# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' ruc10sc8 in P -1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 229.59 _exptl_crystal_F_000 1144.00 _reflns_d_resolution_high 0.7691 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.0020 _cell_length_b 13.3040 _cell_length_c 26.7230 _cell_angle_alpha 83.427 _cell_angle_beta 85.045 _cell_angle_gamma 74.051 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1894.16 368.37 436.23 o 2 0 0 568.38 786.08 20.97 o 3 0 0 4566.67 4685.71 87.42 o 4 0 0 1803.82 1742.82 62.77 o 5 0 0 1713.38 2045.78 97.62 o 6 0 0 14.02 13.06 22.79 o 8 0 0 1.34 33.02 65.90 o -8 1 0 178.01 192.84 45.09 o -7 1 0 380.06 414.65 31.40 o -6 1 0 23.03 47.49 27.78 o -5 1 0 12.30 -1.19 49.27 o -4 1 0 9055.78 10011.29 272.42 o -3 1 0 157.49 196.41 11.73 o -2 1 0 4434.03 4533.07 92.30 o -1 1 0 21196.13 16294.49 1794.17 o 0 1 0 271.41 -0.93 0.93 o 1 1 0 20845.93 404.36 3159.33 o 2 1 0 12675.43 13521.47 333.75 o 3 1 0 2928.47 3030.39 64.02 o 4 1 0 223.83 224.38 14.15 o 5 1 0 1964.78 1818.87 87.77 o 6 1 0 128.35 176.34 26.67 o 8 1 0 3851.41 4654.32 230.72 o 9 1 0 404.39 514.11 67.87 o -9 2 0 115.58 77.36 60.30 o -7 2 0 232.44 288.31 46.63 o -6 2 0 771.13 687.00 55.40 o -5 2 0 615.75 609.59 37.66 o -4 2 0 272.80 280.69 12.55 o -3 2 0 18988.62 19369.61 567.97 o -2 2 0 981.25 856.66 17.42 o -1 2 0 34894.80 31305.09 1049.65 o 0 2 0 5314.07 4950.73 809.72 o 1 2 0 3595.45 3074.69 332.93 o 2 2 0 574.10 675.36 13.36 o 3 2 0 55.95 90.10 7.25 o 4 2 0 11507.94 13034.40 668.09 o 5 2 0 54.11 43.55 17.55 o 6 2 0 2288.93 2284.08 116.41 o 7 2 0 207.64 201.41 35.23 o 8 2 0 15.36 -31.23 39.73 o 9 2 0 1175.18 1249.45 60.50 o 10 2 0 72.35 52.23 65.23 o -8 3 0 13.90 42.68 47.24 o -7 3 0 1149.65 1361.43 96.95 o -6 3 0 218.42 195.10 24.01 o -5 3 0 2578.96 2797.26 168.82 o -4 3 0 3377.11 3305.29 147.81 o -3 3 0 1.04 5.81 7.83 o -2 3 0 12266.60 11897.43 280.55 o -1 3 0 117.26 129.53 13.42 o 0 3 0 1350.02 1203.80 45.65 o 1 3 0 89.48 207.62 15.60 o 2 3 0 5236.70 5700.05 136.83 o 3 3 0 62.29 102.36 6.38 o 4 3 0 485.78 430.99 14.38 o 5 3 0 10209.42 10283.70 298.74 o 6 3 0 574.42 566.52 39.73 o 7 3 0 144.95 141.65 29.29 o 8 3 0 624.75 671.72 57.22 o 9 3 0 25.89 -34.54 34.69 o 10 3 0 304.25 228.20 67.14 o -8 4 0 378.46 471.55 71.02 o -7 4 0 606.98 683.24 42.67 o -6 4 0 4957.98 5576.70 218.41 o -5 4 0 625.38 612.66 51.18 o -4 4 0 2070.42 2141.94 68.09 o -3 4 0 7801.79 7503.91 284.55 o -2 4 0 5806.56 6168.45 206.40 o -1 4 0 1351.93 1247.61 59.24 o 0 4 0 68.86 102.40 5.85 o 1 4 0 17063.16 17771.75 784.20 o 2 4 0 487.64 533.30 21.42 o 3 4 0 2138.77 2165.28 68.18 o 4 4 0 2753.42 2883.77 64.10 o 5 4 0 585.66 678.18 23.62 o 6 4 0 10334.79 11589.16 362.39 o 7 4 0 483.53 564.76 27.43 o 8 4 0 285.73 336.83 46.05 o 9 4 0 635.25 687.08 46.97 o 10 4 0 161.89 294.41 68.37 o -8 5 0 627.25 554.94 80.13 o -7 5 0 1210.41 1222.93 80.93 o -6 5 0 60.19 63.89 58.11 o -5 5 0 2832.90 2983.14 97.40 o -4 5 0 1.26 20.26 18.29 o -3 5 0 168.50 158.15 15.72 o -2 5 0 1732.32 1730.89 63.68 o -1 5 0 3562.76 3095.73 134.90 o 0 5 0 1126.05 1100.96 41.57 o 1 5 0 861.85 875.37 39.00 o 2 5 0 35966.78 37509.41 1407.84 o 3 5 0 234.65 184.35 11.56 o 4 5 0 4499.37 4565.74 113.50 o 5 5 0 6373.73 6900.62 168.08 o 6 5 0 46.77 100.52 30.20 o 7 5 0 685.13 769.36 31.04 o 9 5 0 329.44 301.38 31.75 o 10 5 0 6.42 -25.82 35.30 o -8 6 0 28.87 35.97 61.90 o -7 6 0 213.01 174.10 41.20 o -6 6 0 678.30 732.36 48.05 o -5 6 0 220.49 249.55 27.69 o -4 6 0 286.38 249.95 52.14 o -3 6 0 147.74 142.43 12.08 o -2 6 0 1378.67 1406.10 45.28 o -1 6 0 3095.72 3268.53 200.36 o 0 6 0 1621.10 1708.59 58.88 o 1 6 0 4455.84 5042.80 179.80 o 2 6 0 2.28 -7.41 7.41 o 3 6 0 16482.64 17996.84 708.91 o 4 6 0 33.68 47.78 8.74 o 5 6 0 11.93 -11.01 11.01 o 6 6 0 522.88 543.82 22.66 o 7 6 0 193.53 213.14 26.91 o 8 6 0 41.04 -9.33 24.82 o 9 6 0 22.65 131.01 56.42 o 10 6 0 630.44 650.18 105.01 o -7 7 0 139.22 150.65 66.40 o -6 7 0 1.18 58.13 29.73 o -5 7 0 478.12 495.42 25.55 o -4 7 0 244.49 243.61 20.62 o -3 7 0 126.24 131.01 11.31 o -2 7 0 28.23 28.25 11.86 o -1 7 0 7722.11 8381.86 483.70 o 0 7 0 841.58 893.86 39.20 o 1 7 0 2503.81 2600.73 115.66 o 2 7 0 6707.56 7186.21 224.48 o 3 7 0 390.32 362.84 15.38 o 4 7 0 1254.47 1287.79 34.78 o 5 7 0 16.08 19.54 18.04 o 6 7 0 249.33 248.03 17.39 o 7 7 0 26.88 20.28 24.97 o 8 7 0 75.71 84.50 22.60 o 9 7 0 42.56 32.01 28.38 o 10 7 0 26.37 18.73 59.68 o -7 8 0 160.64 100.03 50.22 o -6 8 0 15.57 15.41 36.98 o -5 8 0 626.12 656.00 92.56 o -4 8 0 12.82 20.13 14.86 o -3 8 0 3764.25 4186.73 129.03 o -2 8 0 3681.25 3978.27 144.49 o -1 8 0 94.48 91.21 12.15 o 0 8 0 10831.71 10765.15 566.73 o 1 8 0 68.28 37.21 6.36 o 2 8 0 627.54 550.69 17.80 o 3 8 0 4783.47 4724.92 145.84 o 4 8 0 166.91 170.98 12.80 o 5 8 0 33.21 49.36 14.63 o 6 8 0 495.95 487.50 42.71 o 7 8 0 2365.37 2248.29 117.46 o 8 8 0 7.36 -13.91 44.71 o 9 8 0 775.23 615.18 44.13 o 10 8 0 465.34 428.19 88.75 o -7 9 0 186.22 250.09 67.07 o -6 9 0 29.86 -38.34 40.79 o -5 9 0 170.20 247.04 57.59 o -4 9 0 1953.33 2222.77 176.11 o -3 9 0 346.52 315.62 39.41 o -2 9 0 2887.99 3000.64 123.38 o -1 9 0 4096.87 4171.15 304.58 o 0 9 0 2364.67 2494.73 180.85 o 1 9 0 2426.29 2796.05 179.55 o 2 9 0 320.60 296.43 32.85 o 3 9 0 1626.12 1606.32 51.57 o 4 9 0 461.33 474.41 41.05 o 5 9 0 1119.73 1177.17 51.59 o 6 9 0 1243.75 1307.46 125.71 o 7 9 0 1027.10 991.21 58.11 o 8 9 0 2867.64 3474.09 190.07 o 9 9 0 280.25 316.96 44.56 o -6 10 0 156.29 87.63 49.17 o -5 10 0 248.20 232.14 41.08 o -4 10 0 36.22 27.97 25.29 o -3 10 0 3682.74 3996.35 164.89 o -2 10 0 197.73 187.82 23.61 o -1 10 0 17.96 14.14 15.13 o 0 10 0 2204.34 2268.98 127.52 o 1 10 0 2551.22 2911.78 209.70 o 2 10 0 51.45 38.20 13.02 o 3 10 0 62.17 65.89 11.42 o 4 10 0 1293.90 1403.79 41.13 o 5 10 0 50.63 36.17 20.72 o 6 10 0 952.16 1063.53 97.13 o 7 10 0 2375.08 2802.43 149.24 o 8 10 0 54.94 84.94 37.63 o 9 10 0 826.04 883.97 81.73 o -5 11 0 302.18 236.27 68.92 o -4 11 0 647.78 754.02 53.08 o -3 11 0 79.24 42.31 24.98 o -2 11 0 1853.73 2032.72 75.33 o -1 11 0 83.54 57.12 36.19 o 0 11 0 427.93 474.29 31.15 o 1 11 0 1052.12 1110.63 70.02 o 2 11 0 185.62 215.52 20.36 o 3 11 0 212.83 218.54 23.43 o 4 11 0 31.42 47.89 17.49 o 5 11 0 1858.04 2059.76 104.15 o 6 11 0 49.00 -31.17 31.17 o 7 11 0 525.81 530.74 51.24 o 9 11 0 8.57 113.39 76.44 o -5 12 0 12.26 67.44 69.54 o -4 12 0 11.97 -53.95 53.95 o -3 12 0 460.73 480.58 75.02 o -2 12 0 180.94 176.52 26.83 o -1 12 0 67.56 48.96 27.85 o 0 12 0 4.86 -3.80 21.39 o 1 12 0 1649.82 1703.08 106.55 o 2 12 0 12.23 61.72 26.55 o 3 12 0 2502.14 2824.11 153.80 o 4 12 0 1746.36 1769.17 95.47 o 5 12 0 35.71 -2.59 29.93 o 6 12 0 1052.06 1161.56 67.57 o 7 12 0 50.44 77.85 40.22 o 8 12 0 7.23 -35.61 35.61 o 9 12 0 145.94 242.32 48.76 o -4 13 0 101.29 58.88 67.94 o -3 13 0 276.55 361.73 63.69 o -2 13 0 186.72 99.06 51.92 o -1 13 0 947.13 1021.06 55.36 o 0 13 0 332.05 413.95 37.70 o 1 13 0 95.72 85.24 25.59 o 2 13 0 4161.38 4791.30 259.86 o 3 13 0 111.31 86.11 32.21 o 4 13 0 655.78 676.71 51.68 o 5 13 0 527.98 710.52 57.96 o 6 13 0 126.83 154.60 40.28 o 7 13 0 59.06 122.48 37.50 o 8 13 0 21.23 -38.85 38.85 o -3 14 0 1.00 -12.63 63.69 o -2 14 0 613.59 507.81 53.41 o -1 14 0 30.82 -46.81 46.81 o 0 14 0 757.79 667.71 50.91 o 1 14 0 454.79 391.75 36.23 o 2 14 0 132.73 153.55 43.05 o 3 14 0 1509.32 1594.25 91.96 o 4 14 0 0.21 93.50 34.68 o 5 14 0 73.05 70.34 39.73 o 6 14 0 149.19 158.43 33.96 o 7 14 0 268.36 393.53 79.45 o 8 14 0 123.80 31.37 60.33 o -2 15 0 2.38 9.24 43.46 o -1 15 0 1052.71 831.59 73.35 o 0 15 0 1.42 48.78 100.15 o 1 15 0 350.19 387.73 112.59 o 2 15 0 1035.44 1018.39 52.56 o 3 15 0 383.03 373.06 70.31 o 4 15 0 495.50 520.21 55.56 o 5 15 0 1.24 73.15 33.28 o 6 15 0 112.22 156.27 38.07 o 7 15 0 4.45 71.38 41.02 o 0 16 0 1600.49 1521.86 82.57 o 1 16 0 38.80 45.31 41.10 o 2 16 0 14.54 -37.80 37.80 o 3 16 0 538.83 556.73 100.09 o 4 16 0 142.76 124.93 36.83 o 5 16 0 0.16 99.01 75.51 o 6 16 0 15.67 91.12 42.75 o 2 17 0 36.08 -39.58 39.58 o 3 17 0 382.70 354.93 45.02 o -3 -17 1 275.46 376.84 109.14 o -2 -17 1 60.28 171.34 44.29 o -6 -16 1 22.76 22.92 47.43 o -5 -16 1 1.26 12.85 79.05 o -4 -16 1 135.21 224.26 40.36 o -3 -16 1 313.65 272.36 41.61 o -2 -16 1 76.00 -7.47 68.55 o -1 -16 1 5.88 37.87 40.62 o 0 -16 1 1012.61 991.25 62.83 o -7 -15 1 1.91 -1.56 71.72 o -6 -15 1 160.82 119.68 50.54 o -5 -15 1 11.14 6.26 52.35 o -4 -15 1 203.65 242.67 46.99 o -3 -15 1 272.95 302.60 50.44 o -2 -15 1 1209.20 1269.66 60.85 o -1 -15 1 133.19 140.80 38.43 o 0 -15 1 11.78 31.34 37.41 o 1 -15 1 1043.32 942.82 80.68 o 2 -15 1 4.20 115.24 67.01 o -7 -14 1 281.01 390.64 63.90 o -6 -14 1 115.32 72.68 44.10 o -5 -14 1 214.30 305.62 42.25 o -4 -14 1 0.51 19.59 35.91 o -3 -14 1 1218.87 1277.48 77.36 o -2 -14 1 288.10 322.74 44.22 o -1 -14 1 759.02 741.32 77.30 o 0 -14 1 521.68 342.11 52.72 o 1 -14 1 37.70 40.22 48.16 o 2 -14 1 456.73 318.37 49.65 o 3 -14 1 0.04 57.28 61.47 o -8 -13 1 13.42 -32.11 38.97 o -7 -13 1 4.96 -5.63 35.01 o -6 -13 1 302.81 312.82 36.00 o -5 -13 1 623.97 669.75 54.63 o -4 -13 1 227.50 285.23 37.20 o -3 -13 1 19.51 29.50 30.80 o -2 -13 1 4206.89 4613.98 231.34 o -1 -13 1 1.54 -20.11 46.93 o 0 -13 1 679.61 675.75 57.92 o 1 -13 1 690.01 818.93 97.43 o 2 -13 1 122.78 85.31 57.77 o 3 -13 1 292.50 296.01 63.50 o 4 -13 1 46.86 123.74 67.14 o -8 -12 1 13.62 76.22 37.95 o -7 -12 1 31.79 44.10 38.86 o -6 -12 1 954.63 917.54 59.68 o -5 -12 1 171.69 117.02 35.78 o -4 -12 1 2305.38 2653.38 133.78 o -3 -12 1 2444.99 2700.38 137.72 o -2 -12 1 3.85 -25.81 25.81 o -1 -12 1 2492.52 2898.95 333.58 o 0 -12 1 92.28 58.02 40.63 o 1 -12 1 1.33 15.94 47.33 o 2 -12 1 149.39 159.87 27.01 o 3 -12 1 444.42 432.66 29.38 o 5 -12 1 1.21 89.06 71.51 o -9 -11 1 48.80 95.96 79.76 o -8 -11 1 874.31 782.69 52.46 o -7 -11 1 523.03 539.69 39.60 o -6 -11 1 93.61 78.53 33.07 o -5 -11 1 2306.57 2669.70 135.19 o -4 -11 1 74.54 64.61 24.14 o -3 -11 1 446.27 356.15 24.22 o -2 -11 1 392.29 416.61 75.20 o -1 -11 1 1399.71 1525.88 61.87 o 0 -11 1 535.21 585.38 58.52 o 1 -11 1 105.34 101.31 50.60 o 2 -11 1 1352.59 1532.03 96.10 o 3 -11 1 111.01 109.85 26.20 o 4 -11 1 935.89 1108.07 157.98 o 5 -11 1 302.90 331.26 49.30 o -9 -10 1 304.88 180.60 88.17 o -8 -10 1 44.28 20.08 55.74 o -7 -10 1 2669.90 3049.17 159.52 o -6 -10 1 1231.56 1308.09 72.00 o -5 -10 1 55.79 40.31 21.10 o -4 -10 1 1330.13 1317.87 51.94 o -3 -10 1 14.53 52.72 12.02 o -2 -10 1 22.20 25.65 24.83 o -1 -10 1 2361.60 2705.80 199.78 o 0 -10 1 1777.53 1965.77 84.45 o 1 -10 1 54.78 24.35 21.93 o 2 -10 1 166.27 141.57 18.72 o 3 -10 1 2912.11 3063.70 214.93 o 4 -10 1 5.92 52.96 56.26 o 5 -10 1 368.31 316.52 43.01 o 6 -10 1 196.69 246.55 132.42 o -9 -9 1 124.68 109.40 41.45 o -7 -9 1 722.86 689.31 58.76 o -6 -9 1 1780.33 1728.26 146.03 o -5 -9 1 1876.57 1871.70 65.87 o -4 -9 1 602.61 578.38 27.51 o -3 -9 1 2564.86 2696.53 64.99 o -2 -9 1 353.30 328.83 16.62 o -1 -9 1 1524.23 1641.06 73.94 o 0 -9 1 3729.34 3889.26 202.71 o 1 -9 1 3021.78 3339.14 208.08 o 2 -9 1 1374.40 1408.65 61.79 o 3 -9 1 178.33 161.30 28.63 o 4 -9 1 2219.56 2496.77 169.48 o 5 -9 1 207.26 212.69 33.33 o 6 -9 1 90.97 80.54 38.28 o 7 -9 1 178.69 167.76 57.16 o -10 -8 1 687.89 409.83 89.49 o -9 -8 1 593.24 429.42 77.85 o -8 -8 1 4.75 39.59 22.28 o -7 -8 1 2749.43 2721.44 140.12 o -6 -8 1 743.22 713.91 42.83 o -5 -8 1 119.09 154.67 19.52 o -4 -8 1 548.30 585.56 25.40 o -3 -8 1 5525.06 5835.28 200.27 o -2 -8 1 589.08 595.79 24.58 o -1 -8 1 11.24 8.81 12.27 o 0 -8 1 9419.75 9839.37 629.03 o 1 -8 1 88.83 100.60 10.15 o 2 -8 1 2923.76 3136.83 155.52 o 3 -8 1 2888.45 3237.24 117.55 o 4 -8 1 14.25 39.91 18.20 o 5 -8 1 1076.46 1377.89 106.80 o 6 -8 1 63.56 61.14 36.21 o 7 -8 1 53.34 71.21 37.35 o -10 -7 1 22.83 32.96 45.27 o -9 -7 1 45.75 92.82 66.21 o -8 -7 1 120.67 110.78 43.71 o -7 -7 1 80.79 75.23 18.16 o -6 -7 1 303.92 336.77 20.79 o -5 -7 1 23.23 33.61 12.08 o -4 -7 1 1101.96 1059.62 31.42 o -3 -7 1 334.54 380.87 13.33 o -2 -7 1 11737.77 12268.33 468.76 o -1 -7 1 1924.43 1887.44 87.11 o 0 -7 1 710.85 786.13 45.98 o 1 -7 1 9189.00 9866.37 713.99 o 2 -7 1 163.75 183.87 9.99 o 3 -7 1 340.37 326.99 20.44 o 4 -7 1 240.26 251.56 17.17 o 5 -7 1 578.55 609.48 25.93 o 6 -7 1 0.08 -13.43 50.26 o 7 -7 1 32.20 142.59 66.27 o -10 -6 1 652.66 643.08 94.11 o -9 -6 1 28.11 -31.82 34.49 o -8 -6 1 106.43 122.97 22.21 o -7 -6 1 68.72 52.08 20.40 o -6 -6 1 1122.59 1145.56 36.46 o -5 -6 1 136.66 172.74 19.59 o -4 -6 1 28.84 21.20 10.85 o -3 -6 1 14066.03 15425.80 397.54 o -2 -6 1 186.89 127.64 9.36 o -1 -6 1 6804.34 7806.11 297.50 o 0 -6 1 3109.79 3092.16 107.30 o 1 -6 1 2393.52 2478.33 196.68 o 2 -6 1 518.62 493.54 16.72 o 3 -6 1 74.39 49.94 8.87 o 4 -6 1 209.45 189.11 11.84 o 5 -6 1 79.74 55.49 58.17 o 6 -6 1 600.33 687.24 64.55 o 7 -6 1 138.09 201.47 55.00 o 8 -6 1 41.15 116.35 69.66 o -10 -5 1 25.95 61.04 80.50 o -9 -5 1 508.81 495.13 71.26 o -8 -5 1 74.53 67.99 28.13 o -7 -5 1 412.43 424.79 70.15 o -6 -5 1 2.07 37.69 25.38 o -5 -5 1 7049.80 7776.06 189.67 o -4 -5 1 3904.64 3983.81 85.96 o -3 -5 1 20.92 7.16 8.91 o -2 -5 1 45197.87 47198.45 1202.43 o -1 -5 1 1665.05 1862.78 58.48 o 0 -5 1 2195.81 1870.71 62.78 o 1 -5 1 3328.84 2927.04 204.66 o 2 -5 1 1989.45 2032.68 52.00 o 3 -5 1 700.13 627.27 25.52 o 4 -5 1 6.99 -21.40 21.40 o 5 -5 1 2115.25 2290.39 116.19 o 6 -5 1 194.46 181.48 63.72 o 7 -5 1 1362.96 1400.23 102.43 o 8 -5 1 473.06 451.47 77.73 o -10 -4 1 181.42 275.99 65.10 o -9 -4 1 693.01 759.92 44.82 o -8 -4 1 42.19 -13.30 37.73 o -7 -4 1 102.07 93.74 34.49 o -6 -4 1 8814.88 9991.08 281.10 o -5 -4 1 571.02 754.13 31.24 o -4 -4 1 6886.42 7068.85 179.44 o -3 -4 1 1784.59 1342.86 43.79 o -2 -4 1 343.82 399.95 11.57 o -1 -4 1 9173.81 9605.22 280.97 o 0 -4 1 1821.51 1860.16 66.29 o 1 -4 1 162.82 152.97 10.98 o 2 -4 1 2176.89 1986.20 59.88 o 3 -4 1 2808.74 2948.79 105.08 o 4 -4 1 500.44 544.79 34.88 o 5 -4 1 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