Crystal Structure Communications

 

Acta Cryst. (2002). C58, e1  [ doi:10.1107/S0108270101021400 ]

Further developments for Acta Crystallographica Section C

G. Ferguson

Synopsis: Editorial for 2002.

Online 22 December 2001

 

Acta Cryst. (2002). C58, e2-e8  [ doi:10.1107/S0108270101019461 ]

Notes for authors

Online 22 December 2001

 

Acta Cryst. (2002). C58, i1-i2  [ doi:10.1107/S0108270101015463 ]

Dicaesium silver zinc thiocyanate, Cs₂[AgZn(SCN)₅]

M. Günes and J. Valkonen

Synopsis: The structure of Cs₂[AgZn(SCN)₅] contains units of composition AgZn(SCN)₃ lying on a mirror plane and bonded together through Cs⁺ ions and thiocyanate groups. The crystal studied contained equal numbers of inversion twins.

Formula: Cs₂[AgZn(SCN)₅]

Online 14 December 2001

 

Acta Cryst. (2002). C58, i3-i5  [ doi:10.1107/S0108270101018492 ]

Ca₃Mn₂O₇

N. Guiblin, D. Grebille, H. Leligny and C. Martin

Synopsis: Single crystals of Ca₃Mn₂O₇ were prepared in an optical floating-zone furnace. The symmetry, which was previously reported as tetragonal according to powder X-ray diffraction studies, is shown to be orthorhombic, A2₁am.

Formula: Ca₃Mn₂O₇

Online 14 December 2001

 

Acta Cryst. (2002). C58, i6-i8  [ doi:10.1107/S010827010101767X ]

The mixed oxide MoVAlO₇

J. Galy, R. Enjalbert, P. Rozier and P. Millet

Synopsis: The complex oxide MoVAlO₇, vanadium aluminium molybdate, crystallizes in the orthorhombic system (space group Pnma). All the metal atoms and three O atoms lie on the mirror plane. Infinite strings of VO₅ square pyramids associated by opposite basal edges develop along [010] and are surrounded by a sequence of eight corner-sharing alternating AlO₆ octahedra and MoO₄ tetrahedra.

Formula: MoVAlO₇

Online 14 December 2001

    

Acta Cryst. (2002). C58, i9-i13  [ doi:10.1107/S0108270101017553 ]

Synchrotron-radiation study of the two-leg spin-ladder (VO)₂P₂O₇ at 120  K

S. Geupel, K. Pilz, S. van Smaalen, F. Büllesfeld, A. Prokofiev and W. Assmus

Synopsis: The crystal structure of the ambient-pressure phase of vanadyl pyrophosphate, (VO)₂P₂O₇, determined from single-crystal synchrotron data, consists of infinite two-leg ladders of vanadyl cations, (VO)²⁺, which are separated by pyrophosphate anions, (P₂O₇)^4-.

Formula: (VO)₂P₂O₇

Online 14 December 2001

 

Acta Cryst. (2002). C58, i14-i15  [ doi:10.1107/S0108270101016882 ]

-Sm(OH)₂Cl: a new lamellar variety

C. Jouve, J. Marrot and D. Riou

Synopsis: A new variety of dihydroxysamarium chloride is presented. The orthorhombic structure is built up from the stacking of neutral layers stabilized via strong hydrogen bonds between the hydroxyl H atoms and the chlorides.

Formula: Sm(OH)₂Cl

Online 14 December 2001

 

Acta Cryst. (2002). C58, i16-i17  [ doi:10.1107/S0108270101017759 ]

AgCo₃PO₄(HPO₄)₂

A. Guesmi and A. Driss

Synopsis: AgCo₃PO₄(HPO₄)₂ consists of edge-sharing CoO₆ chains linked together by the phosphate groups and hydrogen bonds. The three-dimensional framework delimits two types of tunnels which accommodate Ag⁺ cations and OH groups.

Formula: AgCo₃PO₄(HPO₄)₂

Online 22 December 2001

 

Acta Cryst. (2002). C58, i18-i20  [ doi:10.1107/S0108270101015773 ]

Monoclinic AlPO₄ tridymite at 473 and 463  K from X-ray powder data

H. A. Graetsch

Synopsis: AlPO₄ tridymite forms an intermediate phase between 373 and 573  K with space-group symmetry P112₁. The crystal structure is dynamically disordered and develops an incommensurate displacive modulation below 473  K.

Formula: AlPO₄

Online 22 December 2001

 

Acta Cryst. (2002). C58, i21-i22  [ doi:10.1107/S0108270101017413 ]

Calcium dicaesium silver thiocyanate dihydrate

M. Günes, K. Nättinen and J. Valkonen

Synopsis: CaCs₂[Ag₂(SCN)₆]·2H₂O forms a continuous structure where the Ag atoms form chains with S atoms in the c-axis direction. The chains are bonded together through Cs and Ca atoms. The crystal water of the structure is bonded to the Ca atoms, which lie on centers of symmetry.

Formula: CaCs₂[Ag₂(SCN)₆]·2H₂O

Online 22 December 2001

 

Acta Cryst. (2002). C58, m1-m4  [ doi:10.1107/S0108270101017152 ]

Hydrogen-bonded adducts of ferrocene-1,1'-diylbis(diphenylmethanol): monomeric and polymeric adducts with 1,2-bis(4-pyridyl)ethene and 1,6-diaminohexane

C. M. Zakaria, G. Ferguson, A. J. Lough and C. Glidewell

Formula: [Fe(C₁₈H₁₅O)₂]·C₁₂H₁₀N₂ and 2[Fe(C₁₈H₁₅O)₂]·C₆H₁₆N₂

Online 14 December 2001

 

Acta Cryst. (2002). C58, m5-m7  [ doi:10.1107/S0108270101018844 ]

Hydrogen-bonded adducts of ferrocene-1,1'-diylbis(diphenylmethanol): a finite cyclic 1:1  adduct with 2,2'-dipyridylamine

C. M. Zakaria, G. Ferguson, A. J. Lough and C. Glidewell

Formula: [Fe(C₁₈H₁₅O)₂]·C₁₀H₉N₃

Online 14 December 2001

 

Acta Cryst. (2002). C58, m8-m9  [ doi:10.1107/S0108270101016961 ]

A dinuclear uranium(IV) complex of the chelating ligand 1,2,3,4-tetramethyl-5-(2-pyridyl)cyclopentadiene

T. Le Borgne, P. Thuéry and M. Ephritikhine

Formula: [U₂Cl₂O₂(C₄H₁₀O)₂(C₁₄H₁₆N)₂]

Online 14 December 2001

 

Acta Cryst. (2002). C58, m10-m11  [ doi:10.1107/S0108270101017656 ]

Bis[2-(pyrazol-3-yl)phenolato-²N²,O]copper(II) dimethanol solvate

X.-M. Liu, C. A. Kilner, M. Thornton-Pett and M. A. Halcrow

Formula: [Cu(C₉H₇N₂O)₂]·2CH₄O

Online 14 December 2001

    

Acta Cryst. (2002). C58, m12-m13  [ doi:10.1107/S0108270101016948 ]

_1,3-Azido-diazidotetrakis(1,10-phenanthroline)dicopper(II) azide tetrahydrate

Y.-Q. Cheng, M.-L. Hu, S. Wang and M.-D. Ye

Formula: [Cu₂(N₃)₃(C₁₂H₈N₂)₄](N₃)·4H₂O

Online 14 December 2001

 

Acta Cryst. (2002). C58, m14-m16  [ doi:10.1107/S0108270101018546 ]

trans-Bis(diethanolamine-N,O)bis(saccharinato-N)cadmium(II)

O. Andac, Y. Topcu, V. T. Yilmaz and W. T. A. Harrison

Formula: [Cd(C₇H₄NO₃S)₂(C₄H₁₁NO₂)₂]

Online 14 December 2001

 

Acta Cryst. (2002). C58, m17-m20  [ doi:10.1107/S0108270101018807 ]

Bis(pyridine-2,6-dimethanol-N,O,O')cobalt(II) and -copper(II) disaccharinate dihydrate: three-dimensional structures with extensive hydrogen bonds and aromatic --stacking interactions

O. Andac, S. Guney, Y. Topcu, V. T. Yilmaz and W. T. A. Harrison

Formula: [Co(C₇H₉NO₂)₂](C₇H₄NO₃S)₂·2H₂O and [Cu(C₇H₉NO₂)₂](C₇H₄NO₃S)₂·2H₂O

Online 14 December 2001

 

Acta Cryst. (2002). C58, m21-m22  [ doi:10.1107/S0108270101017930 ]

Sodium p-nitrobenzoxasulfamate monohydrate

T. K. Yazicilar, O. Andac, Y. Bekdemir, H. Kutuk, V. T. Yilmaz and W. T. A. Harrison

Formula: Na⁺·C₆H₃N₂O₅S^-·H₂O

Online 14 December 2001

 

Acta Cryst. (2002). C58, m23-m25  [ doi:10.1107/S0108270101017590 ]

Tetrakis[phthalocyaninato(2-)antimony(III)] hexadecaiodotetraantimony(III)

J. Janczak and Y. M. Idemori

Formula: [Sb(C₃₂H₁₆N₈)]₄[Sb₄I₁₆]

Online 14 December 2001

 

Acta Cryst. (2002). C58, m26-m28  [ doi:10.1107/S0108270101014147 ]

Two orthopalladated chromophores

R. Centore, A. Roviello, A. Tuzi and B. Panunzi

Formula: [Pd(C₁₄H₁₁N₂O₄)(C₁₆H₁₇N₂O)] and [Pd(C₁₄H₁₁N₂O₃)(C₁₈H₂₁N₂O₂)]·0.5CH₂Cl₂

Online 14 December 2001

 

Acta Cryst. (2002). C58, m29-m30  [ doi:10.1107/S0108270101016870 ]

Hexa--chloro-₄-oxo-tetrakis[(4,5-dihydro-2-methyl-1,2-thiazole-N)copper(II)]

C. A. Bolos and P. C. Christidis

Formula: [Cu₄Cl₆O(C₄H₇NS)₄]

Online 14 December 2001

 

Acta Cryst. (2002). C58, m31-m33  [ doi:10.1107/S0108270101017577 ]

Diacetatobis(trimethylenethiourea)zinc(II) monohydrate

I. A. Razak, A. Usman, H.-K. Fun, B. M. Yamin and G. W. Keat

Formula: [Zn(C₂H₃O₂)₂(C₄H₈N₂S)₂]·H₂O

Online 14 December 2001

 

Acta Cryst. (2002). C58, m34-m35  [ doi:10.1107/S0108270101017036 ]

Aqua(nitrilotriacetato)(1,10-phenanthroline)iron(III) monohydrate: a seven-coordinate iron(III) complex

Y.-Y. Feng, S.-L. Ong, J.-Y. Hu and W.-J. Ng

Formula: [Fe(C₆H₆NO₆)(C₁₂H₈N₂)(H₂O)]·H₂O

Online 14 December 2001

 

Acta Cryst. (2002). C58, m36-m38  [ doi:10.1107/S010827010101719X ]

Poly[[[tri(urea-O)manganese(II)]--thiocyanato-²N:S-mercury(II)]-tri--tetrathiocyanato]

X. Q. Wang, W. T. Yu, D. Xu, M. K. Lu and D. R. Yuan

Formula: [MnHg(SCN)₄(CH₄N₂O)₃]

Online 14 December 2001

 

Acta Cryst. (2002). C58, m39-m40  [ doi:10.1107/S0108270101018613 ]

Aquabromo(6-carboxypyridine-2-carboxylato-O,N,O')mercury(II)

D. Matkovic-Calogovic, J. Popovic, Z. Popovic, I. Picek and Z. Soldin

Formula: [HgBr(C₇H₄NO₄)(H₂O)]

Online 22 December 2001

 

Acta Cryst. (2002). C58, m41-m42  [ doi:10.1107/S0108270101016754 ]

A dimeric constrained-geometry titanium complex linked by double Ti-CH₂-Al-CH₂ heterocycles

K. A. Abboud, P. N. Nickias and E.Y.-X. Chen

Formula: [Ti₂(C₂₁H₇AlF₁₅)₂(C₂₁H₃₁NSi)₂]·2C₆D₆

Online 22 December 2001

 

Acta Cryst. (2002). C58, m43-m44  [ doi:10.1107/S0108270101018303 ]

N-(Ferrocenecarbonyl)-N'-(quinolin-8-yl)thiourea

J.-X. Yang, Y.-P. Tian, Q.-L. Liu, Y.-S. Xie, H.-K. Fun, S. Chantrapromma and I. A. Razak

Formula: [Fe(C₅H₅)(C₁₆H₁₂N₃OS)]

Online 22 December 2001

 

Acta Cryst. (2002). C58, m45-m47  [ doi:10.1107/S0108270101018339 ]

Barium(II)-2,4-dinitrophenolate-18-crown-6 at 183  K

A. Usman, S. Chantrapromma and H.-K. Fun

Formula: [Ba(C₆H₃N₂O₅)₂(C₁₂H₂₄O₆)]

Online 22 December 2002

 

Acta Cryst. (2002). C58, m48-m49  [ doi:10.1107/S010827010101873X ]

trans-Bis(benzoato-O)tetrakis(methanol-O)iron(II): ligand bulk is not structure-determining

S. E. McMullen and K. S. Hagen

Formula: [Fe(C₇H₅O₂)₂(CH₄O)₄]

Online 22 December 2001

 

Acta Cryst. (2002). C58, m50-m52  [ doi:10.1107/S0108270101016432 ]

A triboluminescent europium(III) complex

Z.-P. Zheng, J.-F. Wang, H. Liu, M. D. Carducci, N. Peyghambarian and G. E. Jabbourb

Formula: [Eu(C₈H₄F₃O₂S)₃(C₁₂H₁₂N₂)]

Online 22 December 2001

 

Acta Cryst. (2002). C58, m53-m55  [ doi:10.1107/S0108270101019746 ]

A second polymorph of 1,1,4,4-tetramethylpiperazinium pentabromothallate(III)

A. Linden, A. Petridis and B. D. James

Formula: (C₈H₂₀N₂)[TlBr₅]

Online 22 December 2001

 

Acta Cryst. (2002). C58, m56-m58  [ doi:10.1107/S0108270101018091 ]

trans-Diacetonitrilebis(di-2-pyridyl sulfide-N,N')ruthenium(II) bis(tetrafluoroborate) monohydrate

G. Bruno, F. Nicoló, G. Tresoldi and S. Lanza

Formula: [Ru(C₂H₃N)₂(C₁₀H₈N₂S)₂](BF₄)₂·H₂O

Online 22 December 2001

 

Acta Cryst. (2002). C58, m59-m60  [ doi:10.1107/S010827010101561X ]

Di--chloro-bis({2-[N,N-bis(2-aminoethyl)amino-³N]ethylaminium}copper(II)) bis(naphthalene-1,5-disulfonate) pentahydrate

C.-H. Chen, J.-W. Cai and X.-M. Chen

Formula: [Cu₂(C₆H₁₉N₄)₂Cl₂](C₁₀H₆O₆S₂)₂·5H₂O

Online 22 December 2001

 

Acta Cryst. (2002). C58, m61-m64  [ doi:10.1107/S0108270101017887 ]

catena-Poly[[[{N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl)glycinato-O}pentaaquastrontium]--N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl)glycinato-O:O'] monohydrate]: coordination polymer chains linked by hydrogen bonds into a three-dimensional framework

C. Glidewell, J. N. Low, P. Arranz Mascarós, R. Cuesta Martos and M. D. Gutiérrez Valero

Formula: [Sr(C₇H₈N₅O₄)₂(H₂O)₅]·H₂O

Online 22 December 2001

 

Acta Cryst. (2002). C58, o1-o5  [ doi:10.1107/S0108270101017139 ]

Adducts of 1,1,1-tris(4-hydroxyphenyl)ethane with 1,2-bis(4-pyridyl)ethane and 1,2-bis(4-pyridyl)ethene: continuously interwoven structures in three dimensions

C. M. Zakaria, G. Ferguson, A. J. Lough and C. Glidewell

Formula: C₁₂H₁₂N₂·2C₂₀H₁₈O₃ and C₁₂H₁₀N₂·C₂₀H₁₈O₃·CH₄O

Online 14 December 2001

 

Acta Cryst. (2002). C58, o6-o8  [ doi:10.1107/S0108270101017449 ]

A structural hierarchy in the hydrogen-bonded adduct N,N'-dimethylpiperazine-tartaric acid-water (1/2/2): an N-component N-dimensional structure (N = 3) with substructures having N = 1 and 2

D. M. M. Farrell, G. Ferguson, A. J. Lough and C. Glidewell

Formula: C₆H₁₆N₂²⁺·2C₄H₅O₆^-·2H₂O

Online 14 December 2001

 

Acta Cryst. (2002). C58, o9-o10  [ doi:10.1107/S0108270101018212 ]

Phthalimide at 120  K: perforated molecular ribbons containing three different ring motifs

C. M. Zakaria, J. N. Low and C. Glidewell

Formula: C₈H₅NO₂

Online 14 December 2001

 

Acta Cryst. (2002). C58, o11-o13  [ doi:10.1107/S0108270101016146 ]

A novel binucleating macrocyclic ligand with two alcohol pendants

D.-X. Yang, S.-A. Li, D.-F. Li and W.-X. Tang

Formula: C₂₈H₅₀N₆O₂⁴⁺·4Br^-·4H₂O

Online 14 December 2001

 

Acta Cryst. (2002). C58, o14-o15  [ doi:10.1107/S010827010101664X ]

Bis[2-(2-hydroxyphenoxy)ethyl] ether methanol solvate

P. Thuéry, M. Nierlich and B. Masci

Formula: C₁₆H₁₈O₅·CH₄O

Online 14 December 2001

 

Acta Cryst. (2002). C58, o16-o18  [ doi:10.1107/S0108270101016985 ]

An anthracene dimer with a fused 1,3-dithiole ring at 193  K

J. Kansikas and K. Sipilä

Formula: C₂₉H₂₀S₂

Online 14 December 2001

 

Acta Cryst. (2002). C58, o19-o21  [ doi:10.1107/S0108270101018224 ]

Powder diffraction study of the hydrogen bonds in nitroxoline and its hydrochloride

A. V. Yatsenko, K. A. Paseshnichenko, V. V. Chernyshev and H. Schenk

Formula: C₉H₆N₂O₃ and C₉H₇N₂O₃⁺·Cl^-

Online 14 December 2001

 

Acta Cryst. (2002). C58, o22-o23  [ doi:10.1107/S0108270101018601 ]

(+)-3-Oxo-4-pregnene-20-carboxylic acid: catemeric hydrogen bonding in a steroidal keto acid

H. W. Thompson and R. A. Lalancette

Formula: C₂₂H₃₂O₃

Online 14 December 2001

 

Acta Cryst. (2002). C58, o24-o25  [ doi:10.1107/S0108270101017875 ]

1,1'-Diacetyl-3-hydroxy-2,2',3,3'-tetrahydro-3,3'-bi(1H-indole)-2,2'-dione

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, B.-G. Zhao and J.-H. Xu

Formula: C₂₀H₁₆N₂O₅

Online 22 December 2001

 

Acta Cryst. (2002). C58, o26-o28  [ doi:10.1107/S0108270101018273 ]

4-[3-(3,4-Dimethoxyphenyl)prop-2-enoyl]phenyl methacrylate and 4-[3-(2-bromophenyl)prop-2-enoyl]phenyl methacrylate

A. Jeyabharathi, M. N. Ponnuswamy, S. Nanjundan, H.-K. Fun, S. Chantrapromma, A. Usman and I. A. Razak

Formula: C₂₁H₂₀O₅ and C₁₉H₁₅BrO₃

Online 22 December 2001

 

Acta Cryst. (2002). C58, o29-o31  [ doi:10.1107/S0108270101019163 ]

2,4-Dihydroxy-1,3-bis(methoxycarbonylmethoxy)calix[4]arene and 1,3-bis(ethoxycarbonylmethoxy)-2,4-dihydroxycalix[4]arene chloroform solvate

S. J. Coles, C. W. Hall and M. B. Hursthouse

Formula: C₃₄H₃₂O₈ and C₃₆H₃₆O₈·CH₃Cl

Online 22 December 2001

 

Acta Cryst. (2002). C58, o32-o33  [ doi:10.1107/S0108270101018029 ]

Azinyl Sulfides. LXVII. 1-Methylpyridine-4(1H)-thione

A. Zieba, A. Maslankiewicz and K. Suwinska

Formula: C₆H₇NS

Online 22 December 2001

 

Acta Cryst. (2002). C58, o34-o35  [ doi:10.1107/S0108270101017693 ]

2,6-Diphenylpyridine-4-carboxylic acid

A. Crispini and F. Neve

Formula: C₁₈H₁₃NO₂

Online 22 December 2001

 

Acta Cryst. (2002). C58, o36-o38  [ doi:10.1107/S0108270101017632 ]

2,2'-[2,3-Dihydro-2-(prop-2-enyl)-1H-isoindole-1,3-diylidene]bis(propanedinitrile)-tetrathiafulvalene (1/1), TCPI-TTF

C. Crean, J. F. Gallagher and A. C. Pratt

Formula: C₁₇H₉N₅·C₆H₄S₄

Online 22 December 2001

 

Acta Cryst. (2002). C58, o39-o41  [ doi:10.1107/S0108270101018765 ]

Supramolecular structures of 5-[3-(4-methylphenyl)- and 5-[3-(4-chlorophenyl)-2-propenylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione

J. N. Low, J. Cobo, M. Nogueras, A. Sánchez, B. Insuasty and H. Torres

Formula: C₁₆H₁₆O₄ and C₁₅H₁₃ClO₄

Online 22 December 2001

 

Acta Cryst. (2002). C58, o42-o45  [ doi:10.1107/S0108270101018297 ]

A comparison of the supramolecular structures of 1-(6-amino-1,3-benzodioxol-5-yl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one and 1-(6-amino-1,3-benzodioxol-5-yl)-3-[4-(N,N-dimethylamino)phenyl]prop-2-en-1-one

J. N. Low, J. Cobo, M. Nogueras, A. Sánchez, A. Albornoz and R. Abonia

Formula: C₁₉H₁₉NO₆ and C₁₈H₁₈N₂O₃

Online 22 December 2001

 

Acta Cryst. (2002). C58, o46-o47  [ doi:10.1107/S0108270101018571 ]

Hexamethylenetetraminium 2,4,6-trinitrophenolate

A. Usman, S. Chantrapromma, H.-K. Fun, B.-L. Poh and C. Karalai

Formula: C₆H₁₃N₄⁺·C₆H₂N₃O₇^-

Online 22 December 2001

 

Acta Cryst. (2002). C58, o48-o50  [ doi:10.1107/S0108270101020194 ]

A 1:1 adduct of hexamethylenetetramine and 4-hydroxy-3-methoxybenzaldehyde

A. Usman, S. Chantrapromma, H.-K. Fun, B.-L. Poh and C. Karalai

Formula: C₆H₁₂N₄·C₈H₈O₃

Online 22 December 2001

 

Acta Cryst. (2002). C58, o51-o54  [ doi:10.1107/S010827010101770X ]

Conformational polymorphism in a chiral spiro-cis-ansa-bridged cyclotriphosphazene derivative

S. J. Coles, D. B. Davies, M. B. Hursthouse, H. Ibisoglu, A. Kiliç and R. A. Shaw

Formula: Two polymorphs of C₁₉H₂₆ClN₆P₃

Online 22 December 2001

 

Acta Cryst. (2002). C58, o55-o56  [ doi:10.1107/S0108270101018625 ]

Macrocalyxin I

H. Shi, Y. J. Pan, S. H. Wu and X. X. Zhang

Formula: C₂₀H₃₀O₃

Online 22 December 2001