Acta Crystallographica Section C

Crystal Structure Communications

Volume 58, Part 5 (May 2002)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: A view of the molecular structure of bis(2,2'-methyliminodiethanolato)tetrakis(propane-1,3-diolato)trititanium(IV). Only the major conformations for the N-methyldiethoxoamine rings are shown. Displacement ellipsoids are drawn at the 30% probability level and H atoms have been omitted for clarity. See Kemmitt, Gainsford & Robson-Marsden [Acta Cryst. (2002), C58, m310-m312].

inorganic compounds


 

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Acta Cryst. (2002). C58, i53-i54  [ doi:10.1107/S0108270102004316 ]

A new quaternary thiophosphate, RbNb2(S2)3(PS4)

C.-K. Kim and H.-S. Yun

Synopsis: The structure of the new quaternary thiophosphate RbNb2(S2)3(PS4) is made up of one-dimensional {^{\kern 4pt 1}_{\infty}}[Nb2(S2)3(PS4)-] chains and these are stabilized by Rb+ ions.

Formula: RbNb2(S2)3(PS4)

Online 19 April 2002


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Acta Cryst. (2002). C58, i55-i60  [ doi:10.1107/S0108270102005176 ]

Copper(II) hypophosphite: the [alpha]- and [beta]-forms at 270 and 100 K, and the [gamma]-form at 270 K

D. Yu. Naumov, M. I. Naumova, N. V. Kuratieva, E. V. Boldyreva and J. A. K. Howard

Synopsis: The crystal structures of monoclinic [alpha]-, orthorhombic [beta]- and orthorhombic [gamma]-Cu(H2PO2)2 have been determined at different temperatures. Despite having different space groups, the structures of the [alpha]- and [beta]-polymorphs are very similar. The structures of the polymeric layers in the [gamma]-polymorph are quite different.

Formula: [alpha]-, [beta]- and [gamma]-Cu(H2PO2)2

Online 19 April 2002


 

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Acta Cryst. (2002). C58, i61-i62  [ doi:10.1107/S0108270102003153 ]

AgNi3(PO4)(HPO4)2: an alluaudite-like structure

R. Ben Smail and T. Jouini

Synopsis: AgNi3(PO4)(HPO4)2 has an alluaudite-like structure but shows some differences, owing to the presence of the H atoms. The Ag atom, one Ni atom and one P atom lie on twofold axes.

Formula: AgNi3(PO4)(HPO4)2

Online 19 April 2002


 

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Acta Cryst. (2002). C58, i63-i65  [ doi:10.1107/S0108270102005085 ]

Tl2Te and its relationship with Tl5Te3

R. Cerný, J.-M. Joubert, Y. Filinchuk and Y. Feutelais

Synopsis: Tl2Te is formed from Tl5Te3 by ordering of shear planes.

Formula: Tl2Te

Online 19 April 2002


 

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Acta Cryst. (2002). C58, i66-i68  [ doi:10.1107/S010827010200553X ]

Bis(ammonium) fluorophosphate at room temperature

R. Krupková, J. Fábry, I. Císarová and P. Vanek

Synopsis: The structure of a room-temperature phase of (NH4)2(PO3F) is related to [beta]-K2SO4. Phase transitions were detected at 251±2 and 274±2 K during cooling and heating, respectively.

Formula: (NH4)2(PO3F)

Online 19 April 2002


 

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Acta Cryst. (2002). C58, i69-i70  [ doi:10.1107/S0108270102003049 ]

[gamma]-Sodium gallate: a Rietveld refinement using X-ray powder diffraction

M.-E. Villafuerte-Castrejón, L. Bucio, A. Sánchez-Arjona, J. Duque and R. Pomés

Synopsis: A Rietveld refinement of a new [gamma] polymorph for sodium gallate is reported. The structure shows the normal distribution of cations over two different sets of tetrahedral sites, as normally presented by other [gamma] structures in many tetrahedral oxides.

Formula: NaGaO2

Online 30 April 2002


metal-organic compounds


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Acta Cryst. (2002). C58, m273-m274  [ doi:10.1107/S0108270102003797 ]

trans-(2-Acetylpyridine-[kappa]2N,O)dichlorobis(dimethyl sulfoxide-[kappa]S)ruthenium(II)

Satyanarayan Pal and Samudranil Pal

Formula: [RuCl2(C7H7NO)(C2H6OS)2]

Online 11 April 2002


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Acta Cryst. (2002). C58, m275-m279  [ doi:10.1107/S0108270102004341 ]

Comparison of two polymeric transition metal complexes with 1,4-benzenedicarboxylate ions as bridging ligands, [Co(C8H4O4)(C12H8N2)(H2O)] and [Cu(C8H4O4)(C10H9N3)]·H2O

L. Karanovic, D. Poleti, J. Rogan, G. A. Bogdanovic and A. Spasojevic-de Biré

Formula: [Co(C8H4O4)(C12H8N2)(H2O)] and [Cu(C8H4O4)(C10H9N3)]·H2O

Online 11 April 2002


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Acta Cryst. (2002). C58, m280-m282  [ doi:10.1107/S0108270102004298 ]

A three-dimensional CuII-WIV bimetallic porous assembly containing a zigzag ladder structure

D.-F. Li, T. Okamura, W.-Y. Sun, N. Ueyama and W.-X. Tang

Formula: [Cu2W(CN)8(C2H8N2)3]·4H2O

Online 11 April 2002


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Acta Cryst. (2002). C58, m283-m285  [ doi:10.1107/S010827010200464X ]

Polymeric aqua(nitrilotriacetato)erbium(III)

C.-D. Wu, C.-Z. Lu, H.-H. Zhuang and J.-S. Huang

Formula: [Er(C6H6NO6)(H2O)]

Online 11 April 2002


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Acta Cryst. (2002). C58, m286-m287  [ doi:10.1107/S0108270102004602 ]

trans-Bis[3-(2-fluorophenyl)-1-(4-nitrophenyl)triazenido-[kappa]N3]bis(pyridine-[kappa]N)palladium(II)

M. Hörner, L. do C. Visentin, M. Dahmer and J. Bordinhao

Formula: [Pd(C12H8FN4O2)2(C5H5N)2]

Online 11 April 2002


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Acta Cryst. (2002). C58, m288-m289  [ doi:10.1107/S0108270102004754 ]

catena-Poly[[bis(cis-1-tert-butyltetrazole-[kappa]N4)copper(II)]-di-[mu]-chloro]

D. O. Ivashkevich, M. M. Degtyarik, P. N. Gaponik and A. S. Lyakhov

Formula: [CuCl2(C5H10N4)2]

Online 11 April 2002


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Acta Cryst. (2002). C58, m290-m291  [ doi:10.1107/S0108270102004948 ]

Tetrakis(5-tert-butylpyrazole-1[kappa]N2)tetrachloro-1[kappa]Cl,2[kappa]3Cl-[mu]-oxo-1:2[kappa]2O-diiron(III)

X.-M. Liu, C. A. Kilner and M. A. Halcrow

Formula: [Fe2Cl4O(C7H12N2)4]

Online 11 April 2002


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Acta Cryst. (2002). C58, m292-m294  [ doi:10.1107/S0108270102004249 ]

Tetrakis([mu]-benzothiazole-2-thiolato)-1:2[kappa]4N:S2;1:2[kappa]4S2:N-dichloro-1[kappa]Cl,2[kappa]Cl-dirhenium(III)(Re-Re) dichloromethane solvate: a bridged complex with a long Re-Re quadruple bond

K. T. Horne, G. L. Powell and L. M. Daniels

Formula: [Re2(C7H4NS2)4Cl2]·CH2Cl2

Online 11 April 2002


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Acta Cryst. (2002). C58, m295-m296  [ doi:10.1107/S0108270102004766 ]

Tetraaquatetrakis(trimethylphosphine oxide-[kappa]O)cerium(III) trichloride trihydrate

N. J. Hill, L.-S. Leung, W. Levason and M. Webster

Formula: [Ce(C3H9OP)4(H2O)4]Cl3·3H2O

Online 11 April 2002


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Acta Cryst. (2002). C58, m297-m299  [ doi:10.1107/S0108270102004377 ]

Pentacarbonyl{tris[4-(methylsulfonyl)phenyl]stannyl}manganese(I): an unexpected tetragonal structure

D. Christendat, I. Wharf, A.-M. Lebuis, I. S. Butler and D. F. R. Gilson

Formula: [MnSn(C7H7O2S)3(CO)5]

Online 19 April 2002


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Acta Cryst. (2002). C58, m300-m301  [ doi:10.1107/S0108270102005292 ]

Dichlorobis(2-methylquinoline N-oxide-[kappa]O)zinc(II) from powder data

S. N. Ivashevskaja, L. A. Aleshina, V. P. Andreev, Y. P. Nizhnik, V. V. Chernyshev and H. Schenk

Formula: [ZnCl2(C10H9NO)2]

Online 19 April 2002


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Acta Cryst. (2002). C58, m302-m303  [ doi:10.1107/S0108270102005644 ]

Pentachloro-1,3,6-tris(diethylphenylphosphino)dirhenium(II,III)

K. T. Horne, G. L. Powell and L. M. Daniels

Formula: [Re2Cl5(C10H15P)3]

Online 19 April 2002


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Acta Cryst. (2002). C58, m304-m306  [ doi:10.1107/S0108270102005620 ]

{2,6-Bis[(dimethylamino-[kappa]N)methyl]phenyl-[kappa]C}iodopalladium(II) bis(diiodine)

A. M. Mills, J. A. M. van Beek, G. van Koten and A. L. Spek

Formula: [Pd(C12H19N2)I]·2I2

Online 19 April 2002


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Acta Cryst. (2002). C58, m307-m309  [ doi:10.1107/S0108270102006030 ]

Intermolecular interactions in cyanodimethylarsine and cyanodimethylstibine

D. Britton, V. G. Young and E. O. Schlemper

Formula: [As(CH3)2(CN)] and [Sb(CH3)2(CN)]

Online 30 April 2002


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Acta Cryst. (2002). C58, m310-m312  [ doi:10.1107/S0108270102006273 ]

Multiple bridging modes in a novel trinuclear titanium 1,3-dioxypropane compound, Ti3(methyliminodiethanolate)2(1,3-propanediolate)4

T. Kemmitt, G. J. Gainsford and H. Robson-Marsden

Formula: [Ti3(C5H11NO2)2(C3H6O2)4]

Online 30 April 2002


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Acta Cryst. (2002). C58, m313-m315  [ doi:10.1107/S0108270102006297 ]

Enantiomeric bis([mu]-N,N'-hexamethylenedisalicylaldiminato)dicopper(II) complexes

T. Friscic, A. J. Lough, G. Ferguson and B. Kaitner

Formula: Two enantiomorphs of [Cu2(C20H22N2O2)2]

Online 30 April 2002


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Acta Cryst. (2002). C58, m316-m318  [ doi:10.1107/S0108270102006303 ]

([eta]3-Allyl-2[kappa]3C)(chloro-1[kappa]Cl)([mu]-N,N'-diethyldithioxamidato-1:2[kappa]4S,S':N,N')[diphenyl(2-pyridyl)phosphine-1[kappa]P]palladium(II)platinum(II) chloroform solvate

G. Bruno, S. Lanza, F. Nicoló, G. Tresoldi and G. Rosace

Formula: [PdPtCl(C3H5)(C6H10N2S2)(C17H14NP)]·CHCl3

Online 30 April 2002


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Acta Cryst. (2002). C58, m319-m322  [ doi:10.1107/S0108270102006285 ]

Dichlorobis(1-propylimidazolidine-2-thione-[kappa]S)cobalt(II)

J. Castro, P. Pérez Lourido, A. Sousa-Pedrares, E. Labisbal, J. Piso and J. A. García-Vázquez

Formula: [CoCl2(C6H12N2S)2]

Online 30 April 2002


organic compounds


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Acta Cryst. (2002). C58, o251-o253  [ doi:10.1107/S0108270102004365 ]

(+)-2-(1,2,3,4,4a,5,6,7-Octahydro-4a,8-dimethyl-7-oxo-2-naphthyl)propionic acid: catemeric hydrogen bonding in a bicyclic sesquiterpenoid keto acid

A. P. J. Brunskill, H. W. Thompson and R. A. Lalancette

Formula: C15H22O3

Online 11 April 2002


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Acta Cryst. (2002). C58, o254-o256  [ doi:10.1107/S0108270102003955 ]

Arene-arene stacking in the revised structure of 2,2'-bipyridinium hexafluorophosphate

F. Kraus and J. Breu

Formula: C10H9N2+·PF6-

Online 11 April 2002


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Acta Cryst. (2002). C58, o257-o259  [ doi:10.1107/S0108270102004389 ]

2-[1-(Phenylsulfonyl)ethyl]benzoic acid and 2-[1-(phenylsulfonyl)propyl]benzoic acid

K. Sethu Sankar, D. Velmurugan, B. T. S. Thirumamagal, S. Shanmuga Sundara Raj, H.-K. Fun and J.-K. Moon

Formula: C15H14O4S and C16H16O4S

Online 11 April 2002


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Acta Cryst. (2002). C58, o260-o262  [ doi:10.1107/S0108270102004547 ]

4-Methoxyphenylphosphonic acid: reactivity of Lawesson's reagent

M. C. Aragoni, M. Arca, A. J. Blake, V. Lippolis, M. Schröder and C. Wilson

Formula: C7H9O4P

Online 11 April 2002


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Acta Cryst. (2002). C58, o263-o265  [ doi:10.1107/S0108270102004511 ]

Di-2-pyridyl ketone p-aminobenzoylhydrazone hydrate

M. Bakir and O. Green

Formula: C18H15N5O·H2O

Online 11 April 2002


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Acta Cryst. (2002). C58, o266-o267  [ doi:10.1107/S0108270102004687 ]

Ethyl 6-acetylamino-6,7-dihydro-5H-dibenzo[a,c]cycloheptene-6-carboxylate

L. Damodharan, N. Shamaladevi, V. Pattabhi, M. Behera and S. Kotha

Formula: C20H21NO3

Online 11 April 2002


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Acta Cryst. (2002). C58, o268-o271  [ doi:10.1107/S0108270102004432 ]

Pseudophomins A and B, a class of cyclic lipodepsipeptides isolated from a Pseudomonas species

J. W. Quail, N. Ismail, M. S. C. Pedras and S. M. Boyetchko

Formula: C55H97N9O16·H2O and C57H101N9O16·H2O

Online 11 April 2002


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Acta Cryst. (2002). C58, o272-o274  [ doi:10.1107/S0108270102004730 ]

N,N',N'',N'''-Tetraethylterephthalamidinium bis(tetrazolate)

A. Kraft, L. Peters and R. Fröhlich

Formula: C16H28N42+·2CHN4-

Online 11 April 2002


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Acta Cryst. (2002). C58, o275-o276  [ doi:10.1107/S0108270102004717 ]

Reactive intermediates in peptide synthesis: the N-oxysuccinimido ester of N[alpha]-para-toluenesulfonyl-[alpha]-aminoisobutyric acid

M. Crisma and C. Toniolo

Formula: C15H18N2O6S

Online 11 April 2002


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Acta Cryst. (2002). C58, o277-o279  [ doi:10.1107/S0108270102005152 ]

Ethyl [beta]-{2-[4-(dimethylamino)phenyliminomethyl]-1-(phenylsulfonyl)indol-3-yl}acrylate

K. Sethu Sankar, S. Kannadasan, D. Velmurugan, P. C. Srinivasan, S. Shanmuga Sundara Raj and H.-K. Fun

Formula: C28H27N3O4S

Online 19 April 2002


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Acta Cryst. (2002). C58, o280-o281  [ doi:10.1107/S0108270102005218 ]

5,5-Dimethyl-2-[6-methyl-2-(methylsulfanyl)pyrimidin-4-yloxy]-1,3,2-dioxaphosphorinane-2-thione

M. Pop, G. Borodi, K. Goubitz, R. Peschar, J. Fraanje, I. Fenesan and H. Schenk

Formula: C11H17N2O3PS2

Online 19 April 2002


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Acta Cryst. (2002). C58, o282-o283  [ doi:10.1107/S0108270102004882 ]

Secondary interactions in 4-bromo-N,N-dimethylanilinium bromide

P. G. Jones and L. Gray

Formula: C8H11BrN+·Br-

Online 19 April 2002


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Acta Cryst. (2002). C58, o284-o286  [ doi:10.1107/S0108270102005735 ]

4-Amino-6-benzyloxy-2-(methylsulfanyl)-5-nitrosopyrimidine: hydrogen-bonded dimers linked into [pi]-stacked chains

J. N. Low, A. Quesada, A. Marchal, M. Nogueras, A. Sánchez and C. Glidewell

Formula: C12H12N4O2S

Online 30 April 2002


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Acta Cryst. (2002). C58, o287-o288  [ doi:10.1107/S0108270102005681 ]

1-Acetyl-3'-(4-bromophenyl)-3'-chlorospiro[3H-indole-3,2'-oxetan]-2(1H)-one

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Zhang and J.-H. Xu

Formula: C18H13BrClNO3

Online 30 April 2002


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Acta Cryst. (2002). C58, o289-o294  [ doi:10.1107/S0108270102005632 ]

Hydrogen bonding in 2-amino-4,6-dimethoxypyrimidine, 2-benzylamino-4,6-bis(benzyloxy)pyrimidine and 2-amino-4,6-bis(N-pyrrolidino)pyrimidine: chains of fused rings and a centrosymmetric dimer

J. N. Low, A. Quesada, A. Marchal, M. Melguizo, M. Nogueras and C. Glidewell

Formula: C6H9N3O2, C25H23N3O2 and C12H19N5

Online 30 April 2002


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Acta Cryst. (2002). C58, o295-o297  [ doi:10.1107/S0108270102004912 ]

9-Cyano-10-methylacridinium hydrogen dinitrate

O. M. Huta, I. O. Patsaj, A. Konitz, J. Meszko and J. Blazejowski

Formula: C15H11N2+·HN2O6-

Online 30 April 2002


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Acta Cryst. (2002). C58, o298-o300  [ doi:10.1107/S0108270102006340 ]

C-H...[pi] and [pi]-[pi] interactions in the supramolecular structure of 3-methyl-1,4-diphenyl-1H-pyrazolo[3,4-b]pyridine

J. N. Low, J. Cobo, M. Nogueras, A. Sánchez, H. Torres and B. Insuasty

Formula: C19H15N3

Online 30 April 2002


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Acta Cryst. (2002). C58, o301-o304  [ doi:10.1107/S0108270102005140 ]

Three isomeric bis(methoxycarbonyl)[2.2]paracyclophanes

P. G. Jones, J. Hillmer and H. Hopf

Formula: Three isomers of C20H20O4

Online 30 April 2002


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Acta Cryst. (2002). C58, o305-o310  [ doi:10.1107/S0108270102006200 ]

The molecular and supramolecular structures of four 1,5,6,10b-tetrahydropyrazolo[1,5-c]quinazolines

J. N. Low, J. Cobo, M. Nogueras, A. Sánchez, H. Torres and B. Insuasty

Formula: C23H21N3, C22H18BrN3, C22H18ClN3 and C22H17BrClN3

Online 30 April 2002


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