# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I #data_0121 _shelx_title ' 0121 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 693.33 _exptl_crystal_F_000 2720.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 14.8287 _cell_length_b 16.1465 _cell_length_c 19.2824 _cell_angle_alpha 90.000 _cell_angle_beta 91.275 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 97689.38 99082.43 592.67 o 3 0 0 1165.34 673.46 167.01 o 4 0 0 24101.93 24014.59 468.49 o 5 0 0 1399.58 1326.85 241.84 o 6 0 0 54760.65 60852.00 864.33 o 7 0 0 10826.46 10911.98 466.87 o 8 0 0 211130.58 213887.03 1812.16 o 9 0 0 15125.79 15175.04 718.46 o 10 0 0 1318.97 717.92 595.92 o 11 0 0 1168.13 1329.57 439.75 o 12 0 0 27344.96 26857.54 973.86 o 13 0 0 754.43 916.92 519.46 o 14 0 0 2246.03 2557.19 626.83 o 15 0 0 3298.34 3911.16 669.66 o 16 0 0 7360.31 6509.55 871.92 o 17 0 0 457.43 1333.90 597.55 o 1 1 0 208.03 205.53 67.86 o 2 1 0 373766.63 335828.91 5115.19 o 3 1 0 312.39 359.50 178.94 o 4 1 0 7152.72 7698.36 241.26 o 5 1 0 409.32 962.58 927.77 o 6 1 0 34860.90 34512.31 495.50 o 7 1 0 3459.69 3223.73 271.72 o 8 1 0 22377.92 22605.91 794.65 o 9 1 0 4154.87 3837.29 317.37 o 10 1 0 63197.47 60691.91 1416.33 o 11 1 0 670.80 663.87 607.58 o 12 1 0 13300.74 12602.44 796.27 o 13 1 0 558.42 1105.40 392.01 o 14 1 0 4044.75 3916.58 515.65 o 15 1 0 1079.61 1412.91 383.03 o 16 1 0 711.69 874.89 463.70 o 17 1 0 384.95 97.78 449.60 o 0 2 0 3872.19 3893.80 164.30 o 1 2 0 433.67 237.78 84.92 o 2 2 0 2731.40 2751.31 196.83 o 3 2 0 3529.37 4068.95 258.65 o 4 2 0 56838.88 62297.61 760.76 o 5 2 0 1786.14 1697.74 276.54 o 6 2 0 4309.73 4303.74 343.78 o 7 2 0 924.76 1196.17 329.14 o 8 2 0 36236.17 37209.93 854.57 o 9 2 0 127.65 -293.35 293.35 o 10 2 0 5408.51 5411.53 510.24 o 11 2 0 506.64 781.36 618.69 o 12 2 0 1780.50 1197.26 473.92 o 13 2 0 391.03 -140.44 501.57 o 14 2 0 171.85 407.76 475.00 o 15 2 0 223.39 381.19 495.60 o 16 2 0 69.37 229.91 494.52 o 17 2 0 18.61 633.33 580.19 o 1 3 0 87.10 54.87 190.33 o 2 3 0 326268.59 316330.75 1475.43 o 3 3 0 299.41 201.71 235.87 o 4 3 0 3761.91 3667.69 303.11 o 5 3 0 3483.73 4173.06 375.77 o 6 3 0 12286.52 11884.75 492.35 o 7 3 0 7281.16 7704.65 465.78 o 8 3 0 25006.20 25428.20 782.99 o 9 3 0 1448.16 1670.09 468.49 o 10 3 0 56636.75 53970.48 1165.81 o 11 3 0 1853.09 2276.85 452.23 o 12 3 0 6995.34 6494.37 626.28 o 13 3 0 1217.35 2264.38 535.73 o 14 3 0 2698.21 2019.29 652.85 o 15 3 0 1084.08 1828.42 681.05 o 16 3 0 548.96 358.42 521.63 o 17 3 0 352.03 163.21 604.59 o 0 4 0 473099.19 441058.84 1822.46 o 1 4 0 3529.23 3770.34 202.85 o 2 4 0 2603.86 4485.93 302.03 o 3 4 0 12327.98 12819.03 433.25 o 4 4 0 60755.05 64335.88 886.56 o 5 4 0 4125.87 5422.91 388.78 o 6 4 0 38237.48 41876.42 865.41 o 7 4 0 88.69 -162.13 284.13 o 8 4 0 138716.17 134826.69 1620.20 o 9 4 0 796.24 700.57 362.76 o 10 4 0 2762.81 2972.00 475.54 o 11 4 0 7937.42 6819.17 659.90 o 12 4 0 22110.98 22499.04 955.96 o 13 4 0 3651.80 2437.36 604.05 o 14 4 0 1549.40 3114.07 708.16 o 15 4 0 1121.79 1920.60 820.40 o 16 4 0 2331.72 875.17 672.37 o 17 4 0 522.02 1368.61 729.31 o 1 5 0 2532.12 2817.32 365.74 o 2 5 0 48235.25 51868.76 787.87 o 3 5 0 137.65 262.98 244.01 o 4 5 0 16949.76 17178.07 554.17 o 5 5 0 21.63 -204.97 317.21 o 6 5 0 9530.85 11266.60 531.93 o 7 5 0 2261.69 1879.94 372.52 o 8 5 0 12494.36 13218.11 639.84 o 9 5 0 1551.24 2395.06 495.06 o 10 5 0 36316.74 36413.93 1045.98 o 11 5 0 101.47 130.68 426.74 o 12 5 0 6396.34 6108.84 683.22 o 13 5 0 661.95 777.57 557.96 o 14 5 0 651.51 736.90 543.86 o 15 5 0 1678.13 712.50 648.52 o 16 5 0 1833.38 1461.33 695.15 o 17 5 0 42.52 -226.66 739.61 o 0 6 0 1758.90 1649.48 296.06 o 1 6 0 466.79 601.09 173.11 o 2 6 0 2133.59 2068.63 332.93 o 3 6 0 522.36 891.98 291.18 o 4 6 0 9146.84 9257.07 496.15 o 5 6 0 1162.48 1103.99 343.24 o 6 6 0 9925.64 10816.54 561.22 o 7 6 0 1991.63 2091.95 384.45 o 8 6 0 212.22 -267.32 396.38 o 9 6 0 1183.29 1642.44 434.87 o 10 6 0 1199.94 1780.71 529.77 o 11 6 0 150.63 56.93 466.32 o 12 6 0 954.73 1599.06 598.63 o 13 6 0 38.78 -13.56 13.56 o 14 6 0 9.70 -615.98 615.98 o 15 6 0 284.91 198.46 854.57 o 16 6 0 4.59 1026.45 670.20 o 1 7 0 808.71 1320.72 218.72 o 2 7 0 177972.77 187613.45 1674.97 o 3 7 0 13.31 450.06 286.84 o 4 7 0 1051.45 1757.93 334.56 o 5 7 0 1276.10 1079.59 366.55 o 6 7 0 19544.50 19579.63 713.04 o 7 7 0 1274.88 789.50 402.34 o 8 7 0 4113.41 3823.86 505.91 o 9 7 0 1303.90 1321.97 660.44 o 10 7 0 37411.38 36044.66 1126.77 o 11 7 0 2422.34 3537.01 581.28 o 12 7 0 1898.98 2748.06 615.98 o 13 7 0 908.53 1529.11 585.62 o 14 7 0 2085.13 2103.34 692.44 o 15 7 0 539.93 169.72 626.28 o 16 7 0 80.51 151.28 523.26 o 0 8 0 287253.97 278989.63 2137.50 o 1 8 0 1453.25 1411.17 255.48 o 2 8 0 84351.92 88422.59 1254.74 o 3 8 0 1474.79 1299.74 397.46 o 4 8 0 24140.17 24560.63 761.84 o 5 8 0 112.91 -20.06 349.20 o 6 8 0 9521.46 9787.92 607.31 o 7 8 0 1404.97 1532.36 464.15 o 8 8 0 61160.04 64067.47 1366.44 o 9 8 0 3825.02 5037.38 677.80 o 10 8 0 496.65 548.20 541.15 o 11 8 0 918.87 1327.94 621.95 o 12 8 0 17778.80 19293.33 1012.90 o 13 8 0 1147.05 256.48 833.42 o 14 8 0 85.90 -501.03 594.83 o 15 8 0 446.44 -639.30 639.30 o 16 8 0 1753.84 1390.84 681.05 o 1 9 0 775.82 634.38 255.34 o 2 9 0 28115.54 28565.04 821.49 o 3 9 0 25.26 -328.05 328.05 o 4 9 0 8315.74 10015.66 578.02 o 5 9 0 6.71 -39.04 407.76 o 6 9 0 7046.01 8212.72 607.85 o 7 9 0 259.63 765.10 457.11 o 8 9 0 7861.91 6477.56 660.99 o 9 9 0 445.22 347.03 503.20 o 10 9 0 30238.76 32844.92 1142.49 o 11 9 0 251.85 -189.24 506.99 o 12 9 0 4128.53 5124.68 747.74 o 13 9 0 21.08 192.49 728.22 o 14 9 0 73.87 -87.30 650.68 o 15 9 0 265.42 1268.83 956.51 o 0 10 0 2395.63 2425.97 435.42 o 1 10 0 182.03 399.12 409.93 o 2 10 0 1953.59 2510.56 452.77 o 3 10 0 278.16 383.36 434.87 o 4 10 0 5997.73 6320.31 606.76 o 5 10 0 7.84 133.93 428.91 o 6 10 0 996.20 1948.26 505.36 o 7 10 0 921.97 1320.35 506.45 o 8 10 0 65.38 -172.43 508.62 o 9 10 0 315.25 637.67 540.61 o 10 10 0 795.05 1047.60 550.37 o 11 10 0 324.12 -564.47 655.56 o 12 10 0 1305.24 562.84 679.97 o 13 10 0 43.66 931.56 823.12 o 14 10 0 134.45 901.20 569.35 o 15 10 0 87.16 582.36 615.98 o 1 11 0 165.79 148.67 277.79 o 2 11 0 49392.55 47600.27 1171.77 o 3 11 0 11.02 338.90 410.47 o 4 11 0 356.99 807.39 421.86 o 5 11 0 685.25 458.19 495.60 o 6 11 0 26355.21 27728.37 989.58 o 7 11 0 638.22 736.90 527.05 o 8 11 0 614.16 2179.25 516.75 o 9 11 0 107.48 152.37 737.44 o 10 11 0 21141.95 22358.60 1064.95 o 11 11 0 469.63 243.46 857.28 o 12 11 0 960.07 899.03 934.82 o 13 11 0 510.54 678.34 662.07 o 14 11 0 1125.95 1261.24 637.13 o 0 12 0 72106.45 76230.39 1478.14 o 1 12 0 19.74 -134.75 348.87 o 2 12 0 14881.42 14086.23 782.45 o 3 12 0 65.90 -432.71 432.71 o 4 12 0 11856.14 12123.88 749.91 o 5 12 0 456.24 497.77 471.75 o 6 12 0 1371.46 452.77 611.10 o 7 12 0 486.75 1049.23 520.01 o 8 12 0 34858.91 34176.66 1194.01 o 9 12 0 468.14 568.26 804.14 o 10 12 0 388.64 -589.41 649.60 o 11 12 0 310.83 -159.42 608.39 o 12 12 0 5661.78 5803.56 831.79 o 13 12 0 490.04 -31.45 981.99 o 1 13 0 816.26 849.42 396.05 o 2 13 0 13933.66 14396.39 836.13 o 3 13 0 188.35 357.88 515.67 o 4 13 0 4676.01 5300.91 734.19 o 5 13 0 18.94 -533.02 533.02 o 6 13 0 1931.13 2067.55 560.13 o 7 13 0 52.81 225.57 786.79 o 8 13 0 941.30 791.12 613.27 o 9 13 0 152.39 952.17 653.40 o 10 13 0 6636.67 8181.27 927.77 o 11 13 0 9.27 -29.28 919.63 o 12 13 0 463.03 1194.01 664.24 o 0 14 0 99.37 383.90 517.29 o 1 14 0 9.44 190.05 356.44 o 2 14 0 1401.61 1339.87 544.95 o 3 14 0 205.61 316.67 437.59 o 4 14 0 3467.57 3269.69 613.27 o 5 14 0 5.43 515.13 568.26 o 6 14 0 503.89 149.66 610.02 o 7 14 0 448.42 -249.97 543.86 o 8 14 0 25.77 219.06 578.02 o 9 14 0 490.85 122.00 543.86 o 10 14 0 548.66 326.97 877.34 o 11 14 0 39.89 -303.11 566.10 o 12 14 0 247.51 481.51 807.39 o 1 15 0 426.82 838.24 394.29 o 2 15 0 13692.22 15790.48 909.87 o 3 15 0 3.87 51.51 525.97 o 4 15 0 2495.07 3914.41 667.49 o 5 15 0 935.52 1712.38 847.52 o 6 15 0 2803.33 4640.46 893.06 o 7 15 0 891.02 734.19 552.00 o 8 15 0 985.90 508.08 641.47 o 9 15 0 107.40 329.68 603.51 o 10 15 0 5258.49 5951.05 919.09 o 11 15 0 385.34 671.83 633.33 o 0 16 0 16762.65 17754.46 1008.56 o 1 16 0 9.67 395.66 444.27 o 2 16 0 2718.90 1826.25 863.78 o 3 16 0 4.01 -386.07 500.48 o 4 16 0 1642.98 3077.20 802.51 o 5 16 0 120.80 987.41 590.50 o 6 16 0 288.59 22.77 609.47 o 7 16 0 130.54 13.56 686.47 o 8 16 0 6823.08 8423.65 856.73 o 9 16 0 202.30 1496.57 688.64 o 1 17 0 31.34 -516.02 853.21 o 2 17 0 1053.51 2812.58 767.81 o 3 17 0 5.79 1063.33 705.99 o 4 17 0 141.20 656.11 581.82 o 5 17 0 30.75 1240.64 674.00 o 6 17 0 287.13 636.59 833.42 o 7 17 0 0.07 -330.76 701.65 o 8 17 0 282.53 344.86 742.86 o 0 18 0 327.33 -384.99 665.87 o 1 18 0 44.86 117.48 577.75 o 2 18 0 52.44 2768.12 773.23 o 3 18 0 19.75 353.54 595.92 o 4 18 0 1439.06 2075.14 711.96 o 5 18 0 3.85 62.90 970.06 o 6 18 0 2.83 -112.24 844.26 o 1 19 0 163.06 402.08 556.52 o 2 19 0 2613.05 1940.12 800.88 o -17 1 1 385.36 717.86 549.01 o -16 1 1 121.76 105.54 377.83 o -15 1 1 12796.48 12432.51 657.23 o -14 1 1 3041.11 3795.62 468.69 o -13 1 1 7185.99 7948.19 544.29 o -12 1 1 7.47 -55.74 436.23 o -11 1 1 1469.09 849.90 315.43 o -10 1 1 16582.91 15948.72 489.27 o -9 1 1 975.89 640.12 611.37 o -8 1 1 2678.27 2266.06 258.99 o -7 1 1 64737.85 63967.00 1111.31 o -6 1 1 12558.21 11804.45 396.10 o -5 1 1 67649.23 66815.56 580.62 o -4 1 1 42279.50 41886.67 424.58 o -3 1 1 21417.24 21341.12 281.79 o -2 1 1 125042.50 119234.25 2038.82 o -1 1 1 26007.53 23710.24 1042.07 o 1 1 1 23276.39 22570.09 275.26 o 2 1 1 128806.28 124947.16 2849.73 o 3 1 1 9723.09 10839.30 294.16 o 4 1 1 94225.16 94783.11 2229.95 o 5 1 1 18419.78 19290.23 391.77 o 6 1 1 37286.35 37572.73 547.55 o 7 1 1 21278.37 21750.82 489.00 o 8 1 1 3399.60 3516.55 311.24 o 9 1 1 14963.37 16431.50 494.01 o 10 1 1 39132.83 41024.76 741.95 o 11 1 1 1630.76 1396.51 364.53 o 12 1 1 64.13 -14.62 325.88 o 13 1 1 5523.88 5643.36 477.54 o 14 1 1 11998.69 11837.54 623.57 o 15 1 1 3081.20 2512.95 545.80 o 16 1 1 49.65 -9.42 397.02 o 17 1 1 375.91 -258.42 602.70 o -17 2 1 5133.13 4785.24 778.65 o -16 2 1 952.52 1792.09 607.85 o -15 2 1 9889.12 9393.17 863.78 o -14 2 1 255.65 707.08 709.25 o -13 2 1 15675.99 15114.31 847.52 o -12 2 1 10866.26 11212.92 688.64 o -11 2 1 6997.69 8157.41 581.28 o -10 2 1 116.69 885.47 384.99 o -9 2 1 8524.14 8676.88 502.65 o -8 2 1 79494.91 80952.73 1136.53 o -7 2 1 7691.61 8761.47 445.18 o -6 2 1 440.48 650.68 245.63 o -5 2 1 122998.54 117788.52 1098.57 o -4 2 1 75102.78 72745.44 795.46 o -3 2 1 282119.53 266598.94 1312.76 o -2 2 1 16047.06 16679.75 336.73 o -1 2 1 7902.53 7285.07 294.98 o 0 2 1 432358.31 357998.50 3009.14 o 1 2 1 8711.79 9120.39 239.40 o 2 2 1 12734.52 13866.63 353.54 o 3 2 1 269991.78 257283.36 1392.46 o 4 2 1 126148.77 128159.88 1113.75 o 5 2 1 72890.28 77818.60 977.11 o 6 2 1 22.72 -105.19 303.11 o 7 2 1 2352.84 2710.64 361.13 o 8 2 1 165838.50 165864.88 1742.75 o 9 2 1 281.18 203.34 355.17 o 10 2 1 3.86 -402.34 402.34 o 11 2 1 742.17 1449.94 509.16 o 12 2 1 32277.51 29223.32 1025.91 o 13 2 1 853.78 1294.86 758.59 o 14 2 1 491.53 663.16 588.33 o 15 2 1 283.06 104.65 627.91 o 16 2 1 8328.15 8645.97 903.91 o 17 2 1 1108.31 604.59 830.16 o -17 3 1 70.92 -616.52 616.52 o -16 3 1 228.23 -195.21 627.91 o -15 3 1 10664.76 11458.55 968.98 o -14 3 1 845.47 440.84 478.25 o -13 3 1 9034.13 10335.58 728.77 o -12 3 1 2427.23 1881.56 550.37 o -11 3 1 377.92 597.00 401.26 o -10 3 1 20001.91 19702.72 738.53 o -9 3 1 681.61 520.55 375.77 o -8 3 1 318.28 547.66 310.70 o -7 3 1 46764.84 46038.63 870.29 o -6 3 1 46621.37 48965.09 838.84 o -5 3 1 81134.25 85311.77 1000.43 o -4 3 1 9977.95 9990.72 386.61 o -3 3 1 3194.88 4232.70 278.71 o -2 3 1 31683.50 30116.93 503.20 o -1 3 1 69589.89 67705.33 470.41 o 0 3 1 2024.06 2059.03 138.61 o 1 3 1 33664.38 34381.75 851.85 o 2 3 1 22326.45 22761.48 471.75 o 3 3 1 387.44 276.54 216.89 o 4 3 1 3308.77 3504.48 306.91 o 5 3 1 105651.35 109645.73 1199.43 o 6 3 1 89709.00 89306.43 1186.41 o 7 3 1 25139.90 25960.14 728.22 o 8 3 1 473.93 828.00 317.21 o 9 3 1 4592.63 5067.75 498.86 o 10 3 1 39595.76 39010.16 1037.84 o 11 3 1 1565.99 1676.60 539.53 o 12 3 1 1319.96 1879.39 781.91 o 13 3 1 3652.07 2941.64 639.30 o 14 3 1 4703.85 4620.94 676.17 o 15 3 1 765.82 1094.78 803.60 o 16 3 1 667.65 1905.42 764.55 o 17 3 1 509.21 861.07 832.88 o -17 4 1 272.77 1493.86 796.55 o -16 4 1 1.14 -394.21 528.14 o -15 4 1 7.36 -455.48 622.49 o -14 4 1 194.04 -18.98 515.67 o -13 4 1 51.39 619.23 483.13 o -12 4 1 430.15 829.08 511.33 o -11 4 1 53.63 1191.84 586.70 o -10 4 1 190.61 150.74 560.67 o -9 4 1 5638.71 5700.54 469.58 o -8 4 1 672.49 619.23 432.71 o -7 4 1 185.16 276.00 303.11 o -6 4 1 2093.16 2183.05 353.54 o -5 4 1 1362.52 1568.69 277.63 o -4 4 1 2969.67 3510.44 306.36 o -3 4 1 7666.29 8562.46 369.26 o -2 4 1 9036.24 9780.33 379.57 o -1 4 1 2102.44 2685.15 187.31 o 0 4 1 953.48 1064.41 227.74 o 1 4 1 544.47 696.48 170.53 o 2 4 1 1594.98 1845.23 278.17 o 3 4 1 2531.11 2981.22 291.18 o 4 4 1 1628.95 1518.26 281.96 o 5 4 1 1867.24 1891.86 325.88 o 6 4 1 2.23 -434.33 434.33 o 7 4 1 1086.00 1506.88 368.72 o 8 4 1 1862.56 1211.90 584.53 o 9 4 1 1173.32 1914.10 482.59 o 10 4 1 8.19 232.08 648.52 o 11 4 1 1433.46 1182.62 702.74 o 12 4 1 2902.40 3592.32 586.70 o 13 4 1 269.59 664.78 555.79 o 14 4 1 0.04 341.07 503.20 o 15 4 1 52.77 54.22 630.08 o 16 4 1 1.63 854.57 656.11 o 17 4 1 3.35 205.51 583.99 o -17 5 1 899.20 986.33 652.31 o -16 5 1 169.60 -39.04 608.39 o -15 5 1 6532.57 6087.69 805.76 o -14 5 1 391.96 746.66 619.78 o -13 5 1 10012.78 9017.40 844.81 o -12 5 1 2944.98 3505.02 595.92 o -11 5 1 1162.09 1094.78 533.02 o -10 5 1 19394.04 19426.18 831.79 o -9 5 1 219.12 286.30 439.75 o -8 5 1 3699.79 4414.89 472.83 o -7 5 1 30454.30 31428.60 828.54 o -6 5 1 42009.95 42837.27 873.54 o -5 5 1 84123.08 83731.16 1127.85 o -4 5 1 1627.06 2652.62 414.27 o -3 5 1 1728.05 1764.98 292.81 o -2 5 1 72501.59 76246.66 916.38 o -1 5 1 7215.30 6622.08 383.09 o 0 5 1 737.84 1060.29 186.25 o 1 5 1 20187.81 19761.26 361.18 o 2 5 1 90841.55 90726.55 1030.25 o 3 5 1 1146.32 1046.52 272.20 o 4 5 1 83.87 450.06 288.47 o 5 5 1 50839.58 52624.64 929.94 o 6 5 1 72074.04 71110.05 1146.29 o 7 5 1 7557.38 7077.82 520.01 o 8 5 1 2161.30 2049.11 460.90 o 9 5 1 2692.07 2517.61 514.58 o 10 5 1 44598.79 44337.09 1172.32 o 11 5 1 423.57 524.34 530.85 o 12 5 1 3808.82 4828.62 728.22 o 13 5 1 997.37 405.05 593.75 o 14 5 1 5130.27 5058.53 781.91 o 15 5 1 866.77 561.22 596.46 o 16 5 1 109.89 1246.06 705.45 o -16 6 1 369.52 1388.67 858.36 o -15 6 1 5388.24 3165.58 1039.47 o -14 6 1 0.30 273.29 553.62 o -13 6 1 5040.68 5871.88 748.29 o -12 6 1 8518.60 8016.43 717.92 o -11 6 1 16658.51 17533.78 874.63 o -10 6 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