Crystal Structure Communications

 

Acta Cryst. (2002). C58, i103-i105  [ doi:10.1107/S0108270102010600 ]

Rb(GaPO₄)₂(OH)(H₂O)·H₂O: a hydrated rubidium gallium phosphate analogue of GaPO₄·2H₂O and leucophosphite

L. Beitone, T. Loiseau and G. Ferey

Synopsis: Rb(GaPO₄)₂(OH)(H₂O)·H₂O exhibits a three-dimensional framework with intersecting eight-ring channels, in which the alkali cations and the water molecule are encapsulated. This network belongs to the leucophosphite structural type.

Formula: Rb(GaPO₄)₂(OH)(H₂O)·H₂O

Online 12 July 2002

 

Acta Cryst. (2002). C58, i106-i108  [ doi:10.1107/S0108270102007886 ]

KMo₅O₁₃ and KNb_1.76Sb_3.24O₁₃

M. M. Ftini, M. Krifa and H. Amor

Synopsis: The title compounds are isotypic. KMo₅O₁₃ has a three-dimensional tunnel built by the corner-sharing of MoO₆ octahedra; K⁺ cations are located in the tunnels. In KNb_1.76Sb_3.24O₁₃, the Nb and Sb atoms occupy the same sites.

Formula: KMo₅O₁₃ and KNb_1.76Sb_3.24O₁₃

Online 20 July 2002

 

Acta Cryst. (2002). C58, i109-i110  [ doi:10.1107/S0108270102009873 ]

Heptairon bis(phosphate) tetrakis(hydrogenphosphate)

B.-C. Zhou, Y.-W. Yao and R.-J. Wang

Synopsis: Fe₇(PO₄)₂(HPO₄)₄ is isostructural with Mn₇(PO₄)₂(HPO₄)₄ and Co₇(PO₄)₂(HPO₄)₄. The structure is based on a framework of edge- and corner-sharing FeO₆, Fe₅ and PO₄ polyhedra, isotypic with that found in the mixed-valence iron phosphate Fe₇(PO₄)₆. The Fe atoms are purely in the divalent state, just like the Co atoms in Co₇(PO₄)₂(HPO₄)₄, the necessary charge balance being maintained by the addition of H atoms in the form of bridging Fe-OH-P groups.

Formula: Fe₇(PO₄)₂(HPO₄)₄

Online 31 July 2002

 

Acta Cryst. (2002). C58, m427-m430  [ doi:10.1107/S0108270102010491 ]

Bis(2-pyridylmethanol)bis(saccharinato)zinc(II) and -cadmium(II) at 120  K: three-dimensional structures containing both N-and O-coordinated ambidentate saccharinate ligands

V. T. Yilmaz, S. Guney, O. Andac and W. T. A. Harrison

Formula: [Zn(C₇H₄NO₃S)₂(C₆H₇NO)₂] and [Cd(C₇H₄NO₃S)₂(C₆H₇NO)₂]

Online 12 July 2002

 

Acta Cryst. (2002). C58, m431-m433  [ doi:10.1107/S0108270102010430 ]

Bis(tetra-n-butylammonium) bis(-1,2-dicyanoethene-1,2-dithiolato-³S,S':S')bis[(1,2-dicyanoethene-1,2-dithiolato-²S,S')cobalt(III)]

T. Mochida, K. Takazawa, M. M. Matsushita and T. Sugawara

Formula: (C₁₆H₃₆N)₂[Co(C₄N₂S₂)₂]₂

Online 12 July 2002

 

Acta Cryst. (2002). C58, m434-m435  [ doi:10.1107/S0108270102009939 ]

Aquachlorobis(4,4',4''-tri-tert-butyl-2,2';6',2''-terpyridine-³N)terbium(III) diperchlorate ethanol disolvate

H.-R. Mürner, R. Scopelliti and J.-C.G. Bünzli

Formula: [TbCl(C₂₇H₃₅N₃)₂(H₂O)](ClO₄)₂·2C₂H₆O

Online 12 July 2002

 

Acta Cryst. (2002). C58, m436-m438  [ doi:10.1107/S0108270102010764 ]

Tetra-n-butylammonium bis(2-thioxo-1,3-dithiole-4,5-dithiolato-²S⁴,S⁵)nickelate(III)

G.-Q. Liu, G. Xue, W.-T. Yu and W. Xu

Formula: (C₁₆H₃₆N)[Ni(C₃S₅)₂]

Online 12 July 2002

 

Acta Cryst. (2002). C58, m439-m440  [ doi:10.1107/S0108270102010636 ]

Tetraphenylarsonium tetraiodothallate(III)

A. Linden and B. D. James

Formula: (C₂₄H₂₀As)[TlI₄]

Online 12 July 2002

 

Acta Cryst. (2002). C58, m441-m442  [ doi:10.1107/S0108270102010508 ]

catena-Poly[[diaquadichloroiron(II)]--1,4-dioxane-²O:O']

R. L. Speer and A. A. Pinkerton

Formula: [FeCl₂(C₄H₈O₂)(H₂O)₂]

Online 12 July 2002

 

Acta Cryst. (2002). C58, m443-m444  [ doi:10.1107/S0108270102011605 ]

(5,10,15,20-Tetraphenylporphyrinato-⁴N)bis(L-valine-N methyl ester)iron(III) trifluoromethylsulfonate dichloromethane solvate

M. Kobeissi, L. Toupet and G. Simonneaux

Formula: [Fe(C₄₄H₂₈N₄)(C₆H₁₃NO₂)₂](CF₃O₃S)·CH₂Cl₂

Online 20 July 2002

 

Acta Cryst. (2002). C58, m445-m446  [ doi:10.1107/S010827010201154X ]

Bis[-3{5}-(2-pyridyl)pyrazolido]bis[(acetonitrile)copper(II)] diperchlorate

M. J. Hallam, C. A. Kilner and M. A. Halcrow

Formula: [Cu₂(C₈H₆N₃)₂(C₂H₃N)₂](ClO₄)₂

Online 20 July 2002

 

Acta Cryst. (2002). C58, m447-m449  [ doi:10.1107/S0108270102011307 ]

Bis{[diphenyl(piperidinomethyl)silyl]methyl}cadmium and -magnesium

C. Strohmann and D. Schildbach

Formula: [Cd(C₁₉H₂₄NSi)₂] and [Mg(C₁₉H₂₄NSi)₂]

Online 20 July 2002

 

Acta Cryst. (2002). C58, m450-m452  [ doi:10.1107/S010827010201123X ]

Methyl 2,3-dideoxy-2-S-methylmercurio-2-thio--D-manno-oct-2-ulopyranosonate-(2,6)

V. Belakhov, M. Botoshansky and T. Baasov

Formula: [Hg(CH₃)(C₉H₁₅O₇S)]

Online 20 July 2002

 

Acta Cryst. (2002). C58, m453-m454  [ doi:10.1107/S0108270102011988 ]

Dibromo[(-)-sparteine-²N,N']zinc(II)

Y.-M. Lee, S. K. Kang, Y.-I. Kim and S.-N. Choi

Formula: [ZnBr₂(C₁₅H₂₆N₂)]

Online 31 July 2002

 

Acta Cryst. (2002). C58, m455-m458  [ doi:10.1107/S0108270102012404 ]

Bis(1,10-phenanthroline)(thiosulfato)manganese(II) methanol solvate and catena-poly[[diaqua(2,9-dimethyl-1,10-phenanthroline)manganese(II)]--thiosulfato]

E. Freire, S. Baggio, J. C. Muñoz and R. Baggio

Formula: [Mn(S₂O₃)(C₁₂H₈N₂)₂]·CH₄O and [Mn(S₂O₃)(C₁₄H₁₂N₂)(H₂O)₂]

Online 31 July 2002

 

Acta Cryst. (2002). C58, m459-m460  [ doi:10.1107/S0108270102011423 ]

The mononuclear cobalt(II) complex Co^II(DMBDIZ)₂(NCS)₂, where DMBDIZ is 2,6-dimethylbenzo[1,2-d:4,5-d']diimidazole

C.-X. Cai, Y.-Q. Tian, Y.-Z. Li and X.-Z. You

Formula: [Co(NCS)₂(C₁₀H₁₀N₄)₂]

Online 31 July 2002

 

Acta Cryst. (2002). C58, o445-o446  [ doi:10.1107/S0108270102010247 ]

2'-Hydroxy-4''-dimethylaminochalcone

Z.-Q. Liu, Q. Fang, W.-T. Yu, G. Xue, D.-X. Cao and M.-H. Jiang

Formula: C₁₇H₁₇NO₂

Online 12 July 2002

 

Acta Cryst. (2002). C58, o447-o449  [ doi:10.1107/S0108270102007503 ]

Two (E,E)- and (Z,E)-thiazol-5-ylpenta-2,4-dienones

L. Breydo, C. L. Barnes and K. S. Gates

Formula: C₁₆H₂₂N₂O₄S and C₁₄H₁₆N₂O₃S

Online 12 July 2002

 

Acta Cryst. (2002). C58, o450-o454  [ doi:10.1107/S0108270102009587 ]

Diethyl {3-[-(2,4-dichlorophenyl)vinyl]-N-(phenylsulfonyl)indol-2-ylmethyl}phosphonate and diethyl {3-[-(4-bromophenyl)vinyl]-N-(phenylsulfonyl)indol-2-ylmethyl}phosphonate

K. Sethu Sankar, S. Kannadasan, D. Velmurugan, P. C. Srinivasan and J.-K. Moon

Formula: C₂₇H₂₆Cl₂NO₅PS and C₂₇H₂₇BrNO₅PS

Online 12 July 2002

 

Acta Cryst. (2002). C58, o455-o459  [ doi:10.1107/S0108270102010521 ]

Hexakis(melaminium) tetrakis(dihydrogenphosphate) monohydrogenphosphate tetrahydrate

J. Janczak and G. J. Perpétuo

Formula: 6C₃H₇N₆⁺·4H₂PO₄^-·HPO₄^2-·4H₂O

Online 12 July 2002

 

Acta Cryst. (2002). C58, o460-o462  [ doi:10.1107/S0108270102010399 ]

9-(Trichloroacetylimino)acridine monohydrate

J. Meszko, K. Krzyminski, A. Konitz and J. Blazejowski

Formula: C₁₅H₉Cl₃N₂O·H₂O

Online 12 July 2002

 

Acta Cryst. (2002). C58, o463-o466  [ doi:10.1107/S0108270102010776 ]

2,6-Diiodo-4-nitrophenol, 2,6-diiodo-4-nitrophenyl acetate and 2,6-diiodo-4-nitroanisole: interplay of hydrogen bonds, iodo-nitro interactions and aromatic --stacking interactions to give supramolecular structures in one, two and three dimensions

S. J. Garden, F. R. da Cunha, J. L. Wardell, J. M. S. Skakle, J. N. Low and C. Glidewell

Formula: C₆H₃I₂NO₃, C₈H₅I₂NO₄ and C₇H₅I₂NO₃

Online 12 July 2002

 

Acta Cryst. (2002). C58, o467-o469  [ doi:10.1107/S0108270102010648 ]

Self-assembled hydrogen-bonded bilayers in 1,4-diazabicyclo[2.2.2]octane-N-(phosphonomethyl)iminodiacetic acid-water (1/1/1.5)

K. F. Bowes, G. Ferguson, C. Glidewell and A. J. Lough

Formula: C₆H₁₄N₂²⁺·C₅H₈NO₇P^2-·1.5H₂O

Online 12 July 2002

 

Acta Cryst. (2002). C58, o470-o473  [ doi:10.1107/S0108270102010958 ]

The salt-type 1:2 adduct of meso-5,5,7,12,12,14-hexa-C-methyl-1,4,8,11-tetraazacyclotetradecane (tet-a) and 5-nitroisophthalic acid forms a hydrogen-bonded sheet structure containing two configurational isomers of [(tet-a)H₂]²⁺

E. J. MacLean, S. J. Teat, D. M. M. Farrell, G. Ferguson and C. Glidewell

Formula: C₁₆H₃₈N₄⁺·2C₈H₄NO₆^-

Online 12 July 2002

 

Acta Cryst. (2002). C58, o474-o476  [ doi:10.1107/S0108270102010843 ]

(1SR,2RS,5RS,6SR,8RS)-7,7-Dimethyltricyclo[6.2.1.0^1,6]undecane-2,5,6-triol: a supramolecular framework built from O-HO hydrogen bonds

S. Mondal, M. Mukherjee, A. Roy, D. Mukherjee and M. Helliwell

Formula: C₁₃H₂₂O₃

Online 12 July 2002

 

Acta Cryst. (2002). C58, o477-o479  [ doi:10.1107/S0108270102011083 ]

11-Methyl-12a-phenyl-9a,12a-dihydrophenanthro[9',10':5,6][1,4]dioxino[2,3-d]oxazole and 9a-(10-hydroxyphenanthren-9-yl)-11,12a-diphenyl-9a,12a-dihydrophenanthro[9',10':5,6][1,4]dioxino[2,3-d]oxazole

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Zhang and J.-H. Xu

Formula: C₂₄H₁₇NO₃ and C₄₃H₂₇NO₅

Online 12 July 2002

 

Acta Cryst. (2002). C58, o480-o484  [ doi:10.1107/S0108270102011319 ]

Four bis(1-chloro-2,2,4,4-tetramethyl-3-oxocyclobutan-1-yl)oligosulfanes

A. Linden, A. Majchrzak, J. Cavegn, G. Mloston and H. Heimgartner

Formula: C₁₆H₂₄Cl₂O₂S₂, C₁₆H₂₄Cl₂O₂S₃, C₁₆H₂₄Cl₂O₂S₄ and C₁₆H₂₄Cl₂O₂S₆

Online 20 July 2002

 

Acta Cryst. (2002). C58, o485-o486  [ doi:10.1107/S0108270102011344 ]

2-Nitrophenyl 4-nitrophenyl disulfide

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C₁₂H₈N₂O₄S₂

Online 20 July 2002

 

Acta Cryst. (2002). C58, o487-o490  [ doi:10.1107/S010827010201140X ]

2-Iodo-N-(3-nitrobenzyl)aniline and 3-iodo-N-(3-nitrobenzyl)aniline exhibit entirely different patterns of supramolecular aggregation

C. Glidewell, J. N. Low, J. M. S. Skakle, S. M. S. V. Wardell and J. L. Wardell

Formula: Two isomers of C₁₃H₁₁IN₂O₂

Online 20 July 2002

 

Acta Cryst. (2002). C58, o491-o493  [ doi:10.1107/S0108270102011526 ]

(±)-(2,3,4,4a,5,6,7,8-Octahydro-2-oxonaphthalen-1-yl)acetic acid: hydrogen-bonding pattern of the monohydrate of an unsaturated bicyclic -keto acid

R. A. Lalancette, A. P. J. Brunskill and H. W. Thompson

Formula: C₁₂H₁₆O₃·H₂O

Online 20 July 2002

 

Acta Cryst. (2002). C58, o494-o495  [ doi:10.1107/S0108270102012039 ]

A stacked pyrazolo[3,4-d]pyrimidine-based flexible molecule: the effect of a bulky benzyl group on intermolecular stacking in comparison with methyl and ethyl groups

K. Avasthi, A. Tewari, D. S. Rawat, A. Sharon and P. R. Maulik

Formula: C₂₉H₂₈N₈O₂S₂

Online 20 July 2002

 

Acta Cryst. (2002). C58, o496-o498  [ doi:10.1107/S0108270102011964 ]

2-[2-Methyl-5-nitro-4-(phenylsulfonylmethyl)imidazol-1-yl]ethanol and 2-methyl-5-nitro-4-phenylsulfonylmethyl-1,3-thiazole

M. D. Crozet, P. Vanelle, M. Giorgi and A. Gellis

Formula: C₁₃H₁₅N₃O₅S and C₁₁H₁₀N₂O₄S₂

Online 20 July 2002

 

Acta Cryst. (2002). C58, o499-o502  [ doi:10.1107/S0108270102011800 ]

Hydrogen bonding in 2-(hydroxymethyl)-1,3-propanediol and N,N'-bis[2-hydroxy-1,1-bis(hydroxymethyl)ethyl]malonamide

C. Fernandes, J. L. Wardell and J. M. S. Skakle

Formula: C₄H₁₀O₃ and C₁₁H₂₂N₂O₈

Online 20 July 2002

 

Acta Cryst. (2002). C58, o503-o506  [ doi:10.1107/S0108270102011915 ]

Two optically active isoquinoline derivatives

A. Gzella, D. Brózda, L. Koroniak and M. D. Rozwadowska

Formula: C₁₆H₁₈NO⁺·Br^-·0.5CH₄O and C₁₇H₁₇NO₂

Online 20 July 2002

 

Acta Cryst. (2002). C58, o507-o509  [ doi:10.1107/S0108270102011538 ]

tert-Butyl (3S,6R,9R)-(5-oxo-3-{[1(R)-phenylethyl]carbamoyl}-1,2,3,5,6,7,8,8a-octahydroindolizin-6-yl)carbamate monohydrate at 95  K

R. Soave and R. Destro

Formula: C₂₂H₃₁N₃O₄·H₂O

Online 31 July 2002

 

Acta Cryst. (2002). C58, o510-o512  [ doi:10.1107/S0108270102011150 ]

A pseudo-quadruple hydrogen-bonding motif consisting of six N-HO hydrogen bonds in trimethoprim formate

B. Umadevi, P. Prabakaran and P. T. Muthiah

Formula: C₁₄H₁₉N₄O₃⁺·CHO₂^-

Online 31 July 2002

 

Acta Cryst. (2002). C58, o513-o514  [ doi:10.1107/S0108270102011411 ]

Dibenzyl 2,2'-(ethane-1,2-diylidene)dihydrazinecarbodithioate bis(dimethylformamide) solvate

L. Xu, J.-H. Zhou, X.-T. Chen and X.-Z. You

Formula: C₁₈H₁₈N₄S₄·2C₃H₇NO

Online 31 July 2002

 

Acta Cryst. (2002). C58, o515-o517  [ doi:10.1107/S0108270102010594 ]

Coordinative NB bond formation and hydrogen-bonded molecular ladders in 2,5-bis[(NB)-(2-aminoethoxy)phenylboryl]thiophene

P. J. Cox and J. L. Wardell

Formula: C₂₀H₂₄B₂N₂O₂S

Online 31 July 2002

    

Acta Cryst. (2002). C58, o518-o520  [ doi:10.1107/S0108270102012283 ]

(1S,3R,8S,9S,10R)-2,2-Dichloro-9,10-epoxy-3,7,7,10-tetramethyltricyclo[6.4.0.0^1,3]dodecane and (1S,3R,8S,10R)-2,2-dichloro-3,7,7,10-tetramethyltricyclo[6.4.0.0^1,3]dodecan-9-one

F. Sbai, M. Dakir, A. Auhmani, H. El Jamili, M. Akssira, A. Benharref, A. Kenz and M. Pierrot

Formula: Two isomers of C₁₆H₂₄Cl₂O

Online 31 July 2002

 

Acta Cryst. (2002). C58, o521-o524  [ doi:10.1107/S0108270102012386 ]

[Hydroxy(aryl)methylene]diphosphonic acids, a class of drugs in bone pathology treatments, crystallize as head-to-head dimers

M. Lecouvey, C. Barbey, A. Navaza, A. Neuman and T. Prangé

Formula: C₇H₁₀O₇P₂·H₂O and C₇H₉NO₉P₂·2C₄H₈O

Online 31 July 2002

 

Acta Cryst. (2002). C58, o525-o527  [ doi:10.1107/S0108270102012544 ]

Polymorphic forms of cilostazol

L. B. Whittall, R. R. Whittle and G. W. Stowell

Formula: Two polymorphs of C₂₀H₂₇N₅O₂

Online 31 July 2002

 

Acta Cryst. (2002). C58, o528-o532  [ doi:10.1107/S0108270102011514 ]

(n-Nitrophenyl)acetonitrile, with n = 2, 3 and 4

S. Boitsov, J. Songstad and K. W. Törnroos

Formula: Three isomers of C₈H₆N₂O₂

Online 31 July 2002

 

Acta Cryst. (2002). C58, o533-o536  [ doi:10.1107/S0108270102011691 ]

N-(L-2-Aminobutyryl)-L-alanine and 2-(L-alanylamino)-L-butyric acid 0.33-hydrate

C. H. Görbitz

Formula: C₇H₁₄N₂O₃ and C₇H₁₄N₂O₃·0.33H₂O

Online 31 July 2002