Crystal Structure Communications

 

Acta Cryst. (2002). C58, i87-i89  [ doi:10.1107/S0108270102008922 ]

Sodium silver tricobalt bis(diphosphate) and sodium silver copper(II) diphosphate

J. Bennazha, A. Boukhari and E. M. Holt

Synopsis: The title compounds crystallize with Na and Ag sharing sites. The small differences in ionic radii of the two monocations do not lead to significant differences in the structural details. In the latter compound, the Cu atom lies on an inversion center.

Formula: (Na_1.42Ag_0.58)Co₃(P₂O₇)₂ and (Na_1.12Ag_0.88)CuP₂O₇

Online 12 June 2002

 

Acta Cryst. (2002). C58, i90-i91  [ doi:10.1107/S0108270102008107 ]

K₂CsYb(PO₄)₂

L. Rghioui, L. El Ammari, L. Benarafa and J. P. Wignacourt

Synopsis: K₂CsYb(PO₄)₂ crystallizes in the trigonal system in space group Pm1. The structure is built up from regular independent PO₄ tetrahedra and LnO₆ octahedra sharing corners and arranged in layers. The structure is similar to that of glaserite.

Formula: K₂CsYb(PO₄)₂

Online 12 juin 2002

 

Acta Cryst. (2002). C58, i92-i94  [ doi:10.1107/S0108270102008569 ]

Trithallium hydrogen bis(sulfate), Tl₃H(SO₄)₂, in the super-ionic phase by X-ray powder diffraction

Y. Matsuo, S. Kawachi, Y. Shimizu and S. Ikehata

Synopsis: Rietveld refinement shows that the structure of Tl₃H(SO₄)₂ in the super-ionic phase consists of SO₄ tetrahedra, between which Tl atoms are situated. The distortion of the SO₄ tetrahedra in this crystal is less than that in isotypic crystals.

Formula: Tl₃H(SO₄)₂

Online 12 June 2002

 

Acta Cryst. (2002). C58, i95-i97  [ doi:10.1107/S0108270102009253 ]

MgNB₉, a new magnesium nitridoboride

A. Mironov, S. Kazakov, J. Jun and J. Karpinski

Synopsis: The structure of the new magnesium nitridoboride MgNB₉ consists of two layers alternating along the c axis. The NB₆ layer, with B₁₂ icosahedra, has the C₂B₁₃ structure type. Within this layer, boron icosahedra are bonded to N atoms, each coordinating to three boron polyhedra. Another MgB₃ layer, with B₆ octahedra, does not belong to any known structure type. The boron icosahedra and octahedra are connected to each other, thus forming a three-dimensional boron framework.

Formula: MgNB₉

Online 20 June 2002

 

Acta Cryst. (2002). C58, i98-i100  [ doi:10.1107/S010827010200882X ]

Na_1.72Mn_3.28(AsO₄)₃

B. Ayed, M. Krifa and A. Haddad

Synopsis: The structure of sodium manganese arsenate (1.72/3.28/12) is similar to the alluaudite structure type, and consists of a complex network of edge-sharing MnO₆ octahedral chains, linked together by AsO₄ tetrahedra, forming two distinct channels, one containing Na⁺ cations and the other occupied statistically by Mn⁺ and Na⁺ cations.

Formula: Na_1.72Mn_3.28(AsO₄)₃

Online 29 June 2002

 

Acta Cryst. (2002). C58, i101-i102  [ doi:10.1107/S0108270102010351 ]

Germanium(IV) chloride at 193  K

K. Merz and M. Driess

Synopsis: Single crystals of germanium(IV) tetrachloride, GeCl₄, were grown at 193  K. In the crystal structure, the isolated molecules have very well realised tetrahedral geometry.

Formula: GeCl₄

Online 29 June 2002

 

Acta Cryst. (2002). C58, m365-m367  [ doi:10.1107/S0108270102007734 ]

Bis(trimethylphosphine)silver(I) hexafluorophosphate

E. C. Alyea, S. Kannan and P. R. Meehan

Formula: [Ag(C₃H₉P)₂]PF₆

Online 12 June 2002

 

Acta Cryst. (2002). C58, m368-m370  [ doi:10.1107/S010827010200848X ]

(Dibenzyl sulfoxide-O)bis(1,3-diphenylpropane-1,3-dionato-²O,O')dioxouranium(VI)

H.-K. Fun, S. Kannan, A. Usman, I. A. Razak and S. Chantrapromma

Formula: [UO₂(C₁₅H₁₁O₂)₂(C₁₄H₁₄OS)]

Online 12 June 2002

 

Acta Cryst. (2002). C58, m371-m373  [ doi:10.1107/S0108270102009010 ]

Disorder effects in Mn₁₂-acetate at 83  K

A. Cornia, A. C. Fabretti, R. Sessoli, L. Sorace, D. Gatteschi, A.-L. Barra, C. Daiguebonne and T. Roisnel

Formula: [Mn₁₂O₁₂(C₂H₃O₂)₁₆(H₂O)₄]·2C₂H₄O₂·4H₂O

Online 12 June 2002

 

Acta Cryst. (2002). C58, m374-m376  [ doi:10.1107/S0108270102009022 ]

Chlorobis(thiourea-S)copper(I) bis(4,5-diazafluoren-9-one) monohydrate

Z.-Y. Wu, D.-J. Xu, J.-Y. Wu and M. Y. Chiang

Formula: [CuCl(CH₄N₂S)₂]·2C₁₁H₆N₂O·H₂O

Online 12 June 2002

 

Acta Cryst. (2002). C58, m377-m378  [ doi:10.1107/S010827010200865X ]

Di--methoxy-bis[(⁵-cyclopentadienyl)(nitrosyl-N)(trimethylsilylmethyl)molybdenum(II)]

T. W. Hayton, P. Legzdins and S. J. Rettig

Formula: [Mo₂(C₅H₅)₂(CH₃O)₂(C₄H₁₁Si)₂(NO)₂]

Online 12 June 2002

 

Acta Cryst. (2002). C58, m379-m381  [ doi:10.1107/S0108270102008934 ]

GaFPO₃(C₆H₅): a new fluorinated gallium phenylphosphonate with a layered network

T. Loiseau, S. Neeraj and A. K. Cheetham

Synopsis: Fluorinated gallium phenylphosphonate exhibits a layered structure built up from zigzag chains of edge-sharing gallium octahedra, connected to phenylphosphonate groups.

Formula: GaFPO₃(C₆H₅)

Online 12 June 2002

 

Acta Cryst. (2002). C58, m382-m384  [ doi:10.1107/S0108270102009149 ]

-Cyano-1:2²C:N-tetracyano-1⁴C-(5-methyl-5-nitro-3,7-diazanonane-1,9-diamine-2⁴N^1,3,7,9)-nitrosyl-1N-copper(II)iron(II) dihydrate

L. Shen, Y.-J. Zhang, G.-D. Sheng and H.-T. Wang

Formula: [CuFe(CN)₅(C₈H₂₁N₅O₂)(NO)]·2H₂O

Online 20 June 2002

 

Acta Cryst. (2002). C58, m385-m387  [ doi:10.1107/S0108270102009186 ]

[Bis(2-diphenylphosphinoethyl) sulfide-³P,S,P'](triphenylphosphine-P)platinum(II) diperchlorate acetone solvate

L. V. Andreasen, A. Hazell and O. Wernberg

Formula: [Pt(C₁₈H₁₅P)(C₂₈H₂₈P₂S)](ClO₄)₂·C₃H₆O

Online 20 June 2002

 

Acta Cryst. (2002). C58, m388-m389  [ doi:10.1107/S0108270102008764 ]

trans-Bis[O-2,4-di-tert-butylphenyl (4-methoxyphenyl)dithiophosphonato-²S,S']nickel(II)

Y. Özcan, S. Ide, M. Karakus and H. Yilmaz

Formula: [Ni(C₂₁H₂₈O₂PS₂)₂]

Online 20 June 2002

 

Acta Cryst. (2002). C58, m390-m392  [ doi:10.1107/S0108270102009435 ]

Tris[2-(2-oxazolin-2-yl)phenolato]iron(III)

H. Kooijman, A. L. Spek, M. Hoogenraad, E. Bouwman, J. G. Haasnoot and J. Reedijk

Formula: [Fe(C₉H₈NO₂)₃]

Online 20 June 2002

 

Acta Cryst. (2002). C58, m393-m395  [ doi:10.1107/S0108270102009460 ]

A pyrazine bis-adduct of a binuclear rhodium(II) carboxylate containing 3,4,5-triethoxybenzoate as the equatorial ligand

M. A. Castro, Z. D. Chaia, O. E. Piro, F. D. Cukiernik, E. E. Castellano and M. Rusjan

Formula: [Rh₂(C₁₃H₁₇O₅)₄(C₄H₄N₂)₂]

Online 20 June 2002

 

Acta Cryst. (2002). C58, m396-m397  [ doi:10.1107/S0108270102009198 ]

catena-Poly[[[bis(-4,5-dihydrothiazole-2-thiolato)-tetrahedro-tetracopper(I)]-di--4,5-dihydrothiazole-2-thiolato] dihydrate]

J.-M. Du, H.-Y. Zeng, Z.-C. Dong, G.-C. Guo and J.-S. Huang

Formula: [Cu₄(C₃H₄NS₂)₄]·2H₂O

Online 20 June 2002

 

Acta Cryst. (2002). C58, m398-m400  [ doi:10.1107/S0108270102008831 ]

Aquachlorobis[4,4,5,5-tetramethyl-2-(2-pyridyl)-4,5-dihydro-1H-imidazol-1-oxyl 3-oxide-²O¹,N²]nickel(II) nitrate methanol disolvate monohydrate

G. R. Lewis and A. J. Blake

Formula: [NiCl(C₁₂H₁₆N₃O₂)₂(H₂O)]NO₃·2CH₄O·H₂O

Online 20 June 2002

 

Acta Cryst. (2002). C58, m401-m403  [ doi:10.1107/S0108270102009320 ]

Tetraaqua(1,10-phenanthroline-²N,N')manganese(II) sulfate dihydrate

C.-B. Ma, F. Chen, X.-F. Zhang, C.-N. Chen and Q.-T. Liu

Formula: [Mn(C₁₂H₈N₂)(H₂O)₄]SO₄·2H₂O

Online 20 June 2002

 

Acta Cryst. (2002). C58, m404-m406  [ doi:10.1107/S0108270102009642 ]

Bis(tetra-n-butylammonium) di--chloro-bis[(tetramethyl buta-1,3-diene-1,2,3,4-tetracarboxylato-²C¹,C⁴)palladium]

J. Pérez, L. García, J. L. Serrano, E. Pérez, G. Sánchez and J. Vives

Formula: (C₁₆H₃₆N)₂[Pd₂(C₁₂H₁₂O₈)₂Cl₂]

Online 29 June 2002

 

Acta Cryst. (2002). C58, m407-m408  [ doi:10.1107/S0108270102009654 ]

Dabconium orthofluoroberyllate hemihydrate

L. A. Gerrard and M. T. Weller

Formula: (C₆H₁₄N₂)[BeF₄]·0.5H₂O

Online 29 June 2002

 

Acta Cryst. (2002). C58, m409-m412  [ doi:10.1107/S0108270102009885 ]

Ethylenediammonium bis{bis[N-(2-aminoethyl)glycinato-³N,N',O]chromium(III)} tetrachloride dihydrate at 293 and 100 K

J.-H. Choi, T. Suzuki, M. A. Subhan, S. Kaizaki and Y. C. Park

Formula: (C₂H₁₀N₂)[Cr(C₄H₉N₂O₂)₂]₂Cl₄·2H₂O at 293 and 100  K

Online 29 June 2002

 

Acta Cryst. (2002). C58, m413-m417  [ doi:10.1107/S0108270102010375 ]

(4-Nitrophenylsulfanylmethyl)triphenylstannane and (4-nitrophenylsulfonylmethyl)triphenylstannane: R(X) rings (X is 10, 18 or 24) and C-H interactions

J. M. S. Skakle, J. L. Wardell and S. M. S. V. Wardell

Formula: [Sn(C₆H₅)₃(C₇H₆NO₂S)] and [Sn(C₆H₅)₃(C₇H₆NO₄S)]

Online 29 June 2002

 

Acta Cryst. (2002). C58, m418-m420  [ doi:10.1107/S0108270102009745 ]

Losartan potassium, a non-peptide agent for the treatment of arterial hypertension

D. Fernández, D. Vega, J. A. Ellena and G. Echeverría

Formula: K⁺·C₂₂H₂₂ClN₆O^-

Online 29 June 2002

 

Acta Cryst. (2002). C58, m421-m423  [ doi:10.1107/S0108270102009897 ]

Diaquabis(1,3-propanediamine-²N,N')nickel(II) bis(sulfanilate)

C.-H. Kim and S.-G. Lee

Formula: [Ni(C₃H₁₀N₂)₂(H₂O)₂](C₆H₆NO₃S)₂

Online 29 June 2002

 

Acta Cryst. (2002). C58, m424-m426  [ doi:10.1107/S0108270102010053 ]

[2,6-Bis(3,5-dimethylpyrazol-1-ylmethyl)pyridine]iodocopper(I) dichloromethane solvate

M. A. Halcrow and C. A. Kilner

Formula: [CuI(C₁₇H₂₁N₅)]·CH₂Cl₂

Online 29 June 2002

 

Acta Cryst. (2002). C58, o373-o375  [ doi:10.1107/S0108270102008296 ]

4,7-Diiodo-2,1,3-benzothiadiazole and 7,7'-diiodo-4,4'-bi(2,1,3-benzothiadiazole)

M. Tomura, M. Akhtaruzzaman, K. Suzuki and Y. Yamashita

Formula: C₆H₂I₂N₂S and C₁₂H₄I₂N₄S₂

Online 12 June 2002

 

Acta Cryst. (2002). C58, o376-o377  [ doi:10.1107/S0108270102008077 ]

5,11,17,23-Tetra-tert-butyl-25,26,27,28-tetrakis(2-cyanobenzyloxy)-2,8,14,20-tetrathiacalix[4]arene-dichloromethane (1/2)

S.-J. Dong, W.-X. Zhu, D.-Q. Yuan and X. Yan

Formula: C₇₂H₆₈N₄O₄S₄·2CH₂Cl₂

Online 12 June 2002

 

Acta Cryst. (2002). C58, o378-o380  [ doi:10.1107/S0108270102007515 ]

4-Vinylbenzyl analogs of adenine and uracil: reactive monomers for nucleobase polymeric resins

S. G. Srivatsan, S. Verma and M. Parvez

Formula: C₁₄H₁₃N₅ and C₁₃H₁₂N₂O₂

Online 12 June 2002

 

Acta Cryst. (2002). C58, o381-o383  [ doi:10.1107/S0108270102008466 ]

Bis(5-phenyltetrazol-2-yl)methane

A. S. Lyakhov, P. N. Gaponik, Y. V. Grigoriev and L. S. Ivashkevich

Formula: C₁₅H₁₂N₈

Online 12 June 2002

 

Acta Cryst. (2002). C58, o384-o385  [ doi:10.1107/S0108270102008491 ]

2,4,6-Trimethylphenyl isocyanide

M. A. Fernandes, M. Layh and B. Omondi

Formula: C₁₀H₁₁N

Online 12 June 2002

 

Acta Cryst. (2002). C58, o386-o388  [ doi:10.1107/S0108270102008636 ]

1-Substituted derivatives of 2-phenylpyrrolidine-2-carboxamide

R. Tamazyan, H. Karapetyan, A. Martirosyan, V. Hovhannesyan and S. Gasparyan

Formula: C₁₈H₁₇ClN₂O₂ and C₁₆H₁₆N₂O₃

Online 12 June 2002

 

Acta Cryst. (2002). C58, o389-o393  [ doi:10.1107/S0108270102008041 ]

Structural properties of a series of photochromic fluorinated indolylfulgides

M. A. Wolak, R. C. Finn, R. S. Rarig, C. J. Thomas, R. P. Hammond, R. R. Birge, J. Zubieta and W. J. Lees

Formula: Five photochromic fluorinated indolylfulgides

Online 12 June 2002

 

Acta Cryst. (2002). C58, o394-o396  [ doi:10.1107/S0108270102008715 ]

A pipecolic acid (Pip)-containing dipeptide, Boc-D-Ala-L-Pip-NHⁱPr

C. Didierjean, G. Boussard and A. Aubry

Formula: C₁₇H₃₁N₃O₄

Online 12 June 2002

 

Acta Cryst. (2002). C58, o397-o398  [ doi:10.1107/S0108270102008284 ]

Bis(1-naphthyl) ditelluride

E. Schulz Lang, R. A. Burrow and E. T. Silveira

Formula: C₂₀H₁₄Te₂

Online 20 June 2002

 

Acta Cryst. (2002). C58, o399-o401  [ doi:10.1107/S0108270102009241 ]

1-Substituted derivatives of 2-aryl-5-oxopyrrolidine-2-carboxylic acid

H. Karapetyan, R. Tamazyan, A. Martirosyan, V. Hovhannesyan and S. Gasparyan

Formula: C₁₈H₁₈N₂O₂ and C₂₁H₂₂N₂O₂

Online 20 June 2002

 

Acta Cryst. (2002). C58, o402-o404  [ doi:10.1107/S0108270102009393 ]

(+)-3,11-Dioxoandrost-4-ene-17-carboxylic acid: catemeric hydrogen bonding in a steroidal keto acid

J. M. Newman, R. A. Lalancette and H. W. Thompson

Formula: C₂₀H₂₆O₄

Online 20 June 2002

 

Acta Cryst. (2002). C58, o405-o406  [ doi:10.1107/S0108270102008508 ]

A benzopyran derivative substituted at position 3

A. J. Rybarczyk-Pirek, M. Malecka, S. J. Grabowski and J. Nawrot-Modranka

Formula: C₂₃H₁₉N₂O₅P

Online 20 June 2002

 

Acta Cryst. (2002). C58, o407-o408  [ doi:10.1107/S0108270102009629 ]

N-(2-Hydroxyethyl)ethylenediammonium hydrogenphosphate monohydrate

S. Demir, V. T. Yilmaz, O. Andac and W. T. A. Harrison

Formula: C₄H₁₄N₂O²⁺·HPO₄^2-·H₂O

Online 20 June 2002

 

Acta Cryst. (2002). C58, o409-o415  [ doi:10.1107/S0108270102009381 ]

Tetrameric triphenylsilanol, (Ph₃SiOH)₄, and the adduct (Ph₃SiOH)₂-dimethyl sulfoxide, both at 120  K, and the adduct (Ph₃SiOH)₄-1,4-dioxan at 150  K: interplay of O-HO and C-H(arene) interactions

K. F. Bowes, C. Glidewell and J. N. Low

Formula: C₁₈H₁₆OSi, 2C₁₈H₁₆OSi·C₂H₆OS and 4C₁₈H₁₆OSi·C₄H₈O₂

Online 20 June 2002

 

Acta Cryst. (2002). C58, o416-o420  [ doi:10.1107/S0108270102009472 ]

A comparative study of intermolecular interactions in the crystal structures of phenyl/phenyl end-capped oligoanilines

A. Gawlicka-Chruszcz and K. Stadnicka

Formula: C₁₈H₁₄N₂, C₁₈H₁₆N₂ and C₁₈H₁₈N₂²⁺·2C₇H₇O₃S^-

Online 20 June 2002

 

Acta Cryst. (2002). C58, o421-o422  [ doi:10.1107/S0108270102009319 ]

16-(4-Cyanobenzylidene)-3-pyrrolidinoandrost-5-en-17-ol monohydrate

R. Hema, V. Parthasarathi, S. Thamotharan, S. Dubey and D. P. Jindal

Formula: C₃₁H₄₀N₂O·H₂O

Online 20 June 2002

 

Acta Cryst. (2002). C58, o423-o424  [ doi:10.1107/S010827010200937X ]

4,5-Dihydro-3-methyl-5-(4-methylphenyl)-1H-pyrazole-1-carboxamidinium acetate acetone hemisolvate

V. Kettmann and J. Svetlík

Formula: C₁₂H₁₇N₄⁺·C₂H₃O₂^-·0.5C₃H₆O

Online 20 June 2002

 

Acta Cryst. (2002). C58, o425-o427  [ doi:10.1107/S0108270102009575 ]

Ethyl N-(2-benzylamino-6-benzyloxy-5-nitrosopyrimidin-4-yl)glycinate: sheets built from a three-centre N-H(N,O), and two-centre C-HO and C-H(arene) hydrogen bonds

J. N. Low, C. Glidewell, A. Quesada, M. Nogueras and A. Sánchez

Formula: C₂₂H₂₃N₅O₄

Online 20 June 2002

 

Acta Cryst. (2002). C58, o428-o430  [ doi:10.1107/S0108270102008624 ]

N-(2-Iodobenzylidene)-3-nitroaniline: sheets formed by a combination of C-HO hydrogen bonds and two aromatic --stacking interactions

J. L. Wardell, S. M. S. V. Wardell, J. M. S. Skakle, J. N. Low and C. Glidewell

Formula: C₁₃H₉IN₂O₂

Online 29 June 2002

 

Acta Cryst. (2002). C58, o431-o432  [ doi:10.1107/S0108270102009733 ]

3-Amino-1,2,4-triazine

G. J. Perpétuo and J. Janczak

Formula: C₃H₄N₄

Online 29 June 2002

 

Acta Cryst. (2002). C58, o433-o435  [ doi:10.1107/S010827010200968X ]

2-(exo-Tricyclo[5.2.1.0^2,6]deca-4,8-dien-3-endo-yl)acetaldehyde 2,4-dinitrophenylhydrazone

A. Abdul Ajees, N. Palani and K. K. Balasubramanian

Formula: C₁₈H₁₈N₄O₄

Online 29 June 2002

 

Acta Cryst. (2002). C58, o436-o438  [ doi:10.1107/S0108270102010314 ]

N,N-Diethyl-2,6,6-trimethyl-4-(3-nitrophenyl)-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide

A. Linden, C. Safak and E. Kismetli

Formula: C₂₃H₂₉N₃O₄

Online 29 June 2002

 

Acta Cryst. (2002). C58, o439-o441  [ doi:10.1107/S010827010201034X ]

The low-temperature phase of di-tert-butylsilanediol

J. W. Bats, S. Scholz and H.-W. Lerner

Formula: C₈H₂₀O₂Si

Online 29 June 2002

 

Acta Cryst. (2002). C58, o442-o444  [ doi:10.1107/S0108270102010387 ]

4-(Allylamino)-2-amino-6-benzyloxy-5-nitrosopyrimidine from synchrotron data at 150  K: double chains built from N-HN, N-HO, N-H(arene) and aromatic --stacking interactions

E. J. MacLean, J. N. Low, A. Quesada, M. Melguizo, M. Nogueras and C. Glidewell

Formula: C₁₄H₁₅N₅O₂

Online 29 June 2002