# Structure factors for Acta Cryst. Section C, paper: NA1515 # # Dispiro[fluorene-9,5'-[1,2,3,4]tetrathiane-6',9''-fluorene] # # Data for compound (IV) # # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # Absorption correction applied # Extinction correction not applied # data_IV _shelx_title ' AG 104.1 (HG9822)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 325.78 _exptl_crystal_F_000 1888.00 _reflns_d_resolution_high 0.7699 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y, z-1/2' _cell_length_a 13.5095 _cell_length_b 18.0142 _cell_length_c 16.7946 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4969.97 5336.40 61.89 o 4 0 0 1336.19 1423.37 57.14 o 6 0 0 14650.08 14970.61 178.89 o 8 0 0 32927.66 33942.51 322.50 o 10 0 0 19447.56 18854.95 285.54 o 12 0 0 495.40 538.75 48.29 o 14 0 0 4266.60 4344.66 204.51 o 16 0 0 1130.10 1102.72 89.53 o 3 1 0 25756.45 26873.62 222.56 o 5 1 0 7.12 -35.57 35.57 o 7 1 0 11176.00 11682.39 125.72 o 9 1 0 5688.04 5424.53 111.22 o 11 1 0 11977.41 11963.01 203.76 o 13 1 0 763.46 766.47 91.01 o 15 1 0 92.19 5.96 82.12 o 17 1 0 767.47 734.45 111.54 o 2 2 0 4292.36 4275.03 63.27 o 4 2 0 724.92 801.62 51.76 o 6 2 0 7072.09 7983.48 138.23 o 8 2 0 885.79 1022.85 86.81 o 10 2 0 1001.10 1215.74 95.55 o 12 2 0 59.70 -77.73 97.80 o 14 2 0 103.86 97.98 115.44 o 16 2 0 49.44 23.66 74.55 o 1 3 0 17986.29 17912.34 178.43 o 3 3 0 4722.83 4874.39 85.25 o 5 3 0 10770.56 11806.98 151.01 o 7 3 0 40.83 -54.83 54.83 o 9 3 0 825.65 923.14 64.55 o 11 3 0 592.60 701.39 67.50 o 13 3 0 4120.02 3828.24 180.97 o 15 3 0 409.59 348.41 59.75 o 17 3 0 23.45 26.89 141.41 o 0 4 0 19940.61 19982.66 140.08 o 2 4 0 2084.62 2187.51 60.32 o 4 4 0 1770.03 1722.85 65.07 o 6 4 0 26.49 46.27 51.82 o 8 4 0 4153.14 4298.05 137.07 o 10 4 0 1506.43 1677.39 117.52 o 12 4 0 3785.73 4143.56 179.82 o 14 4 0 2831.10 2359.12 168.42 o 16 4 0 251.29 242.05 66.34 o 1 5 0 154.30 181.45 13.76 o 3 5 0 4271.95 4412.68 91.85 o 5 5 0 14302.79 15789.24 188.95 o 7 5 0 66.69 53.79 27.59 o 9 5 0 5119.00 5144.55 165.88 o 11 5 0 7903.90 8138.72 226.43 o 13 5 0 2239.90 2332.97 164.49 o 15 5 0 49.17 39.39 79.01 o 17 5 0 1427.35 1509.49 128.40 o 0 6 0 46780.87 46941.86 260.90 o 2 6 0 34908.00 34065.00 234.07 o 4 6 0 862.52 775.94 59.86 o 6 6 0 1204.51 1314.93 74.61 o 8 6 0 15846.42 16428.22 249.39 o 10 6 0 4053.48 3990.64 160.73 o 12 6 0 13243.19 13243.94 296.88 o 14 6 0 0.21 -8.62 108.39 o 16 6 0 0.29 106.07 126.03 o 1 7 0 50994.84 49724.98 359.86 o 3 7 0 5144.45 4969.88 106.94 o 5 7 0 733.77 700.12 64.55 o 7 7 0 3582.83 3349.06 118.05 o 9 7 0 23273.96 24463.06 333.78 o 11 7 0 3495.46 3646.69 164.78 o 13 7 0 528.27 690.63 66.51 o 15 7 0 1659.29 1743.09 171.26 o 0 8 0 79.59 130.54 22.33 o 2 8 0 11172.93 11617.91 162.29 o 4 8 0 566.23 589.82 43.55 o 6 8 0 2871.51 3219.04 116.19 o 8 8 0 4091.04 3878.15 147.95 o 10 8 0 16.61 -85.37 85.37 o 12 8 0 111.80 178.20 49.45 o 14 8 0 509.67 494.16 64.20 o 16 8 0 76.20 -78.08 134.70 o 1 9 0 418.82 366.21 29.96 o 3 9 0 3036.27 2825.40 99.36 o 5 9 0 2362.75 2881.62 107.06 o 7 9 0 120.58 70.62 71.60 o 9 9 0 5384.34 5019.39 177.33 o 11 9 0 2584.15 2736.45 151.82 o 13 9 0 223.82 310.59 54.71 o 15 9 0 1477.03 1326.55 119.38 o 0 10 0 9082.17 9221.89 161.94 o 2 10 0 11739.35 12410.51 189.01 o 4 10 0 4369.85 4730.67 133.31 o 6 10 0 2983.09 2991.10 125.39 o 8 10 0 3810.04 3713.08 157.90 o 10 10 0 146.24 123.83 43.67 o 12 10 0 332.79 422.21 53.33 o 14 10 0 896.10 896.82 83.63 o 1 11 0 1127.13 891.98 51.75 o 3 11 0 5307.40 5490.94 145.23 o 5 11 0 1817.59 1802.78 104.22 o 7 11 0 12118.20 12076.33 248.29 o 9 11 0 422.26 426.95 48.99 o 11 11 0 349.95 390.75 52.28 o 13 11 0 136.35 -58.65 111.80 o 15 11 0 1009.05 985.78 79.87 o 0 12 0 21605.30 21500.59 279.12 o 2 12 0 459.91 341.18 35.86 o 4 12 0 7231.33 8916.80 193.47 o 6 12 0 1245.81 1085.08 107.98 o 8 12 0 6179.30 6398.92 202.66 o 10 12 0 1862.84 1882.71 147.08 o 12 12 0 1290.47 1291.68 101.04 o 14 12 0 280.56 66.40 139.39 o 1 13 0 5541.86 5143.80 295.49 o 3 13 0 4502.51 4670.52 149.34 o 5 13 0 13.35 13.71 71.20 o 7 13 0 32.83 62.12 78.83 o 9 13 0 3245.92 3651.54 173.05 o 11 13 0 7487.87 8517.44 266.74 o 13 13 0 1917.76 1895.50 179.06 o 0 14 0 3515.26 3582.26 142.16 o 2 14 0 300.13 283.05 38.06 o 4 14 0 446.63 389.30 44.36 o 6 14 0 2561.86 2571.84 136.38 o 8 14 0 647.58 801.74 76.23 o 10 14 0 1982.95 2092.60 160.61 o 12 14 0 1133.98 1142.40 92.77 o 14 14 0 60.85 16.31 129.27 o 1 15 0 706.90 717.12 46.91 o 3 15 0 2414.35 2578.09 138.64 o 5 15 0 0.63 69.00 71.49 o 7 15 0 331.45 301.74 45.29 o 9 15 0 71.58 148.47 49.34 o 11 15 0 1186.86 1140.89 111.97 o 13 15 0 12.71 -48.93 142.45 o 0 16 0 1533.53 1509.84 122.09 o 2 16 0 1592.15 1526.38 131.23 o 4 16 0 5.99 -100.58 100.58 o 6 16 0 0.35 -47.25 84.27 o 8 16 0 50.54 51.65 92.08 o 10 16 0 2958.28 3049.11 191.96 o 12 16 0 3545.50 3451.37 230.71 o 1 17 0 4941.73 5320.42 222.59 o 3 17 0 15.37 121.80 44.82 o 5 17 0 48.02 -93.70 101.10 o 7 17 0 1457.13 1702.38 145.40 o 9 17 0 1.32 93.00 101.10 o 11 17 0 1186.32 1308.97 114.75 o 0 18 0 1504.12 1518.74 138.52 o 2 18 0 484.24 546.73 54.19 o 4 18 0 159.95 196.24 47.60 o 6 18 0 2313.45 2525.98 157.66 o 8 18 0 801.66 897.23 74.67 o 10 18 0 72.45 83.23 83.98 o 1 19 0 3565.49 3564.58 136.08 o 3 19 0 69.98 137.88 49.57 o 5 19 0 84.14 46.91 91.96 o 7 19 0 1666.30 1704.69 167.79 o 9 19 0 3999.07 4206.95 225.80 o 0 20 0 4864.42 5185.38 224.52 o 2 20 0 1043.89 1105.79 94.62 o 4 20 0 223.64 297.11 55.58 o 6 20 0 102.85 -107.35 107.35 o 8 20 0 3.67 71.37 83.23 o 1 21 0 796.45 832.39 56.35 o 3 21 0 59.05 -14.69 114.17 o 5 21 0 1322.31 1373.63 110.18 o 7 21 0 688.61 714.52 75.48 o 0 22 0 3253.75 3351.78 212.55 o 2 22 0 1644.99 1946.51 172.64 o 4 22 0 57.35 21.17 119.84 o 1 23 0 762.26 819.01 56.30 o 3 23 0 70.78 102.78 112.61 o 2 1 1 5109.57 6002.90 627.50 o 3 1 1 5935.69 5961.27 60.63 o 4 1 1 75.22 62.59 30.97 o 5 1 1 876.06 788.42 39.66 o 6 1 1 4891.87 5113.66 80.68 o 7 1 1 8049.62 8215.29 108.78 o 8 1 1 4315.54 3691.14 445.78 o 9 1 1 6505.56 6084.13 171.81 o 10 1 1 3032.26 3206.82 242.63 o 11 1 1 25.90 -21.43 62.06 o 12 1 1 1267.29 1140.73 102.95 o 13 1 1 54.83 -60.30 98.27 o 14 1 1 1684.65 1808.96 126.61 o 15 1 1 3.08 -13.05 83.82 o 16 1 1 2436.94 2351.63 191.12 o 17 1 1 21.81 59.12 89.74 o 0 2 1 16598.62 16342.79 93.81 o 1 2 1 7297.79 7389.90 49.92 o 2 2 1 9808.11 9521.31 93.12 o 3 2 1 5257.20 5409.10 85.48 o 4 2 1 1752.45 1787.74 65.59 o 5 2 1 168.67 169.52 22.96 o 6 2 1 370.99 389.30 38.81 o 7 2 1 3.09 -57.72 57.72 o 8 2 1 5952.46 5802.51 149.28 o 9 2 1 61.80 97.40 38.46 o 10 2 1 450.29 462.47 43.67 o 11 2 1 1004.91 893.53 76.52 o 12 2 1 547.49 517.12 52.63 o 13 2 1 436.92 566.11 56.45 o 14 2 1 69.92 8.10 110.99 o 15 2 1 7.10 -125.22 125.22 o 16 2 1 125.39 182.13 65.65 o 17 2 1 24.61 133.66 66.28 o 1 3 1 4.03 30.80 11.31 o 2 3 1 12465.04 13385.99 121.69 o 3 3 1 818.41 952.23 50.78 o 4 3 1 1524.86 1470.51 63.51 o 5 3 1 3001.68 3212.27 87.04 o 6 3 1 89.84 84.79 24.81 o 7 3 1 21.10 -0.87 57.03 o 8 3 1 4792.06 4799.32 137.36 o 9 3 1 352.33 440.20 43.72 o 10 3 1 2514.69 2360.16 127.07 o 11 3 1 7.95 24.87 84.50 o 12 3 1 1044.69 879.99 79.18 o 13 3 1 25.14 53.38 60.21 o 14 3 1 286.09 265.18 58.76 o 15 3 1 63.28 8.62 123.71 o 16 3 1 1253.91 1381.61 115.62 o 17 3 1 208.16 127.42 158.70 o 0 4 1 11168.34 11195.24 108.27 o 1 4 1 23846.61 24456.15 113.84 o 2 4 1 27716.05 23054.68 170.27 o 3 4 1 11621.03 12209.00 138.98 o 4 4 1 237.90 250.32 22.38 o 5 4 1 1421.41 1615.51 66.86 o 6 4 1 3434.68 3522.63 101.62 o 7 4 1 664.69 675.25 64.78 o 8 4 1 998.72 946.56 84.67 o 9 4 1 7685.06 7516.51 182.07 o 10 4 1 91.56 11.74 82.82 o 11 4 1 315.93 355.93 46.85 o 12 4 1 502.88 513.48 54.25 o 13 4 1 214.41 246.33 54.14 o 14 4 1 650.74 651.42 65.18 o 15 4 1 117.98 92.19 127.42 o 16 4 1 446.75 477.97 72.47 o 17 4 1 977.84 915.62 89.47 o 1 5 1 10203.94 9629.76 82.02 o 2 5 1 880.06 945.93 51.48 o 3 5 1 2766.83 2674.56 75.42 o 4 5 1 6091.46 7170.87 124.58 o 5 5 1 0.92 5.67 29.38 o 6 5 1 243.45 287.33 29.27 o 7 5 1 526.35 538.35 46.67 o 8 5 1 72.80 4.57 70.10 o 9 5 1 837.39 860.50 66.74 o 10 5 1 11.53 -27.53 57.55 o 11 5 1 3397.44 3511.12 163.62 o 12 5 1 691.55 603.30 57.49 o 13 5 1 529.89 561.08 58.88 o 14 5 1 201.26 208.85 56.56 o 15 5 1 668.15 701.74 66.74 o 16 5 1 1.64 104.28 121.17 o 17 5 1 1031.13 1055.82 98.67 o 0 6 1 39649.05 27696.33 205.55 o 1 6 1 1546.96 1580.37 44.05 o 2 6 1 1863.26 1834.07 68.77 o 3 6 1 397.66 350.78 33.49 o 4 6 1 268.23 339.97 29.09 o 5 6 1 7023.92 8000.08 148.87 o 6 6 1 1736.76 1840.14 87.39 o 7 6 1 2104.69 2039.80 98.03 o 8 6 1 3303.75 2927.94 123.71 o 9 6 1 71.07 34.36 38.87 o 10 6 1 445.84 432.45 45.40 o 11 6 1 822.57 843.32 63.04 o 12 6 1 41.29 -111.28 111.28 o 13 6 1 574.20 514.00 59.23 o 14 6 1 31.82 -114.00 114.00 o 15 6 1 199.84 275.25 61.19 o 16 6 1 1.83 -0.64 113.36 o 1 7 1 1165.70 1043.92 99.10 o 2 7 1 7739.76 7647.57 126.14 o 3 7 1 2679.24 2520.60 84.67 o 4 7 1 6617.09 6168.21 126.95 o 5 7 1 56.75 39.97 54.14 o 6 7 1 383.82 315.27 31.93 o 7 7 1 130.59 146.15 32.50 o 8 7 1 779.30 837.42 60.96 o 9 7 1 170.92 214.52 41.64 o 10 7 1 62.15 59.05 80.62 o 11 7 1 3810.64 3585.78 172.76 o 12 7 1 2044.97 2050.38 145.63 o 13 7 1 837.14 953.85 88.95 o 14 7 1 189.55 320.48 57.43 o 15 7 1 9.88 125.33 57.09 o 16 7 1 41.53 -12.96 133.55 o 0 8 1 17947.58 14157.94 174.26 o 1 8 1 653.10 769.57 41.96 o 2 8 1 1146.83 1072.30 64.84 o 3 8 1 2786.74 2732.69 90.46 o 4 8 1 1240.78 1183.52 73.05 o 5 8 1 940.09 785.49 71.60 o 6 8 1 156.66 172.59 32.22 o 7 8 1 1320.35 1272.99 97.86 o 8 8 1 4858.53 4509.15 156.16 o 9 8 1 1633.20 1834.25 120.88 o 10 8 1 1087.17 1115.68 76.40 o 11 8 1 331.40 280.80 51.19 o 12 8 1 1356.67 1372.42 96.59 o 13 8 1 695.54 845.52 83.11 o 14 8 1 449.90 391.85 63.56 o 15 8 1 33.38 76.63 84.38 o 16 8 1 150.53 83.46 133.84 o 1 9 1 6019.24 5192.69 729.44 o 2 9 1 2922.22 3096.89 101.91 o 3 9 1 4.53 -54.14 54.14 o 4 9 1 1772.83 1670.28 83.34 o 5 9 1 1897.06 2492.78 100.12 o 6 9 1 205.99 211.68 36.09 o 7 9 1 1187.33 1015.79 72.53 o 8 9 1 316.04 344.77 43.26 o 9 9 1 18.60 4.97 55.93 o 10 9 1 111.92 233.20 40.66 o 11 9 1 46.59 -100.93 100.93 o 12 9 1 127.88 247.66 48.76 o 13 9 1 0.90 42.11 108.44 o 14 9 1 1673.58 1688.50 162.18 o 15 9 1 56.50 3.82 138.23 o 16 9 1 170.28 104.57 142.34 o 0 10 1 115.27 135.22 26.08 o 1 10 1 31.51 -22.63 48.58 o 2 10 1 360.71 437.42 42.97 o 3 10 1 374.27 277.62 31.52 o 4 10 1 627.51 655.58 51.71 o 5 10 1 2891.14 2845.24 120.19 o 6 10 1 319.23 407.12 38.46 o 7 10 1 255.79 284.33 38.58 o 8 10 1 716.32 633.08 54.89 o 9 10 1 2192.79 2107.06 131.87 o 10 10 1 1011.57 916.66 78.31 o 11 10 1 549.67 540.49 50.14 o 12 10 1 245.40 347.60 51.94 o 13 10 1 38.58 -44.65 109.14 o 14 10 1 0.86 -117.18 117.18 o 15 10 1 8.28 -19.03 96.93 o 1 11 1 213.96 219.45 42.68 o 2 11 1 86.57 101.33 29.27 o 3 11 1 283.79 255.52 33.08 o 4 11 1 169.50 190.75 34.01 o 5 11 1 269.13 242.92 36.50 o 6 11 1 33.89 -3.93 64.31 o 7 11 1 1166.23 1255.06 108.56 o 8 11 1 546.42 592.83 58.30 o 9 11 1 1271.15 1207.81 82.24 o 10 11 1 283.80 311.86 50.67 o 11 11 1 86.22 84.62 100.29 o 12 11 1 427.59 364.43 58.18 o 13 11 1 289.40 319.55 58.70 o 14 11 1 428.97 454.95 65.18 o 15 11 1 5.32 64.66 121.98 o 0 12 1 26.92 50.67 54.83 o 1 12 1 1913.94 1692.21 190.05 o 2 12 1 1099.14 1087.57 90.69 o 3 12 1 171.03 266.86 33.20 o 4 12 1 940.56 815.50 63.27 o 5 12 1 256.00 234.99 36.61 o 6 12 1 709.84 810.99 64.60 o 7 12 1 149.33 128.05 41.30 o 8 12 1 1721.92 1872.88 131.70 o 9 12 1 782.09 826.95 77.15 o 10 12 1 989.46 1245.75 123.77 o 11 12 1 1139.77 1240.20 89.82 o 12 12 1 1066.13 1082.31 97.46 o 13 12 1 406.04 481.03 62.12 o 14 12 1 313.43 410.12 65.99 o 15 12 1 104.61 244.82 64.84 o 1 13 1 0.28 -49.63 49.63 o 2 13 1 13.53 21.63 33.02 o 3 13 1 122.56 123.66 36.44 o 4 13 1 112.51 67.21 77.91 o 5 13 1 47.36 68.77 70.91 o 6 13 1 2866.12 2691.04 141.06 o 7 13 1 331.91 248.18 44.30 o 8 13 1 12.17 -86.93 86.93 o 9 13 1 330.45 485.31 53.38 o 10 13 1 43.43 70.62 72.30 o 11 13 1 18.51 -126.43 126.43 o 12 13 1 2.05 -27.53 113.77 o 13 13 1 77.71 127.88 60.27 o 14 13 1 617.65 681.90 70.10 o 0 14 1 1827.57 1567.67 108.62 o 1 14 1 1941.65 1887.03 80.70 o 2 14 1 781.36 764.72 65.82 o 3 14 1 3623.80 3784.74 147.72 o 4 14 1 996.89 900.81 73.05 o 5 14 1 699.89 584.21 55.12 o 6 14 1 28.22 104.92 36.55 o 7 14 1 91.95 70.45 79.58 o 8 14 1 335.10 324.00 47.08 o 9 14 1 1586.75 1617.76 144.48 o 10 14 1 2222.45 2448.82 168.94 o 11 14 1 1566.90 1868.95 162.52 o 12 14 1 2692.01 3185.90 186.41 o 13 14 1 246.35 86.93 133.95 o 14 14 1 0.40 63.74 87.39 o 1 15 1 655.36 438.70 62.98 o 2 15 1 334.47 241.70 43.15 o 3 15 1 229.82 132.16 48.64 o 4 15 1 1344.42 1424.06 119.66 o 5 15 1 2275.72 2688.44 140.02 o 6 15 1 186.73 184.10 43.44 o 7 15 1 438.91 440.83 48.70 o 8 15 1 543.47 472.41 53.79 o 9 15 1 953.41 936.27 88.26 o 10 15 1 269.53 347.77 61.60 o 11 15 1 484.79 507.93 69.17 o 12 15 1 1318.22 1342.86 126.84 o 13 15 1 746.22 873.22 82.82 o 0 16 1 136.41 155.76 41.87 o 1 16 1 2280.85 2223.64 96.46 o 2 16 1 287.89 244.88 47.60 o 3 16 1 695.04 808.91 77.15 o 4 16 1 86.61 -12.43 95.78 o 5 16 1 369.42 353.62 49.51 o 6 16 1 281.19 172.99 49.45 o 7 16 1 54.43 -6.65 86.93 o 8 16 1 155.29 142.51 48.81 o 9 16 1 10.24 -36.96 102.95 o 10 16 1 7.60 20.30 107.06 o 11 16 1 20.24 47.66 83.98 o 12 16 1 318.89 374.09 71.83 o 1 17 1 86.27 -74.72 74.72 o 2 17 1 3554.87 3853.80 177.73 o 3 17 1 3.02 -97.05 97.05 o 4 17 1 1919.77 2233.03 145.63 o 5 17 1 59.41 22.85 91.15 o 6 17 1 702.13 684.96 58.82 o 7 17 1 277.76 408.21 52.17 o 8 17 1 63.01 108.21 49.39 o 9 17 1 12.65 16.77 107.58 o 10 17 1 9.71 18.22 116.48 o 11 17 1 75.97 -12.49 130.83 o 12 17 1 13.22 -141.82 141.82 o 0 18 1 3948.11 3976.94 186.41 o 1 18 1 1159.75 1104.53 62.50 o 2 18 1 243.40 -90.46 118.16 o 3 18 1 447.65 403.12 55.29 o 4 18 1 36.98 -103.88 103.88 o 5 18 1 757.01 772.47 71.95 o 6 18 1 7.15 -33.37 98.90 o 7 18 1 214.24 243.32 55.87 o 8 18 1 236.27 88.03 115.44 o 9 18 1 2.79 -80.68 109.77 o 10 18 1 72.21 80.68 122.56 o 11 18 1 133.00 -60.32 139.04 o 1 19 1 0.48 -80.34 80.34 o 2 19 1 1035.22 1062.81 97.92 o 3 19 1 140.18 191.85 51.65 o 4 19 1 6.78 59.98 93.58 o 5 19 1 0.03 -6.54 101.91 o 6 19 1 98.42 -29.32 107.35 o 7 19 1 60.77 188.14 51.76 o 8 19 1 83.95 30.08 121.23 o 9 19 1 71.64 -2.60 115.39 o 10 19 1 76.33 40.37 124.99 o 0 20 1 822.02 932.74 76.40 o 1 20 1 147.19 186.17 40.14 o 2 20 1 507.51 565.24 64.95 o 3 20 1 27.90 86.18 47.89 o 4 20 1 10.06 65.01 102.95 o 5 20 1 0.75 -3.18 108.16 o 6 20 1 449.04 503.30 60.32 o 7 20 1 511.06 526.95 70.73 o 8 20 1 292.52 243.32 68.54 o 9 20 1 92.89 7.06 95.43 o 1 21 1 742.30 766.16 86.78 o 2 21 1 763.88 711.97 70.27 o 3 21 1 155.73 282.42 54.95 o 4 21 1 304.23 439.10 59.51 o 5 21 1 18.63 -116.66 116.66 o 6 21 1 108.61 65.93 61.89 o 7 21 1 134.43 242.45 63.79 o 0 22 1 0.08 -127.88 127.88 o 1 22 1 26.85 -90.40 90.40 o 2 22 1 99.55 124.52 125.10 o 3 22 1 152.91 126.08 62.35 o 4 22 1 26.16 81.55 121.63 o 5 22 1 61.89 -24.58 122.85 o 1 23 1 158.70 33.40 92.09 o 2 23 1 126.30 34.24 129.50 o 3 23 1 15.38 -26.55 126.37 o 1 0 2 28754.81 30060.41 600.64 o 2 0 2 5440.67 5224.37 70.50 o 3 0 2 50198.79 51565.59 239.62 o 4 0 2 285.10 291.90 27.13 o 5 0 2 22614.76 23561.68 207.46 o 6 0 2 2548.54 2360.74 86.70 o 7 0 2 1307.09 1419.26 85.54 o 8 0 2 5750.79 5900.77 145.98 o 9 0 2 5730.97 5483.48 159.40 o 10 0 2 1422.97 1332.57 104.34 o 11 0 2 0.07 -27.59 86.29 o 12 0 2 547.50 602.26 58.76 o 13 0 2 3418.21 3390.58 167.79 o 14 0 2 1149.48 1213.60 98.21 o 15 0 2 465.74 455.00 64.66 o 16 0 2 716.12 618.45 74.38 o 17 0 2 1.75 155.81 63.04 o 1 1 2 1805.37 1755.54 19.43 o 2 1 2 4843.98 5051.51 50.00 o 3 1 2 10926.58 11119.14 151.27 o 4 1 2 5602.05 5469.72 68.13 o 5 1 2 556.85 654.49 31.47 o 6 1 2 2154.06 2108.29 142.77 o 7 1 2 730.76 720.11 46.93 o 8 1 2 533.06 577.27 37.46 o 9 1 2 4369.29 4274.42 192.19 o 10 1 2 42.12 55.81 65.88 o 11 1 2 3209.11 3282.44 175.68 o 12 1 2 1115.46 1161.04 68.22 o 13 1 2 337.93 312.02 37.44 o 14 1 2 321.50 341.02 60.44 o 15 1 2 359.88 347.97 43.83 o 16 1 2 253.39 255.18 44.21 o 17 1 2 187.10 231.93 49.12 o 0 2 2 918.99 989.01 33.31 o 1 2 2 162.23 163.50 20.36 o 2 2 2 13397.91 13122.37 115.67 o 3 2 2 1.93 10.12 37.13 o 4 2 2 41.12 31.87 38.92 o 5 2 2 7283.62 7829.35 125.62 o 6 2 2 972.88 974.15 66.28 o 7 2 2 382.74 149.57 29.27 o 8 2 2 4105.69 4111.81 126.61 o 9 2 2 7291.15 7167.87 178.66 o 10 2 2 482.84 382.71 44.30 o 11 2 2 26.67 64.03 81.72 o 12 2 2 1357.19 1346.16 122.67 o 13 2 2 1852.11 1868.66 144.07 o 14 2 2 493.07 440.37 60.21 o 15 2 2 1938.54 1773.75 168.42 o 16 2 2 8.42 -137.94 137.94 o 17 2 2 1620.04 1407.06 134.76 o 1 3 2 5072.28 5032.49 107.49 o 2 3 2 30304.20 32087.27 193.64 o 3 3 2 761.31 854.25 51.82 o 4 3 2 3900.31 4173.93 90.57 o 5 3 2 679.48 860.56 57.14 o 6 3 2 11.52 13.94 49.39 o 7 3 2 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12 942.21 870.74 76.11 o 5 6 12 209.61 247.25 44.07 o 6 6 12 17.48 2.89 81.84 o 7 6 12 325.11 314.46 48.12 o 8 6 12 7242.77 7204.36 231.81 o 9 6 12 171.58 160.96 51.59 o 10 6 12 2012.18 1882.94 162.06 o 11 6 12 511.32 487.80 65.65 o 12 6 12 481.46 633.37 65.93 o 13 6 12 2.49 -103.47 123.08 o 1 7 12 2496.07 2388.33 97.93 o 2 7 12 1752.02 1616.60 126.55 o 3 7 12 6203.90 6352.65 193.81 o 4 7 12 1663.10 1460.73 115.91 o 5 7 12 175.48 168.65 44.48 o 6 7 12 42.24 86.12 89.36 o 7 7 12 897.18 916.95 86.24 o 8 7 12 137.98 160.21 51.19 o 9 7 12 4375.65 4666.82 209.72 o 10 7 12 266.53 271.66 60.50 o 11 7 12 2040.78 2166.00 173.80 o 12 7 12 9.14 -0.29 112.55 o 13 7 12 158.04 69.52 119.14 o 0 8 12 185.12 24.52 69.40 o 1 8 12 1.21 -64.51 64.51 o 2 8 12 718.32 606.54 59.28 o 3 8 12 557.93 528.46 50.09 o 4 8 12 342.58 274.61 46.44 o 5 8 12 1414.63 1539.91 119.43 o 6 8 12 910.57 906.60 80.05 o 7 8 12 5.40 -98.96 98.96 o 8 8 12 31.72 -95.32 108.27 o 9 8 12 13.56 95.55 53.56 o 10 8 12 82.33 104.51 60.90 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283.81 66.69 o 4 5 20 291.71 17.70 145.98 o 5 5 20 12.19 -33.49 77.27 o 0 6 20 398.45 374.55 71.14 o 1 6 20 193.77 151.86 100.23 o 2 6 20 523.58 415.39 75.77 o 3 6 20 2398.26 2680.69 203.53 o 4 6 20 17.07 -64.84 136.38 o 5 6 20 2683.80 3136.04 212.20 o 1 7 20 154.62 237.53 102.57 o 2 7 20 12.09 107.23 130.19 o 3 7 20 293.33 89.36 152.40 o 4 7 20 97.37 48.12 135.98 o 0 8 20 0.54 121.86 131.46 o 1 8 20 47.63 91.89 92.10 o 2 8 20 39.19 -140.49 140.49 o 3 8 20 232.84 218.51 70.33 o 1 9 20 0.11 106.26 56.63 o 1 1 21 816.86 884.93 40.65 o 2 1 21 24.40 33.62 95.98 o 3 1 21 105.39 -95.45 97.99 o 4 1 21 25.58 29.71 76.02 o 0 2 21 1405.98 1492.89 140.89 o 1 2 21 172.64 35.54 104.99 o 2 2 21 469.54 383.11 74.49 o 3 2 21 73.20 100.93 63.97 o 4 2 21 0.79 -58.01 123.54 o 1 3 21 43.34 91.68 59.44 o 2 3 21 58.45 -41.01 139.91 o 3 3 21 32.72 -93.12 132.39 o 4 3 21 3.86 -22.38 120.07 o 0 4 21 53.76 -154.37 154.37 o 1 4 21 103.67 154.42 48.68 o 2 4 21 19.45 50.61 129.15 o 3 4 21 5.17 27.07 130.71 o 1 5 21 340.80 165.70 77.53 o 2 5 21 417.92 331.06 79.76 o 0 6 21 32.55 -65.93 133.08 o 1 6 21 237.09 129.67 66.10 o