Acta Crystallographica Section C

Crystal Structure Communications

Volume 58, Part 3 (March 2002)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The cation of hexakis(pyrazole-[kappa]N2)copper(II) bis(hexafluoroarsenate). Displacement ellipsoids are plotted at the 50% probability level and H atoms have been omitted for clarity. See Otieno, Blanton, Hatfield, Asher & Parkin [Acta Cryst. (2002), C58, m182-m185].

inorganic compounds


 

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Acta Cryst. (2002). C58, i27-i28  [ doi:10.1107/S0108270101018017 ]

High-temperature synthesis of Rb2MnP2S6 in molten salt medium

S. P. Taylor, M. Krawiec and S.-J. Hwu

Synopsis: Rubidium manganese hexathiodiphosphate, Rb2MnP2S6, crystallizes in a structure typical of compounds of the type A2MP2Q6 (A = K, Rb, Cs; M = Mn, Fe; Q = S, Se). Its structure can be viewed as columns of [MnP2S6]2- polyhedra parallel to the a axis, interconnected by Rb+.

Formula: Rb2MnP2S6

Online 13 February 2002


 

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Acta Cryst. (2002). C58, i29-i30  [ doi:10.1107/S0108270101021588 ]

Barium tetraphosphate

J. Bennazha, A. Boukhari and E. M. Holt

Synopsis: The structure of the low-temperature form of barium tetraphosphate shows the tetraphosphate to exist in an S conformation.

Formula: Ba3P4O13

Online 13 February 2002


 

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Acta Cryst. (2002). C58, i31-i32  [ doi:10.1107/S0108270101021928 ]

A tetragonal polymorph of caesium hydroxide monohydrate, CsOH·H2O, from X-ray powder data

R. Cerný, V. Favre-Nicolin and B. Bertheville

Synopsis: The tetragonal polymorph of caesium hydroxide monohydrate, CsOH·H2O (or CsH3O2), a clathrate hydrate, contains an infinite three-dimensional hydrogen-bonded oxygen framework that is locally identical to layers found in the hexagonal modification.

Formula: CsOH·H2O

Online 13 February 2002


 

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Acta Cryst. (2002). C58, i33-i34  [ doi:10.1107/S0108270102001208 ]

Strontium manganese diselenite, SrMn(SeO3)2, containing unusual MnO5+1 polyhedra

M. G. Johnston and W. T. A. Harrison

Synopsis: SrMn(SeO3)2 is built up from sheets of irregular MnO5+1 units and pyramidal SeO3 groups, sharing vertices and edges. Nine-coordinate Sr2+ cations complete the structure.

Formula: SrMn(SeO3)2

Online 13 February 2002


 

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Acta Cryst. (2002). C58, i35-i36  [ doi:10.1107/S0108270102000379 ]

HgWO4 synthesized at high pressure and temperature

M. B. Åsberg Dahlborg and G. Svensson

Synopsis: The structure of HgWO4 consists of zigzag chains of edge-sharing WO6 octahedra running along the c axis and layers of corner-sharing HgO6 octahedra in the bc plane.

Formula: HgWO4

Online 20 February 2002


 

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Acta Cryst. (2002). C58, i37-i39  [ doi:10.1107/S0108270102000690 ]

Hg3AlF6O2H, a structure with a short interpolyhedral O...O distance

M. Weil

Synopsis: The crystal structure of Hg3AlF6O2H has been determined at room temperature. It comprises [HgO2F6] polyhedra and [AlF6] octahedra. Assumed hydrogen bonding between two O atoms, with O...O = 2.562 (9) Å, provides additional bonds in the framework.

Formula: Hg3AlF6O2H

Online 20 February 2002


 

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Acta Cryst. (2002). C58, i40-i44  [ doi:10.1107/S010827010101890X ]

Synchrotron X-ray study of orthorhombic Rb3Ta5O14 with a modified pyrochlore structure

D. du Boulay, R. Yamashita and N. Ishizawa

Synopsis: The structure of a new variant orthorhombic Rb3Ta5O14 phase with Pnma symmetry was identified from a half sphere of synchrotron X-ray data measured at a wavelength of 0.85 Å.

Formula: Rb3Ta5O14

Online 20 February 2002


metal-organic compounds


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Acta Cryst. (2002). C58, m139-m140  [ doi:10.1107/S0108270101020492 ]

Chloroheptakis(dimethyl sulfoxide)uranium(IV) trichloride

W. J. Oldham, B. L. Scott, K. D. Abney, W. H. Smith and D. A. Costa

Formula: [UCl(C2H6OS)7]Cl3

Online 13 February 2002


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Acta Cryst. (2002). C58, m141-m143  [ doi:10.1107/S0108270101021886 ]

Pseudosymmetry in pyridinium tetrachloro(oxo)pyridineniobate(V) pyridine solvate

I. A. Guzei, J. Roberts and D. A. Saulys

Formula: (C5H6N)[NbCl4O(C5H5N)]·C5H5N

Online 13 February 2002


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Acta Cryst. (2002). C58, m144-m146  [ doi:10.1107/S0108270101021540 ]

A liquid crystal derived from ruthenium(II,III) and a long-chain carboxylate

A. Zelcer, Z. D. Chaia, F. D. Cukiernik, E. E. Castellano and O. E. Piro

Formula: [Ru2(C10H19O2)4(C8H17O3S)]

Online 13 February 2002


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Acta Cryst. (2002). C58, m147-m149  [ doi:10.1107/S0108270102000045 ]

Bis(8-quinolinolato-N,O)platinum(II) and its synthetic intermediate, 8-hydroxyquinolinium dichloro(8-quinolinolato-N,O)platinate(II) tetrahydrate

M. Kato, Y. Ogawa, M. Kozakai and Y. Sugimoto

Formula: [Pt(C9H6NO)2] and (C9H8NO)[PtCl2(C9H6NO)]·4H2O

Online 13 February 2002


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Acta Cryst. (2002). C58, m150-m151  [ doi:10.1107/S0108270102000069 ]

The sodium salt of 2-hydroxy-5-nitrobenzylsulfonic acid

M. Chruszcz and K. Lewinski

Formula: Na+·C7H6NO6S-·H2O

Online 13 February 2002


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Acta Cryst. (2002). C58, m152-m154  [ doi:10.1107/S0108270102000859 ]

Interpenetrating nets in cis-bis(pyridine-4-carboxylate)nickel(II)

T.-B. Lu and R. L. Luck

Formula: [Ni(C6H4NO2)2]

Online 13 February 2002


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Acta Cryst. (2002). C58, m155-m157  [ doi:10.1107/S0108270102000458 ]

Aquachloro(1,10-phenanthroline-[kappa]2N,N')(p-toluenesulfonato-[kappa]O)copper(II)

C. Aller, J. Castro, P. Pérez-Lourido, E. Labisbal and J. A. García-Vázquez

Formula: [CuCl(C7H7O3S)(C12H8N2)(H2O)]

Online 13 February 2002


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Acta Cryst. (2002). C58, m158-m159  [ doi:10.1107/S0108270102000549 ]

Trichloro(1,1-dimethylbiguanidium-[kappa]N3)zinc(II)

M.-L. Zhu, L.-P. Lu, X.-L. Jin and P. Yang

Formula: [ZnCl3(C4H12N5)]

Online 13 February 2002


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Acta Cryst. (2002). C58, m160-m161  [ doi:10.1107/S010827010200032X ]

Chlorobis(triphenylphosphine)nickel(I)

N. C. Norman, A. G. Orpen, M. J. Quayle and G. R. Whittell

Formula: [NiCl(C18H15P)2]

Online 13 February 2002


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Acta Cryst. (2002). C58, m162-m164  [ doi:10.1107/S0108270101021370 ]

Bis[1,1'-bis(diphenylphosphino)ferrocenium] hexadecachlorotetraantimony(III) ethanol solvate

I. A. Razak, A. Usman, H.-K. Fun, B. M. Yamin and N. A. Kasim

Formula: [Fe(C17H14P)2]2[Sb4Cl16]·C2H6O

Online 13 February 2002


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Acta Cryst. (2002). C58, m165-m166  [ doi:10.1107/S0108270102000665 ]

A pseudo-cage complex of silver(I) with tripodal tetraamine having benzyl end groups, {tris[2-(benzylamino)ethyl]amine-[kappa]4N}silver(I) perchlorate

I. Yoon, Y. W. Shin, J. Kim, K.-M. Park, S. B. Park and S. S. Lee

Formula: [Ag(C27H36N4)]ClO4

Online 20 February 2002


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Acta Cryst. (2002). C58, m167-m170  [ doi:10.1107/S0108270101021898 ]

Three different bonding modes of cyano groups in the coordination polymer [Cu(en)2(H2O)][Cu(en)2Ni2Cu2(CN)10]·2H2O (en is 1,2-diaminoethane)

J. Cernák and K. A. Abboud

Formula: [Cu(C2H8N2)2(H2O)][Ni2Cu3(CN)10(C2H8N2)2]·2H2O

Online 20 February 2002


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Acta Cryst. (2002). C58, m171-m173  [ doi:10.1107/S0108270102000057 ]

Decacarbonylbis(methylcyclopentadienyl)-tetrahedro-diiridiumdimolybdenum and decacarbonylbis(tetramethylcyclopentadienyl)-tetrahedro-diiridiumdimolybdenum dichloromethane hemisolvate

N. T. Lucas and M. G. Humphrey

Formula: [Mo2Ir2(C6H7)2(CO)10] and [Mo2Ir2(C9H13)2(CO)10]·0.5CH2Cl2

Online 20 February 2002


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Acta Cryst. (2002). C58, m174-m176  [ doi:10.1107/S0108270102001518 ]

catena-Poly[[di-[mu]-chloro-bis[(triphenylphosphine)silver(I)]]-[mu]-2-aminopyrimidine-[kappa]2N1:N3]

Q.-H. Jin, X.-L. Xin, X.-Y. Ci and K.-B. Yu

Formula: [Ag2Cl2(C4H5N3)(C18H15P)2]

Online 20 February 2002


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Acta Cryst. (2002). C58, m177-m178  [ doi:10.1107/S0108270101020649 ]

The trigonal-bipyramidal triiodothallium(III) complex [TlI3{(CH3)2SO}2]

G. Ma, A. Fischer and J. Glaser

Formula: [TlI3(C2H6OS)2]

Online 20 February 2002


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Acta Cryst. (2002). C58, m179-m181  [ doi:10.1107/S0108270102000860 ]

Aqua[bis(pyrimidin-2-yl-[kappa]N)amine](carbonato-[kappa]2O,O')copper(II) dihydrate

G. A. van Albada, I. Mutikainen, U. Turpeinen and J. Reedijk

Formula: [Cu(CO3)(C8H7N5)(H2O)]·2H2O

Online 20 February 2002


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Acta Cryst. (2002). C58, m182-m185  [ doi:10.1107/S010827010200152X ]

A copper(II)-pyrazole complex cation with \bf \overline 3 imposed symmetry

T. Otieno, J. R. Blanton, M. J. Hatfield, S. L. Asher and S. Parkin

Formula: [Cu(C3H4N2)6](AsF6)2 and [Cu(C3H4N2)6](PF6)1.29(ClO4)0.71

Online 20 February 2002


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Acta Cryst. (2002). C58, m186-m187  [ doi:10.1107/S0108270101020601 ]

Tris(1-ethyl-3-methylimidazolium) hexachlorolanthanate

K. Matsumoto, T. Tsuda, T. Nohira, R. Hagiwara, Y. Ito and O. Tamada

Formula: (C6H11N2)3[LaCl6]

Online 20 February 2002


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Acta Cryst. (2002). C58, m188-m189  [ doi:10.1107/S0108270102000343 ]

Tetrakis[(4-aminopyridinio)acetato-[kappa]O]diaquamanganese(II) diperchlorate

Y. Zhang, H.-B. Tao, C.-Y. Duan, Y.-Z. Li and L.-G. Zhu

Formula: [Mn(C7H8N2O2)4(H2O)2](ClO4)2

Online 28 February 2002


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Acta Cryst. (2002). C58, m190-m192  [ doi:10.1107/S0108270102001592 ]

catena-Poly[[bis(nicotinamide-[kappa]N1)copper(I)]-[mu]-thiocyanato-[kappa]2N:S]

C. Näther and I. Jeß

Formula: [Cu(NCS)(C6H6N2O)2]

Online 28 February 2002


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Acta Cryst. (2002). C58, m193-m196  [ doi:10.1107/S0108270102001609 ]

Three heterotrinuclear Schiff base complexes of nickel(II) with cobalt(II), copper(II) and manganese(II)

F. Ercan, O. Atakol, C. Arici, I. Svoboda and H. Fuess

Online 28 February 2002


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Acta Cryst. (2002). C58, m197-m198  [ doi:10.1107/S0108270102001579 ]

catena-Poly[bis[tetraaquacobalt(II)-[mu]-4,4'-bipyridine-[kappa]2N:N'] benzene-1,2,4,5-tetracarboxylate(4-) dihydrate]

C.-D. Wu, C.-Z. Lu, Y.-Q. Yu, H.-H. Zhuang and J.-S. Huang

Formula: [Co(C10H8N2)(H2O)4]2(C10H2O8)·2H2O

Online 28 February 2002


organic compounds


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Acta Cryst. (2002). C58, o129-o130  [ doi:10.1107/S0108270101020777 ]

The binary adduct of 3,6,9,16,19,22-hexaazatricyclo[22.2.2.211,14]triaconta-11,13,24,26(1),27,29-hexaene and benzene-1,2,4,5-tetracarboxylic acid

L.-G. Zhu, A. M. Ellern and N. M. Kostic

Online 13 February 2002


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Acta Cryst. (2002). C58, o131-o132  [ doi:10.1107/S0108270102000434 ]

Stigmasterol hemihydrate

G. A. Benavides, F. R. Fronczek and N. H. Fischer

Formula: C29H48O·0.5H2O

Online 13 February 2002


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Acta Cryst. (2002). C58, o133-o135  [ doi:10.1107/S0108270101021904 ]

3,4-Dihydro-6-methyl-3-[beta]-D-ribofuranosyl-4,5'-cyclo-9H-imidazo[1,2-a]purin-9-one hydrate

I. Leban, B. Golankiewicz, J. Zeidler, G. Giester and J. Kobe

Formula: C13H13N5O4·H2O

Online 13 February 2002


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Acta Cryst. (2002). C58, o136-o138  [ doi:10.1107/S0108270101021667 ]

Piperazine-1,4-diium-2,4-dinitrophenolate-water (1/2/2)

A. Usman, S. Chantrapromma, H.-K. Fun, B.-L. Poh and C. Karalai

Formula: C4H12N22+·2C6H3N2O5-·2H2O

Online 13 February 2002


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Acta Cryst. (2002). C58, o139-o141  [ doi:10.1107/S0108270101020571 ]

Ethyl 2-{[2-(3-nitrophenyl)-5-phenyl-1H-imidazol-4-yl]sulfanyl}acetate: synthesis via a microwave-mediated combinatorial chemistry approach

J. F. Gallagher, C. M. Coleman and D. F. O'Shea

Formula: C19H17N3O4S

Online 13 February 2002


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Acta Cryst. (2002). C58, o142-o144  [ doi:10.1107/S0108270101021916 ]

The [alpha]-D anomer of 5-aza-7-deaza-2'-deoxyguanosine

F. Seela, H. Rosemeyer, A. Melenewski, E.-M. Heithoff, H. Eickmeier and H. Reuter

Formula: C10H13N5O4·H2O

Online 13 February 2002


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Acta Cryst. (2002). C58, o145-o147  [ doi:10.1107/S0108270102000707 ]

[4-(Trifluoromethyl)phenyl]acetonitrile

S. Boitsov, J. Songstad and K. W. Törnroos

Formula: C9H6F3N

Online 13 February 2002


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Acta Cryst. (2002). C58, o148-o150  [ doi:10.1107/S0108270102001087 ]

1-Methyl-5,6,7,8-tetrahydroquinoxalin-2(1H)-one

A. B. Zolotoy, M. Botoshansky and M. Kaftory

Formula: C9H12N2O

Online 13 February 2002


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Acta Cryst. (2002). C58, o151-o153  [ doi:10.1107/S0108270102000598 ]

Flat versus twisted rotamers of 2,4-disubstituted thiazoles: the effect of intermolecular hydrogen bonds

S. Bernès, M. I. Berros, C. Rodríguez de Barbarín and F. Sánchez-Viesca

Formula: C11H11ClN2O2S and C12H12ClNO2S

Online 13 February 2002


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Acta Cryst. (2002). C58, o154-o156  [ doi:10.1107/S0108270101020595 ]

({\bf \pm})-3-Oxocyclohexanecarboxylic and -acetic acids: contrasting hydrogen-bonding patterns in two homologous keto acids

A. Barcon, A. P. J. Brunskill, R. A. Lalancette and H. W. Thompson

Formula: C7H10O3 and C8H12O3

Online 13 February 2002


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Acta Cryst. (2002). C58, o157-o158  [ doi:10.1107/S0108270102000574 ]

2-Methylphenyl 2-methoxyacridine-9-carboxylate

J. Meszko, K. Krzyminski, A. Konitz and J. Blazejowski

Formula: C22H17NO3

Online 20 February 2002


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Acta Cryst. (2002). C58, o159-o161  [ doi:10.1107/S0108270102000252 ]

trans-3-Ethyl-cis-2,6,6-trimethyl-4-oxocyclohexanecarboxylic acid: an intermediate in the synthesis of a highly potent estrogen

S. Xie, Y. Hou, C. Y. Meyers and P. D. Robinson

Formula: C12H20O3

Online 20 February 2002


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Acta Cryst. (2002). C58, o162-o163  [ doi:10.1107/S0108270102000197 ]

4-(3,17-Dioxoandrost-4-en-16-ylidenemethyl)benzonitrile

G. Vasuki, V. Parthasarathi, K. Ramamurthi, D. P. Jindal and S. Dubey

Formula: C27H29NO2

Online 20 February 2002


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Acta Cryst. (2002). C58, o164-o167  [ doi:10.1107/S0108270102000896 ]

Three tetrahydroisoquinolinedione derivatives

A. Subbiah Pandi, V. Rajakannan, D. Velmurugan, M. Parvez, M.-J. Kim, A. Senthilvelan and S. Narasinga Rao

Formula: C16H12ClNO2, C16H12BrNO2 and C15H9Cl2NO2

Online 20 February 2002


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Acta Cryst. (2002). C58, o168-o169  [ doi:10.1107/S0108270101017942 ]

5-Butyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(2,4,6-trimethylphenyl)isoxazole

J. P. A. Harrity, H. Adams, M. W. Davies, R. A. J. Wybrow and C. N. Johnson

Formula: C22H32BNO3

Online 20 February 2002


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Acta Cryst. (2002). C58, o170-o171  [ doi:10.1107/S0108270102001002 ]

Steroid 19,B-dinor-8,10-iso-analogues

M. S. Egorov, G. L. Starova and A. G. Shavva

Formula: C20H30O2

Online 20 February 2002


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Acta Cryst. (2002). C58, o172-o173  [ doi:10.1107/S0108270101020807 ]

D-Secoestrone derivatives. VI. 17[beta]-Benzyl-17[alpha]-hydroxy-3-methoxyestra-1,3,5(10)-trien-16-one

S. Stankovic, D. Lazar, L. Medic-Mijacevic, K. Penov-Gasi, M. Sakac, S. Andric and B. Milenko

Formula: C26H30O3

Online 20 February 2002


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Acta Cryst. (2002). C58, o174-o177  [ doi:10.1107/S0108270102000173 ]

4-Amino derivatives of 7-nitro-2,1,3-benzoxadiazole: the effect of the amino moiety on the structure of fluorophores

S. Saha

Formula: C10H10N4O3, C11H12N4O3 and C12H14N4O3

Online 20 February 2002


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Acta Cryst. (2002). C58, o178-o180  [ doi:10.1107/S0108270101021552 ]

The diastereoisomers methyl 5-(S)-[2-(R)/(S)-methoxycarbonyl)-2,3,4,5-tetrahydropyrrol-1-ylcarbonyl]-1-(4-methylphenyl)-4,5-dihydropyrazole-3-carboxylate

T. Pilati and G. Casalone

Formula: C19H23N3O5·C19H23N3O5 and C19H23N3O5

Online 28 February 2002


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Acta Cryst. (2002). C58, o181-o182  [ doi:10.1107/S0108270102001464 ]

The [beta]-polymorph of phenazine

W. Jankowski and M. Gdaniec

Formula: C12H8N2

Online 28 February 2002


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Acta Cryst. (2002). C58, o183-o186  [ doi:10.1107/S0108270102001099 ]

Dispiro[2H-benzimidazole-2,1'-cyclohexane-4',2''-[2H]benzimidazole] 1-oxide and dispiro[2H-benzimidazole-2,1'-cyclohexane-4',2''-[2H]benzimidazole] 1,1''-dioxide

M. Kaftory, V. Shteiman and M. Botoshansky

Formula: C18H16N4O and C18H16N4O2

Online 28 February 2002


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Acta Cryst. (2002). C58, o187-o188  [ doi:10.1107/S0108270102001439 ]

Cyclohexylphosphonic acid

K. Merz and A. Knüfer

Formula: C6H13O3P

Online 28 February 2002


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Acta Cryst. (2002). C58, o189-o190  [ doi:10.1107/S0108270102001543 ]

Tetrakis(chloromethyl)phosphonium chloride monohydrate

R. Weisbarth and M. Jansen

Formula: C4H8Cl4P+·Cl-·H2O

Online 28 February 2002


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Acta Cryst. (2002). C58, o191-o192  [ doi:10.1107/S0108270102000185 ]

1,3-Dimethyl-2-oxo-4,6-diphenyl-1,2,3,4-tetrahydropyridine-3-carbonitrile

U. H. Patel, C. G. Dave, M. M. Jotani and H. C. Shah

Formula: C20H18N2O

Online 28 February 2002


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Acta Cryst. (2002). C58, o193-o194  [ doi:10.1107/S0108270102001683 ]

1,3-Bis(2,4-dibromophenyl)triazene

M. Hörner, I. C. Casagrande, J. Bordinhao and C. M. Mössmer

Formula: C12H7Br4N3

Online 28 February 2002


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Acta Cryst. (2002). C58, o195-o198  [ doi:10.1107/S0108270102000689 ]

Three ginkgolide hydrates from Ginkgo biloba L.: ginkgolide A monohydrate, ginkgolide C sesquihydrate and ginkgolide J dihydrate, all determined at 120 K

J.-P. Zhao, I. Muhammad, D. C. Dunbar, I. A. Khan, N. H. Fischer and F. R. Fronczek

Formula: C20H24O9·H2O, C20H24O11·1.5H2O and C20H24O10·2H2O

Online 28 February 2002


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Acta Cryst. (2002). C58, o199-o200  [ doi:10.1107/S010827010102176X ]

The anti-inflammatory triterpenoid methyl 2-cyano-3,12-dioxooleana-1,9(11)-dien-28-oate methanol solvate hydrate

L. Bore, T. Honda, G. W. Gribble, E. Lork and J. P. Jasinski

Formula: C32H43NO4·CH4O·H2O

Online 28 February 2002


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