Acta Crystallographica Section C

Crystal Structure Communications

Volume 58, Part 8 (August 2002)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The hydrogen-bonded layer perpendicular to the Fe-Odioxane vector in the polymer chains of catena-poly[[diaquadichloroiron(II)]-[mu]-1,4-dioxane-[kappa]2O:O']. See Speer Jr & Pinkerton [Acta Cryst. (2002), C58, m441-m442].

inorganic compounds


 

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Acta Cryst. (2002). C58, i103-i105  [ doi:10.1107/S0108270102010600 ]

Rb(GaPO4)2(OH)(H2O)·H2O: a hydrated rubidium gallium phosphate analogue of GaPO4·2H2O and leucophosphite

L. Beitone, T. Loiseau and G. Ferey

Synopsis: Rb(GaPO4)2(OH)(H2O)·H2O exhibits a three-dimensional framework with intersecting eight-ring channels, in which the alkali cations and the water molecule are encapsulated. This network belongs to the leucophosphite structural type.

Formula: Rb(GaPO4)2(OH)(H2O)·H2O

Online 12 July 2002


 

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Acta Cryst. (2002). C58, i106-i108  [ doi:10.1107/S0108270102007886 ]

KMo5O13 and KNb1.76Sb3.24O13

M. M. Ftini, M. Krifa and H. Amor

Synopsis: The title compounds are isotypic. KMo5O13 has a three-dimensional tunnel built by the corner-sharing of MoO6 octahedra; K+ cations are located in the tunnels. In KNb1.76Sb3.24O13, the Nb and Sb atoms occupy the same sites.

Formula: KMo5O13 and KNb1.76Sb3.24O13

Online 20 July 2002


 

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Acta Cryst. (2002). C58, i109-i110  [ doi:10.1107/S0108270102009873 ]

Heptairon bis(phosphate) tetrakis(hydrogenphosphate)

B.-C. Zhou, Y.-W. Yao and R.-J. Wang

Synopsis: Fe7(PO4)2(HPO4)4 is isostructural with Mn7(PO4)2(HPO4)4 and Co7(PO4)2(HPO4)4. The structure is based on a framework of edge- and corner-sharing FeO6, Fe5 and PO4 polyhedra, isotypic with that found in the mixed-valence iron phosphate Fe7(PO4)6. The Fe atoms are purely in the divalent state, just like the Co atoms in Co7(PO4)2(HPO4)4, the necessary charge balance being maintained by the addition of H atoms in the form of bridging Fe-OH-P groups.

Formula: Fe7(PO4)2(HPO4)4

Online 31 July 2002


metal-organic compounds


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Acta Cryst. (2002). C58, m427-m430  [ doi:10.1107/S0108270102010491 ]

Bis(2-pyridylmethanol)bis(saccharinato)zinc(II) and -cadmium(II) at 120 K: three-dimensional structures containing both N-and O-coordinated ambidentate saccharinate ligands

V. T. Yilmaz, S. Guney, O. Andac and W. T. A. Harrison

Formula: [Zn(C7H4NO3S)2(C6H7NO)2] and [Cd(C7H4NO3S)2(C6H7NO)2]

Online 12 July 2002


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Acta Cryst. (2002). C58, m431-m433  [ doi:10.1107/S0108270102010430 ]

Bis(tetra-n-butylammonium) bis([mu]-1,2-dicyanoethene-1,2-dithiolato-[kappa]3S,S':S')bis[(1,2-dicyanoethene-1,2-dithiolato-[kappa]2S,S')cobalt(III)]

T. Mochida, K. Takazawa, M. M. Matsushita and T. Sugawara

Formula: (C16H36N)2[Co(C4N2S2)2]2

Online 12 July 2002


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Acta Cryst. (2002). C58, m434-m435  [ doi:10.1107/S0108270102009939 ]

Aquachlorobis(4,4',4''-tri-tert-butyl-2,2';6',2''-terpyridine-[kappa]3N)terbium(III) diperchlorate ethanol disolvate

H.-R. Mürner, R. Scopelliti and J.-C.G. Bünzli

Formula: [TbCl(C27H35N3)2(H2O)](ClO4)2·2C2H6O

Online 12 July 2002


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Acta Cryst. (2002). C58, m436-m438  [ doi:10.1107/S0108270102010764 ]

Tetra-n-butylammonium bis(2-thioxo-1,3-dithiole-4,5-dithiolato-[kappa]2S4,S5)nickelate(III)

G.-Q. Liu, G. Xue, W.-T. Yu and W. Xu

Formula: (C16H36N)[Ni(C3S5)2]

Online 12 July 2002


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Acta Cryst. (2002). C58, m439-m440  [ doi:10.1107/S0108270102010636 ]

Tetraphenylarsonium tetraiodothallate(III)

A. Linden and B. D. James

Formula: (C24H20As)[TlI4]

Online 12 July 2002


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Acta Cryst. (2002). C58, m441-m442  [ doi:10.1107/S0108270102010508 ]

catena-Poly[[diaquadichloroiron(II)]-[mu]-1,4-dioxane-[kappa]2O:O']

R. L. Speer and A. A. Pinkerton

Formula: [FeCl2(C4H8O2)(H2O)2]

Online 12 July 2002


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Acta Cryst. (2002). C58, m443-m444  [ doi:10.1107/S0108270102011605 ]

(5,10,15,20-Tetraphenylporphyrinato-[kappa]4N)bis(L-valine-[kappa]N methyl ester)iron(III) trifluoromethylsulfonate dichloromethane solvate

M. Kobeissi, L. Toupet and G. Simonneaux

Formula: [Fe(C44H28N4)(C6H13NO2)2](CF3O3S)·CH2Cl2

Online 20 July 2002


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Acta Cryst. (2002). C58, m445-m446  [ doi:10.1107/S010827010201154X ]

Bis[[mu]-3{5}-(2-pyridyl)pyrazolido]bis[(acetonitrile)copper(II)] diperchlorate

M. J. Hallam, C. A. Kilner and M. A. Halcrow

Formula: [Cu2(C8H6N3)2(C2H3N)2](ClO4)2

Online 20 July 2002


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Acta Cryst. (2002). C58, m447-m449  [ doi:10.1107/S0108270102011307 ]

Bis{[diphenyl(piperidinomethyl)silyl]methyl}cadmium and -magnesium

C. Strohmann and D. Schildbach

Formula: [Cd(C19H24NSi)2] and [Mg(C19H24NSi)2]

Online 20 July 2002


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Acta Cryst. (2002). C58, m450-m452  [ doi:10.1107/S010827010201123X ]

Methyl 2,3-dideoxy-2-S-methylmercurio-2-thio-[beta]-D-manno-oct-2-ulopyranosonate-(2,6)

V. Belakhov, M. Botoshansky and T. Baasov

Formula: [Hg(CH3)(C9H15O7S)]

Online 20 July 2002


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Acta Cryst. (2002). C58, m453-m454  [ doi:10.1107/S0108270102011988 ]

Dibromo[(-)-sparteine-[kappa]2N,N']zinc(II)

Y.-M. Lee, S. K. Kang, Y.-I. Kim and S.-N. Choi

Formula: [ZnBr2(C15H26N2)]

Online 31 July 2002


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Acta Cryst. (2002). C58, m455-m458  [ doi:10.1107/S0108270102012404 ]

Bis(1,10-phenanthroline)(thiosulfato)manganese(II) methanol solvate and catena-poly[[diaqua(2,9-dimethyl-1,10-phenanthroline)manganese(II)]-[mu]-thiosulfato]

E. Freire, S. Baggio, J. C. Muñoz and R. Baggio

Formula: [Mn(S2O3)(C12H8N2)2]·CH4O and [Mn(S2O3)(C14H12N2)(H2O)2]

Online 31 July 2002


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Acta Cryst. (2002). C58, m459-m460  [ doi:10.1107/S0108270102011423 ]

The mononuclear cobalt(II) complex CoII(DMBDIZ)2(NCS)2, where DMBDIZ is 2,6-dimethylbenzo[1,2-d:4,5-d']diimidazole

C.-X. Cai, Y.-Q. Tian, Y.-Z. Li and X.-Z. You

Formula: [Co(NCS)2(C10H10N4)2]

Online 31 July 2002


organic compounds


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Acta Cryst. (2002). C58, o445-o446  [ doi:10.1107/S0108270102010247 ]

2'-Hydroxy-4''-dimethylaminochalcone

Z.-Q. Liu, Q. Fang, W.-T. Yu, G. Xue, D.-X. Cao and M.-H. Jiang

Formula: C17H17NO2

Online 12 July 2002


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Acta Cryst. (2002). C58, o447-o449  [ doi:10.1107/S0108270102007503 ]

Two (E,E)- and (Z,E)-thiazol-5-ylpenta-2,4-dienones

L. Breydo, C. L. Barnes and K. S. Gates

Formula: C16H22N2O4S and C14H16N2O3S

Online 12 July 2002


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Acta Cryst. (2002). C58, o450-o454  [ doi:10.1107/S0108270102009587 ]

Diethyl {3-[[beta]-(2,4-dichlorophenyl)vinyl]-N-(phenylsulfonyl)indol-2-ylmethyl}phosphonate and diethyl {3-[[beta]-(4-bromophenyl)vinyl]-N-(phenylsulfonyl)indol-2-ylmethyl}phosphonate

K. Sethu Sankar, S. Kannadasan, D. Velmurugan, P. C. Srinivasan and J.-K. Moon

Formula: C27H26Cl2NO5PS and C27H27BrNO5PS

Online 12 July 2002


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Acta Cryst. (2002). C58, o455-o459  [ doi:10.1107/S0108270102010521 ]

Hexakis(melaminium) tetrakis(dihydrogenphosphate) monohydrogenphosphate tetrahydrate

J. Janczak and G. J. Perpétuo

Formula: 6C3H7N6+·4H2PO4-·HPO42-·4H2O

Online 12 July 2002


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Acta Cryst. (2002). C58, o460-o462  [ doi:10.1107/S0108270102010399 ]

9-(Trichloroacetylimino)acridine monohydrate

J. Meszko, K. Krzyminski, A. Konitz and J. Blazejowski

Formula: C15H9Cl3N2O·H2O

Online 12 July 2002


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Acta Cryst. (2002). C58, o463-o466  [ doi:10.1107/S0108270102010776 ]

2,6-Diiodo-4-nitrophenol, 2,6-diiodo-4-nitrophenyl acetate and 2,6-diiodo-4-nitroanisole: interplay of hydrogen bonds, iodo-nitro interactions and aromatic [pi]-[pi]-stacking interactions to give supramolecular structures in one, two and three dimensions

S. J. Garden, F. R. da Cunha, J. L. Wardell, J. M. S. Skakle, J. N. Low and C. Glidewell

Formula: C6H3I2NO3, C8H5I2NO4 and C7H5I2NO3

Online 12 July 2002


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Acta Cryst. (2002). C58, o467-o469  [ doi:10.1107/S0108270102010648 ]

Self-assembled hydrogen-bonded bilayers in 1,4-diazabicyclo[2.2.2]octane-N-(phosphonomethyl)iminodiacetic acid-water (1/1/1.5)

K. F. Bowes, G. Ferguson, C. Glidewell and A. J. Lough

Formula: C6H14N22+·C5H8NO7P2-·1.5H2O

Online 12 July 2002


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Acta Cryst. (2002). C58, o470-o473  [ doi:10.1107/S0108270102010958 ]

The salt-type 1:2 adduct of meso-5,5,7,12,12,14-hexa-C-methyl-1,4,8,11-tetraazacyclotetradecane (tet-a) and 5-nitroisophthalic acid forms a hydrogen-bonded sheet structure containing two configurational isomers of [(tet-a)H2]2+

E. J. MacLean, S. J. Teat, D. M. M. Farrell, G. Ferguson and C. Glidewell

Formula: C16H38N4+·2C8H4NO6-

Online 12 July 2002


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Acta Cryst. (2002). C58, o474-o476  [ doi:10.1107/S0108270102010843 ]

(1SR,2RS,5RS,6SR,8RS)-7,7-Dimethyltricyclo[6.2.1.01,6]undecane-2,5,6-triol: a supramolecular framework built from O-H...O hydrogen bonds

S. Mondal, M. Mukherjee, A. Roy, D. Mukherjee and M. Helliwell

Formula: C13H22O3

Online 12 July 2002


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Acta Cryst. (2002). C58, o477-o479  [ doi:10.1107/S0108270102011083 ]

11-Methyl-12a-phenyl-9a,12a-dihydrophenanthro[9',10':5,6][1,4]dioxino[2,3-d]oxazole and 9a-(10-hydroxyphenanthren-9-yl)-11,12a-diphenyl-9a,12a-dihydrophenanthro[9',10':5,6][1,4]dioxino[2,3-d]oxazole

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Zhang and J.-H. Xu

Formula: C24H17NO3 and C43H27NO5

Online 12 July 2002


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Acta Cryst. (2002). C58, o480-o484  [ doi:10.1107/S0108270102011319 ]

Four bis(1-chloro-2,2,4,4-tetramethyl-3-oxocyclobutan-1-yl)oligosulfanes

A. Linden, A. Majchrzak, J. Cavegn, G. Mloston and H. Heimgartner

Formula: C16H24Cl2O2S2, C16H24Cl2O2S3, C16H24Cl2O2S4 and C16H24Cl2O2S6

Online 20 July 2002


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Acta Cryst. (2002). C58, o485-o486  [ doi:10.1107/S0108270102011344 ]

2-Nitrophenyl 4-nitrophenyl disulfide

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C12H8N2O4S2

Online 20 July 2002


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Acta Cryst. (2002). C58, o487-o490  [ doi:10.1107/S010827010201140X ]

2-Iodo-N-(3-nitrobenzyl)aniline and 3-iodo-N-(3-nitrobenzyl)aniline exhibit entirely different patterns of supramolecular aggregation

C. Glidewell, J. N. Low, J. M. S. Skakle, S. M. S. V. Wardell and J. L. Wardell

Formula: Two isomers of C13H11IN2O2

Online 20 July 2002


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Acta Cryst. (2002). C58, o491-o493  [ doi:10.1107/S0108270102011526 ]

(±)-(2,3,4,4a,5,6,7,8-Octahydro-2-oxonaphthalen-1-yl)acetic acid: hydrogen-bonding pattern of the monohydrate of an unsaturated bicyclic [gamma]-keto acid

R. A. Lalancette, A. P. J. Brunskill and H. W. Thompson

Formula: C12H16O3·H2O

Online 20 July 2002


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Acta Cryst. (2002). C58, o494-o495  [ doi:10.1107/S0108270102012039 ]

A stacked pyrazolo[3,4-d]pyrimidine-based flexible molecule: the effect of a bulky benzyl group on intermolecular stacking in comparison with methyl and ethyl groups

K. Avasthi, A. Tewari, D. S. Rawat, A. Sharon and P. R. Maulik

Formula: C29H28N8O2S2

Online 20 July 2002


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Acta Cryst. (2002). C58, o496-o498  [ doi:10.1107/S0108270102011964 ]

2-[2-Methyl-5-nitro-4-(phenylsulfonylmethyl)imidazol-1-yl]ethanol and 2-methyl-5-nitro-4-phenylsulfonylmethyl-1,3-thiazole

M. D. Crozet, P. Vanelle, M. Giorgi and A. Gellis

Formula: C13H15N3O5S and C11H10N2O4S2

Online 20 July 2002


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Acta Cryst. (2002). C58, o499-o502  [ doi:10.1107/S0108270102011800 ]

Hydrogen bonding in 2-(hydroxymethyl)-1,3-propanediol and N,N'-bis[2-hydroxy-1,1-bis(hydroxymethyl)ethyl]malonamide

C. Fernandes, J. L. Wardell and J. M. S. Skakle

Formula: C4H10O3 and C11H22N2O8

Online 20 July 2002


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Acta Cryst. (2002). C58, o503-o506  [ doi:10.1107/S0108270102011915 ]

Two optically active isoquinoline derivatives

A. Gzella, D. Brózda, L. Koroniak and M. D. Rozwadowska

Formula: C16H18NO+·Br-·0.5CH4O and C17H17NO2

Online 20 July 2002


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Acta Cryst. (2002). C58, o507-o509  [ doi:10.1107/S0108270102011538 ]

tert-Butyl (3S,6R,9R)-(5-oxo-3-{[1(R)-phenylethyl]carbamoyl}-1,2,3,5,6,7,8,8a-octahydroindolizin-6-yl)carbamate monohydrate at 95 K

R. Soave and R. Destro

Formula: C22H31N3O4·H2O

Online 31 July 2002


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Acta Cryst. (2002). C58, o510-o512  [ doi:10.1107/S0108270102011150 ]

A pseudo-quadruple hydrogen-bonding motif consisting of six N-H...O hydrogen bonds in trimethoprim formate

B. Umadevi, P. Prabakaran and P. T. Muthiah

Formula: C14H19N4O3+·CHO2-

Online 31 July 2002


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Acta Cryst. (2002). C58, o513-o514  [ doi:10.1107/S0108270102011411 ]

Dibenzyl 2,2'-(ethane-1,2-diylidene)dihydrazinecarbodithioate bis(dimethylformamide) solvate

L. Xu, J.-H. Zhou, X.-T. Chen and X.-Z. You

Formula: C18H18N4S4·2C3H7NO

Online 31 July 2002


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Acta Cryst. (2002). C58, o515-o517  [ doi:10.1107/S0108270102010594 ]

Coordinative N\rightarrowB bond formation and hydrogen-bonded molecular ladders in 2,5-bis[(N[rightwards arrow]B)-(2-aminoethoxy)phenylboryl]thiophene

P. J. Cox and J. L. Wardell

Formula: C20H24B2N2O2S

Online 31 July 2002


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Acta Cryst. (2002). C58, o518-o520  [ doi:10.1107/S0108270102012283 ]

(1S,3R,8S,9S,10R)-2,2-Dichloro-9,10-epoxy-3,7,7,10-tetramethyltricyclo[6.4.0.01,3]dodecane and (1S,3R,8S,10R)-2,2-dichloro-3,7,7,10-tetramethyltricyclo[6.4.0.01,3]dodecan-9-one

F. Sbai, M. Dakir, A. Auhmani, H. El Jamili, M. Akssira, A. Benharref, A. Kenz and M. Pierrot

Formula: Two isomers of C16H24Cl2O

Online 31 July 2002


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Acta Cryst. (2002). C58, o521-o524  [ doi:10.1107/S0108270102012386 ]

[Hydroxy(aryl)methylene]diphosphonic acids, a class of drugs in bone pathology treatments, crystallize as head-to-head dimers

M. Lecouvey, C. Barbey, A. Navaza, A. Neuman and T. Prangé

Formula: C7H10O7P2·H2O and C7H9NO9P2·2C4H8O

Online 31 July 2002


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Acta Cryst. (2002). C58, o525-o527  [ doi:10.1107/S0108270102012544 ]

Polymorphic forms of cilostazol

L. B. Whittall, R. R. Whittle and G. W. Stowell

Formula: Two polymorphs of C20H27N5O2

Online 31 July 2002


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Acta Cryst. (2002). C58, o528-o532  [ doi:10.1107/S0108270102011514 ]

(n-Nitrophenyl)acetonitrile, with n = 2, 3 and 4

S. Boitsov, J. Songstad and K. W. Törnroos

Formula: Three isomers of C8H6N2O2

Online 31 July 2002


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Acta Cryst. (2002). C58, o533-o536  [ doi:10.1107/S0108270102011691 ]

N-(L-2-Aminobutyryl)-L-alanine and 2-(L-alanylamino)-L-butyric acid 0.33-hydrate

C. H. Görbitz

Formula: C7H14N2O3 and C7H14N2O3·0.33H2O

Online 31 July 2002


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