Acta Crystallographica Section C

Crystal Structure Communications

Volume 58, Part 2 (February 2002)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: 1'-Acetylferrocene-1-carboxylic acid: an instance of hydrogen bonding in the rare dimeric acid-to-ketone mode. Displacement ellipsoids are plotted at the 20% probability level. See Newman, Papadakis, Thompson & Lalancette [Acta Cryst. (2002), C58, m89-m91].

inorganic compounds


 

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Acta Cryst. (2002). C58, i23-i24  [ doi:10.1107/S010827010102087X ]

Dilead mercury chromate(VI), Pb2HgCrO6

W. Klein, J. Curda, K. Friese and M. Jansen

Synopsis: The structure of Pb2HgCrO6 consists of isolated [CrO4]2- tetrahedra, [HgO2]2- dumb-bells and stereochemically active Pb2+ ions with coordination 3+5.

Formula: Pb2HgCrO6

Online 23 January 2002


 

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Acta Cryst. (2002). C58, i25-i26  [ doi:10.1107/S0108270101019643 ]

Bismuth octaborate, Bi2B8O15

B. Teng, W. T. Yu, J. Y. Wang, X. F. Cheng, S. M. Dong and Y. G. Liu

Synopsis: In Bi2B8O15, the Bi atom is coordinated to five or six O atoms. The B atoms exhibit two kinds of hybridization, sp2 and sp3, seen in the BO3 triangles and BO4 tetrahedra, respectively. Three BO3 triangles are connected to form a B3O6 planar ring. All atoms in the structure are connected together to form an infinite three-dimensional network.

Formula: Bi2B8O15

Online 31 January 2002


metal-organic compounds


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Acta Cryst. (2002). C58, m65-m67  [ doi:10.1107/S0108270101019825 ]

catena-Poly[[[tetrakis(1-methylimidazole-[kappa]N3)copper(II)]-[mu]2-sulfato-[kappa]2O:O'] acetonitrile hemisolvate sesquihydrate]

J. Castro, P. Pérez Lourido, A. Sousa-Pedrares, E. Labisbal, M. Carabel and J. A. García-Vázquez

Formula: [Cu(C4H8N2)4]SO4·0.5C2H3N·1.5H2O

Online 16 January 2002


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Acta Cryst. (2002). C58, m68-m69  [ doi:10.1107/S0108270101019382 ]

([eta]5-Cyclopentadienyl)(p-fluorophenoxo)(nitrosyl)(trimethylsilylmethyl)molybdenum(II)

T. W. Hayton, P. Legzdins and S. J. Rettig

Formula: [Mo(C5H5)(C6H4FO)(C4H11Si)(NO)]

Online 16 January 2002


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Acta Cryst. (2002). C58, m70-m73  [ doi:10.1107/S0108270101015992 ]

Two new [Ni(tren)2]2+ complexes: [Ni(tren)2]Cl2 and [Ni(tren)2]WS4

J. Ellermeier, R. Stähler and W. Bensch

Formula: [Ni(C6H18N4)2]Cl2 and [Ni(C6H18N4)2]WS4

Online 16 January 2002


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Acta Cryst. (2002). C58, m74-m76  [ doi:10.1107/S0108270101019527 ]

fac-Tricarbonyl[hydroxybis(2-pyridyl)methanolato-[kappa]3N,O,N']rhenium(I)

M. Bakir

Formula: [Re(C11H9N2O2)(CO)3]

Online 16 January 2002


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Acta Cryst. (2002). C58, m77-m80  [ doi:10.1107/S0108270101019655 ]

Disodium pamidronate

D. Vega, D. Fernández and J. A. Ellena

Formula: 2Na+·C3H9NO7P22-·5H2O

Online 16 January 2002


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Acta Cryst. (2002). C58, m81-m83  [ doi:10.1107/S0108270101019072 ]

([mu]-Oxalato-O1,O2:O1',O2')bis[aqua(diethylenetriamine)nickel(II)] bis(hexafluorophosphate) dihydrate

I. Muga, P. Vitoria, J. M. Gutiérrez-Zorrilla, A. Luque, C. Guzmán-Miralles and P. Román

Formula: [Ni2(C2O4)(C4H13N3)2(H2O)2](PF6)2·2H2O

Online 16 January 2002


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Acta Cryst. (2002). C58, m84-m86  [ doi:10.1107/S0108270101019047 ]

First- and second- sphere coordination of the uranyl ion by bis[2-(2-hydroxyphenoxy)ethoxy]ethane

P. Thuéry, M. Nierlich and B. Masci

Formula: (C6H16N)[UO2(H2O)(C18H20O6)(NO3)]

Online 16 January 2002


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Acta Cryst. (2002). C58, m87-m88  [ doi:10.1107/S0108270101020789 ]

Bis(ethylenediamine)copper(II) bis(O,O'-diethyl dithiophosphate)

H.-K. Fun, Q.-L. Hao, J. Wu, X.-J. Yang, L.-D. Lu, X. Wang, S. Chantrapromma, I. A. Razak and A. Usman

Formula: [Cu(C2H8N2)2](C4H10O2PS2)2

Online 16 January 2002


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Acta Cryst. (2002). C58, m89-m91  [ doi:10.1107/S0108270101021771 ]

1'-Acetylferrocene-1-carboxylic acid: an instance of hydrogen bonding in the rare dimeric acid-to-ketone mode

J. M. Newman, M. M. Papadakis, H. W. Thompson and R. A. Lalancette

Formula: [Fe(C6H5O2)(C7H7O)]

Online 23 January 2002


 

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Acta Cryst. (2002). C58, m92-m94  [ doi:10.1107/S0108270101017206 ]

New girdle-like Mo18 polyanions linked into chains

G. Liu and S.-W. Zhang

Synopsis: The structure of the polyoxomolybdate [Na_{6}^{+}(H2O)16(NH2CH2COO)_{2}^{-}]4+·{Na+[H9Mo_{10}^{\rm VI}Mo_{8}^{\rm V}O56(NH2CH2COO)_{2}^{-}]5-}4-·20H2O is reported. The 18 Mo atoms connected by O atoms form a centrosymmetric girdle-like structure, in which MoV-MoV units are found. An Na+ cation occupies the central hole of the girdle, while four Na+ cations are bonded to O atoms on the girdle edge. The girdles are linked into a one-dimensional chain by the remaining Na+ cations.

Formula: An Mo18 polyoxomolybdate

Online 23 January 2002


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Acta Cryst. (2002). C58, m95-m97  [ doi:10.1107/S0108270101018406 ]

Bis([mu]-N,N-dimethyldithiocarbamato-[kappa]3S,S':S')bis[(dimethoxyphenylphosphane-[kappa]P)(N,N-dimethyldithiocarbamato-[kappa]2S,S')cobalt(III)] bis(hexafluorophosphate)

T. Suzuki, H. D. Takagi and K. Kashiwabara

Formula: [Co2(C3H6NS2)4(C8H11O2P)2](PF6)2

Online 23 January 2002


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Acta Cryst. (2002). C58, m98-m101  [ doi:10.1107/S0108270101020029 ]

An ion pair formed by protonated Fe(cp*py)2 and the octanuclear cluster U8Cl24O4(cp*py)2 [cp*py is tetramethyl-5-(2-pyridyl)cyclopentadiene]

L. Moisan, T. Le Borgne, P. Thuéry and M. Ephritikhine

Formula: [Fe(C14H17N)(C14H16N)]2[U8Cl24O4(C14H16N)2]·4CH2Cl2

Online 23 January 2002


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Acta Cryst. (2002). C58, m102-m104  [ doi:10.1107/S0108270101019357 ]

Tetrakis(dimethyl sulfide)palladium(II) bis(tetrafluoroborate) and tetrakis(1,4-oxathiane-[kappa]S)palladium(II) bis(tetrafluoroborate)

M. H. Johansson and Å. Oskarsson

Formula: [Pd(C2H6S)4](BF4)2 and [Pd(C4H8OS)4](BF4)2

Online 23 January 2002


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Acta Cryst. (2002). C58, m105-m108  [ doi:10.1107/S0108270101018534 ]

Bis(tetra-n-butylammonium) (a redetermination at 150 K) and bis(tetraphenylarsonium) bis(1,3-dithiole-2-thione-4,5-dithiolato)zinc(II) (at 300 K)

N. M. Comerlato, W. T. A. Harrison, R. A. Howie, J. N. Low, A. C. Silvino, J. L. Wardell and S. M. S. V. Wardell

Formula: (C16H36N)2[Zn(C3S5)2] and (C24H20As)2[Zn(C3S5)2]

Online 23 January 2002


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Acta Cryst. (2002). C58, m109-m110  [ doi:10.1107/S0108270101020182 ]

[2,6-Bis(isopropylthiomethyl)phenyl-[kappa]3S,C1,S']bromopalladium(II)

J. Bacsa, R. M. Moutloali and J. Darkwa

Formula: [PdBr(C14H21S2)]

Online 23 January 2002


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Acta Cryst. (2002). C58, m111-m115  [ doi:10.1107/S0108270101020364 ]

Platinum complexes of oxopurines: cis-bis(theophyllinato-N7)bis(triphenylphosphine)platinum(II) and cis-chloro(theobrominato-N1)bis(triphenylphosphine)platinum(II) ethanol hemisolvate

E. Dubler, H. W. Schmalle, F. Arod and A. Schneider

Formula: [Pt(C7H7N4O2)2(C18H15P)2] and [PtCl(C7H7N4O2)(C18H15P)2]·0.5C2H6O

Online 23 January 2002


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Acta Cryst. (2002). C58, m116-m118  [ doi:10.1107/S0108270101019370 ]

[[mu]-1[kappa]2O,O':2([eta]5)-Cyclopentadienylcarboxylato][2([eta]5)-diphenylphosphinocyclopentadienyl]bis[1,1([eta]5)-tetramethylcyclopentadienyl]iron(II)titanium(III)

K. Mach, J. Kubista, I. Císarová and P. Stepnicka

Formula: [FeTi(C9H13)2(C6H4O2)(C17H14P)]

Online 23 January 2002


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Acta Cryst. (2002). C58, m119-m121  [ doi:10.1107/S0108270101021060 ]

[(1,4,8,11-Tetraazacyclotetradeca-1,4,8,11-tetrayl)tetraacetamide-[kappa]6N1,N4,N8,N11,O1,O8]copper(II) sulfate 4.5-hydrate

E. Espinosa, M. Meyer, D. Berard and R. Guilard

Formula: [Cu(C18H36N8O4)]SO4·4.5H2O

Online 23 January 2002


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Acta Cryst. (2002). C58, m122-m123  [ doi:10.1107/S0108270101020911 ]

Dichlorobis(trimethylenethiourea-[kappa]S)antimony(III) chloride

I. A. Razak, A. Usman, H.-K. Fun, B. M. Yamin and G. W. Keat

Formula: [SbCl2(C4H8N2S)2]Cl

Online 31 January 2002


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Acta Cryst. (2002). C58, m124-m126  [ doi:10.1107/S0108270101021515 ]

catena-Poly[[dicyanamido(5,5'-dimethyl-2,2'-bipyridine-[kappa]2N,N')copper(II)]-[mu]-dicyanamido-[kappa]2N1:N5]

H. Kooijman, A. L. Spek, G. A. van Albada and J. Reedijk

Formula: [Cu(C2N3)2(C12H12N2)]

Online 31 January 2002


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Acta Cryst. (2002). C58, m127-m128  [ doi:10.1107/S0108270101020856 ]

(2-Thienylmethyl)ammonium trichlorostannate(II): a hybrid salt

N. Mercier, A. Seyeux, C. Morel and A. Riou

Formula: (C5H8NS)[SnCl3]

Online 31 January 2002


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Acta Cryst. (2002). C58, m129-m132  [ doi:10.1107/S0108270101019679 ]

Isomorphism and phase transition in triferrocenylboroxine and triferrocenylborazine

J. W. Bats, K. Ma and M. Wagner

Formula: [Fe3(C5H5)3(C15H12B3O3)] and [Fe3(C5H5)3(C15H15B3N3)]

Online 31 January 2002


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Acta Cryst. (2002). C58, m133-m134  [ doi:10.1107/S0108270101020017 ]

Bis[[mu]-4-(ethylammoniomethyl)-3,5-dimethylpyrazolato-[kappa]2N1:N2]bis[([eta]4-1,5-cyclooctadiene)rhodium(I)] dichloride dichloromethane methanol solvate

G. Esquius, J. Pons, R. Yáñez, J. Ros, X. Solans and M. Font-Bardia

Formula: [Rh2(C8H15N3)2(C8H12)2]Cl2·CH2Cl2·CH4O

Online 31 January 2002


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Acta Cryst. (2002). C58, m135-m136  [ doi:10.1107/S0108270101021059 ]

Diaquabis[[mu]-(R,R)-tartrato-[kappa]4O1,O2:O3,O4]dinickel(II) trihydrate

S. Scherb, C. Näther and W. Bensch

Formula: [Ni2(C4H4O6)2(H2O)2]·3H2O

Online 31 January 2002


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Acta Cryst. (2002). C58, m137-m138  [ doi:10.1107/S0108270101019709 ]

Bis{[[mu]-N,N'-bis(salicylidene)-1,4-butanediamine-N,N',O,O'-copper(II)]-[mu]-chloro-chloromercury(II)}

I. Ercan, F. Ercan, C. Arici and O. Atakol

Formula: [Cu2Hg2Cl4(C18H18N2O2)2]

Online 31 January 2002


organic compounds


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Acta Cryst. (2002). C58, o57-o58  [ doi:10.1107/S0108270101017164 ]

Ethyl (6aRS,8RS,12bRS)-6-oxo-8-phenyl-6a,7,8,12b-tetrahydro-6H-benzo[b]naphtho[1,2-d]pyran-6a-carboxylate

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, B.-G. Zhao and J.-H. Xu

Formula: C26H22O4

Online 16 January 2002


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Acta Cryst. (2002). C58, o59-o62  [ doi:10.1107/S0108270101020820 ]

Syn- and anticlinal isomers of 2a'-acetoxy-1,7'-diacetyl-7',7a'-dihydro-2-oxospiro[1H-indole-3(2H),2'(2a'H)-oxeto[3,2-b]indole]

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Zhang and J.-H. Xu

Formula: Two isomers of C22H18N2O6

Online 16 January 2002


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Acta Cryst. (2002). C58, o63-o65  [ doi:10.1107/S0108270101018182 ]

D-Secoestrone derivatives. V. 3-Methoxy-17-oxo-17-phenyl-16,17-secoestra-1,3,5(10)-triene-16-nitrile and 17-hydroxy-3-methoxy-17-phenyl-16,17-secoestra-1,3,5(10)-triene-16-nitrile

D. Lazar, S. Stankovic, V. Pejanovic and C. Courseille

Formula: C25H27NO2 and C25H29NO2

Online 16 January 2002


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Acta Cryst. (2002). C58, o66-o68  [ doi:10.1107/S0108270101019540 ]

4-(Trifluoromethyl)benzonitrile

S. Boitsov, J. Songstad and K. W. Törnroos

Formula: C8H4F3N

Online 16 January 2002


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Acta Cryst. (2002). C58, o69-o71  [ doi:10.1107/S0108270101017851 ]

4-Methyl-2-[N-(3,4-methylenedioxybenzylidene)hydrazino]thiazole and its reduction product, 4-methyl-2-[N-(3,4-methylenedioxybenzylidene)hydrazono]-4,5-dihydrothiazole

J. Wouters, B. Norberg and S. Guccione

Formula: C12H11N3O2S and C12H13N3O2S

Online 16 January 2002


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Acta Cryst. (2002). C58, o72-o75  [ doi:10.1107/S0108270101020170 ]

Three polar derivatives of N-ethylcarbazole: materials for optical applications

V. N. Nesterov, N. G. Montoya, M. Yu. Antipin, M. Sanghadasa, R. D. Clark and T. V. Timofeeva

Formula: C18H13N3, C18H15N3S and C26H19N3S

Online 16 January 2002


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Acta Cryst. (2002). C58, o76-o77  [ doi:10.1107/S0108270101019539 ]

Methyl 3-(4-methoxyphenyl)prop-2-enoate

M. Bujak, J. Zaleski, V. Prezhdo and B. Uspenskiy

Formula: C11H12O3

Online 16 January 2002


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Acta Cryst. (2002). C58, o78-o79  [ doi:10.1107/S0108270101020352 ]

6-Aminopyridine-3-thiol

J. R. Sabino, C. H. T. P. da Silva and M. Yonashiro

Formula: C5H6N2S

Online 16 January 2002


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Acta Cryst. (2002). C58, o80-o83  [ doi:10.1107/S0108270101019151 ]

6-Propylamino-2,6-propylepimino-2,4,4,8,8-pentakis(pyrrolidin-1-yl)-1,3,5,7,2[lambda]5,4[lambda]5,6[lambda]5,8[lambda]5-tetraazatetraphosphorocine

L. Öztürk, M. Isiklan, Z. Kiliç and T. Hökelek

Formula: C26H55N11P4

Online 16 January 2002


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Acta Cryst. (2002). C58, o84-o85  [ doi:10.1107/S0108270101019308 ]

(-)-Dimenthyl malonate

G. S. Coumbarides, J. Eames, M. Motevalli and Y. Yohannes

Formula: C23H40O4

Online 16 January 2002


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Acta Cryst. (2002). C58, o86-o87  [ doi:10.1107/S0108270101019035 ]

2,3,6,7-Tetrahydroxy-9,10-dimethyl-9,10-dihydro-9,10-ethanoanthracene bis(1,4-dioxane) solvate

B. Masci, M. Nierlich and P. Thuéry

Formula: C18H18O4·2C4H8O2

Online 16 January 2002


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Acta Cryst. (2002). C58, o88-o89  [ doi:10.1107/S0108270101018595 ]

N-(3-Phenoxy-4-pyridinio)methanesulfonamidate

C. Michaux, C. Charlier, F. Julémont, J.-M. Dogné, X. de Leval, B. Norberg, B. Pirotte and F. Durant

Formula: C12H12N2O3S

Online 23 January 2002


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Acta Cryst. (2002). C58, o90-o93  [ doi:10.1107/S0108270101019680 ]

Stereochemistry of two new polyfunctionalized gem-dihalocyclopropanes

H. Ziyat, M. Y. Ait Itto, M. Ait Ali, A. Karim, A. Riahi and J.-C. Daran

Formula: C11H16Cl2O3 and C11H16Br2O3

Online 23 January 2002


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Acta Cryst. (2002). C58, o94-o96  [ doi:10.1107/S0108270101019400 ]

cis- and trans-2-(4-tert-Butylcyclohexyloxy)-1,3,5-trinitrobenzene

M. Spiniello and J. M. White

Formula: C16H21N3O7

Online 23 January 2002


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Acta Cryst. (2002). C58, o97-o99  [ doi:10.1107/S0108270101021254 ]

Hydrogen bonding in C-substituted nitroanilines: molecular ladders in 2-trifluoromethyl-4-nitroaniline and sheets of R\bf{_4^4}(12) and R\bf{_4^4}(32) rings in 3-trifluoromethyl-4-nitroaniline

C. Glidewell, J. N. Low, S. A. McWilliam, J. M. S. Skakle and J. L. Wardell

Formula: Two isomers of C7H5F3N2O2

Online 23 January 2002


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Acta Cryst. (2002). C58, o100-o102  [ doi:10.1107/S0108270101021485 ]

Hydrogen bonding in C-substituted nitroanilines: sheets built from alternating R\bf{_2^2}(12) and R\bf{_6^6}(36) rings in 2-bromo-6-cyano-4-nitroaniline

C. Glidewell, J. N. Low, S. A. McWilliam, J. M. S. Skakle and J. L. Wardell

Formula: C7H4BrN3O2

Online 23 January 2002


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Acta Cryst. (2002). C58, o103-o105  [ doi:10.1107/S0108270101020625 ]

Supramolecular hydrogen-bonded hexamers in two 5-aryl-3-methyl-1-phenyl-1,6,7,8-tetrahydropyrazolo[3,4-b][1,4]diazepines

J. N. Low, J. Cobo, B. Insuasty, H. Insuasty, M. Nogueras and A. Sánchez

Formula: C19H18N4 and C19H17ClN4

Online 23 January 2002


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Acta Cryst. (2002). C58, o106-o107  [ doi:10.1107/S0108270101020819 ]

(1R,3S)-Camphoramic acid

J.-J. Nie, D.-J. Xu, Z.-Q. Hu, Y.-Z. Xu, J.-Y. Wu and M. Y. Chiang

Formula: C10H17NO3

Online 23 January 2002


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Acta Cryst. (2002). C58, o108-o111  [ doi:10.1107/S0108270101018200 ]

New electron-deficient chiral phosphines: (4R,5R)-1,3-bis(trifluoromethanesulfonyl)perhydro-1,3,2-benzodiazaphosphol-2-yl] substituted amines

D. Konya, C. Philouze, Y. Gimbert and A. E. Greene

Formula: C12H20F6N3O4PS2, C10H16F6N3O4PS2 and C17H23F12N5O8P2S4·0.98CHCl3

Online 23 January 2002


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Acta Cryst. (2002). C58, o112-o114  [ doi:10.1107/S0108270101021631 ]

Melaminium acetate acetic acid solvate monohydrate

G. J. Perpétuo and J. Janczak

Formula: C3H7N6+·C2H3O2-·C2H4O2·H2O

Online 23 January 2002


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Acta Cryst. (2002). C58, o115-o116  [ doi:10.1107/S0108270101021527 ]

Redetermination of the twinned structure of triacetone amine monohydrate

A. D. Bond

Formula: C9H17NO·H2O

Online 31 January 2002


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Acta Cryst. (2002). C58, o117-o121  [ doi:10.1107/S0108270101019084 ]

(Z)-2-Methylbuten-1-yl(aryl)iodonium trifluoromethanesulfonates containing electron-withdrawing groups on the aryl moiety

R. J. Hinkle and R. McDonald

Formula: C12H13F3I+·CF3O3S-, C11H12Cl2I+·CF3O3S- and 2C13H12F6I+·2CF3O3S-·CH2Cl2

Online 31 January 2002


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Acta Cryst. (2002). C58, o122-o124  [ doi:10.1107/S010827010102090X ]

2-(4-Chlorophenyl)-1,3-dicyano-6,7-dihydro-4-imino-9,10-dimethoxybenzo[a]quinolizine-water (2/5)

A. Linden, E. M. Awad, N. M. Elwan, H. M. Hassaneen and H. Heimgartner

Formula: C23H17ClN4O2·2.5H2O

Online 31 January 2002


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Acta Cryst. (2002). C58, o125-o128  [ doi:10.1107/S0108270101021564 ]

2-(4-Bromophenyl)-1,2-dihydropyrimido[1,2-a]benzimidazol-4(3H)-one and 4-(4-methylphenyl)-3,4-dihydropyrimido[1,2-a]benzimidazol-2(1H)-one form hydrogen-bonded base-paired dimers

J. N. Low, J. Cobo, B. Insuasty, M. Nogueras, A. Salcedo and A. Sánchez

Formula: C16H12BrN3O and C17H15N3O

Online 31 January 2002


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