# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' SNBL March 9 and March 25 1998' _shelx_refln_list_code 4 _shelx_F_calc_maximum 91.01 _exptl_crystal_F_000 352.00 _reflns_d_resolution_high 0.7448 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y+1, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+3/2, z+1/2' _cell_length_a 9.2820 _cell_length_b 10.8030 _cell_length_c 7.8870 _cell_angle_alpha 90.000 _cell_angle_beta 111.453 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 242.04 255.38 7.64 o 6 0 0 1326.26 1171.28 13.28 o 8 0 0 23.37 26.68 0.35 o 10 0 0 131.67 139.90 1.99 o 1 1 0 513.83 556.23 19.84 o 3 1 0 1080.98 1087.75 21.22 o 5 1 0 692.41 706.68 12.36 o 7 1 0 201.09 192.48 1.73 o 9 1 0 1.51 1.54 0.07 o 11 1 0 113.00 117.73 2.23 o 0 2 0 3223.14 3664.21 211.34 o 2 2 0 8283.70 7989.45 193.68 o 4 2 0 613.47 706.76 11.95 o 6 2 0 349.33 345.98 3.31 o 8 2 0 20.52 19.23 1.34 o 10 2 0 150.06 148.86 2.11 o 1 3 0 7562.23 7871.89 265.69 o 3 3 0 270.81 292.30 4.93 o 5 3 0 3.22 3.01 0.13 o 7 3 0 57.72 57.01 0.68 o 9 3 0 185.78 184.37 2.14 o 11 3 0 17.63 17.80 0.22 o 0 4 0 522.01 574.00 17.83 o 2 4 0 818.85 797.88 13.75 o 4 4 0 1200.54 1121.97 30.55 o 6 4 0 112.41 108.60 1.01 o 8 4 0 371.55 369.31 3.08 o 10 4 0 72.87 78.36 0.86 o 1 5 0 461.94 519.94 12.60 o 3 5 0 3642.99 4040.81 101.88 o 5 5 0 247.38 271.48 3.22 o 7 5 0 208.04 220.96 1.95 o 9 5 0 69.71 72.96 0.73 o 0 6 0 2.38 1.18 0.60 o 2 6 0 2231.19 1935.25 450.47 o 4 6 0 412.37 419.98 4.19 o 6 6 0 259.41 260.65 2.19 o 8 6 0 33.88 31.35 0.77 o 10 6 0 59.97 67.61 0.82 o 1 7 0 379.68 431.98 6.98 o 3 7 0 240.18 252.48 4.15 o 5 7 0 502.25 511.46 5.17 o 7 7 0 160.41 159.47 1.39 o 9 7 0 36.58 39.35 0.96 o 0 8 0 513.32 451.57 6.68 o 2 8 0 104.28 96.18 1.08 o 4 8 0 30.69 38.33 0.40 o 6 8 0 104.10 102.66 1.64 o 8 8 0 57.93 63.89 0.76 o 1 9 0 212.71 215.91 2.09 o 3 9 0 21.72 27.33 0.42 o 5 9 0 108.22 108.81 1.17 o 7 9 0 8.07 8.85 0.36 o 9 9 0 16.63 15.69 0.58 o 0 10 0 180.15 158.39 2.21 o 2 10 0 134.73 119.81 1.23 o 4 10 0 132.67 134.69 1.63 o 6 10 0 168.78 170.94 2.21 o 8 10 0 21.28 21.56 0.32 o 1 11 0 411.75 401.94 3.74 o 3 11 0 278.07 265.85 3.14 o 5 11 0 13.99 16.84 0.33 o 7 11 0 285.55 299.67 3.50 o 0 12 0 71.89 66.74 1.14 o 2 12 0 2.28 2.19 0.11 o 4 12 0 48.40 46.50 0.67 o 6 12 0 23.57 22.12 0.42 o 1 13 0 121.04 117.53 1.58 o 3 13 0 33.56 34.80 0.43 o 5 13 0 197.98 163.01 14.48 o 0 14 0 32.70 28.97 0.63 o 2 14 0 207.63 197.49 3.04 o -11 1 1 523.31 521.70 5.97 o -9 1 1 491.56 492.44 4.09 o -7 1 1 42.40 43.66 0.48 o -5 1 1 1188.03 1258.07 20.24 o -3 1 1 1335.57 1487.08 22.64 o -1 1 1 638.79 578.42 22.36 o 1 1 1 1663.18 1620.33 42.49 o 3 1 1 475.98 511.56 10.92 o 5 1 1 302.63 362.58 4.19 o 7 1 1 103.36 126.19 1.43 o 9 1 1 224.43 227.83 2.91 o 11 1 1 93.99 75.23 3.61 o -10 2 1 600.90 608.35 5.59 o -8 2 1 134.71 144.83 1.62 o -6 2 1 24.65 25.35 0.30 o -4 2 1 648.20 644.86 18.95 o -2 2 1 3638.96 3943.80 107.36 o 0 2 1 532.85 434.11 25.64 o 2 2 1 2667.16 2807.25 46.63 o 4 2 1 694.62 714.50 18.06 o 6 2 1 86.89 79.00 0.72 o 8 2 1 46.24 45.71 0.54 o 10 2 1 96.41 100.01 1.08 o -11 3 1 85.91 81.16 0.96 o -9 3 1 301.16 298.89 2.69 o -7 3 1 437.32 451.30 4.86 o -5 3 1 1691.27 1258.36 15.02 o -3 3 1 2644.27 3126.19 77.70 o -1 3 1 382.51 398.41 10.89 o 1 3 1 5821.16 6325.56 181.09 o 3 3 1 1072.59 1151.03 21.03 o 5 3 1 255.19 239.65 2.78 o 7 3 1 1419.12 1352.63 29.24 o 9 3 1 351.34 353.04 3.36 o -10 4 1 85.12 90.37 1.16 o -8 4 1 383.60 385.82 4.14 o -6 4 1 293.94 292.73 3.21 o -4 4 1 548.94 589.85 8.14 o -2 4 1 399.12 374.56 6.50 o 0 4 1 953.60 1059.96 21.46 o 2 4 1 71.67 74.08 2.02 o 4 4 1 63.60 74.39 0.83 o 6 4 1 173.87 187.23 1.62 o 8 4 1 91.78 97.26 0.94 o 10 4 1 130.63 133.75 2.30 o -11 5 1 20.01 16.66 0.49 o -9 5 1 114.42 121.19 1.80 o -7 5 1 161.38 171.44 1.75 o -5 5 1 64.10 69.43 0.75 o -3 5 1 559.33 593.76 9.99 o -1 5 1 340.06 371.17 7.24 o 1 5 1 584.89 624.49 13.17 o 3 5 1 3249.65 2837.68 904.69 o 5 5 1 984.00 961.82 14.20 o 7 5 1 271.36 251.39 2.14 o 9 5 1 156.99 160.13 2.10 o -10 6 1 72.20 71.19 0.92 o -8 6 1 53.36 56.05 1.23 o -6 6 1 21.74 26.42 0.46 o -4 6 1 165.20 181.35 1.86 o -2 6 1 1178.17 1107.75 122.25 o 0 6 1 645.43 652.41 10.44 o 2 6 1 113.58 123.57 1.51 o 4 6 1 180.91 190.40 2.13 o 6 6 1 542.22 562.26 4.75 o 8 6 1 228.63 222.14 2.28 o 10 6 1 32.84 30.50 0.44 o -9 7 1 2.32 2.02 0.08 o -7 7 1 636.47 641.97 5.89 o -5 7 1 675.40 689.81 6.81 o -3 7 1 596.77 601.48 10.57 o -1 7 1 273.70 282.11 3.44 o 1 7 1 466.47 494.21 5.53 o 3 7 1 6.71 9.27 0.14 o 5 7 1 78.76 87.60 0.98 o 7 7 1 130.03 130.29 1.84 o 9 7 1 2.22 2.98 0.21 o -10 8 1 77.02 63.96 3.95 o -8 8 1 144.13 142.28 2.16 o -6 8 1 184.53 187.34 1.84 o -4 8 1 2.76 3.55 0.10 o -2 8 1 678.79 718.71 6.95 o 0 8 1 867.55 890.99 9.33 o 2 8 1 0.24 0.09 0.07 o 4 8 1 1388.48 1319.02 12.71 o 6 8 1 208.41 196.21 2.27 o 8 8 1 23.93 23.36 0.31 o -9 9 1 86.04 92.97 2.44 o -7 9 1 14.13 15.47 0.41 o -5 9 1 532.03 514.81 4.89 o -3 9 1 915.95 865.68 7.93 o -1 9 1 266.55 256.86 2.42 o 1 9 1 83.71 77.88 0.81 o 3 9 1 216.46 226.75 2.56 o 5 9 1 203.16 202.49 2.00 o 7 9 1 82.17 87.88 1.12 o -8 10 1 23.43 24.48 0.44 o -6 10 1 197.39 206.24 2.21 o -4 10 1 69.04 78.20 0.88 o -2 10 1 54.83 62.75 0.65 o 0 10 1 345.76 340.13 3.28 o 2 10 1 283.15 273.12 2.75 o 4 10 1 34.95 36.12 0.42 o 6 10 1 324.60 336.33 3.63 o -7 11 1 22.88 22.40 0.36 o -5 11 1 115.19 103.40 1.47 o -3 11 1 51.45 48.21 0.52 o -1 11 1 9.88 7.96 0.27 o 1 11 1 31.01 33.74 0.40 o 3 11 1 142.77 140.19 1.62 o 5 11 1 127.13 118.94 1.47 o 7 11 1 39.82 35.12 0.84 o -6 12 1 11.30 10.74 0.28 o -4 12 1 298.12 297.93 3.56 o -2 12 1 71.15 73.75 0.94 o 0 12 1 45.29 46.47 0.63 o 2 12 1 3.44 2.46 0.10 o 4 12 1 31.53 33.31 0.45 o -5 13 1 4.91 4.02 0.11 o -3 13 1 67.90 65.83 1.79 o -1 13 1 15.42 15.68 0.22 o 1 13 1 84.76 86.20 1.32 o 3 13 1 15.62 15.93 0.23 o -2 14 1 188.28 186.49 2.52 o 0 14 1 286.97 287.18 4.30 o 2 14 1 179.98 160.71 3.62 o -12 0 2 1.83 1.58 0.10 o -10 0 2 84.20 82.51 1.39 o -8 0 2 869.44 888.87 11.08 o -6 0 2 559.81 569.59 7.78 o -4 0 2 1339.79 1383.15 34.62 o 0 0 2 842.30 819.19 25.73 o 2 0 2 3297.58 3638.52 71.49 o 4 0 2 1341.61 1180.61 17.24 o 6 0 2 410.18 463.17 5.70 o 8 0 2 869.92 899.90 11.17 o 10 0 2 240.35 228.29 4.19 o -11 1 2 3.93 3.69 0.28 o -9 1 2 868.96 888.83 7.87 o -7 1 2 160.20 161.87 1.62 o -5 1 2 78.69 68.75 2.01 o -3 1 2 4290.07 4392.15 82.92 o -1 1 2 769.71 739.82 16.38 o 1 1 2 4969.05 4876.27 263.29 o 3 1 2 566.09 572.92 10.16 o 5 1 2 239.59 243.75 2.12 o 7 1 2 109.12 116.78 1.15 o 9 1 2 26.43 27.59 0.34 o -12 2 2 15.73 13.85 0.70 o -10 2 2 302.85 301.25 3.79 o -8 2 2 153.08 160.15 1.51 o -6 2 2 228.83 227.48 2.70 o -4 2 2 2275.34 2575.44 41.41 o -2 2 2 1209.96 1278.59 24.45 o 0 2 2 1831.49 1868.11 32.49 o 2 2 2 195.10 211.13 4.89 o 4 2 2 1477.46 1217.93 16.11 o 6 2 2 47.69 58.01 0.62 o 8 2 2 43.33 39.54 0.56 o 10 2 2 173.25 167.94 2.11 o -11 3 2 63.13 64.66 0.90 o -9 3 2 176.97 173.54 1.91 o -7 3 2 1519.25 1451.62 64.54 o -5 3 2 1794.10 1505.78 309.39 o -3 3 2 545.36 559.12 10.76 o -1 3 2 1800.21 1876.29 39.06 o 1 3 2 226.18 260.17 5.34 o 3 3 2 571.22 539.66 10.65 o 5 3 2 205.26 217.05 2.68 o 7 3 2 324.39 325.65 2.82 o 9 3 2 95.75 91.49 2.15 o -10 4 2 11.43 11.42 0.15 o -8 4 2 492.29 484.11 4.10 o -6 4 2 345.94 369.98 4.01 o -4 4 2 1562.72 1679.50 43.77 o -2 4 2 3907.30 4062.40 205.08 o 0 4 2 1915.21 1911.78 29.76 o 2 4 2 964.09 967.61 19.28 o 4 4 2 291.51 289.49 4.74 o 6 4 2 307.88 291.39 2.81 o 8 4 2 90.22 90.54 1.33 o 10 4 2 122.70 108.96 2.86 o -11 5 2 31.61 31.81 0.44 o -9 5 2 25.13 27.50 0.57 o -7 5 2 24.83 28.34 0.36 o -5 5 2 1140.31 1101.07 10.18 o -3 5 2 459.56 512.44 10.94 o -1 5 2 450.88 452.32 7.18 o 1 5 2 383.76 395.61 6.19 o 3 5 2 66.68 63.88 0.95 o 5 5 2 593.17 595.81 4.78 o 7 5 2 33.04 32.42 0.67 o 9 5 2 12.10 13.44 0.45 o -10 6 2 45.75 48.50 0.58 o -8 6 2 201.11 185.95 2.01 o -6 6 2 1503.85 1371.39 15.25 o -4 6 2 74.73 75.81 0.87 o -2 6 2 677.76 655.44 7.84 o 0 6 2 195.17 201.52 2.18 o 2 6 2 700.65 683.35 8.85 o 4 6 2 1193.89 1139.30 10.49 o 6 6 2 482.87 486.83 4.81 o 8 6 2 262.95 264.93 2.70 o -9 7 2 64.50 67.42 0.69 o -7 7 2 466.01 457.22 4.31 o -5 7 2 322.80 311.00 4.70 o -3 7 2 214.20 217.11 2.68 o -1 7 2 457.58 448.80 6.38 o 1 7 2 280.52 278.09 4.74 o 3 7 2 246.90 236.96 2.82 o 5 7 2 26.39 25.24 0.28 o 7 7 2 10.47 10.83 0.15 o 9 7 2 14.28 10.97 0.18 o -10 8 2 20.47 19.60 0.27 o -8 8 2 230.69 219.56 5.38 o -6 8 2 94.25 92.95 1.34 o -4 8 2 652.69 680.64 7.51 o -2 8 2 189.78 190.61 2.32 o 0 8 2 221.33 216.95 2.53 o 2 8 2 641.60 632.77 6.66 o 4 8 2 357.82 338.74 3.19 o 6 8 2 293.19 288.74 3.52 o 8 8 2 29.19 31.19 0.95 o -9 9 2 7.40 6.29 0.13 o -7 9 2 153.51 150.42 2.24 o -5 9 2 480.42 475.64 4.69 o -3 9 2 72.06 70.25 0.85 o -1 9 2 14.55 16.69 0.22 o 1 9 2 106.73 105.09 1.53 o 3 9 2 338.26 333.93 5.14 o 5 9 2 45.68 47.77 0.55 o 7 9 2 75.77 75.40 1.32 o -8 10 2 6.58 6.03 0.13 o -6 10 2 88.36 94.37 1.93 o -4 10 2 20.41 23.90 0.60 o -2 10 2 410.07 395.17 4.80 o 0 10 2 484.40 475.26 4.18 o 2 10 2 351.05 327.08 3.11 o 4 10 2 247.41 229.68 2.67 o 6 10 2 122.23 121.69 2.30 o -7 11 2 167.81 175.88 5.50 o -5 11 2 31.55 34.69 0.73 o -3 11 2 166.14 179.93 2.85 o -1 11 2 123.72 129.89 2.03 o 1 11 2 402.47 392.92 7.70 o 3 11 2 161.89 167.05 3.06 o 5 11 2 171.39 175.29 2.71 o -6 12 2 21.58 27.32 0.63 o -4 12 2 121.50 121.39 1.90 o -2 12 2 228.09 230.10 2.53 o 0 12 2 61.71 65.29 1.22 o 2 12 2 122.18 118.69 1.57 o 4 12 2 166.01 167.89 3.05 o -5 13 2 2.09 2.53 0.09 o -3 13 2 45.37 47.92 1.86 o -1 13 2 263.52 264.82 3.02 o 1 13 2 275.83 279.09 3.48 o 3 13 2 368.18 347.28 6.60 o -2 14 2 96.04 90.81 4.27 o 0 14 2 8.70 7.49 0.13 o -11 1 3 125.72 127.46 1.54 o -9 1 3 56.67 56.55 0.65 o -7 1 3 170.71 172.89 2.02 o -5 1 3 557.02 598.90 9.11 o -3 1 3 503.18 506.27 10.98 o 1 1 3 2656.95 2887.59 39.31 o 3 1 3 841.72 788.02 7.96 o 5 1 3 490.79 474.11 4.55 o 7 1 3 198.26 194.16 1.77 o 9 1 3 121.90 116.81 1.40 o -12 2 3 28.93 27.95 0.46 o -10 2 3 6.96 6.48 0.36 o -8 2 3 218.88 208.52 2.95 o -6 2 3 714.09 697.01 8.59 o -4 2 3 460.76 526.29 12.86 o -2 2 3 5349.38 4579.12 594.07 o 0 2 3 939.52 893.86 17.16 o 2 2 3 626.64 681.78 11.76 o 4 2 3 118.58 119.59 2.06 o 6 2 3 69.40 67.01 0.84 o 8 2 3 45.61 48.36 0.81 o -11 3 3 81.70 84.81 1.31 o -9 3 3 140.10 134.92 2.03 o -7 3 3 277.79 274.24 2.69 o -5 3 3 242.75 247.77 5.49 o -3 3 3 540.18 578.45 9.46 o -1 3 3 2127.00 2442.55 44.57 o 1 3 3 902.47 923.64 13.53 o 3 3 3 342.90 337.82 4.82 o 5 3 3 161.27 153.80 1.42 o 7 3 3 127.83 120.35 2.14 o 9 3 3 28.09 30.00 0.53 o -10 4 3 144.93 138.53 1.45 o -8 4 3 299.96 285.37 4.89 o -6 4 3 134.73 143.26 1.43 o -4 4 3 909.76 832.89 50.62 o -2 4 3 8.84 12.57 0.45 o 0 4 3 487.67 517.28 9.90 o 2 4 3 243.24 249.02 3.64 o 4 4 3 422.97 434.67 7.23 o 6 4 3 204.76 195.71 1.87 o 8 4 3 145.18 146.64 1.83 o -11 5 3 209.85 204.26 4.24 o -9 5 3 209.85 217.71 3.73 o -7 5 3 562.05 588.63 6.82 o -5 5 3 152.93 153.36 1.52 o -3 5 3 1379.89 1008.90 50.70 o -1 5 3 959.07 859.19 22.82 o 1 5 3 627.42 692.05 7.32 o 3 5 3 223.39 224.82 2.38 o 5 5 3 119.54 125.79 1.24 o 7 5 3 12.85 14.18 0.28 o 9 5 3 133.77 118.27 5.48 o -10 6 3 31.23 31.12 0.45 o -8 6 3 1.45 1.45 0.10 o -6 6 3 573.60 570.42 5.52 o -4 6 3 562.49 546.48 6.02 o -2 6 3 134.85 146.62 1.70 o 0 6 3 511.41 548.54 6.06 o 2 6 3 324.61 316.69 3.40 o 4 6 3 293.73 282.64 2.70 o 6 6 3 191.51 192.27 2.29 o 8 6 3 94.52 93.29 4.64 o -9 7 3 330.71 331.40 3.52 o -7 7 3 261.93 273.62 2.46 o -5 7 3 349.23 354.74 3.77 o -3 7 3 456.46 472.63 5.77 o -1 7 3 621.56 649.71 6.97 o 1 7 3 153.34 154.38 1.88 o 3 7 3 77.76 83.09 0.80 o 5 7 3 143.42 150.09 2.30 o 7 7 3 168.44 172.22 2.49 o -10 8 3 23.16 20.93 0.64 o -8 8 3 12.99 14.70 0.40 o -6 8 3 0.88 2.01 0.15 o -4 8 3 618.21 634.95 6.08 o -2 8 3 668.10 677.43 9.49 o 0 8 3 86.56 85.85 1.00 o 2 8 3 135.38 131.78 2.17 o 4 8 3 124.97 124.95 1.17 o 6 8 3 7.95 8.82 0.13 o -9 9 3 33.14 31.43 0.97 o -7 9 3 15.35 16.03 0.21 o -5 9 3 503.52 490.12 5.18 o -3 9 3 90.27 93.54 2.19 o -1 9 3 768.10 760.68 7.92 o 1 9 3 1365.87 1286.35 12.11 o 3 9 3 56.55 55.57 1.17 o 5 9 3 130.91 136.79 1.46 o 7 9 3 33.86 33.60 1.48 o -8 10 3 227.21 225.16 3.13 o -6 10 3 2.85 2.93 0.10 o -4 10 3 24.23 26.30 0.85 o -2 10 3 53.15 53.53 0.57 o 0 10 3 154.39 159.12 1.96 o 2 10 3 9.50 10.70 0.29 o 4 10 3 73.10 76.93 1.05 o 6 10 3 52.50 54.89 0.87 o -7 11 3 94.79 98.28 2.15 o -5 11 3 90.69 95.50 1.12 o -3 11 3 175.56 181.27 2.19 o -1 11 3 300.44 287.60 3.27 o 1 11 3 63.80 63.28 0.83 o 3 11 3 74.78 77.89 1.19 o 5 11 3 27.63 29.08 0.46 o -6 12 3 265.15 246.55 5.52 o -4 12 3 208.39 206.08 2.88 o -2 12 3 8.79 8.22 0.17 o 0 12 3 187.78 176.46 10.16 o 2 12 3 299.85 294.37 3.68 o 4 12 3 2.17 1.16 0.07 o -5 13 3 44.60 38.33 4.01 o -3 13 3 24.95 26.37 0.35 o -1 13 3 107.88 116.02 1.47 o 1 13 3 173.26 175.32 3.46 o -12 0 4 95.16 102.87 3.33 o -10 0 4 30.17 32.54 0.70 o -8 0 4 788.66 794.89 9.68 o -6 0 4 894.37 900.20 12.00 o -4 0 4 2682.84 2931.86 42.81 o 0 0 4 1323.52 1364.05 34.91 o 2 0 4 864.12 763.24 8.99 o 4 0 4 368.45 394.13 4.88 o 6 0 4 98.84 106.65 1.25 o 8 0 4 118.47 127.36 2.18 o -11 1 4 13.32 13.94 0.18 o -9 1 4 31.47 28.74 0.28 o -7 1 4 355.36 340.58 3.28 o -5 1 4 428.54 416.01 4.58 o -3 1 4 162.91 171.47 3.52 o -1 1 4 2684.56 2577.17 42.40 o 1 1 4 427.26 423.94 4.63 o 3 1 4 116.90 133.33 1.68 o 5 1 4 449.98 443.67 5.55 o 7 1 4 10.95 11.05 0.15 o -12 2 4 231.06 235.53 3.98 o -10 2 4 64.78 62.70 0.64 o -8 2 4 207.15 189.80 2.19 o -6 2 4 1406.60 1490.56 18.97 o -4 2 4 2608.35 1790.31 740.01 o -2 2 4 295.88 279.04 7.82 o 0 2 4 50.29 51.63 1.50 o 2 2 4 345.31 366.66 4.44 o 4 2 4 305.36 295.71 2.86 o 6 2 4 282.74 281.03 4.50 o 8 2 4 147.47 150.05 1.89 o -11 3 4 200.21 197.35 2.38 o -9 3 4 157.54 163.80 2.07 o -7 3 4 248.99 259.71 2.26 o -5 3 4 100.29 96.68 1.31 o -3 3 4 28.32 27.34 0.40 o -1 3 4 80.60 100.57 2.50 o 1 3 4 2402.91 1383.92 18.87 o 3 3 4 1022.19 945.75 7.78 o 5 3 4 34.15 34.38 0.64 o 7 3 4 54.22 55.74 0.56 o -10 4 4 376.03 377.25 3.95 o -8 4 4 7.48 7.54 0.20 o -6 4 4 171.51 151.20 1.44 o -4 4 4 479.22 509.95 7.24 o -2 4 4 607.48 553.97 27.05 o 0 4 4 734.50 742.54 8.15 o 2 4 4 46.47 46.19 0.57 o 4 4 4 151.01 147.98 2.06 o 6 4 4 586.70 576.23 10.22 o 8 4 4 292.57 285.81 4.67 o -11 5 4 76.21 82.39 2.86 o -9 5 4 97.48 93.97 1.25 o -7 5 4 156.26 172.96 1.61 o -5 5 4 1177.36 1130.04 120.57 o -3 5 4 1.32 1.23 0.35 o -1 5 4 51.82 50.21 0.65 o 1 5 4 722.75 712.68 7.89 o 3 5 4 171.45 163.82 1.96 o 5 5 4 268.69 262.76 4.34 o 7 5 4 27.13 28.75 0.77 o -10 6 4 82.24 83.91 1.57 o -8 6 4 272.98 287.57 3.03 o -6 6 4 120.83 123.83 1.15 o -4 6 4 907.50 829.21 9.03 o -2 6 4 205.17 205.74 2.22 o 0 6 4 77.54 80.79 0.78 o 2 6 4 1432.57 1280.11 13.09 o 4 6 4 79.63 80.18 1.07 o 6 6 4 178.69 180.32 2.42 o -9 7 4 251.97 269.41 3.10 o -7 7 4 59.31 61.45 0.94 o -5 7 4 6.98 5.37 0.28 o -3 7 4 1048.27 1005.55 9.90 o -1 7 4 1130.24 1029.00 9.89 o 1 7 4 106.08 112.58 2.19 o 3 7 4 88.61 88.88 0.89 o 5 7 4 47.27 48.53 0.63 o 7 7 4 133.33 126.89 1.67 o -10 8 4 164.41 169.23 5.85 o -8 8 4 8.76 9.12 0.16 o -6 8 4 508.76 507.04 9.86 o -4 8 4 265.04 265.50 2.75 o -2 8 4 436.26 435.33 5.80 o 0 8 4 534.26 544.18 5.97 o 2 8 4 146.41 142.65 2.35 o 4 8 4 251.67 232.30 2.76 o 6 8 4 5.03 5.83 0.18 o -9 9 4 36.45 37.40 0.93 o -7 9 4 173.21 181.52 3.65 o -5 9 4 12.14 11.09 0.16 o -3 9 4 391.63 384.85 4.47 o -1 9 4 275.86 278.13 3.36 o 1 9 4 170.73 171.09 1.79 o 3 9 4 127.47 122.47 2.12 o 5 9 4 81.45 85.56 1.24 o -8 10 4 97.60 106.80 1.88 o -6 10 4 63.52 69.05 1.25 o -4 10 4 262.90 254.77 3.35 o -2 10 4 406.03 401.11 5.84 o 0 10 4 31.81 34.37 0.45 o 2 10 4 15.32 14.26 0.20 o 4 10 4 30.57 31.76 0.46 o -7 11 4 38.89 38.29 1.68 o -5 11 4 33.12 35.94 0.95 o -3 11 4 124.18 128.03 3.77 o -1 11 4 525.32 526.92 6.27 o 1 11 4 47.73 47.36 1.64 o 3 11 4 103.73 110.47 2.85 o -6 12 4 206.23 208.19 4.30 o -4 12 4 5.51 4.61 0.56 o -2 12 4 74.98 76.03 1.34 o 0 12 4 254.81 257.49 15.08 o 2 12 4 47.95 47.24 0.85 o -3 13 4 503.73 510.45 19.45 o -1 13 4 86.28 89.43 2.04 o -11 1 5 270.84 254.84 4.05 o -9 1 5 746.64 729.33 8.19 o -7 1 5 209.15 199.64 2.06 o -5 1 5 607.04 527.74 13.42 o -3 1 5 638.97 382.50 6.51 o -1 1 5 258.50 251.83 51.89 o 1 1 5 301.08 270.74 3.23 o 3 1 5 1112.93 1052.83 9.37 o 5 1 5 557.36 552.65 11.15 o 7 1 5 78.05 80.14 1.43 o -12 2 5 26.29 23.76 0.52 o -10 2 5 193.72 185.28 3.33 o -8 2 5 312.10 282.46 3.04 o -6 2 5 621.44 593.77 6.67 o -4 2 5 187.18 177.79 2.42 o -2 2 5 14.37 13.69 0.20 o 0 2 5 380.48 373.15 8.11 o 2 2 5 965.18 912.88 8.39 o 4 2 5 633.43 654.12 6.09 o 6 2 5 368.96 343.73 4.14 o -11 3 5 148.10 156.18 2.98 o -9 3 5 161.51 159.88 2.28 o -7 3 5 389.30 360.74 4.84 o -5 3 5 35.35 28.69 0.40 o -3 3 5 563.11 448.82 85.85 o -1 3 5 944.70 705.84 83.80 o 1 3 5 109.08 98.53 1.08 o 3 3 5 770.01 734.54 6.54 o 5 3 5 741.13 731.95 8.13 o 7 3 5 169.58 155.99 3.73 o -10 4 5 142.53 128.92 1.71 o -8 4 5 272.27 253.18 2.17 o -6 4 5 341.82 307.37 6.93 o -4 4 5 29.44 29.12 0.34 o -2 4 5 112.90 102.44 1.61 o 0 4 This is a multi-part message in MIME format. --------------8310157BC7ACB093D1C6C8D2 Content-Type: text/plain; charset=us-ascii Content-Transfer-Encoding: 7bit Dear Dr Holmes, > Thank you for your message. Figure 1 for your paper AV1045 has transferred > OK but the hkl file is not complete. Please will you resend this. You can send > it by ftp or by email to checkin@iucr.org. I have attached the structure factor file to this email. best wishes Dennis Madsen -- Dennis Madsen Dept. of Cell & Molecular Biology Uppsala University Biomedical Centre Box 596 S-751 24 Uppsala SWEDEN Ph: +46 18 471 4983 Fax: +46 18 536971 email: dennis@xray.bmc.uu.se http://alpha2.bmc.uu.se/dennis --------------8310157BC7ACB093D1C6C8D2 Content-Type: text/plain; charset=us-ascii; name="asp.fcf" Content-Transfer-Encoding: 7bit Content-Disposition: inline; filename="asp.fcf" # # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_asp _shelx_title ' SNBL March 9 and March 25 1998' _shelx_refln_list_code 4 _shelx_F_calc_maximum 91.01 _exptl_crystal_F_000 352.00 _reflns_d_resolution_high 0.7448 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y+1, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+3/2, z+1/2' _cell_length_a 9.2820 _cell_length_b 10.8030 _cell_length_c 7.8870 _cell_angle_alpha 90.000 _cell_angle_beta 111.453 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 242.04 255.38 7.64 o 6 0 0 1326.26 1171.28 13.28 o 8 0 0 23.37 26.68 0.35 o 10 0 0 131.67 139.90 1.99 o 1 1 0 513.83 556.23 19.84 o 3 1 0 1080.98 1087.75 21.22 o 5 1 0 692.41 706.68 12.36 o 7 1 0 201.09 192.48 1.73 o 9 1 0 1.51 1.54 0.07 o 11 1 0 113.00 117.73 2.23 o 0 2 0 3223.14 3664.21 211.34 o 2 2 0 8283.70 7989.45 193.68 o 4 2 0 613.47 706.76 11.95 o 6 2 0 349.33 345.98 3.31 o 8 2 0 20.52 19.23 1.34 o 10 2 0 150.06 148.86 2.11 o 1 3 0 7562.23 7871.89 265.69 o 3 3 0 270.81 292.30 4.93 o 5 3 0 3.22 3.01 0.13 o 7 3 0 57.72 57.01 0.68 o 9 3 0 185.78 184.37 2.14 o 11 3 0 17.63 17.80 0.22 o 0 4 0 522.01 574.00 17.83 o 2 4 0 818.85 797.88 13.75 o 4 4 0 1200.54 1121.97 30.55 o 6 4 0 112.41 108.60 1.01 o 8 4 0 371.55 369.31 3.08 o 10 4 0 72.87 78.36 0.86 o 1 5 0 461.94 519.94 12.60 o 3 5 0 3642.99 4040.81 101.88 o 5 5 0 247.38 271.48 3.22 o 7 5 0 208.04 220.96 1.95 o 9 5 0 69.71 72.96 0.73 o 0 6 0 2.38 1.18 0.60 o 2 6 0 2231.19 1935.25 450.47 o 4 6 0 412.37 419.98 4.19 o 6 6 0 259.41 260.65 2.19 o 8 6 0 33.88 31.35 0.77 o 10 6 0 59.97 67.61 0.82 o 1 7 0 379.68 431.98 6.98 o 3 7 0 240.18 252.48 4.15 o 5 7 0 502.25 511.46 5.17 o 7 7 0 160.41 159.47 1.39 o 9 7 0 36.58 39.35 0.96 o 0 8 0 513.32 451.57 6.68 o 2 8 0 104.28 96.18 1.08 o 4 8 0 30.69 38.33 0.40 o 6 8 0 104.10 102.66 1.64 o 8 8 0 57.93 63.89 0.76 o 1 9 0 212.71 215.91 2.09 o 3 9 0 21.72 27.33 0.42 o 5 9 0 108.22 108.81 1.17 o 7 9 0 8.07 8.85 0.36 o 9 9 0 16.63 15.69 0.58 o 0 10 0 180.15 158.39 2.21 o 2 10 0 134.73 119.81 1.23 o 4 10 0 132.67 134.69 1.63 o 6 10 0 168.78 170.94 2.21 o 8 10 0 21.28 21.56 0.32 o 1 11 0 411.75 401.94 3.74 o 3 11 0 278.07 265.85 3.14 o 5 11 0 13.99 16.84 0.33 o 7 11 0 285.55 299.67 3.50 o 0 12 0 71.89 66.74 1.14 o 2 12 0 2.28 2.19 0.11 o 4 12 0 48.40 46.50 0.67 o 6 12 0 23.57 22.12 0.42 o 1 13 0 121.04 117.53 1.58 o 3 13 0 33.56 34.80 0.43 o 5 13 0 197.98 163.01 14.48 o 0 14 0 32.70 28.97 0.63 o 2 14 0 207.63 197.49 3.04 o -11 1 1 523.31 521.70 5.97 o -9 1 1 491.56 492.44 4.09 o -7 1 1 42.40 43.66 0.48 o -5 1 1 1188.03 1258.07 20.24 o -3 1 1 1335.57 1487.08 22.64 o -1 1 1 638.79 578.42 22.36 o 1 1 1 1663.18 1620.33 42.49 o 3 1 1 475.98 511.56 10.92 o 5 1 1 302.63 362.58 4.19 o 7 1 1 103.36 126.19 1.43 o 9 1 1 224.43 227.83 2.91 o 11 1 1 93.99 75.23 3.61 o -10 2 1 600.90 608.35 5.59 o -8 2 1 134.71 144.83 1.62 o -6 2 1 24.65 25.35 0.30 o -4 2 1 648.20 644.86 18.95 o -2 2 1 3638.96 3943.80 107.36 o 0 2 1 532.85 434.11 25.64 o 2 2 1 2667.16 2807.25 46.63 o 4 2 1 694.62 714.50 18.06 o 6 2 1 86.89 79.00 0.72 o 8 2 1 46.24 45.71 0.54 o 10 2 1 96.41 100.01 1.08 o -11 3 1 85.91 81.16 0.96 o -9 3 1 301.16 298.89 2.69 o -7 3 1 437.32 451.30 4.86 o -5 3 1 1691.27 1258.36 15.02 o -3 3 1 2644.27 3126.19 77.70 o -1 3 1 382.51 398.41 10.89 o 1 3 1 5821.16 6325.56 181.09 o 3 3 1 1072.59 1151.03 21.03 o 5 3 1 255.19 239.65 2.78 o 7 3 1 1419.12 1352.63 29.24 o 9 3 1 351.34 353.04 3.36 o -10 4 1 85.12 90.37 1.16 o -8 4 1 383.60 385.82 4.14 o -6 4 1 293.94 292.73 3.21 o -4 4 1 548.94 589.85 8.14 o -2 4 1 399.12 374.56 6.50 o 0 4 1 953.60 1059.96 21.46 o 2 4 1 71.67 74.08 2.02 o 4 4 1 63.60 74.39 0.83 o 6 4 1 173.87 187.23 1.62 o 8 4 1 91.78 97.26 0.94 o 10 4 1 130.63 133.75 2.30 o -11 5 1 20.01 16.66 0.49 o -9 5 1 114.42 121.19 1.80 o -7 5 1 161.38 171.44 1.75 o -5 5 1 64.10 69.43 0.75 o -3 5 1 559.33 593.76 9.99 o -1 5 1 340.06 371.17 7.24 o 1 5 1 584.89 624.49 13.17 o 3 5 1 3249.65 2837.68 904.69 o 5 5 1 984.00 961.82 14.20 o 7 5 1 271.36 251.39 2.14 o 9 5 1 156.99 160.13 2.10 o -10 6 1 72.20 71.19 0.92 o -8 6 1 53.36 56.05 1.23 o -6 6 1 21.74 26.42 0.46 o -4 6 1 165.20 181.35 1.86 o -2 6 1 1178.17 1107.75 122.25 o 0 6 1 645.43 652.41 10.44 o 2 6 1 113.58 123.57 1.51 o 4 6 1 180.91 190.40 2.13 o 6 6 1 542.22 562.26 4.75 o 8 6 1 228.63 222.14 2.28 o 10 6 1 32.84 30.50 0.44 o -9 7 1 2.32 2.02 0.08 o -7 7 1 636.47 641.97 5.89 o -5 7 1 675.40 689.81 6.81 o -3 7 1 596.77 601.48 10.57 o -1 7 1 273.70 282.11 3.44 o 1 7 1 466.47 494.21 5.53 o 3 7 1 6.71 9.27 0.14 o 5 7 1 78.76 87.60 0.98 o 7 7 1 130.03 130.29 1.84 o 9 7 1 2.22 2.98 0.21 o -10 8 1 77.02 63.96 3.95 o -8 8 1 144.13 142.28 2.16 o -6 8 1 184.53 187.34 1.84 o -4 8 1 2.76 3.55 0.10 o -2 8 1 678.79 718.71 6.95 o 0 8 1 867.55 890.99 9.33 o 2 8 1 0.24 0.09 0.07 o 4 8 1 1388.48 1319.02 12.71 o 6 8 1 208.41 196.21 2.27 o 8 8 1 23.93 23.36 0.31 o -9 9 1 86.04 92.97 2.44 o -7 9 1 14.13 15.47 0.41 o -5 9 1 532.03 514.81 4.89 o -3 9 1 915.95 865.68 7.93 o -1 9 1 266.55 256.86 2.42 o 1 9 1 83.71 77.88 0.81 o 3 9 1 216.46 226.75 2.56 o 5 9 1 203.16 202.49 2.00 o 7 9 1 82.17 87.88 1.12 o -8 10 1 23.43 24.48 0.44 o -6 10 1 197.39 206.24 2.21 o -4 10 1 69.04 78.20 0.88 o -2 10 1 54.83 62.75 0.65 o 0 10 1 345.76 340.13 3.28 o 2 10 1 283.15 273.12 2.75 o 4 10 1 34.95 36.12 0.42 o 6 10 1 324.60 336.33 3.63 o -7 11 1 22.88 22.40 0.36 o -5 11 1 115.19 103.40 1.47 o -3 11 1 51.45 48.21 0.52 o -1 11 1 9.88 7.96 0.27 o 1 11 1 31.01 33.74 0.40 o 3 11 1 142.77 140.19 1.62 o 5 11 1 127.13 118.94 1.47 o 7 11 1 39.82 35.12 0.84 o -6 12 1 11.30 10.74 0.28 o -4 12 1 298.12 297.93 3.56 o -2 12 1 71.15 73.75 0.94 o 0 12 1 45.29 46.47 0.63 o 2 12 1 3.44 2.46 0.10 o 4 12 1 31.53 33.31 0.45 o -5 13 1 4.91 4.02 0.11 o -3 13 1 67.90 65.83 1.79 o -1 13 1 15.42 15.68 0.22 o 1 13 1 84.76 86.20 1.32 o 3 13 1 15.62 15.93 0.23 o -2 14 1 188.28 186.49 2.52 o 0 14 1 286.97 287.18 4.30 o 2 14 1 179.98 160.71 3.62 o -12 0 2 1.83 1.58 0.10 o -10 0 2 84.20 82.51 1.39 o -8 0 2 869.44 888.87 11.08 o -6 0 2 559.81 569.59 7.78 o -4 0 2 1339.79 1383.15 34.62 o 0 0 2 842.30 819.19 25.73 o 2 0 2 3297.58 3638.52 71.49 o 4 0 2 1341.61 1180.61 17.24 o 6 0 2 410.18 463.17 5.70 o 8 0 2 869.92 899.90 11.17 o 10 0 2 240.35 228.29 4.19 o -11 1 2 3.93 3.69 0.28 o -9 1 2 868.96 888.83 7.87 o -7 1 2 160.20 161.87 1.62 o -5 1 2 78.69 68.75 2.01 o -3 1 2 4290.07 4392.15 82.92 o -1 1 2 769.71 739.82 16.38 o 1 1 2 4969.05 4876.27 263.29 o 3 1 2 566.09 572.92 10.16 o 5 1 2 239.59 243.75 2.12 o 7 1 2 109.12 116.78 1.15 o 9 1 2 26.43 27.59 0.34 o -12 2 2 15.73 13.85 0.70 o -10 2 2 302.85 301.25 3.79 o -8 2 2 153.08 160.15 1.51 o -6 2 2 228.83 227.48 2.70 o -4 2 2 2275.34 2575.44 41.41 o -2 2 2 1209.96 1278.59 24.45 o 0 2 2 1831.49 1868.11 32.49 o 2 2 2 195.10 211.13 4.89 o 4 2 2 1477.46 1217.93 16.11 o 6 2 2 47.69 58.01 0.62 o 8 2 2 43.33 39.54 0.56 o 10 2 2 173.25 167.94 2.11 o -11 3 2 63.13 64.66 0.90 o -9 3 2 176.97 173.54 1.91 o -7 3 2 1519.25 1451.62 64.54 o -5 3 2 1794.10 1505.78 309.39 o -3 3 2 545.36 559.12 10.76 o -1 3 2 1800.21 1876.29 39.06 o 1 3 2 226.18 260.17 5.34 o 3 3 2 571.22 539.66 10.65 o 5 3 2 205.26 217.05 2.68 o 7 3 2 324.39 325.65 2.82 o 9 3 2 95.75 91.49 2.15 o -10 4 2 11.43 11.42 0.15 o -8 4 2 492.29 484.11 4.10 o -6 4 2 345.94 369.98 4.01 o -4 4 2 1562.72 1679.50 43.77 o -2 4 2 3907.30 4062.40 205.08 o 0 4 2 1915.21 1911.78 29.76 o 2 4 2 964.09 967.61 19.28 o 4 4 2 291.51 289.49 4.74 o 6 4 2 307.88 291.39 2.81 o 8 4 2 90.22 90.54 1.33 o 10 4 2 122.70 108.96 2.86 o -11 5 2 31.61 31.81 0.44 o -9 5 2 25.13 27.50 0.57 o -7 5 2 24.83 28.34 0.36 o -5 5 2 1140.31 1101.07 10.18 o -3 5 2 459.56 512.44 10.94 o -1 5 2 450.88 452.32 7.18 o 1 5 2 383.76 395.61 6.19 o 3 5 2 66.68 63.88 0.95 o 5 5 2 593.17 595.81 4.78 o 7 5 2 33.04 32.42 0.67 o 9 5 2 12.10 13.44 0.45 o -10 6 2 45.75 48.50 0.58 o -8 6 2 201.11 185.95 2.01 o -6 6 2 1503.85 1371.39 15.25 o -4 6 2 74.73 75.81 0.87 o -2 6 2 677.76 655.44 7.84 o 0 6 2 195.17 201.52 2.18 o 2 6 2 700.65 683.35 8.85 o 4 6 2 1193.89 1139.30 10.49 o 6 6 2 482.87 486.83 4.81 o 8 6 2 262.95 264.93 2.70 o -9 7 2 64.50 67.42 0.69 o -7 7 2 466.01 457.22 4.31 o -5 7 2 322.80 311.00 4.70 o -3 7 2 214.20 217.11 2.68 o -1 7 2 457.58 448.80 6.38 o 1 7 2 280.52 278.09 4.74 o 3 7 2 246.90 236.96 2.82 o 5 7 2 26.39 25.24 0.28 o 7 7 2 10.47 10.83 0.15 o 9 7 2 14.28 10.97 0.18 o -10 8 2 20.47 19.60 0.27 o -8 8 2 230.69 219.56 5.38 o -6 8 2 94.25 92.95 1.34 o -4 8 2 652.69 680.64 7.51 o -2 8 2 189.78 190.61 2.32 o 0 8 2 221.33 216.95 2.53 o 2 8 2 641.60 632.77 6.66 o 4 8 2 357.82 338.74 3.19 o 6 8 2 293.19 288.74 3.52 o 8 8 2 29.19 31.19 0.95 o -9 9 2 7.40 6.29 0.13 o -7 9 2 153.51 150.42 2.24 o -5 9 2 480.42 475.64 4.69 o -3 9 2 72.06 70.25 0.85 o -1 9 2 14.55 16.69 0.22 o 1 9 2 106.73 105.09 1.53 o 3 9 2 338.26 333.93 5.14 o 5 9 2 45.68 47.77 0.55 o 7 9 2 75.77 75.40 1.32 o -8 10 2 6.58 6.03 0.13 o -6 10 2 88.36 94.37 1.93 o -4 10 2 20.41 23.90 0.60 o -2 10 2 410.07 395.17 4.80 o 0 10 2 484.40 475.26 4.18 o 2 10 2 351.05 327.08 3.11 o 4 10 2 247.41 229.68 2.67 o 6 10 2 122.23 121.69 2.30 o -7 11 2 167.81 175.88 5.50 o -5 11 2 31.55 34.69 0.73 o -3 11 2 166.14 179.93 2.85 o -1 11 2 123.72 129.89 2.03 o 1 11 2 402.47 392.92 7.70 o 3 11 2 161.89 167.05 3.06 o 5 11 2 171.39 175.29 2.71 o -6 12 2 21.58 27.32 0.63 o -4 12 2 121.50 121.39 1.90 o -2 12 2 228.09 230.10 2.53 o 0 12 2 61.71 65.29 1.22 o 2 12 2 122.18 118.69 1.57 o 4 12 2 166.01 167.89 3.05 o -5 13 2 2.09 2.53 0.09 o -3 13 2 45.37 47.92 1.86 o -1 13 2 263.52 264.82 3.02 o 1 13 2 275.83 279.09 3.48 o 3 13 2 368.18 347.28 6.60 o -2 14 2 96.04 90.81 4.27 o 0 14 2 8.70 7.49 0.13 o -11 1 3 125.72 127.46 1.54 o -9 1 3 56.67 56.55 0.65 o -7 1 3 170.71 172.89 2.02 o -5 1 3 557.02 598.90 9.11 o -3 1 3 503.18 506.27 10.98 o 1 1 3 2656.95 2887.59 39.31 o 3 1 3 841.72 788.02 7.96 o 5 1 3 490.79 474.11 4.55 o 7 1 3 198.26 194.16 1.77 o 9 1 3 121.90 116.81 1.40 o -12 2 3 28.93 27.95 0.46 o -10 2 3 6.96 6.48 0.36 o -8 2 3 218.88 208.52 2.95 o -6 2 3 714.09 697.01 8.59 o -4 2 3 460.76 526.29 12.86 o -2 2 3 5349.38 4579.12 594.07 o 0 2 3 939.52 893.86 17.16 o 2 2 3 626.64 681.78 11.76 o 4 2 3 118.58 119.59 2.06 o 6 2 3 69.40 67.01 0.84 o 8 2 3 45.61 48.36 0.81 o -11 3 3 81.70 84.81 1.31 o -9 3 3 140.10 134.92 2.03 o -7 3 3 277.79 274.24 2.69 o -5 3 3 242.75 247.77 5.49 o -3 3 3 540.18 578.45 9.46 o -1 3 3 2127.00 2442.55 44.57 o 1 3 3 902.47 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