# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' isosx in Pna2(1) (C6H11NO2.H2O)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 99.10 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.8297 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' _cell_length_a 11.9647 _cell_length_b 8.3276 _cell_length_c 7.6054 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3972.30 3770.13 9.80 o 4 0 0 155.11 132.85 7.49 o 6 0 0 93.39 92.96 0.69 o 8 0 0 87.23 91.03 2.08 o 10 0 0 115.97 105.74 2.78 o 12 0 0 81.04 73.06 1.50 o 14 0 0 0.13 0.60 0.51 o 1 1 0 762.76 779.12 8.97 o 2 1 0 4401.46 4123.49 23.90 o 3 1 0 1087.36 1074.50 5.69 o 4 1 0 162.20 147.65 2.02 o 5 1 0 59.97 60.02 0.44 o 6 1 0 142.37 149.65 1.98 o 7 1 0 159.35 146.21 2.28 o 8 1 0 45.01 42.78 1.95 o 9 1 0 241.89 225.42 7.18 o 10 1 0 153.65 144.74 2.22 o 11 1 0 141.78 149.94 1.86 o 12 1 0 3.22 3.52 0.38 o 13 1 0 5.98 6.62 0.46 o 14 1 0 0.09 0.02 0.36 o 0 2 0 55.14 60.98 1.72 o 1 2 0 9821.21 8833.14 18.65 o 2 2 0 3524.24 3430.85 32.39 o 3 2 0 638.79 688.83 7.01 o 4 2 0 1658.29 1744.80 27.27 o 5 2 0 48.24 49.05 0.61 o 6 2 0 51.56 46.13 0.71 o 7 2 0 236.59 206.36 2.71 o 8 2 0 150.15 143.21 1.88 o 9 2 0 25.88 22.95 0.53 o 10 2 0 16.54 15.15 0.40 o 11 2 0 33.67 31.86 1.16 o 12 2 0 3.62 3.26 0.34 o 13 2 0 0.01 -0.02 0.34 o 14 2 0 20.67 22.57 1.13 o 1 3 0 697.28 710.30 7.98 o 2 3 0 18.10 16.46 0.36 o 3 3 0 476.61 471.08 11.08 o 4 3 0 13.52 14.41 0.30 o 5 3 0 65.47 63.73 0.80 o 6 3 0 38.47 39.75 0.48 o 7 3 0 0.25 0.72 0.24 o 8 3 0 44.38 43.54 0.77 o 9 3 0 0.05 0.00 0.19 o 10 3 0 135.25 137.20 1.73 o 11 3 0 1.29 0.16 0.26 o 12 3 0 41.85 37.98 0.71 o 13 3 0 15.75 12.60 0.52 o 0 4 0 125.62 143.27 1.46 o 1 4 0 28.64 34.09 1.19 o 2 4 0 256.14 264.75 5.44 o 3 4 0 1001.46 1076.30 24.38 o 4 4 0 46.07 45.47 1.39 o 5 4 0 2.17 1.14 0.18 o 6 4 0 2.01 3.52 0.28 o 7 4 0 18.62 18.83 0.39 o 8 4 0 62.98 54.69 0.84 o 9 4 0 2.13 4.36 0.26 o 10 4 0 3.60 4.65 0.28 o 11 4 0 22.96 21.37 0.50 o 12 4 0 9.86 12.25 0.48 o 13 4 0 12.42 13.09 0.62 o 1 5 0 163.65 169.23 2.20 o 2 5 0 43.92 46.77 0.58 o 3 5 0 26.21 23.47 0.51 o 4 5 0 58.37 65.92 1.42 o 5 5 0 1.40 1.29 0.22 o 6 5 0 11.43 7.65 0.31 o 7 5 0 0.92 1.04 0.25 o 8 5 0 78.37 77.72 1.40 o 9 5 0 1.90 0.97 0.24 o 10 5 0 13.59 13.66 0.43 o 11 5 0 14.20 14.50 0.57 o 12 5 0 15.07 13.43 0.57 o 0 6 0 79.10 68.89 1.51 o 1 6 0 52.95 61.48 1.90 o 2 6 0 113.78 119.21 1.95 o 3 6 0 15.40 18.38 0.47 o 4 6 0 53.07 58.87 1.69 o 5 6 0 124.62 121.23 1.41 o 6 6 0 80.38 77.46 1.72 o 7 6 0 49.01 46.62 0.74 o 8 6 0 0.14 0.03 0.27 o 9 6 0 10.00 10.27 0.48 o 10 6 0 6.39 7.18 0.42 o 11 6 0 8.80 11.81 0.50 o 1 7 0 8.66 6.65 0.35 o 2 7 0 185.70 187.03 3.63 o 3 7 0 84.40 92.95 1.89 o 4 7 0 2.29 2.21 0.30 o 5 7 0 41.27 45.24 0.81 o 6 7 0 2.46 3.39 0.32 o 7 7 0 19.31 21.31 0.57 o 8 7 0 0.04 -0.32 0.32 o 9 7 0 51.59 51.77 0.93 o 10 7 0 2.13 1.34 0.36 o 0 8 0 294.13 290.53 3.30 o 1 8 0 49.41 50.70 1.09 o 2 8 0 28.33 28.94 1.09 o 3 8 0 124.53 117.50 8.11 o 4 8 0 32.41 32.12 0.96 o 5 8 0 1.39 1.58 0.39 o 6 8 0 26.03 28.49 1.17 o 7 8 0 0.44 0.00 0.38 o 8 8 0 25.24 29.69 0.79 o 1 9 0 44.30 43.32 0.93 o 2 9 0 39.22 37.38 0.87 o 3 9 0 31.96 28.79 0.83 o 4 9 0 15.27 17.09 0.78 o 5 9 0 1.78 1.29 0.50 o 6 9 0 0.23 0.26 0.49 o 0 10 0 2.45 3.13 0.78 o 1 10 0 121.81 125.87 1.63 o 2 0 1 629.45 609.86 3.81 o 4 0 1 3067.79 3029.12 37.34 o 6 0 1 337.85 339.02 1.96 o 8 0 1 31.42 29.86 0.67 o 10 0 1 211.06 198.71 2.45 o 12 0 1 2.77 3.22 0.36 o 14 0 1 2.62 2.84 0.43 o 0 1 1 401.14 299.01 2.81 o 1 1 1 537.30 533.45 9.42 o 2 1 1 247.81 256.72 1.59 o 3 1 1 69.64 66.06 0.71 o 4 1 1 407.51 414.81 12.12 o 5 1 1 180.20 174.65 5.35 o 6 1 1 169.66 174.79 1.58 o 7 1 1 13.87 12.99 0.44 o 8 1 1 72.09 66.75 1.08 o 9 1 1 45.45 45.59 0.58 o 10 1 1 14.37 13.23 0.35 o 11 1 1 7.81 8.39 0.31 o 12 1 1 32.57 29.10 0.50 o 13 1 1 4.11 5.43 0.31 o 14 1 1 4.79 5.78 0.35 o 1 2 1 834.55 827.47 7.99 o 2 2 1 351.16 331.40 3.10 o 3 2 1 1303.65 1292.32 6.82 o 4 2 1 675.12 697.69 4.49 o 5 2 1 104.74 105.34 1.34 o 6 2 1 244.18 229.56 2.17 o 7 2 1 66.74 65.70 0.80 o 8 2 1 132.71 125.39 1.50 o 9 2 1 206.10 185.04 2.20 o 10 2 1 72.95 77.66 1.72 o 11 2 1 23.61 24.33 0.51 o 12 2 1 8.14 8.20 0.28 o 13 2 1 2.93 2.38 0.28 o 14 2 1 0.05 0.20 0.28 o 0 3 1 400.73 488.55 18.82 o 1 3 1 501.06 513.65 9.13 o 2 3 1 736.50 796.78 8.38 o 3 3 1 317.43 343.03 2.68 o 4 3 1 164.31 171.89 2.61 o 5 3 1 403.07 414.59 4.24 o 6 3 1 353.71 393.69 2.89 o 7 3 1 112.40 115.66 1.10 o 8 3 1 159.90 159.57 1.45 o 9 3 1 50.42 44.77 0.68 o 10 3 1 39.38 36.10 0.60 o 11 3 1 35.91 35.87 0.62 o 12 3 1 5.09 5.83 0.27 o 13 3 1 8.47 7.94 0.32 o 1 4 1 156.48 153.39 3.11 o 2 4 1 14.89 17.64 0.26 o 3 4 1 473.78 477.41 10.75 o 4 4 1 185.57 176.32 2.09 o 5 4 1 278.36 289.35 3.91 o 6 4 1 8.17 6.38 0.20 o 7 4 1 409.97 401.65 2.51 o 8 4 1 45.12 46.40 1.21 o 9 4 1 68.72 68.65 0.72 o 10 4 1 21.97 20.62 0.35 o 11 4 1 28.24 29.07 0.48 o 12 4 1 0.64 0.42 0.23 o 13 4 1 9.27 9.92 0.35 o 0 5 1 197.50 201.42 2.21 o 1 5 1 246.26 277.08 2.12 o 2 5 1 108.60 120.60 1.31 o 3 5 1 195.71 206.75 3.33 o 4 5 1 59.34 56.22 0.96 o 5 5 1 92.50 94.98 1.60 o 6 5 1 86.11 91.84 1.26 o 7 5 1 204.23 206.43 2.75 o 8 5 1 174.32 175.38 1.90 o 9 5 1 92.34 87.61 1.27 o 10 5 1 22.18 18.72 0.52 o 11 5 1 1.73 2.37 0.23 o 12 5 1 2.68 2.83 0.26 o 1 6 1 0.19 0.34 0.17 o 2 6 1 94.26 96.23 1.18 o 3 6 1 2.79 3.70 0.22 o 4 6 1 129.33 135.14 1.67 o 5 6 1 0.72 1.02 0.21 o 6 6 1 195.25 186.71 2.65 o 7 6 1 6.02 8.05 0.29 o 8 6 1 68.42 71.82 1.24 o 9 6 1 0.03 0.14 0.20 o 10 6 1 24.64 22.99 0.73 o 11 6 1 5.76 6.12 0.32 o 0 7 1 44.72 49.81 1.62 o 1 7 1 64.58 57.61 0.66 o 2 7 1 24.00 23.22 0.42 o 3 7 1 51.80 62.19 1.91 o 4 7 1 19.13 19.02 0.44 o 5 7 1 42.44 39.69 0.86 o 6 7 1 10.87 9.79 0.31 o 7 7 1 52.41 54.10 0.81 o 8 7 1 16.17 15.50 0.39 o 9 7 1 27.78 25.42 0.47 o 10 7 1 0.55 0.57 0.25 o 1 8 1 8.21 6.06 0.31 o 2 8 1 12.66 12.29 0.31 o 3 8 1 3.34 4.36 0.29 o 4 8 1 13.62 17.06 0.46 o 5 8 1 9.50 9.10 0.35 o 6 8 1 0.20 0.18 0.23 o 7 8 1 25.28 22.26 0.47 o 8 8 1 0.74 0.96 0.27 o 0 9 1 6.79 8.14 0.54 o 1 9 1 8.29 8.63 0.38 o 2 9 1 0.63 1.25 0.32 o 3 9 1 3.48 3.17 0.31 o 4 9 1 0.04 -0.05 0.28 o 5 9 1 19.90 19.49 0.52 o 6 9 1 1.23 1.18 0.29 o 0 0 2 3954.64 3953.78 61.65 o 2 0 2 2081.22 1941.54 12.95 o 4 0 2 348.26 363.21 2.04 o 6 0 2 801.79 906.41 6.56 o 8 0 2 147.31 156.16 1.15 o 10 0 2 40.46 35.70 0.70 o 12 0 2 12.93 13.16 0.56 o 14 0 2 26.00 27.02 0.79 o 1 1 2 378.32 332.28 8.96 o 2 1 2 761.28 731.48 7.02 o 3 1 2 44.87 42.30 0.50 o 4 1 2 161.55 165.72 0.76 o 5 1 2 305.49 320.77 2.47 o 6 1 2 375.65 407.27 4.70 o 7 1 2 48.67 49.70 0.35 o 8 1 2 30.58 34.38 0.49 o 9 1 2 5.09 6.31 0.21 o 10 1 2 9.89 7.89 0.24 o 11 1 2 0.43 0.52 0.19 o 12 1 2 2.50 2.64 0.25 o 13 1 2 21.30 24.15 0.52 o 14 1 2 13.16 15.09 0.64 o 0 2 2 74.76 76.23 0.51 o 1 2 2 168.84 169.46 1.49 o 2 2 2 623.52 625.89 4.65 o 3 2 2 425.29 473.73 1.69 o 4 2 2 891.84 1003.92 7.28 o 5 2 2 283.39 300.44 2.92 o 6 2 2 559.65 532.92 3.32 o 7 2 2 36.85 43.49 1.03 o 8 2 2 28.91 32.00 0.40 o 9 2 2 7.16 7.92 0.28 o 10 2 2 0.48 0.55 0.18 o 11 2 2 3.92 4.17 0.24 o 12 2 2 5.06 4.93 0.27 o 13 2 2 22.28 21.76 1.08 o 1 3 2 303.61 326.56 3.17 o 2 3 2 46.71 47.94 0.53 o 3 3 2 230.49 226.70 2.66 o 4 3 2 56.12 62.07 0.67 o 5 3 2 108.28 112.99 0.84 o 6 3 2 69.10 66.86 0.66 o 7 3 2 13.07 10.34 0.35 o 8 3 2 26.94 25.66 0.39 o 9 3 2 30.42 24.89 0.35 o 10 3 2 8.75 8.98 0.28 o 11 3 2 22.32 23.96 0.44 o 12 3 2 10.39 9.36 0.35 o 13 3 2 2.20 2.27 0.26 o 0 4 2 93.38 103.78 1.77 o 1 4 2 132.41 165.89 2.37 o 2 4 2 147.46 148.32 2.09 o 3 4 2 147.32 161.35 1.93 o 4 4 2 204.65 193.83 2.04 o 5 4 2 89.91 95.71 1.18 o 6 4 2 16.60 18.92 0.30 o 7 4 2 17.35 16.47 0.40 o 8 4 2 25.66 23.74 0.40 o 9 4 2 38.37 33.00 0.87 o 10 4 2 9.03 8.77 0.28 o 11 4 2 15.84 17.19 0.39 o 12 4 2 7.67 7.34 0.34 o 1 5 2 16.71 18.72 0.34 o 2 5 2 92.63 101.47 2.68 o 3 5 2 31.92 30.47 0.62 o 4 5 2 4.16 3.64 0.19 o 5 5 2 10.93 9.81 0.25 o 6 5 2 9.71 5.77 0.25 o 7 5 2 55.53 52.15 0.84 o 8 5 2 9.56 8.44 0.29 o 9 5 2 22.73 21.16 0.58 o 10 5 2 0.67 0.49 0.22 o 11 5 2 9.14 9.78 0.36 o 12 5 2 7.08 6.05 0.33 o 0 6 2 111.00 107.29 1.91 o 1 6 2 35.49 34.55 0.53 o 2 6 2 14.80 15.87 0.35 o 3 6 2 16.98 19.64 0.41 o 4 6 2 12.90 14.08 0.31 o 5 6 2 9.25 7.67 0.25 o 6 6 2 11.67 11.20 0.33 o 7 6 2 12.74 13.59 0.36 o 8 6 2 11.16 10.52 0.44 o 9 6 2 2.00 2.78 0.29 o 10 6 2 18.03 16.82 0.69 o 11 6 2 4.64 4.70 0.33 o 1 7 2 6.67 10.55 0.27 o 2 7 2 5.16 6.30 0.27 o 3 7 2 21.64 21.98 0.45 o 4 7 2 13.12 12.74 0.37 o 5 7 2 21.38 19.40 0.47 o 6 7 2 6.49 5.24 0.30 o 7 7 2 0.84 0.55 0.27 o 8 7 2 7.40 6.09 0.38 o 9 7 2 3.20 3.11 0.33 o 0 8 2 13.54 11.42 0.63 o 1 8 2 13.39 15.29 0.50 o 2 8 2 22.93 22.52 0.43 o 3 8 2 39.05 33.27 0.71 o 4 8 2 2.75 2.38 0.29 o 5 8 2 4.96 4.93 0.35 o 6 8 2 13.53 16.10 0.73 o 7 8 2 1.16 0.94 0.34 o 8 8 2 2.69 2.40 0.32 o 1 9 2 0.55 0.71 0.27 o 2 9 2 4.98 6.03 0.38 o 3 9 2 2.08 1.72 0.31 o 4 9 2 29.85 28.13 0.60 o 5 9 2 3.91 4.27 0.34 o 2 0 3 1692.47 1663.75 32.85 o 4 0 3 144.64 187.32 2.43 o 6 0 3 125.18 129.04 2.01 o 8 0 3 77.70 81.24 0.70 o 10 0 3 30.26 29.90 0.87 o 12 0 3 18.01 22.85 1.05 o 0 1 3 2643.70 2932.43 38.11 o 1 1 3 2053.05 2100.11 25.72 o 2 1 3 334.84 337.70 4.21 o 3 1 3 485.44 497.92 4.58 o 4 1 3 383.95 402.95 1.71 o 5 1 3 17.36 15.10 0.21 o 6 1 3 83.54 84.88 0.76 o 7 1 3 60.04 60.96 1.58 o 8 1 3 12.19 11.57 0.35 o 9 1 3 43.03 47.10 0.67 o 10 1 3 30.31 35.18 0.54 o 11 1 3 42.28 36.02 0.50 o 12 1 3 9.05 9.85 0.36 o 13 1 3 7.51 8.41 0.42 o 1 2 3 411.30 371.23 4.30 o 2 2 3 397.80 366.12 9.53 o 3 2 3 170.59 179.30 1.96 o 4 2 3 44.52 47.90 0.49 o 5 2 3 18.67 20.93 0.22 o 6 2 3 6.20 6.49 0.30 o 7 2 3 50.91 52.18 0.38 o 8 2 3 6.92 4.74 0.19 o 9 2 3 16.47 16.12 0.31 o 10 2 3 1.21 0.87 0.19 o 11 2 3 8.47 6.71 0.28 o 12 2 3 8.81 9.71 0.36 o 13 2 3 8.29 9.39 0.43 o 0 3 3 74.61 82.16 1.71 o 1 3 3 67.65 69.72 0.69 o 2 3 3 22.62 18.84 0.32 o 3 3 3 310.97 311.26 2.74 o 4 3 3 6.06 4.55 0.19 o 5 3 3 432.08 451.29 5.30 o 6 3 3 12.56 13.42 0.26 o 7 3 3 23.29 20.14 0.40 o 8 3 3 33.87 33.30 0.41 o 9 3 3 20.40 19.98 0.35 o 10 3 3 44.52 41.92 0.58 o 11 3 3 9.64 8.65 0.37 o 12 3 3 8.22 8.00 0.37 o 1 4 3 147.17 165.72 2.69 o 2 4 3 11.26 12.83 0.27 o 3 4 3 177.05 176.34 2.96 o 4 4 3 7.86 7.41 0.32 o 5 4 3 36.33 35.09 0.54 o 6 4 3 11.29 9.93 0.27 o 7 4 3 1.24 0.95 0.20 o 8 4 3 6.59 7.57 0.29 o 9 4 3 2.69 2.20 0.24 o 10 4 3 1.68 2.64 0.28 o 11 4 3 3.32 2.18 0.29 o 12 4 3 2.15 2.42 0.30 o 0 5 3 63.99 56.24 1.50 o 1 5 3 218.90 232.02 3.01 o 2 5 3 50.53 55.89 1.10 o 3 5 3 0.68 0.58 0.17 o 4 5 3 2.51 3.29 0.23 o 5 5 3 9.14 8.49 0.28 o 6 5 3 15.10 11.32 0.39 o 7 5 3 20.52 18.75 0.40 o 8 5 3 59.28 52.60 1.11 o 9 5 3 28.15 27.99 0.53 o 10 5 3 5.34 6.23 0.32 o 11 5 3 7.56 7.72 0.37 o 1 6 3 18.67 13.13 0.41 o 2 6 3 53.22 61.71 1.98 o 3 6 3 55.62 57.60 1.07 o 4 6 3 8.32 7.55 0.33 o 5 6 3 5.88 5.75 0.31 o 6 6 3 13.04 12.01 0.46 o 7 6 3 11.78 13.17 0.48 o 8 6 3 4.50 2.96 0.30 o 9 6 3 18.28 17.76 0.48 o 10 6 3 1.18 0.50 0.28 o 0 7 3 70.82 62.39 1.92 o 1 7 3 4.93 4.63 0.28 o 2 7 3 19.99 20.86 0.53 o 3 7 3 11.90 11.90 0.39 o 4 7 3 69.40 65.29 1.05 o 5 7 3 17.90 14.37 0.61 o 6 7 3 24.70 28.69 0.77 o 7 7 3 29.10 30.20 0.75 o 8 7 3 9.46 9.80 0.43 o 9 7 3 12.65 11.69 0.47 o 1 8 3 2.95 4.19 0.32 o 2 8 3 62.53 60.67 1.54 o 3 8 3 1.46 1.15 0.26 o 4 8 3 18.67 18.02 0.51 o 5 8 3 0.34 0.34 0.30 o 6 8 3 1.23 1.03 0.33 o 7 8 3 1.05 1.87 0.35 o 0 9 3 66.15 70.33 2.91 o 1 9 3 13.18 10.04 0.50 o 2 9 3 17.01 16.08 0.54 o 3 9 3 7.54 5.68 0.38 o 4 9 3 0.96 0.81 0.32 o 0 0 4 1905.42 1766.39 6.12 o 2 0 4 247.24 270.88 18.82 o 4 0 4 143.35 143.29 3.81 o 6 0 4 36.23 41.71 0.51 o 8 0 4 269.18 296.07 2.17 o 10 0 4 50.51 53.24 0.89 o 12 0 4 33.96 30.58 1.18 o 1 1 4 323.42 344.32 5.39 o 2 1 4 269.48 271.54 1.95 o 3 1 4 28.17 31.19 0.51 o 4 1 4 166.22 187.16 1.96 o 5 1 4 2.66 4.37 0.65 o 6 1 4 37.54 36.12 0.33 o 7 1 4 5.49 4.50 0.18 o 8 1 4 8.50 10.39 0.24 o 9 1 4 75.35 64.86 0.99 o 10 1 4 102.68 100.42 1.57 o 11 1 4 53.82 56.15 0.87 o 12 1 4 20.29 23.85 0.59 o 0 2 4 442.50 418.36 6.53 o 1 2 4 389.79 376.22 5.21 o 2 2 4 398.93 384.95 8.06 o 3 2 4 83.59 88.59 1.22 o 4 2 4 55.57 60.60 0.63 o 5 2 4 294.75 297.49 2.53 o 6 2 4 41.02 34.86 0.41 o 7 2 4 17.38 18.36 0.31 o 8 2 4 16.61 12.97 0.30 o 9 2 4 43.54 44.08 1.04 o 10 2 4 6.12 5.97 0.29 o 11 2 4 17.04 18.91 0.44 o 12 2 4 33.91 39.44 0.74 o 1 3 4 125.31 127.41 1.60 o 2 3 4 94.10 94.25 1.09 o 3 3 4 80.28 73.38 2.82 o 4 3 4 99.06 86.83 2.28 o 5 3 4 46.83 50.16 0.43 o 6 3 4 41.63 39.46 0.51 o 7 3 4 80.77 76.05 0.86 o 8 3 4 30.12 30.03 0.58 o 9 3 4 13.25 12.62 0.43 o 10 3 4 26.67 23.73 1.04 o 11 3 4 55.22 62.84 1.50 o 12 3 4 11.93 13.45 0.45 o 0 4 4 158.70 184.73 2.31 o 1 4 4 169.98 178.91 1.75 o 2 4 4 83.34 76.87 1.09 o 3 4 4 158.91 166.09 2.65 o 4 4 4 132.04 134.47 3.07 o 5 4 4 69.35 69.68 1.52 o 6 4 4 31.01 28.98 0.46 o 7 4 4 106.57 101.16 2.01 o 8 4 4 12.38 13.64 0.45 o 9 4 4 66.97 63.56 1.60 o 10 4 4 6.77 7.17 0.35 o 11 4 4 11.73 13.01 0.43 o 1 5 4 6.49 6.11 0.25 o 2 5 4 3.32 5.30 0.24 o 3 5 4 65.53 59.49 1.14 o 4 5 4 129.97 116.93 3.08 o 5 5 4 83.19 81.37 2.00 o 6 5 4 3.52 1.96 0.26 o 7 5 4 37.13 40.42 0.66 o 8 5 4 12.02 12.78 0.44 o 9 5 4 2.93 3.43 0.30 o 10 5 4 10.59 10.22 0.42 o 0 6 4 70.46 60.26 2.27 o 1 6 4 14.92 13.38 0.34 o 2 6 4 113.83 134.78 2.71 o 3 6 4 9.97 9.65 0.54 o 4 6 4 38.52 37.50 0.99 o 5 6 4 11.68 11.49 0.40 o 6 6 4 65.95 64.68 2.40 o 7 6 4 9.94 10.58 0.44 o 8 6 4 53.44 53.34 1.55 o 9 6 4 2.34 3.21 0.35 o 1 7 4 1.56 3.65 0.29 o 2 7 4 3.87 3.37 0.28 o 3 7 4 34.27 29.20 0.79 o 4 7 4 18.46 16.72 0.48 o 5 7 4 14.33 13.54 0.45 o 6 7 4 18.80 19.77 0.65 o 7 7 4 2.33 1.46 0.33 o 8 7 4 8.61 7.27 0.45 o 0 8 4 50.46 48.30 3.88 o 1 8 4 9.09 6.61 0.40 o 2 8 4 15.28 15.72 0.49 o 3 8 4 14.76 15.97 0.70 o 4 8 4 13.09 10.93 0.45 o 5 8 4 2.99 4.01 0.38 o 6 8 4 10.35 11.10 0.68 o 1 9 4 8.26 6.01 0.47 o 2 0 5 39.82 41.14 0.68 o 4 0 5 1113.69 1169.92 83.67 o 6 0 5 94.09 87.27 1.11 o 8 0 5 36.49 40.74 0.87 o 10 0 5 4.56 4.50 0.41 o 12 0 5 11.46 14.65 0.89 o 0 1 5 100.30 116.74 2.79 o 1 1 5 169.13 157.35 2.23 o 2 1 5 141.29 148.00 2.38 o 3 1 5 245.45 248.08 2.31 o 4 1 5 36.30 35.40 0.60 o 5 1 5 240.72 242.42 1.65 o 6 1 5 280.74 288.72 4.06 o 7 1 5 350.47 379.45 5.30 o 8 1 5 50.47 56.94 0.75 o 9 1 5 54.76 54.85 0.91 o 10 1 5 0.45 0.24 0.25 o 11 1 5 1.27 0.89 0.28 o 12 1 5 1.58 1.20 0.56 o 1 2 5 88.04 86.11 2.08 o 2 2 5 312.79 271.99 9.62 o 3 2 5 262.45 246.72 2.33 o 4 2 5 147.85 149.52 1.38 o 5 2 5 370.22 366.91 2.95 o 6 2 5 4.24 3.89 0.23 o 7 2 5 32.71 36.64 0.57 o 8 2 5 9.64 6.85 0.30 o 9 2 5 5.91 7.58 0.32 o 10 2 5 6.41 5.18 0.34 o 11 2 5 2.16 2.27 0.32 o 0 3 5 72.41 87.68 2.10 o 1 3 5 24.18 25.10 0.44 o 2 3 5 53.06 47.71 0.76 o 3 3 5 123.96 120.87 1.99 o 4 3 5 78.79 85.03 0.97 o 5 3 5 399.55 389.47 3.56 o 6 3 5 200.23 192.17 2.99 o 7 3 5 37.28 40.29 0.59 o 8 3 5 52.68 55.61 0.66 o 9 3 5 9.78 10.33 0.40 o 10 3 5 2.14 1.34 0.29 o 11 3 5 16.46 17.42 0.51 o 1 4 5 186.41 193.83 3.52 o 2 4 5 5.77 8.43 0.29 o 3 4 5 303.91 308.77 5.56 o 4 4 5 74.50 80.65 1.45 o 5 4 5 34.68 33.36 0.61 o 6 4 5 6.23 3.88 0.28 o 7 4 5 64.68 60.74 0.96 o 8 4 5 5.53 6.26 0.36 o 9 4 5 3.21 3.32 0.35 o 10 4 5 9.24 9.71 0.42 o 0 5 5 75.85 75.76 2.29 o 1 5 5 90.51 96.77 2.46 o 2 5 5 59.39 59.07 1.04 o 3 5 5 99.29 98.65 1.69 o 4 5 5 75.65 72.20 1.12 o 5 5 5 37.82 34.18 0.83 o 6 5 5 19.14 20.14 0.60 o 7 5 5 13.47 12.41 0.43 o 8 5 5 27.53 25.88 0.63 o 9 5 5 12.10 12.86 0.50 o 1 6 5 4.61 7.89 0.32 o 2 6 5 152.62 158.76 3.61 o 3 6 5 22.45 18.88 0.47 o 4 6 5 45.58 44.95 1.23 o 5 6 5 12.90 14.64 0.52 o 6 6 5 18.36 22.39 0.58 o 7 6 5 4.09 3.25 0.36 o 8 6 5 16.82 15.36 0.57 o 0 7 5 3.54 3.11 0.40 o 1 7 5 12.93 12.36 0.64 o 2 7 5 22.98 24.45 1.00 o 3 7 5 16.84 13.23 0.47 o 4 7 5 25.17 23.96 1.02 o 5 7 5 33.98 37.03 1.27 o 6 7 5 38.24 42.89 1.33 o 1 8 5 13.74 15.64 1.00 o 2 8 5 8.78 8.74 0.54 o 3 8 5 8.39 6.83 0.43 o 0 0 6 113.64 82.88 1.07 o 2 0 6 16.26 11.83 0.37 o 4 0 6 234.52 225.40 2.12 o 6 0 6 400.51 434.48 14.62 o 8 0 6 42.97 39.65 0.98 o 10 0 6 3.92 5.16 0.53 o 1 1 6 23.87 21.10 0.38 o 2 1 6 140.41 126.86 1.75 o 3 1 6 111.44 105.86 1.91 o 4 1 6 161.41 159.68 2.98 o 5 1 6 135.82 134.06 2.04 o 6 1 6 16.25 19.55 0.57 o 7 1 6 0.35 0.33 0.22 o 8 1 6 8.49 10.83 0.34 o 9 1 6 17.31 17.90 0.47 o 10 1 6 6.49 8.22 0.39 o 0 2 6 115.74 106.02 1.29 o 1 2 6 25.03 20.71 0.71 o 2 2 6 98.45 93.33 1.38 o 3 2 6 99.63 92.67 1.41 o 4 2 6 103.38 101.20 0.89 o 5 2 6 243.23 253.78 2.76 o 6 2 6 34.22 34.70 0.46 o 7 2 6 17.67 15.61 0.39 o 8 2 6 27.90 27.16 0.52 o 9 2 6 3.43 3.83 0.44 o 10 2 6 1.29 1.72 0.34 o 1 3 6 103.55 102.01 2.13 o 2 3 6 88.10 84.89 1.08 o 3 3 6 57.58 58.46 0.98 o 4 3 6 38.12 38.71 0.66 o 5 3 6 19.04 22.14 0.41 o 6 3 6 15.16 14.62 0.39 o 7 3 6 23.68 22.80 0.51 o 8 3 6 10.74 10.35 0.63 o 9 3 6 2.31 2.21 0.35 o 10 3 6 32.93 38.76 0.84 o 0 4 6 63.17 70.62 1.93 o 1 4 6 357.41 355.52 6.33 o 2 4 6 40.75 43.66 0.82 o 3 4 6 80.36 82.81 1.50 o 4 4 6 25.37 25.85 0.57 o 5 4 6 11.69 10.38 0.37 o 6 4 6 4.73 5.02 0.31 o 7 4 6 0.42 0.85 0.27 o 8 4 6 10.36 12.86 0.45 o 9 4 6 2.72 3.34 0.40 o 1 5 6 44.91 46.74 1.18 o 2 5 6 63.85 65.02 1.71 o 3 5 6 49.85 52.62 1.58 o 4 5 6 7.16 8.41 0.38 o 5 5 6 1.32 1.04 0.26 o 6 5 6 3.08 2.56 0.30 o 7 5 6 11.02 11.83 0.44 o 8 5 6 3.90 3.19 0.39 o 0 6 6 227.39 249.43 11.48 o 1 6 6 32.59 33.64 1.04 o 2 6 6 89.54 90.99 2.08 o 3 6 6 25.58 24.44 0.60 o 4 6 6 6.17 5.67 0.36 o 5 6 6 9.20 10.12 0.47 o 6 6 6 5.62 6.19 0.39 o 1 7 6 7.55 5.38 0.37 o 2 7 6 21.12 22.07 0.62 o 3 7 6 17.78 20.18 0.63 o 4 7 6 21.19 20.07 0.66 o 2 0 7 23.41 17.67 0.47 o 4 0 7 21.80 22.82 0.55 o 6 0 7 58.38 56.75 0.99 o 8 0 7 16.81 19.80 0.71 o 0 1 7 5.43 3.45 0.28 o 1 1 7 38.23 35.54 0.47 o 2 1 7 13.62 12.61 0.32 o 3 1 7 9.68 8.15 0.28 o 4 1 7 5.92 6.48 0.27 o 5 1 7 20.76 20.30 0.41 o 6 1 7 1.08 1.36 0.30 o 7 1 7 41.48 45.55 1.68 o 8 1 7 43.95 49.24 1.76 o 9 1 7 65.00 76.79 6.27 o 1 2 7 26.83 24.33 0.48 o 2 2 7 4.22 5.12 0.24 o 3 2 7 2.47 3.20 0.23 o 4 2 7 17.35 15.53 0.41 o 5 2 7 22.32 19.72 0.44 o 6 2 7 1.62 2.42 0.28 o 7 2 7 19.00 21.52 0.78 o 8 2 7 2.31 2.18 0.38 o 0 3 7 64.64 53.87 1.26 o 1 3 7 62.26 58.44 1.92 o 2 3 7 34.85 31.90 0.75 o 3 3 7 42.86 46.64 0.80 o 4 3 7 1.48 2.28 0.26 o 5 3 7 24.92 22.14 0.48 o 6 3 7 0.14 0.39 0.27 o 7 3 7 10.50 9.92 0.46 o 8 3 7 2.15 2.49 0.38 o 1 4 7 2.24 3.23 0.28 o 2 4 7 3.59 5.01 0.27 o 3 4 7 9.00 8.00 0.32 o 4 4 7 10.96 12.86 0.38 o 5 4 7 3.75 4.82 0.33 o 6 4 7 1.15 1.64 0.30 o 7 4 7 10.66 11.52 0.45 o 0 5 7 7.02 8.01 0.48 o 1 5 7 34.86 34.80 0.90 o 2 5 7 13.92 13.34 0.39 o 3 5 7 22.62 22.99 0.51 o 4 5 7 3.34 3.45 0.33 o 5 5 7 0.69 0.65 0.30 o 1 6 7 1.38 1.29 0.30 o 2 6 7 1.17 2.01 0.34 o 3 6 7 0.38 0.35 0.30 o 0 0 8 127.86 110.42 2.56 o 2 0 8 29.03 29.31 0.73 o 4 0 8 2.77 1.74 0.35 o 6 0 8 15.09 17.32 0.66 o 1 1 8 0.86 1.31 0.20 o 2 1 8 20.42 17.06 0.42 o 3 1 8 2.88 2.91 0.24 o 4 1 8 34.55 35.08 0.58 o 5 1 8 5.29 6.38 0.33 o 6 1 8 20.38 24.12 0.55 o 0 2 8 17.04 18.36 0.55 o 1 2 8 11.80 11.60 0.33 o 2 2 8 1.08 0.65 0.20 o 3 2 8 6.31 6.56 0.30 o 4 2 8 29.45 27.15 0.52 o 5 2 8 18.73 17.63 0.47 o 6 2 8 31.29 38.85 2.73 o 1 3 8 7.36 5.91 0.29 o 2 3 8 20.19 23.52 0.79 o 3 3 8 42.73 47.29 0.97 o 4 3 8 17.13 17.57 0.47 o 5 3 8 18.18 18.62 0.69 o 0 4 8 9.56 9.85 0.53 o 1 4 8 68.58 74.95 2.17 o 2 4 8 14.62 16.92 0.47 o 3 4 8 18.89 20.89 0.61 o 4 4 8 3.06 2.98 0.35 o 2 0 9 60.80 56.85 1.40 o 0 1 9 38.24 39.23 0.89 o 1 1 9 2.64 3.22 0.29 o 2 1 9 23.09 24.47 0.53 o