Acta Crystallographica Section C

Crystal Structure Communications

Volume 58, Part 7 (July 2002)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: Packing diagram of 4,7-diiodo-2,1,3-benzothiadiazole, viewed along the c axis. Dotted lines show the short S...N and I...I contacts. See Tomura, Akhtaruzzaman, Suzuki & Yamashita [Acta Cryst. (2002), C58, o373-o375].

inorganic compounds


 

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Acta Cryst. (2002). C58, i87-i89  [ doi:10.1107/S0108270102008922 ]

Sodium silver tricobalt bis(diphosphate) and sodium silver copper(II) diphosphate

J. Bennazha, A. Boukhari and E. M. Holt

Synopsis: The title compounds crystallize with Na and Ag sharing sites. The small differences in ionic radii of the two monocations do not lead to significant differences in the structural details. In the latter compound, the Cu atom lies on an inversion center.

Formula: (Na1.42Ag0.58)Co3(P2O7)2 and (Na1.12Ag0.88)CuP2O7

Online 12 June 2002


 

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Acta Cryst. (2002). C58, i90-i91  [ doi:10.1107/S0108270102008107 ]

K2CsYb(PO4)2

L. Rghioui, L. El Ammari, L. Benarafa and J. P. Wignacourt

Synopsis: K2CsYb(PO4)2 crystallizes in the trigonal system in space group P\overline 3m1. The structure is built up from regular independent PO4 tetrahedra and LnO6 octahedra sharing corners and arranged in layers. The structure is similar to that of glaserite.

Formula: K2CsYb(PO4)2

Online 12 juin 2002


 

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Acta Cryst. (2002). C58, i92-i94  [ doi:10.1107/S0108270102008569 ]

Trithallium hydrogen bis(sulfate), Tl3H(SO4)2, in the super-ionic phase by X-ray powder diffraction

Y. Matsuo, S. Kawachi, Y. Shimizu and S. Ikehata

Synopsis: Rietveld refinement shows that the structure of Tl3H(SO4)2 in the super-ionic phase consists of SO4 tetrahedra, between which Tl atoms are situated. The distortion of the SO4 tetrahedra in this crystal is less than that in isotypic crystals.

Formula: Tl3H(SO4)2

Online 12 June 2002


 

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Acta Cryst. (2002). C58, i95-i97  [ doi:10.1107/S0108270102009253 ]

MgNB9, a new magnesium nitridoboride

A. Mironov, S. Kazakov, J. Jun and J. Karpinski

Synopsis: The structure of the new magnesium nitridoboride MgNB9 consists of two layers alternating along the c axis. The NB6 layer, with B12 icosahedra, has the C2B13 structure type. Within this layer, boron icosahedra are bonded to N atoms, each coordinating to three boron polyhedra. Another MgB3 layer, with B6 octahedra, does not belong to any known structure type. The boron icosahedra and octahedra are connected to each other, thus forming a three-dimensional boron framework.

Formula: MgNB9

Online 20 June 2002


 

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Acta Cryst. (2002). C58, i98-i100  [ doi:10.1107/S010827010200882X ]

Na1.72Mn3.28(AsO4)3

B. Ayed, M. Krifa and A. Haddad

Synopsis: The structure of sodium manganese arsenate (1.72/3.28/12) is similar to the alluaudite structure type, and consists of a complex network of edge-sharing MnO6 octahedral chains, linked together by AsO4 tetrahedra, forming two distinct channels, one containing Na+ cations and the other occupied statistically by Mn+ and Na+ cations.

Formula: Na1.72Mn3.28(AsO4)3

Online 29 June 2002


 

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Acta Cryst. (2002). C58, i101-i102  [ doi:10.1107/S0108270102010351 ]

Germanium(IV) chloride at 193 K

K. Merz and M. Driess

Synopsis: Single crystals of germanium(IV) tetrachloride, GeCl4, were grown at 193 K. In the crystal structure, the isolated molecules have very well realised tetrahedral geometry.

Formula: GeCl4

Online 29 June 2002


metal-organic compounds


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Acta Cryst. (2002). C58, m365-m367  [ doi:10.1107/S0108270102007734 ]

Bis(trimethylphosphine)silver(I) hexafluorophosphate

E. C. Alyea, S. Kannan and P. R. Meehan

Formula: [Ag(C3H9P)2]PF6

Online 12 June 2002


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Acta Cryst. (2002). C58, m368-m370  [ doi:10.1107/S010827010200848X ]

(Dibenzyl sulfoxide-[kappa]O)bis(1,3-diphenylpropane-1,3-dionato-[kappa]2O,O')dioxouranium(VI)

H.-K. Fun, S. Kannan, A. Usman, I. A. Razak and S. Chantrapromma

Formula: [UO2(C15H11O2)2(C14H14OS)]

Online 12 June 2002


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Acta Cryst. (2002). C58, m371-m373  [ doi:10.1107/S0108270102009010 ]

Disorder effects in Mn12-acetate at 83 K

A. Cornia, A. C. Fabretti, R. Sessoli, L. Sorace, D. Gatteschi, A.-L. Barra, C. Daiguebonne and T. Roisnel

Formula: [Mn12O12(C2H3O2)16(H2O)4]·2C2H4O2·4H2O

Online 12 June 2002


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Acta Cryst. (2002). C58, m374-m376  [ doi:10.1107/S0108270102009022 ]

Chlorobis(thiourea-[kappa]S)copper(I) bis(4,5-diazafluoren-9-one) monohydrate

Z.-Y. Wu, D.-J. Xu, J.-Y. Wu and M. Y. Chiang

Formula: [CuCl(CH4N2S)2]·2C11H6N2O·H2O

Online 12 June 2002


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Acta Cryst. (2002). C58, m377-m378  [ doi:10.1107/S010827010200865X ]

Di-[mu]-methoxy-bis[([eta]5-cyclopentadienyl)(nitrosyl-[kappa]N)(trimethylsilylmethyl)molybdenum(II)]

T. W. Hayton, P. Legzdins and S. J. Rettig

Formula: [Mo2(C5H5)2(CH3O)2(C4H11Si)2(NO)2]

Online 12 June 2002


 

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Acta Cryst. (2002). C58, m379-m381  [ doi:10.1107/S0108270102008934 ]

GaFPO3(C6H5): a new fluorinated gallium phenylphosphonate with a layered network

T. Loiseau, S. Neeraj and A. K. Cheetham

Synopsis: Fluorinated gallium phenylphosphonate exhibits a layered structure built up from zigzag chains of edge-sharing gallium octahedra, connected to phenylphosphonate groups.

Formula: GaFPO3(C6H5)

Online 12 June 2002


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Acta Cryst. (2002). C58, m382-m384  [ doi:10.1107/S0108270102009149 ]

[mu]-Cyano-1:2[kappa]2C:N-tetracyano-1[kappa]4C-(5-methyl-5-nitro-3,7-diazanonane-1,9-diamine-2[kappa]4N1,3,7,9)-nitrosyl-1[kappa]N-copper(II)iron(II) dihydrate

L. Shen, Y.-J. Zhang, G.-D. Sheng and H.-T. Wang

Formula: [CuFe(CN)5(C8H21N5O2)(NO)]·2H2O

Online 20 June 2002


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Acta Cryst. (2002). C58, m385-m387  [ doi:10.1107/S0108270102009186 ]

[Bis(2-diphenylphosphinoethyl) sulfide-[kappa]3P,S,P'](triphenylphosphine-[kappa]P)platinum(II) diperchlorate acetone solvate

L. V. Andreasen, A. Hazell and O. Wernberg

Formula: [Pt(C18H15P)(C28H28P2S)](ClO4)2·C3H6O

Online 20 June 2002


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Acta Cryst. (2002). C58, m388-m389  [ doi:10.1107/S0108270102008764 ]

trans-Bis[O-2,4-di-tert-butylphenyl (4-methoxyphenyl)dithiophosphonato-[kappa]2S,S']nickel(II)

Y. Özcan, S. Ide, M. Karakus and H. Yilmaz

Formula: [Ni(C21H28O2PS2)2]

Online 20 June 2002


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Acta Cryst. (2002). C58, m390-m392  [ doi:10.1107/S0108270102009435 ]

Tris[2-(2-oxazolin-2-yl)phenolato]iron(III)

H. Kooijman, A. L. Spek, M. Hoogenraad, E. Bouwman, J. G. Haasnoot and J. Reedijk

Formula: [Fe(C9H8NO2)3]

Online 20 June 2002


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Acta Cryst. (2002). C58, m393-m395  [ doi:10.1107/S0108270102009460 ]

A pyrazine bis-adduct of a binuclear rhodium(II) carboxylate containing 3,4,5-triethoxybenzoate as the equatorial ligand

M. A. Castro, Z. D. Chaia, O. E. Piro, F. D. Cukiernik, E. E. Castellano and M. Rusjan

Formula: [Rh2(C13H17O5)4(C4H4N2)2]

Online 20 June 2002


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Acta Cryst. (2002). C58, m396-m397  [ doi:10.1107/S0108270102009198 ]

catena-Poly[[[bis([mu]-4,5-dihydrothiazole-2-thiolato)-tetrahedro-tetracopper(I)]-di-[mu]-4,5-dihydrothiazole-2-thiolato] dihydrate]

J.-M. Du, H.-Y. Zeng, Z.-C. Dong, G.-C. Guo and J.-S. Huang

Formula: [Cu4(C3H4NS2)4]·2H2O

Online 20 June 2002


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Acta Cryst. (2002). C58, m398-m400  [ doi:10.1107/S0108270102008831 ]

Aquachlorobis[4,4,5,5-tetramethyl-2-(2-pyridyl)-4,5-dihydro-1H-imidazol-1-oxyl 3-oxide-[kappa]2O1,N2]nickel(II) nitrate methanol disolvate monohydrate

G. R. Lewis and A. J. Blake

Formula: [NiCl(C12H16N3O2)2(H2O)]NO3·2CH4O·H2O

Online 20 June 2002


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Acta Cryst. (2002). C58, m401-m403  [ doi:10.1107/S0108270102009320 ]

Tetraaqua(1,10-phenanthroline-[kappa]2N,N')manganese(II) sulfate dihydrate

C.-B. Ma, F. Chen, X.-F. Zhang, C.-N. Chen and Q.-T. Liu

Formula: [Mn(C12H8N2)(H2O)4]SO4·2H2O

Online 20 June 2002


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Acta Cryst. (2002). C58, m404-m406  [ doi:10.1107/S0108270102009642 ]

Bis(tetra-n-butylammonium) di-[mu]-chloro-bis[(tetramethyl buta-1,3-diene-1,2,3,4-tetracarboxylato-[kappa]2C1,C4)palladium]

J. Pérez, L. García, J. L. Serrano, E. Pérez, G. Sánchez and J. Vives

Formula: (C16H36N)2[Pd2(C12H12O8)2Cl2]

Online 29 June 2002


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Acta Cryst. (2002). C58, m407-m408  [ doi:10.1107/S0108270102009654 ]

Dabconium orthofluoroberyllate hemihydrate

L. A. Gerrard and M. T. Weller

Formula: (C6H14N2)[BeF4]·0.5H2O

Online 29 June 2002


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Acta Cryst. (2002). C58, m409-m412  [ doi:10.1107/S0108270102009885 ]

Ethylenediammonium bis{bis[N-(2-aminoethyl)glycinato-[kappa]3N,N',O]chromium(III)} tetrachloride dihydrate at 293 and 100 K

J.-H. Choi, T. Suzuki, M. A. Subhan, S. Kaizaki and Y. C. Park

Formula: (C2H10N2)[Cr(C4H9N2O2)2]2Cl4·2H2O at 293 and 100 K

Online 29 June 2002


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Acta Cryst. (2002). C58, m413-m417  [ doi:10.1107/S0108270102010375 ]

(4-Nitrophenylsulfanylmethyl)triphenylstannane and (4-nitrophenylsulfonylmethyl)triphenylstannane: R\bf{_2^2}(X) rings (X is 10, 18 or 24) and C-H...[pi] interactions

J. M. S. Skakle, J. L. Wardell and S. M. S. V. Wardell

Formula: [Sn(C6H5)3(C7H6NO2S)] and [Sn(C6H5)3(C7H6NO4S)]

Online 29 June 2002


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Acta Cryst. (2002). C58, m418-m420  [ doi:10.1107/S0108270102009745 ]

Losartan potassium, a non-peptide agent for the treatment of arterial hypertension

D. Fernández, D. Vega, J. A. Ellena and G. Echeverría

Formula: K+·C22H22ClN6O-

Online 29 June 2002


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Acta Cryst. (2002). C58, m421-m423  [ doi:10.1107/S0108270102009897 ]

Diaquabis(1,3-propanediamine-[kappa]2N,N')nickel(II) bis(sulfanilate)

C.-H. Kim and S.-G. Lee

Formula: [Ni(C3H10N2)2(H2O)2](C6H6NO3S)2

Online 29 June 2002


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Acta Cryst. (2002). C58, m424-m426  [ doi:10.1107/S0108270102010053 ]

[2,6-Bis(3,5-dimethylpyrazol-1-ylmethyl)pyridine]iodocopper(I) dichloromethane solvate

M. A. Halcrow and C. A. Kilner

Formula: [CuI(C17H21N5)]·CH2Cl2

Online 29 June 2002


organic compounds


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Acta Cryst. (2002). C58, o373-o375  [ doi:10.1107/S0108270102008296 ]

4,7-Diiodo-2,1,3-benzothiadiazole and 7,7'-diiodo-4,4'-bi(2,1,3-benzothiadiazole)

M. Tomura, M. Akhtaruzzaman, K. Suzuki and Y. Yamashita

Formula: C6H2I2N2S and C12H4I2N4S2

Online 12 June 2002


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Acta Cryst. (2002). C58, o376-o377  [ doi:10.1107/S0108270102008077 ]

5,11,17,23-Tetra-tert-butyl-25,26,27,28-tetrakis(2-cyanobenzyloxy)-2,8,14,20-tetrathiacalix[4]arene-dichloromethane (1/2)

S.-J. Dong, W.-X. Zhu, D.-Q. Yuan and X. Yan

Formula: C72H68N4O4S4·2CH2Cl2

Online 12 June 2002


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Acta Cryst. (2002). C58, o378-o380  [ doi:10.1107/S0108270102007515 ]

4-Vinylbenzyl analogs of adenine and uracil: reactive monomers for nucleobase polymeric resins

S. G. Srivatsan, S. Verma and M. Parvez

Formula: C14H13N5 and C13H12N2O2

Online 12 June 2002


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Acta Cryst. (2002). C58, o381-o383  [ doi:10.1107/S0108270102008466 ]

Bis(5-phenyltetrazol-2-yl)methane

A. S. Lyakhov, P. N. Gaponik, Y. V. Grigoriev and L. S. Ivashkevich

Formula: C15H12N8

Online 12 June 2002


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Acta Cryst. (2002). C58, o384-o385  [ doi:10.1107/S0108270102008491 ]

2,4,6-Trimethylphenyl isocyanide

M. A. Fernandes, M. Layh and B. Omondi

Formula: C10H11N

Online 12 June 2002


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Acta Cryst. (2002). C58, o386-o388  [ doi:10.1107/S0108270102008636 ]

1-Substituted derivatives of 2-phenylpyrrolidine-2-carboxamide

R. Tamazyan, H. Karapetyan, A. Martirosyan, V. Hovhannesyan and S. Gasparyan

Formula: C18H17ClN2O2 and C16H16N2O3

Online 12 June 2002


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Acta Cryst. (2002). C58, o389-o393  [ doi:10.1107/S0108270102008041 ]

Structural properties of a series of photochromic fluorinated indolylfulgides

M. A. Wolak, R. C. Finn, R. S. Rarig, C. J. Thomas, R. P. Hammond, R. R. Birge, J. Zubieta and W. J. Lees

Formula: Five photochromic fluorinated indolylfulgides

Online 12 June 2002


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Acta Cryst. (2002). C58, o394-o396  [ doi:10.1107/S0108270102008715 ]

A pipecolic acid (Pip)-containing dipeptide, Boc-D-Ala-L-Pip-NHiPr

C. Didierjean, G. Boussard and A. Aubry

Formula: C17H31N3O4

Online 12 June 2002


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Acta Cryst. (2002). C58, o397-o398  [ doi:10.1107/S0108270102008284 ]

Bis(1-naphthyl) ditelluride

E. Schulz Lang, R. A. Burrow and E. T. Silveira

Formula: C20H14Te2

Online 20 June 2002


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Acta Cryst. (2002). C58, o399-o401  [ doi:10.1107/S0108270102009241 ]

1-Substituted derivatives of 2-aryl-5-oxopyrrolidine-2-carboxylic acid

H. Karapetyan, R. Tamazyan, A. Martirosyan, V. Hovhannesyan and S. Gasparyan

Formula: C18H18N2O2 and C21H22N2O2

Online 20 June 2002


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Acta Cryst. (2002). C58, o402-o404  [ doi:10.1107/S0108270102009393 ]

(+)-3,11-Dioxoandrost-4-ene-17[beta]-carboxylic acid: catemeric hydrogen bonding in a steroidal keto acid

J. M. Newman, R. A. Lalancette and H. W. Thompson

Formula: C20H26O4

Online 20 June 2002


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Acta Cryst. (2002). C58, o405-o406  [ doi:10.1107/S0108270102008508 ]

A benzopyran derivative substituted at position 3

A. J. Rybarczyk-Pirek, M. Malecka, S. J. Grabowski and J. Nawrot-Modranka

Formula: C23H19N2O5P

Online 20 June 2002


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Acta Cryst. (2002). C58, o407-o408  [ doi:10.1107/S0108270102009629 ]

N-(2-Hydroxyethyl)ethylenediammonium hydrogenphosphate monohydrate

S. Demir, V. T. Yilmaz, O. Andac and W. T. A. Harrison

Formula: C4H14N2O2+·HPO42-·H2O

Online 20 June 2002


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Acta Cryst. (2002). C58, o409-o415  [ doi:10.1107/S0108270102009381 ]

Tetrameric triphenylsilanol, (Ph3SiOH)4, and the adduct (Ph3SiOH)2-dimethyl sulfoxide, both at 120 K, and the adduct (Ph3SiOH)4-1,4-dioxan at 150 K: interplay of O-H...O and C-H...[pi](arene) interactions

K. F. Bowes, C. Glidewell and J. N. Low

Formula: C18H16OSi, 2C18H16OSi·C2H6OS and 4C18H16OSi·C4H8O2

Online 20 June 2002


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Acta Cryst. (2002). C58, o416-o420  [ doi:10.1107/S0108270102009472 ]

A comparative study of intermolecular interactions in the crystal structures of phenyl/phenyl end-capped oligoanilines

A. Gawlicka-Chruszcz and K. Stadnicka

Formula: C18H14N2, C18H16N2 and C18H18N22+·2C7H7O3S-

Online 20 June 2002


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Acta Cryst. (2002). C58, o421-o422  [ doi:10.1107/S0108270102009319 ]

16-(4-Cyanobenzylidene)-3[beta]-pyrrolidinoandrost-5-en-17[beta]-ol monohydrate

R. Hema, V. Parthasarathi, S. Thamotharan, S. Dubey and D. P. Jindal

Formula: C31H40N2O·H2O

Online 20 June 2002


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Acta Cryst. (2002). C58, o423-o424  [ doi:10.1107/S010827010200937X ]

4,5-Dihydro-3-methyl-5-(4-methylphenyl)-1H-pyrazole-1-carboxamidinium acetate acetone hemisolvate

V. Kettmann and J. Svetlík

Formula: C12H17N4+·C2H3O2-·0.5C3H6O

Online 20 June 2002


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Acta Cryst. (2002). C58, o425-o427  [ doi:10.1107/S0108270102009575 ]

Ethyl N-(2-benzylamino-6-benzyloxy-5-nitrosopyrimidin-4-yl)glycinate: sheets built from a three-centre N-H...(N,O), and two-centre C-H...O and C-H...[pi](arene) hydrogen bonds

J. N. Low, C. Glidewell, A. Quesada, M. Nogueras and A. Sánchez

Formula: C22H23N5O4

Online 20 June 2002


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Acta Cryst. (2002). C58, o428-o430  [ doi:10.1107/S0108270102008624 ]

N-(2-Iodobenzylidene)-3-nitroaniline: sheets formed by a combination of C-H...O hydrogen bonds and two aromatic [pi]-[pi]-stacking interactions

J. L. Wardell, S. M. S. V. Wardell, J. M. S. Skakle, J. N. Low and C. Glidewell

Formula: C13H9IN2O2

Online 29 June 2002


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Acta Cryst. (2002). C58, o431-o432  [ doi:10.1107/S0108270102009733 ]

3-Amino-1,2,4-triazine

G. J. Perpétuo and J. Janczak

Formula: C3H4N4

Online 29 June 2002


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Acta Cryst. (2002). C58, o433-o435  [ doi:10.1107/S010827010200968X ]

2-(exo-Tricyclo[5.2.1.02,6]deca-4,8-dien-3-endo-yl)acetaldehyde 2,4-dinitrophenylhydrazone

A. Abdul Ajees, N. Palani and K. K. Balasubramanian

Formula: C18H18N4O4

Online 29 June 2002


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Acta Cryst. (2002). C58, o436-o438  [ doi:10.1107/S0108270102010314 ]

N,N-Diethyl-2,6,6-trimethyl-4-(3-nitrophenyl)-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide

A. Linden, C. Safak and E. Kismetli

Formula: C23H29N3O4

Online 29 June 2002


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Acta Cryst. (2002). C58, o439-o441  [ doi:10.1107/S010827010201034X ]

The low-temperature phase of di-tert-butylsilanediol

J. W. Bats, S. Scholz and H.-W. Lerner

Formula: C8H20O2Si

Online 29 June 2002


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Acta Cryst. (2002). C58, o442-o444  [ doi:10.1107/S0108270102010387 ]

4-(Allylamino)-2-amino-6-benzyloxy-5-nitrosopyrimidine from synchrotron data at 150 K: double chains built from N-H...N, N-H...O, N-H...[pi](arene) and aromatic [pi]-[pi]-stacking interactions

E. J. MacLean, J. N. Low, A. Quesada, M. Melguizo, M. Nogueras and C. Glidewell

Formula: C14H15N5O2

Online 29 June 2002


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