Acta Crystallographica Section C

Crystal Structure Communications

Volume 58, Part 4 (April 2002)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The molecular structure of (BETS)2[Fe(tdas)2]2, showing the dimerization of each entity. Displacement ellipsoids are drawn at the 50% probability level and H atoms have been omitted for clarity. See Pilia, Faulmann, Malfant, Collière, Mercuri, Deplano & Cassoux [Acta Cryst. (2002), C58, m240-m242].

inorganic compounds


 

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Acta Cryst. (2002). C58, i45-i46  [ doi:10.1107/S0108270102002032 ]

Tetrapotassium nonastannide, K4Sn9

C. Hoch, M. Wendorff and C. Röhr

Synopsis: K4Sn9 contains isolated nido-[Sn9]4- clusters of approximate C4v symmetry.

Formula: K4Sn9

Online 12 March 2002


 

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Acta Cryst. (2002). C58, i47-i49  [ doi:10.1107/S0108270102001920 ]

Hg3Se3O10, a mercury(II) compound with mixed-valence oxoselenium(IV/VI) anions

M. Weil and U. Kolitsch

Synopsis: Hg3Se3O10 was obtained after hydrothermal treatment of microcrystalline HgSeO4. The structure consists of three crystallographically independent Hg atoms, two selenite(IV) anions and one selenate(VI) anion.

Formula: Hg3Se3O10

Online 29 March 2002


 

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Acta Cryst. (2002). C58, i50-i52  [ doi:10.1107/S010827010200361X ]

Ba14Cu2In4N7, a new subnitride with isolated nitridocuprate groups and indium clusters

H. Yamane, S. Sasaki, S. Kubota, T. Kajiwara and M. Shimada

Synopsis: Ba14Cu2In4N7 crystallizes in the monoclinic space group P2/m with Z = 2, and contains 0[CuN2] nitridocuprate units and distorted 0[In4] clusters. One Ba atom, not connected to any N atoms, is surrounded by 12 other Ba atoms in a barium cuboctahedron.

Formula: Ba14Cu2In4N7

Online 29 March 2002


metal-organic compounds


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Acta Cryst. (2002). C58, m199-m201  [ doi:10.1107/S0108270102001798 ]

catena-Poly[[triphenyltin(IV)]-[mu]-hydroxo-[kappa]2O:O] at 120 K

C. Glidewell, J. N. Low, J. A. S. Bomfim, C. A. L. Filgueiras and J. L. Wardell

Formula: [Sn(C6H5)3(OH)]

Online 12 March 2002


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Acta Cryst. (2002). C58, m202-m203  [ doi:10.1107/S0108270102002822 ]

Triaquatris(2,6-dinitrophenolato-[kappa]2O1,O2)yttrium(III)

H. R. Suh, H. S. Suh, S. S. Yun, E. K. Lee and S. K. Kang

Formula: [Y(C6H3N2O5)3(H2O)3]

Online 12 March 2002


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Acta Cryst. (2002). C58, m204-m206  [ doi:10.1107/S0108270102001713 ]

trans-Bis(cyano-[kappa]C)(1,4,8,11-tetraazacyclotetradecane-[kappa]4N)manganese(III) perchlorate, a low-spin manganese(III) complex

S. Mossin, H. O. Sørensen and H. Weihe

Formula: [Mn(CN)2(C10H24N4)]ClO4

Online 12 March 2002


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Acta Cryst. (2002). C58, m207-m209  [ doi:10.1107/S0108270101021722 ]

(2,2'-Bipyridine-[kappa]2N,N')(dichromato-[kappa]O)copper(II)

P. A. Maggard, A. L. Kopf, C. L. Stern and K. R. Poeppelmeier

Formula: [Cu(Cr2O7)(C10H8N2)2]

Online 12 March 2002


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Acta Cryst. (2002). C58, m210-m212  [ doi:10.1107/S0108270102001932 ]

Bis(isoquinoline-1-carboxylato-[kappa]2O,N)(1,10-phenanthroline-[kappa]2N,N')zinc(II) dimethylformamide sesquisolvate

J.-C. Daran, P. Lemoine and B. Viossat

Formula: [Zn(C10H6NO2)2(C12H8N2)]·1.5C3H7NO

Online 12 March 2002


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Acta Cryst. (2002). C58, m213-m214  [ doi:10.1107/S0108270102001075 ]

A cyclic tetramer of [Ag(1,4,7-trithiacyclononane)]+, cyclo-tetrakis([mu]-1,4,7-trithiacyclononane-[kappa]3S1,S4,S7:[kappa]S1)tetrasilver(I) tetrakis(trifluoromethanesulfonate) nitromethane disolvate

T. Yamaguchi, F. Yamazaki and T. Ito

Formula: [Ag4(C6H12S3)4](CF3SO3)4·2CH3NO2

Online 12 March 2002


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Acta Cryst. (2002). C58, m215-m216  [ doi:10.1107/S0108270102002718 ]

A lithium complex of pyridine-2,6-dicarboxylic acid

M. Odoko, A. Kusano, N. Oya and N. Okabe

Formula: [Li(C7H4NO4)(H2O)]

Online 12 March 2002


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Acta Cryst. (2002). C58, m217-m218  [ doi:10.1107/S0108270102001737 ]

Tin-halide compounds. IV. tert-Butyltrichlorotin(IV)

H. Reuter, H. Eickmeier, H. Puff, N. Beckermann and D. Hänssgen

Formula: [Sn(C4H9)Cl3]

Online 12 March 2002


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Acta Cryst. (2002). C58, m219-m220  [ doi:10.1107/S0108270102001841 ]

Bis(tetramethylammonium) hexaaquadodeca-[mu]-bromo-octahedro-hexatantalum tetrabromide dihydrate

M. Vojnovic, D. Jozic, G. Giester, B. Peric, P. Planinic and N. Brnicevic

Formula: (C4H12N)2[Ta6Br12(H2O)6]Br4·2H2O

Online 12 March 2002


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Acta Cryst. (2002). C58, m221-m224  [ doi:10.1107/S0108270102002834 ]

Two nickel complexes stabilized by nitrate counter-ions

E. Freire, S. Baggio, J. C. Muñoz and R. Baggio

Formula: Two Ni-NO3 compounds

Online 12 March 2002


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Acta Cryst. (2002). C58, m225-m227  [ doi:10.1107/S0108270102002056 ]

Bis[hydrogen 1,1'-bis(diphenylphosphinato)ferrocenium] octachlorodiantimony(III)

I. A. Razak, A. Usman, H.-K. Fun, B. M. Yamin and N. A. M. Kasim

Formula: [Fe(C34H29O2P2)]2[Sb2Cl8]

Online 12 March 2002


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Acta Cryst. (2002). C58, m228-m229  [ doi:10.1107/S0108270102002044 ]

Bis(3,5-dimethylpyrazole-[kappa]N2)silver(I) nitrate

A. A. Mohamed and J. P. Fackler

Formula: [Ag(C5H7N2)2]NO3

Online 12 March 2002


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Acta Cryst. (2002). C58, m230-m231  [ doi:10.1107/S0108270102002883 ]

The seven-membered nickelacycle [NiBr{o-CH=C(CF3)C6H4CH2PPh2-[kappa]2C,P}{PPh(CH2Ph)2}]

A. J. Edwards and E. Wenger

Formula: [NiBr(C22H17F3P)(C20H19P)]

Online 12 March 2002


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Acta Cryst. (2002). C58, m232-m234  [ doi:10.1107/S0108270102002962 ]

Tetra-[mu]-acetato-[kappa]2O:O'-bis[(4-phenylpyridine-[kappa]N)copper(II)]

M.-L. Tong, W. Li, X.-M. Chen, S.-L. Zheng and S. W. Ng

Formula: [Cu2(C2H3O2)4(C11H9N)2]

Online 12 March 2002


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Acta Cryst. (2002). C58, m235-m236  [ doi:10.1107/S0108270102001701 ]

A complex containing three different kinds of Ru-N bonds: ethoxydinitronitrosyl(N,N,N',N'-tetramethylethylenediamine-[kappa]2N,N')ruthenium(II)

P. Albores, Z. D. Chaia, L. Baraldo, E. E. Castellano and O. E. Piro

Formula: [Ru(C2H5O)(NO)(NO2)2(C6H16N2)]

Online 21 March 2002


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Acta Cryst. (2002). C58, m237-m239  [ doi:10.1107/S0108270102002184 ]

cis-[1,2-Bis(diisopropylphosphino-[kappa]P)-1,2-dicarba-closo-dodecaborane]dichloroplatinum(II) dichloromethane hemisolvate

S. Paavola, F. Teixidor, C. Viñas and R. Kivekäs

Formula: [PtCl2(C14H38B10P2)]·0.5CH2Cl2

Online 21 March 2002


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Acta Cryst. (2002). C58, m240-m242  [ doi:10.1107/S010827010200330X ]

(BETS)2[Fe(tdas)2]2: a new metal in the molecular conductor family

L. Pilia, C. Faulmann, I. Malfant, V. Collière, M. L. Mercuri, P. Deplano and P. Cassoux

Formula: (C10H8S4Se4)2[{Fe(C2N2S3)2}2]

Online 21 March 2002


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Acta Cryst. (2002). C58, m243-m245  [ doi:10.1107/S0108270102003086 ]

Tetrakis[1-(3-chloropropyl)-1,2,4-triazole-[kappa]N4]bis(tetrafluoroborato-[kappa]F)copper(II)

A. M. Mills, K. Flinzner, A. F. Stassen, J. G. Haasnoot and A. L. Spek

Formula: [Cu(BF4)2(C5H8ClN3)4]

Online 21 March 2002


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Acta Cryst. (2002). C58, m246-m248  [ doi:10.1107/S0108270102002123 ]

Low-dimensional compounds containing cyano groups. I. catena-Poly[[[dicyanoargentato(I)-[kappa]N]bis(4-methylpyridine-[kappa]N)copper(II)]-[mu]-dicyanoargentato(I)-[kappa]2N:N']

L. Triscíková, I. Potocnák and C. Wagner

Formula: [Ag2Cu(CN)4(C6H7N)2]

Online 21 March 2002


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Acta Cryst. (2002). C58, m249-m251  [ doi:10.1107/S0108270101020558 ]

Undecacarbonyl(methylcyclopentadienyl)-tetrahedro-triiridiummolybdenum, undecacarbonyl(tetramethylcyclopentadienyl)-tetrahedro-triiridiummolybdenum and undecacarbonyl(pentamethylcyclopentadienyl)-tetrahedro-triiridiummolybdenum

N. T. Lucas, I. R. Whittall and M. G. Humphrey

Formula: [MoIr3(C6H7)(CO)11], [MoIr3(C9H13)(CO)11] and [MoIr3(C10H15)(CO)11]

Online 21 March 2002


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Acta Cryst. (2002). C58, m252-m255  [ doi:10.1107/S0108270102003062 ]

Two thiourea-containing gold(I) complexes

O. E. Piro, E. E. Castellano, R. C. V. Piatti, A. E. Bolzán and A. J. Arvia

Formula: [Au(CH4N2S)2]Cl and [Au(CH4N2S)2]2SO4

Online 21 March 2002


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Acta Cryst. (2002). C58, m256-m257  [ doi:10.1107/S0108270102002706 ]

[P,P-Di-tert-butyl-N-trimethylsilyl-P-(trimethylsilylamino)phosphine imidato-[kappa]2N,N']bis(pyridine-[kappa]N)lithium(I)

M. Schultz, B. F. Straub and P. Hofmann

Formula: [Li(C14H36N2PSi2)(C5H5N)2]

Online 21 March 2002


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Acta Cryst. (2002). C58, m258-m260  [ doi:10.1107/S0108270102003529 ]

Aquachloro[N,N'-ethylenebis(salicylideneiminato)]manganese(III)

D. Martínez, M. Motevalli and M. Watkinson

Formula: [MnCl(C16H14N2O2)(H2O)]

Online 21 March 2002


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Acta Cryst. (2002). C58, m261-m263  [ doi:10.1107/S0108270102003864 ]

Layered (ethylenediamine-[kappa]2N,N')cobalt(II) molybdate(VI)

B.-Z. Lin

Formula: [CoMoO4(C2H8N2)]

Online 29 March 2002


 

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Acta Cryst. (2002). C58, m264-m265  [ doi:10.1107/S0108270102003992 ]

CsMoO2(HO3P-CH2-PO3): a new metallodiphosphonate with a hybrid framework

K. Barthelet, D. Riou and G. Férey

Synopsis: A new variety of caesium molybdenomethylenediphosphonate is presented. Its monoclinic structure is built up from the stacking of hybrid layers, between which the Cs+ cations are intercalated.

Formula: [CsMoO2(CH3O6P2)]

Online 29 March 2002


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Acta Cryst. (2002). C58, m266-m267  [ doi:10.1107/S0108270102003530 ]

[5-Bromo-N-(2-carboxylatophenyl)salicylideniminato]dimethyltin(IV)

G. M. Rosair, D. K. Dey, B. Samanta and S. Mitra

Formula: [Sn(CH3)2(C14H8BrNO3)]

Online 29 March 2002


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Acta Cryst. (2002). C58, m268-m269  [ doi:10.1107/S0108270102003876 ]

Triaqua(2,2'-bipyridine-[kappa]2N,N')(nitrato-[kappa]O)manganese(II) nitrate

X.-F. Zhang, D.-G. Huang, W.-G. Wang, C.-N. Chen and Q.-T. Liu

Formula: [Mn(NO3)(C10H8N2)(H2O)3]NO3

Online 29 March 2002


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Acta Cryst. (2002). C58, m270-m272  [ doi:10.1107/S0108270102003852 ]

catena-Poly[[[diaquabis(5-chloropyridinium-2-olato-[kappa]O)copper(II)]-[mu]-pyrazine-[kappa]2N:N'] diperchlorate]

J.-X. Yuan, M.-L. Hu, Y.-Q. Cheng, L.-C. Chen and S. W. Ng

Formula: [Cu(C5H4ClNO)2(C4H4N2)(H2O)2](ClO4)2

Online 29 March 2002


organic compounds


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Acta Cryst. (2002). C58, o201-o203  [ doi:10.1107/S0108270102001786 ]

Hydrogen-bonded molecular ladders in S-(4-nitrophenyl)thioglycolic acid

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C8H7NO4S

Online 12 March 2002


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Acta Cryst. (2002). C58, o204-o208  [ doi:10.1107/S0108270102001488 ]

Adducts of 1,1,1-tris(4-hydroxyphenyl)ethane with diamines: three-dimensional hydrogen-bonded frameworks formed with 1,6-diaminohexane and 2,2'-bipyridyl

C. M. Zakaria, G. Ferguson, A. J. Lough and C. Glidewell

Formula: C6H18N22+·2C20H17O3- and C10H8N2·2C20H18O3

Online 12 March 2002


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Acta Cryst. (2002). C58, o209-o211  [ doi:10.1107/S0108270102003025 ]

A quasi-diamondoid hydrogen-bonded framework in anhydrous sulfanilic acid

J. N. Low and C. Glidewell

Formula: C6H7NO3S

Online 12 March 2002


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Acta Cryst. (2002). C58, o212-o214  [ doi:10.1107/S0108270101016468 ]

Design of peptides with [alpha],[beta]-dehydro residues: pseudo-tripeptide N-benzyloxycarbonyl-[Delta]Leu-L-Ala-L-Leu-OCH3

J. Makker, S. Dey, P. Kumar and T. P. Singh

Formula: C24H35N3O6

Online 12 March 2002


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Acta Cryst. (2002). C58, o215-o217  [ doi:10.1107/S0108270102002020 ]

Reactive intermediates in peptide synthesis. ortho-Nitrophenyl N[alpha]-para-toluenesulfonyl-[alpha]-aminoisobutyrate

M. Crisma and C. Toniolo

Formula: C17H18N2O6S

Online 12 March 2002


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Acta Cryst. (2002). C58, o218-o219  [ doi:10.1107/S0108270102001816 ]

3,4-(4-Methoxybenzo):8,9-benzobicyclo[4.4.1]undeca-3,8-dien-11-one ethylene acetal

X.-M. Liu, C. A. Kilner and M. A. Halcrow

Formula: C22H24O3

Online 12 March 2002


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Acta Cryst. (2002). C58, o220-o222  [ doi:10.1107/S0108270102001105 ]

1-Methyl-5,6-diphenylpyrazine-2(1H)-thione

A. B. Zolotoy, M. Botoshansky, M. Kaftory, J. R. Scheffer and J. Yang

Formula: C17H14N2S

Online 12 March 2002


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Acta Cryst. (2002). C58, o223-o225  [ doi:10.1107/S0108270102003220 ]

Two triethylammonium ion complexes of monoanionic calix[4]arene

P. Thuéry, Z. Asfari, M. Nierlich and J. Vicens

Formula: C6H16N+·C28H23O4- and 3C6H16N+·3C28H23O4-·C2H3N

Online 21 March 2002


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Acta Cryst. (2002). C58, o226-o227  [ doi:10.1107/S0108270102003165 ]

cis-Dioxocyclam

M. S. Mashuta, K. V. Pimenov and C. A. Grapperhaus

Formula: C10H20N4O2

Online 21 March 2002


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Acta Cryst. (2002). C58, o228-o230  [ doi:10.1107/S0108270102002172 ]

The supramolecular structure of pyridine-2,6-dicarboxylic acid

V. Carranza Téllez, B. Sánchez Gaytán, S. Bernès and E. González Vergara

Formula: C7H5NO4

Online 21 March 2002


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Acta Cryst. (2002). C58, o231-o234  [ doi:10.1107/S0108270102003190 ]

The dimer, trimer and 1,2,4-trithiolane of adamantanethione

A. Linden, C. Fu, A. Majchrzak, G. Mloston and H. Heimgartner

Formula: C20H28S2, C30H42S3 and C20H28S3

Online 21 March 2002


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Acta Cryst. (2002). C58, o235-o238  [ doi:10.1107/S0108270102003591 ]

The crystal packing of 4,7-dichloro- and 4,7-dibromobenzo[c]furazan 1-oxide

D. Britton, F. B. Mallory and C. W. Mallory

Formula: Two polymorphs of C6H2Cl2N2O2, and C6H2Br2N2O2

Online 21 March 2002


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Acta Cryst. (2002). C58, o239-o241  [ doi:10.1107/S0108270102003542 ]

1-Acetyl-3-[1-(4-methoxyphenyl)-2-oxopropylidene]-1H-indol-2(3H)-one: a twinned crystal

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Zhang and J.-H. Xu

Formula: C20H17NO4

Online 21 March 2002


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Acta Cryst. (2002). C58, o242-o246  [ doi:10.1107/S0108270102003657 ]

Two-component molecular crystals composed of chloronitrobenzoic acids and 4-aminopyridine

T. Sugiyama, J.-B. Meng and T. Matsuura

Formula: Four isomers of C5H7N2+·C7H3ClNO4-

Online 21 March 2002


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Acta Cryst. (2002). C58, o247-o250  [ doi:10.1107/S0108270102004080 ]

Triorganophosphine-dithiomonometaphosphoryl halides

A. Rabis, B. Ziemer, D. Wulff-Molder, M. Meisel and S. Beck

Formula: C14H15ClP2S2, C9H21ClP2S2 and C9H21BrP2S2

Online 29 March 2002


addenda and errata


 

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Acta Cryst. (2002). C58, e9  [ doi:10.1107/S0108270102000793 ]

Comment on [mu]1,3-azido-diazidotetrakis(1,10-phenanthroline)dicopper(II) azide tetrahydrate

P. Prabakaran

Synopsis: Comment on Acta Cryst. (2002), C58, m12-m13.

Formula: [Cu2(C12H8N2)4(N3)3](N3)·4H2O

Online 12 March 2002


 

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Acta Cryst. (2002). C58, e10  [ doi:10.1107/S0108270102002974 ]

Synchrotron-radiation study of the two-leg spin ladder (VO)2P2O7 at 120 K. Erratum

S. Geupel, K. Pilz, S. van Smaalen, F. Büllesfeld, A. Prokofiev and W. Assmus

Synopsis: Erratum to Acta Cryst. (2002), C58, i9-i13.

Formula: (VO)2P2O7

Online 12 March 2002


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