37 24.94 o -1 6 0 6658.73 6950.83 282.79 o 0 6 0 1402.82 1361.50 78.88 o 1 6 0 8840.12 7667.88 132.04 o 2 6 0 11895.65 11291.90 588.65 o 3 6 0 5003.41 5573.67 193.39 o 4 6 0 9838.38 9789.40 717.41 o 5 6 0 5581.57 5509.92 366.25 o 6 6 0 5646.83 5826.14 131.50 o 7 6 0 3672.56 3279.70 104.84 o 8 6 0 1053.91 1056.80 100.60 o 9 6 0 2530.30 2229.04 98.12 o 10 6 0 1680.51 1543.66 121.46 o 11 6 0 196.83 196.75 47.20 o 12 6 0 1352.16 1406.44 173.71 o 13 6 0 834.44 777.65 164.04 o 14 6 0 1289.87 1262.12 150.64 o 15 6 0 265.40 291.44 104.16 o 16 6 0 355.46 304.67 66.75 o -16 7 0 483.11 588.99 150.64 o -15 7 0 264.69 216.46 113.66 o -14 7 0 393.75 456.67 123.84 o -13 7 0 65.16 134.02 86.86 o -12 7 0 470.69 484.49 111.28 o -11 7 0 155.28 209.34 81.09 o -10 7 0 3234.02 3199.07 187.96 o -9 7 0 3.34 44.79 51.57 o -8 7 0 2688.51 2593.12 151.66 o -7 7 0 383.65 428.54 53.26 o -6 7 0 12556.92 11140.95 209.00 o -5 7 0 422.33 397.66 46.98 o -4 7 0 11531.28 9603.91 303.83 o -3 7 0 1025.14 1059.33 62.25 o -2 7 0 5341.28 5117.36 278.89 o -1 7 0 3909.74 3734.43 161.67 o 0 7 0 999.00 968.01 60.43 o 1 7 0 3159.70 3975.49 149.28 o 2 7 0 8564.87 7715.42 142.82 o 3 7 0 8215.04 8223.70 387.97 o 4 7 0 5149.81 5285.62 153.69 o 5 7 0 422.87 293.86 43.18 o 6 7 0 3674.70 3418.79 138.94 o 7 7 0 628.20 579.60 99.92 o 8 7 0 3562.77 3113.58 110.59 o 9 7 0 4824.60 4179.18 133.37 o 10 7 0 1382.61 1207.80 83.96 o 11 7 0 1132.06 1124.33 85.10 o 12 7 0 1486.53 1368.76 95.57 o 13 7 0 999.10 1027.55 105.01 o 14 7 0 1141.26 1306.36 103.39 o 15 7 0 854.22 937.77 152.34 o 16 7 0 256.33 172.70 57.14 o -15 8 0 368.91 481.10 143.18 o -14 8 0 602.40 957.11 163.19 o -13 8 0 176.49 141.82 95.34 o -12 8 0 126.16 139.10 84.14 o -11 8 0 488.49 568.97 138.09 o -10 8 0 507.93 563.25 75.32 o -9 8 0 4822.51 4738.64 150.18 o -8 8 0 256.71 261.96 51.22 o -7 8 0 4011.30 3645.69 124.01 o -6 8 0 95.83 138.11 40.99 o -5 8 0 2992.56 2484.17 99.14 o -4 8 0 686.94 672.41 61.24 o -3 8 0 3724.12 3648.27 247.84 o -2 8 0 110.56 90.53 35.45 o -1 8 0 370.78 454.99 60.73 o 0 8 0 2815.23 3000.22 363.03 o 1 8 0 2428.78 2536.84 299.08 o 2 8 0 562.86 535.26 53.04 o 3 8 0 7026.11 6520.86 549.13 o 4 8 0 2204.83 1993.06 87.91 o 5 8 0 2412.76 2385.24 95.70 o 6 8 0 534.43 492.03 55.45 o 7 8 0 4088.51 4181.64 129.71 o 8 8 0 656.02 721.35 69.41 o 9 8 0 2084.69 2103.33 102.20 o 10 8 0 2615.19 2296.78 117.05 o 11 8 0 1364.93 1358.38 93.36 o 12 8 0 760.98 772.06 84.41 o 13 8 0 1745.97 1473.07 104.95 o 14 8 0 712.32 736.93 92.51 o 15 8 0 181.24 111.20 59.27 o 16 8 0 431.82 377.96 122.82 o -15 9 0 459.56 580.85 140.12 o -14 9 0 424.26 565.45 98.56 o -13 9 0 497.05 621.59 92.47 o -12 9 0 403.23 400.61 76.17 o -11 9 0 743.89 819.82 116.37 o -10 9 0 1041.59 1219.32 121.63 o -9 9 0 1406.83 1224.18 93.77 o -8 9 0 3779.21 3371.79 127.22 o -7 9 0 2227.09 1886.60 97.84 o -6 9 0 876.13 822.91 75.13 o -5 9 0 1969.01 1909.11 136.22 o -4 9 0 1904.88 2009.32 93.80 o -3 9 0 695.25 637.48 101.61 o -2 9 0 2864.16 2888.15 117.05 o -1 9 0 31.11 -2.37 25.19 o 0 9 0 1025.72 1098.08 72.64 o 1 9 0 735.99 818.55 64.01 o 2 9 0 8880.62 8850.40 173.10 o 3 9 0 90.25 82.52 35.15 o 4 9 0 4201.00 4462.69 131.64 o 5 9 0 4.27 7.57 28.56 o 6 9 0 1867.64 1847.55 162.18 o 7 9 0 149.37 123.12 39.45 o 8 9 0 2760.80 2518.87 118.07 o 9 9 0 1093.49 991.95 101.44 o 10 9 0 1861.60 1736.72 142.50 o 11 9 0 798.04 769.85 163.70 o 12 9 0 600.53 548.91 77.73 o 13 9 0 252.01 260.78 65.65 o 14 9 0 491.11 503.21 143.52 o 15 9 0 311.48 324.58 111.79 o -14 10 0 339.11 340.30 122.48 o -13 10 0 426.34 470.24 124.86 o -12 10 0 587.79 716.22 135.71 o -11 10 0 771.50 866.87 129.94 o -10 10 0 2873.45 2709.40 132.78 o -9 10 0 1472.63 1452.44 101.70 o -8 10 0 1543.79 1188.54 89.55 o -7 10 0 1754.80 1848.39 136.90 o -6 10 0 2684.23 2518.11 114.68 o -5 10 0 841.05 848.17 76.09 o -4 10 0 2900.91 2763.81 254.12 o -3 10 0 3290.96 3217.63 162.68 o -2 10 0 190.18 248.19 52.08 o -1 10 0 4415.48 4542.62 264.13 o 0 10 0 15.48 7.63 30.91 o 1 10 0 2915.34 3217.15 145.04 o 2 10 0 3101.50 3408.52 202.72 o 3 10 0 8605.81 8940.24 807.49 o 4 10 0 127.63 80.75 38.07 o 5 10 0 3869.63 3705.83 126.08 o 6 10 0 6.21 -4.22 28.97 o 7 10 0 1174.28 1011.40 79.92 o 8 10 0 7.58 -3.76 34.18 o 9 10 0 2759.37 2809.39 125.38 o 10 10 0 236.92 262.90 57.50 o 11 10 0 1086.57 1300.91 99.42 o 12 10 0 105.79 53.10 45.05 o 13 10 0 190.40 228.73 63.55 o 14 10 0 56.38 43.46 53.95 o 15 10 0 246.13 292.15 80.68 o -13 11 0 415.65 492.64 135.03 o -12 11 0 669.02 702.65 137.41 o -11 11 0 810.32 634.12 125.53 o -10 11 0 529.96 527.92 120.44 o -9 11 0 1952.64 2145.95 174.73 o -8 11 0 862.81 934.73 91.99 o -7 11 0 1810.54 1708.02 99.66 o -6 11 0 806.34 792.30 78.99 o -5 11 0 457.27 504.57 76.85 o -4 11 0 1249.72 1367.84 180.67 o -3 11 0 3033.90 3254.49 433.43 o -2 11 0 4636.32 4800.52 142.01 o -1 11 0 986.35 958.61 78.60 o 0 11 0 3817.37 4185.68 157.43 o 1 11 0 423.86 664.20 81.94 o 2 11 0 7292.26 7274.85 230.20 o 3 11 0 1934.96 2077.00 163.19 o 4 11 0 3561.11 3403.48 128.28 o 5 11 0 76.66 92.09 51.40 o 6 11 0 2347.17 2122.44 110.61 o 7 11 0 34.61 9.31 34.87 o 8 11 0 2886.96 3393.79 136.78 o 9 11 0 16.28 -17.00 41.85 o 10 11 0 1121.88 1108.05 94.76 o 11 11 0 2.08 -26.97 39.24 o 12 11 0 411.41 376.93 71.60 o 13 11 0 3.17 -1.83 47.56 o 14 11 0 252.06 269.06 74.48 o -12 12 0 179.57 210.69 105.86 o -11 12 0 29.50 32.57 86.86 o -10 12 0 848.45 867.20 138.43 o -9 12 0 200.25 92.28 87.87 o -8 12 0 1200.00 1142.36 135.03 o -7 12 0 511.36 418.33 100.09 o -6 12 0 1434.00 1644.15 149.62 o -5 12 0 379.62 390.17 100.09 o -4 12 0 499.02 537.12 80.58 o -3 12 0 1875.74 1933.85 102.88 o -2 12 0 3069.66 2747.67 116.85 o -1 12 0 5499.85 5840.25 161.87 o 0 12 0 945.06 1101.44 88.04 o 1 12 0 2904.78 3183.74 198.48 o 2 12 0 1115.52 1198.19 91.75 o 3 12 0 3886.68 3856.40 206.11 o 4 12 0 266.75 165.10 48.97 o 5 12 0 3525.67 3408.75 134.61 o 6 12 0 282.73 352.27 64.97 o 7 12 0 2180.88 2249.03 118.93 o 8 12 0 53.22 61.37 47.28 o 9 12 0 1255.21 1432.59 128.08 o 10 12 0 573.34 536.64 79.19 o 11 12 0 1055.84 1315.82 117.57 o 12 12 0 0.49 -9.58 49.46 o 13 12 0 312.66 311.20 73.98 o -11 13 0 426.39 359.30 119.43 o -10 13 0 2.49 -31.89 74.30 o -9 13 0 1173.80 1268.91 167.27 o -8 13 0 33.59 33.25 79.05 o -7 13 0 782.00 839.72 130.96 o -6 13 0 242.01 214.43 92.28 o -5 13 0 1062.90 1074.16 141.48 o -4 13 0 597.63 623.94 121.80 o -3 13 0 1327.58 1439.91 157.09 o -2 13 0 2096.37 1998.36 181.18 o -1 13 0 879.93 1043.63 154.71 o 0 13 0 2346.94 2362.97 116.57 o 1 13 0 1001.78 926.40 82.89 o 2 13 0 1441.28 1413.95 95.76 o 3 13 0 1209.47 999.85 113.66 o 4 13 0 2934.35 3337.19 139.65 o 5 13 0 250.77 369.71 105.18 o 6 13 0 1658.73 1857.09 112.08 o 7 13 0 584.20 615.45 87.87 o 8 13 0 1252.22 1362.50 108.40 o 9 13 0 348.39 413.96 78.37 o 10 13 0 1164.42 1390.66 115.87 o 11 13 0 83.83 92.76 57.95 o 12 13 0 703.94 775.75 102.00 o -10 14 0 350.17 443.78 121.80 o -9 14 0 5.79 38.34 91.61 o -8 14 0 924.54 1008.34 148.27 o -7 14 0 132.49 58.02 91.27 o -6 14 0 782.74 831.92 136.39 o -5 14 0 227.25 177.10 91.94 o -4 14 0 442.38 430.89 118.07 o -3 14 0 157.87 113.66 97.37 o -2 14 0 2055.06 2095.06 198.82 o -1 14 0 824.77 991.38 165.57 o 0 14 0 769.00 729.45 150.64 o 1 14 0 417.47 432.24 122.48 o 2 14 0 974.31 768.47 150.30 o 3 14 0 621.54 583.56 138.43 o 4 14 0 1082.12 1076.46 96.65 o 5 14 0 1233.54 1221.93 103.30 o 6 14 0 343.90 301.49 78.88 o 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