Crystal Structure Communications

 

Acta Cryst. (2002). C58, i111-i113  [ doi:10.1107/S0108270102011708 ]

KVTeO₅ and a redetermination of the Na homologue

P. Rozier, L. Vendier and J. Galy

Synopsis: The MVTeO₅ crystal structure consists of [VTeO₅]_n ribbons linked together by the M⁺ cations located in a distorted bicapped trigonal prism.

Formula: KVTeO₅ and NaVTeO₅

Online 10 August 2002

 

Acta Cryst. (2002). C58, i114-i118  [ doi:10.1107/S0108270102012532 ]

Bis(trichlorophosphine)iminium salts, [Cl₃P=N=PCl₃]⁺, with transition metal halide counter-ions

E. Rivard, A. R. McWilliams, A. J. Lough and I. Manners

Synopsis: Each of the four title structures contains discrete [Cl₃P=N=PCl₃]⁺ cations and metal halide anions. The [NbCl₆] and [TaCl₆] compounds are isostructural.

Formula: (Cl₆NP₂)[NbCl₆], (Cl₆NP₂)[TaCl₆], (Cl₆NP₂)[Ti₂Cl₉] and (Cl₆NP₂)₂[Zr₂Cl₁₀]

Online 10 August 2002

 

Acta Cryst. (2002). C58, i119-i120  [ doi:10.1107/S0108270102013136 ]

Cs[Ag₄Zn₂(SCN)₉]

M. Günes and J. Valkonen

Synopsis: Cs[Ag₄Zn₂(SCN)₉] forms a continuous structure, where the Ag atoms and the thiocyanate S atoms form chains which run in the ac plane. These chains are bonded together through the Cs and Zn atoms. The structure also contains a disordered thiocyanate group.

Formula: Cs[Ag₄Zn₂(SCN)₉]

Online 10 August 2002

 

Acta Cryst. (2002). C58, i121-i123  [ doi:10.1107/S0108270102011812 ]

A uranyl sulfate cluster in Na₁₀[(UO₂)(SO₄)₄](SO₄)₂·3H₂O

P. C. Burns and L. A. Hayden

Synopsis: Na₁₀[(UO₂)(SO₄)₄](SO₄)₂·3H₂O contains an unusual uranyl sulfate cluster that involves a chelating sulfate group in a pentagonal-bipyramidal coordination around the U atom.

Formula: Na₁₀[(UO₂)(SO₄)₄](SO₄)₂·3H₂O

Online 10 August 2002

 

Acta Cryst. (2002). C58, i124-i125  [ doi:10.1107/S0108270102012635 ]

Dineodymium tritelluride, Nd₂Te₃

I. Ijjaali and J. A. Ibers

Synopsis: Nd₂Te₃ crystallizes in the U₂S₃ structure type, with each of the two non-equivalent Nd atoms surrounded by seven Te atoms in polyhedra best described as a seven-octahedron and a monocapped trigonal prism.

Formula: Nd₂Te₃

Online 21 August 2002

 

Acta Cryst. (2002). C58, i126-i128  [ doi:10.1107/S0108270102013148 ]

The superconductor (Tl,Hg,Ca)₂(Ba,Sr)₂(Ca,Sr,Tl)Cu₂O_7.6

M. Valldor, I. Bryntse and A. Morawski

Synopsis: The reported 2212-type superconductor provides proof of the chemical flexibility of layered cuprates. The data also reveal a remarkably large apical Cu-Cu distance, due to the presence of Tl and Sr in the intermediate layer.

Formula: (Tl,Hg,Ca)₂(Ba,Sr)₂(Ca,Sr,Tl)Cu₂O_7.6

Online 21 August 2002

 

Acta Cryst. (2002). C58, i129-i131  [ doi:10.1107/S0108270102013094 ]

Hexaaquacobalt(II) bis(hypophosphite) and hexaaquacobalt(II)/nickel(II) bis(hypophosphite)

N. V. Kuratieva, M. I. Naumova and D. Yu. Naumov

Synopsis: The crystal structures of tetragonal [Co(H₂O)₆](H₂PO₂)₂ and [Co_0.5Ni_0.05(H₂O)₆](H₂PO₂)₂ have been determined. The crystals of hexaaquacobalt(II)/nickel(II) bis(hypophosphite) are a solid solution of Co^II and Ni^III hypophosphites. The packing of the Co(Ni) and P atoms is the same as in the structure of CaF₂. The coordination number of six for metal is achieved by water molecules. The hypophosphite anion does not coordinate to the metal cation.

Formula: [Co(H₂O)₆](H₂PO₂)₂ and [Co_0.5Ni_0.5(H₂O)₆](H₂PO₂)₂

Online 31 August 2002

 

Acta Cryst. (2002). C58, i132-i134  [ doi:10.1107/S0108270102013884 ]

The ordered hydrocerussite-type structure of (PbCO₃)₂·BaF₂

M. Weil

Synopsis: (PbCO₃)₂·BaF₂ crystallizes in the ordered hydrocerussite-type structure, with a stacking sequence of [c(h)₂]₃ for the close-packed metal atoms.

Formula: (PbCO₃)₂·BaF₂

Online 31 August 2002

 

Acta Cryst. (2002). C58, m461-m463  [ doi:10.1107/S0108270102011976 ]

Bis[1-(pyridin-2-yl)ethanone-N 4-phenylthiosemicarbazonato-²N⁴,S]manganese(II)

A. Usman, I. A. Razak, S. Chantrapromma, H.-K. Fun, A. Sreekanth, S. Sivakumar and M. R. Prathapachandra Kurup

Formula: [Mn(C₁₄H₁₃N₄S)₂]

Online 10 August 2002

 

Acta Cryst. (2002). C58, m464-m465  [ doi:10.1107/S0108270102013008 ]

(Et₄N)₄[V₄O₁₂]·2H₂O

H. Nakano, T. Ozeki and A. Yagasaki

Formula: (C₈H₂₀N)₄[V₄O₁₂]·2H₂O

Online 10 August 2002

 

Acta Cryst. (2002). C58, m466-m468  [ doi:10.1107/S0108270102012362 ]

Chlorotris(2,4,6-trimethylphenyl)tin(IV) and its ethanol hemisolvate

J. Geller, I. Wharf, F. Bélanger-Gariépy, A.-M. Lebuis, I. S. Butler and D. F. R. Gilson

Formula: [Sn(C₉H₁₁)₃Cl] and [Sn(C₉H₁₁)₃Cl]·0.5C₂H₆O

Online 10 August 2002

 

Acta Cryst. (2002). C58, m469-m470  [ doi:10.1107/S0108270102013537 ]

Bis(5-hydroxy-2-hydroxymethyl-4-pyrone-²O⁴,O⁵)bis(2-hydroxymethyl-5-oxido-4-pyrone-²O⁴,O⁵)calcium(II) tetrahydrate

M. Odoko, K. Yamamoto and N. Okabe

Formula: [Ca(C₆H₅O₄)₂(C₆H₆O₄)₂]·4H₂O

Online 10 August 2002

 

Acta Cryst. (2002). C58, m471-m474  [ doi:10.1107/S0108270102013227 ]

Tetrakis(-guanidinoacetic acid-²O:O')bis[(nitrato-O)copper(II)]

J. Lopes de Miranda, J. Felcman, J. L. Wardell and J. M. S. Skakle

Formula: [Cu₂(NO₃)₂(C₃H₇N₃O₂)₄]

Online 21 August 2002

 

Acta Cryst. (2002). C58, m475-m477  [ doi:10.1107/S0108270102013628 ]

8-Hydroxyquinaldinic acid and its nickel(II) complex

N. Okabe and Y. Muranishi

Formula: C₁₀H₇NO₃ and [Ni(C₁₀H₆NO₃)₂]·3H₂O

Online 21 August 2002

 

Acta Cryst. (2002). C58, m478-m480  [ doi:10.1107/S0108270102014026 ]

Tetraaqua-1⁴O-bis(-caprolactam-1O)--cyano-1:2²N:C-pentacyano-2⁵C-iron(III)yttrium(III), a novel cyano-bridged dinuclear complex

B. C. Zhou, H.-Z. Kou, Y. He, M. Xiong, R.-J. Wang and Y.-D. Li

Formula: [FeY(CN)₆(C₆H₁₁NO)₂(H₂O)₄]

Online 21 August 2002

 

Acta Cryst. (2002). C58, m481-m482  [ doi:10.1107/S0108270102013872 ]

Polymeric (3-amino-2-chloropyridine)nitratosilver(I)

M.-L. Tong, X.-M. Chen and S. W. Ng

Formula: [Ag(NO₃)(C₅H₅ClN₂)]

Online 21 August 2002

 

Acta Cryst. (2002). C58, m483-m484  [ doi:10.1107/S0108270102014658 ]

[Cd{C₂(COO)₂}(H₂O)₃]·H₂O, the first cadmium salt of acetylenedicarboxylic acid

U. Ruschewitz and I. Pantenburg

Formula: [Cd(C₄O₄)(H₂O)₃]·H₂O

Online 31 August 2002

 

Acta Cryst. (2002). C58, m485-m486  [ doi:10.1107/S0108270102013859 ]

Dibromo[5,10,15,20-tetrakis(4-methoxyphenyl)porphyrinato-⁴N]platinum(IV) chloroform acetonitrile solvate

J. R. Tate, K. Kantardjieff, G. Crundwell and L. M. Mink

Formula: [PtBr₂(C₄₈H₃₆N₄O₄)]·0.896CHCl₃·0.569C₂H₃N

Online 31 August 2002

 

Acta Cryst. (2002). C58, o537-o539  [ doi:10.1107/S0108270102012556 ]

A comparative analysis of mono- and disaccharide benzyl fucopyranosides

M. Brito-Arias, E. Durán-Páramo, I. Mata and E. Molins

Formula: C₁₇H₂₂O₇ and C₃₃H₄₀O₁₂

Online 10 August 2002

 

Acta Cryst. (2002). C58, o540-o542  [ doi:10.1107/S0108270102012489 ]

L-Tryptophan formic acid solvate at 183 K

C. B. Hübschle, B. Dittrich and P. Luger

Formula: C₁₁H₁₂N₂O₂·CH₂O₂

Online 10 August 2002

 

Acta Cryst. (2002). C58, o543-o544  [ doi:10.1107/S0108270102013112 ]

11-Methyl-12a-phenyl-9a,12a-dihydrophenanthro[9',10:5,6][1,4]dioxino[2,3-d]thiazole

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Zhang and J.-H. Xu

Formula: C₂₄H₁₇NO₂S

Online 10 August 2002

 

Acta Cryst. (2002). C58, o545-o548  [ doi:10.1107/S0108270102011952 ]

Orthorhombic polymorphs of two trans-4-aminoazoxybenzenes

K. Ejsmont, M. Broda, A. Domanski, J. B. Kyziol and J. Zaleski

Formula: Two isomers of C₁₂H₁₁N₃O

Online 10 August 2002

 

Acta Cryst. (2002). C58, o549-o550  [ doi:10.1107/S0108270102012945 ]

1,4-Bis[(1-methyl-1-phenylethyl)peroxymethyl]benzene

N. Kuznik, J. Zawadiak, D. Gilner, A. Wieckol, P. Wagner and M. Kubicki

Formula: C₂₆H₃₀O₄

Online 10 August 2002

 

Acta Cryst. (2002). C58, o551-o554  [ doi:10.1107/S0108270102012830 ]

N,N'-Dithiobisphthalimide-nitrobenzene (2/1): a Pn solvate with localized solvent molecules ordered head-to-tail in channels

K. F. Bowes, G. Ferguson, C. Glidewell, J. N. Low and A. Quesada

Formula: 2C₁₆H₈N₂O₄S₂·C₆H₅NO₂

Online 10 August 2002

 

Acta Cryst. (2002). C58, o555-o557  [ doi:10.1107/S0108270102013379 ]

The low-temperature phase of diisopropylammonium bromide

M. Haberecht, H.-W. Lerner and M. Bolte

Formula: C₆H₁₆N⁺·Br^-

Online 10 August 2002

 

Acta Cryst. (2002). C58, o558-o559  [ doi:10.1107/S0108270102013756 ]

The stable inner salt 2,2-dimorpholino-2-ethylium-1-dithioate

T. Fujihara, T. Ohba, A. Nagasawa, J. Nakayama and K. Yoza

Formula: C₁₀H₁₆N₂O₂S₂

Online 21 August 2002

 

Acta Cryst. (2002). C58, o560-o562  [ doi:10.1107/S0108270102013665 ]

2,3-Dihydro-3,3-dimethylspiro[1H-4-oxanthracene-5,2'-oxiran]-10(5H)-one

V. F. Ferreira, A. V. Pinto, M. C. R. F. Pinto, M. N. da Silva, J. M. S. Skakle, M. C. B. V. de Souza and S. M. S. V. Wardell

Formula: C₁₆H₁₆O₃

Online 21 August 2002

 

Acta Cryst. (2002). C58, o563-o564  [ doi:10.1107/S0108270102013483 ]

3,6,13,16-Tetrabromo-2,7,12,17-tetrapropylporphycene

I. Aritome, H. Shimakoshi and Y. Hisaeda

Formula: C₃₂H₃₄Br₄N₄

Online 21 August 2002

 

Acta Cryst. (2002). C58, o565-o567  [ doi:10.1107/S0108270102013458 ]

1,1'-Di(hydrazinocarbonylmethyl)-2,2'-biimidazole monohydrate and 1,1'-di[2-(hydrazinocarbonyl)ethyl]-2,2'-biimidazole

W. M. Barnett, R. G. Baughman, P. M. Secondo and C. J. Hermansen

Formula: C₁₀H₁₄N₈O₂·H₂O and C₁₂H₁₈N₈O₂

Online 21 August 2002

 

Acta Cryst. (2002). C58, o568-o569  [ doi:10.1107/S010827010201315X ]

5-Methyl-2-thiouracil

D. Matkovic-Calogovic, E. Besic and K. Sankovic

Formula: C₅H₆N₂OS

Online 21 August 2002

 

Acta Cryst. (2002). C58, o570-o571  [ doi:10.1107/S0108270102012982 ]

2-Methyl-1-phenylsulfanyl-1,2-dicarba-closo-dodecaborane(12)

R. Kivekäs, M. A. Flores, C. Viñas and R. Sillanpää

Formula: C₉H₁₈B₁₀S

Online 21 August 2002

 

Acta Cryst. (2002). C58, o572-o574  [ doi:10.1107/S0108270102013653 ]

Ethyl 4-dodecyl-3,5-dimethyl-1H-pyrrole-2-carboxylate: intermolecular interactions in an amphiphilic pyrrole

M. Ramos Silva, A. Matos Beja, J. A. Paixão, A. J. F. N. Sobral, S. H. Lopes and A. M. d'A. Rocha Gonsalves

Formula: C₂₁H₃₇NO₂

Online 31 August 2002

 

Acta Cryst. (2002). C58, o575-o579  [ doi:10.1107/S0108270102013239 ]

Hydrogen-bonded assemblages in 2,6-bis(hydroxymethyl)-4-R-phenol, with R = methyl, methoxy, phenoxy and 1-(4-methoxyphenyl)-1-methylethyl

B. Masci and P. Thuéry

Formula: C₉H₁₂O₃, C₉H₁₂O₄, C₁₄H₁₄O₄ and C₁₈H₂₂O₄

Online 31 August 2002

 

Acta Cryst. (2002). C58, o580-o581  [ doi:10.1107/S0108270102014774 ]

4,10-Dinitro-2,6,8,12-tetraoxa-4,10-diazaisowurtzitane (TEX): a nitramine with an exceptionally high density

K. Karaghiosoff, T. M. Klapötke, A. Michailovski and G. Holl

Formula: C₆H₆N₄O₈

Online 31 August 2002

 

Acta Cryst. (2002). C58, o582-o584  [ doi:10.1107/S0108270102013768 ]

3,6-Bis(dimethylamino)-10-(10-iododecyl)acridinium iodide

R. Puliti, C. A. Mattia and L. Mazzarella

Formula: C₂₇H₃₉IN₃⁺·I^-

Online 31 August 2002

 

Acta Cryst. (2002). C58, o585-o588  [ doi:10.1107/S0108270102012647 ]

Ethyl 5-[2-(2-aminophénylimino)-2-phényléthylidène]-4-(4-chlorophényl)-4,5-dihydro-1,3,4-thiadiazole-2-carboxylate et éthyl 5-{2-[2-(méthylamino)phénylimino]-2-phényléthylidène}-4-(4-nitrophényl)-4,5-dihydro-1,3,4-thiadiazole-2-carboxylate

S. El Hazazi, A. Baouid, A. Hasnaoui and M. Pierrot

Formula: C₂₅H₂₁ClN₄O₂S et C₂₆H₂₃N₅O₄S

Online 31 août 2002

 

Acta Cryst. (2002). C58, o589-o590  [ doi:10.1107/S0108270102013100 ]

The ternary complex 4-(2-pyridyl)pyridinium-3,5-dinitrobenzoate-3,5-dinitrobenzoic acid (1/1/1)

S. Chantrapromma, A. Usman, H.-K. Fun, B.-L. Poh and C. Karalai

Formula: C₁₀H₉N₂⁺·C₇H₃N₂O₆^-·C₇H₄N₂O₆

Online 31 August 2002