Crystal Structure Communications

 

Acta Cryst. (2003). C59, i21-i23  [ doi:10.1107/S0108270103001264 ]

KMnAg₃(CN)₆, a new triply interpenetrating network solid

U. Geiser and J. A. Schlueter

Synopsis: The single-crystal structure of potassium manganese tris[dicyanoargentate(I)], KMnAg₃(CN)₆, is described. This is the first Mn-containing example of the triply interpenetrating MAg₃(CN)₆ type. The K⁺ ion is found to be located in an ordered manner on one of two possible interstitial sites, leading to a chiral space group.

Formula: KMnAg₃(CN)₆

Online 18 February 2003

 

Acta Cryst. (2003). C59, i24-i26  [ doi:10.1107/S0108270103002221 ]

Strontium hexabromodicadmate(II) octahydrate

S. Yahyaoui, R. Ben Hassen, V. Petrícek, M. Dusek and A. Ben Salah

Synopsis: Substitution of Cl by Br atoms into the known structure of SrCd₂Cl₆·8H₂O leads to a disappearance of the twin phenomenon previously observed and a new arrangement of the Sr(H₂O)₉ polyhedra in chains by the sharing of bases of the triangular prisms.

Formula: SrCd₂Br₆·8H₂O

Online 18 February 2003

 

Acta Cryst. (2003). C59, m73-m75  [ doi:10.1107/S0108270103001215 ]

Dibromo(pyridoxal semicarbazone-³N¹,O³,O^3')copper(II)

D. Poleti, L. Karanovic, V. M. Leovac and V. S. Jevtovic

Formula: [CuBr₂(C₉H₁₂N₄O₃)]

Online 11 February 2003

 

Acta Cryst. (2003). C59, m76-m78  [ doi:10.1107/S0108270102023302 ]

Polymeric bis(phosphonomethylcarboxylato)calcium(II) at 85 K

K. Slepokura and T. Lis

Formula: [Ca(C₂H₄O₅P)₂]

Online 11 February 2003

 

Acta Cryst. (2003). C59, m79-m81  [ doi:10.1107/S0108270103001483 ]

The triclinic polymorph of dibromo[(-)-sparteine-²N,N']zinc(II)

J. L. Alcántara-Flores, S. Bernès, Y. Reyes-Ortega and R. Zamorano-Ulloa

Formula: [ZnBr₂(C₁₅H₂₆N₂)]

Online 11 February 2003

 

Acta Cryst. (2003). C59, m82-m83  [ doi:10.1107/S0108270103002087 ]

Tetraaqua(2,2'-bipyridine)nickel(II) terephthalate

H.-P. Xiao, Z. Shi, L.-G. Zhu, R.-R. Xu and W.-Q. Pang

Formula: [Ni(C₁₀H₈N₂)(H₂O)₄](C₈H₄O₄)

Online 18 February 2003

 

Acta Cryst. (2003). C59, m84-m86  [ doi:10.1107/S0108270103002154 ]

[-o-Phenylenebis(diphenylphosphine)-²P:P']bis[chlorogold(I)], dppbz(AuCl)₂

A. A. Mohamed, J. A. Krause Bauer, A. E. Bruce and M. R. M. Bruce

Formula: [Au₂Cl₂(C₃₀H₂₄P₂)]

Online 18 February 2003

 

Acta Cryst. (2003). C59, m87-m89  [ doi:10.1107/S0108270103002683 ]

(C₆H₁₄N₂)₂[VO(HPO₄)₅B₂O]·H₂O·H₃PO₄, a novel borophosphate cluster containing a single vanadium centre and linked by hydrogen bonds into a three-dimensional framework

E. Wikstad and M. Kritikos

Formula: (C₆H₁₄N₂)₂[VB₂O₂(HPO₄)₅]·H₂O·H₃PO₄

Online 28 February 2003

 

Acta Cryst. (2003). C59, m90-m92  [ doi:10.1107/S0108270103002968 ]

catena-Poly[[tetrakis(2-allyltetrazole-N⁴)-tetra--chloro-tricopper(II)]-di--chloro]

A. S. Lyakhov, P. N. Gaponik, M. M. Degtyarik, Vadim E. Matulis, Vitaly E. Matulis and L. S. Ivashkevich

Formula: [Cu₃Cl₆(C₄H₆N₄)₄]

Online 28 February 2003

 

Acta Cryst. (2003). C59, m93-m94  [ doi:10.1107/S0108270103002798 ]

A barium perchlorate complex with a lateral macrobicycle derived from 1,10-diaza-15-crown-5 containing a phenol Schiff base spacer

F. Avecilla, D. Esteban, C. Platas-Iglesias, A. De Blas and T. Rodríguez-Blas

Online 28 February 2003

 

Acta Cryst. (2003). C59, m95-m96  [ doi:10.1107/S0108270103001914 ]

[4-Amino-N-(pyrimidin-2-yl)benzenesulfonamido-N](triphenylphosphine-P)gold(I)

E. Schulz Lang, R. A. Burrow and L. de L. Marques

Formula: [Au(C₁₀H₉N₄O₂S)(C₁₈H₁₅P)]

Online 28 February 2003

 

Acta Cryst. (2003). C59, m97-m99  [ doi:10.1107/S0108270103003433 ]

Polymeric structure of (ethylenediamine)silver(I) 3-nitrobenzoate monohydrate

A. Usman, H.-K. Fun, S. Chantrapromma, H.-L. Zhu and X.-J. Wang

Formula: [Ag(C₂H₈N₂)](C₇H₄NO₄)·H₂O

Online 28 February 2003

 

Acta Cryst. (2003). C59, m100-m102  [ doi:10.1107/S0108270103002853 ]

Hexa--chloro-₄-oxo-tetrakis{[5-(2,4,6-trimethylphenyl)pyrazole-N²]copper(II)}

X.-M. Liu, C. A. Kilner and M. A. Halcrow

Formula: [Cu₄Cl₆O(C₁₂H₁₄N₂)₄]

Online 28 February 2003

 

Acta Cryst. (2003). C59, m103-m106  [ doi:10.1107/S0108270103003329 ]

The nitrate dihydrate of an aquadicopper(II) complex cation with guanidinoacetic acid and a novel trianionic disubstituted guanidine as ligands at 120 K

J. Felcman, R. A. Howie, J. L. de Miranda, J. M. S. Skakle and J. L. Wardell

Formula: [Cu₂(C₅H₆N₃O₅)(C₃H₇N₃O₂)(H₂O)]NO₃·2H₂O

Online 28 February 2003

 

Acta Cryst. (2003). C59, m107-m108  [ doi:10.1107/S0108270103003445 ]

A new polymorph of (O-ethyl dithiocarbonato-²S,S')bis(triphenylphosphine-P)silver(I)

I. Ara, F. El Bahij, M. Lachkar and N. Ben Larbi

Formula: [Ag(C₃H₅OS₂)(C₁₈H₁₅P)₂]

Online 28 February 2003

 

Acta Cryst. (2003). C59, o95-o97  [ doi:10.1107/S0108270103000775 ]

4-Iodo-N-(2-nitrophenylsulfanyl)aniline: -stacked sheets generated by a combination of N-HO and C-HO hydrogen bonds

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C₁₂H₉IN₂O₂S

Online 11 February 2003

 

Acta Cryst. (2003). C59, o98-o101  [ doi:10.1107/S0108270103001379 ]

A chain of edge-fused rings generated by the combination of an N-HO hydrogen bond and an iodo-nitro interaction in 2-iodobenzaldehyde 4-nitrophenylhydrazone versus disordered and effectively isolated molecules in 2-iodobenzaldehyde 2,4-dinitrophenylhydrazone

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C₁₃H₁₀IN₃O₂ and C₁₃H₉IN₄O₄

Online 11 February 2003

 

Acta Cryst. (2003). C59, o102-o104  [ doi:10.1107/S0108270103001458 ]

2-Amino-5-nitro-4,6-dipiperidinopyrimidinium hydrogensulfate monohydrate: hydrogen-bonded sheets containing highly distorted cations

A. Quesada, A. Marchal, J. N. Low and C. Glidewell

Formula: C₁₄H₂₃N₆O₂⁺·HSO₄^-·H₂O

Online 11 February 2003

 

Acta Cryst. (2003). C59, o105-o106  [ doi:10.1107/S0108270103001586 ]

Bis(2-aminopyridinium) maleate

O. Büyükgüngör and M. Odabasoglu

Formula: 2C₅H₇N₂⁺·C₄H₂O₄^2-

Online 11 February 2003

 

Acta Cryst. (2003). C59, o107-o110  [ doi:10.1107/S0108270102023594 ]

Three bis-ortho-diynylarenes (BODA)

K. P. U. Perera, K. A. Abboud, D. W. Smith and M. Krawiec

Formula: C₄₄H₂₆, C₄₄H₂₆O and C₄₇H₃₂

Online 11 February 2003

 

Acta Cryst. (2003). C59, o111-o113  [ doi:10.1107/S0108270103000908 ]

2-(6-Bromopyridin-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane and (6-bromopyridin-3-yl)boronic acid, new bifunctional building blocks for combinatorial chemistry

J. Sopková-de Oliveira Santos, J.-C. Lancelot, A. Bouillon and S. Rault

Formula: C₁₁H₁₅BBrNO₂ and C₅H₅BBrNO₂

Online 11 February 2003

 

Acta Cryst. (2003). C59, o114-o116  [ doi:10.1107/S0108270103001276 ]

1,2,4,5-Tetrakis(2-vinylpyridyl)benzene-dichloromethane (1/2)

B. T. Holmes, C. W. Padgett and W. T. Pennington

Formula: C₃₄H₂₆N₄·2CH₂Cl₂

Online 11 February 2003

 

Acta Cryst. (2003). C59, o117-o119  [ doi:10.1107/S010827010300088X ]

5-Phenyl-9H-1,3-dioxolo[4,5-h][2,3]benzodiazepin-8(7H)-one

G. Bruno, F. Nicoló, R. Gitto, N. Micale and G. Rosace

Formula: C₁₆H₁₂N₂O₃

Online 11 February 2003

 

Acta Cryst. (2003). C59, o120-o123  [ doi:10.1107/S0108270103001471 ]

Bis(tetraethylammonium) hydrogensulfate dihydrogenphosphate at 292 and 150 K

J. Fábry, R. Krupková, I. Císarová and K. Jurek

Formula: 2C₈H₂₀N⁺·HSO₄^-·H₂PO₄^- at 292 and 150 K

Online 11 February 2003

 

Acta Cryst. (2003). C59, o124-o126  [ doi:10.1107/S0108270103001860 ]

(4-Nitrophenylsulfinyl)acetic acid, a three-dimensional hydrogen-bonded framework built from a combination of two-centre O-HO and C-HO hydrogen bonds and a three-centre C-H(O)₂ hydrogen bond

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C₈H₇NO₅S

Online 18 February 2003

 

Acta Cryst. (2003). C59, o127-o128  [ doi:10.1107/S0108270103002300 ]

Pomiferin

J. Marek, D. Veselá, M. Lisková and M. Zemlicka

Formula: C₂₅H₂₄O₆

Online 18 February 2003

 

Acta Cryst. (2003). C59, o129-o131  [ doi:10.1107/S0108270103001963 ]

2,7,12,17-Tetraoxa-3,4:5,6:13,14:15,16-tetrabenzodispiro[8.1.8.0]nonadecane

K. Stadnicka and P. Szlachcic

Formula: C₃₁H₂₆O₄

Online 18 February 2003

 

Acta Cryst. (2003). C59, o132-o134  [ doi:10.1107/S0108270103002452 ]

Dimethyl 6-methoxy-4a-methyl-9-oxo-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1,1-dicarboxylate

S. Mondal, M. Mukherjee, A. Roy and D. Mukherjee

Formula: C₂₀H₂₄O₆

Online 18 February 2003

 

Acta Cryst. (2003). C59, o135-o136  [ doi:10.1107/S0108270103002464 ]

Benzaldehyde 2,4-dinitrophenylhydrazone

S. Shan, D.-J. Xu, C.-H. Hung, J.-Y. Wu and M. Y. Chiang

Formula: C₁₃H₁₀N₄O₄

Online 18 February 2003

 

Acta Cryst. (2003). C59, o137-o140  [ doi:10.1107/S0108270103001410 ]

N-{4-Bromo-2-[(3-bromo-1-phenylsulfonyl-1H-indol-2-yl)methyl]-5-methoxyphenyl}acetamide

T. Ravishankar, K. Chinnakali, N. Arumugam, P. C. Srinivasan, A. Usman and H.-K. Fun

Formula: C₂₄H₂₀Br₂N₂O₄S

Online 18 February 2003

 

Acta Cryst. (2003). C59, o141-o143  [ doi:10.1107/S0108270103002312 ]

Two 2,2-dihalo-N-(1-phenylethyl)cyclopropane-1-carboxamides

D. S. Yufit and J. A. K. Howard

Formula: C₁₂H₁₃Cl₂NO and C₁₂H₁₃F₂NO

Online 18 February 2003

 

Acta Cryst. (2003). C59, o144-o146  [ doi:10.1107/S0108270103002555 ]

3-Nitrophthalic acid: C(4) and R₂²(8) motifs of O-HO hydrogen bonds generate sheets which are linked by C-HO hydrogen bonds

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C₈H₅NO₆

Online 18 February 2003

 

Acta Cryst. (2003). C59, o147-o149  [ doi:10.1107/S0108270103002804 ]

meso-5,5,7,12,12,14-Hexamethyl-1,4-diaza-8,11-diazoniacyclotetradecane bis(2-naphthoate) ethanol disolvate: centrosymmetric five-component aggregates linked into sheets by C-H(arene) hydrogen bonding

K. F. Bowes, G. Ferguson, A. J. Lough and C. Glidewell

Formula: C₁₆H₃₈N₄²⁺·2C₁₁H₇O₂^-·2C₂H₆O

Online 18 February 2003

 

Acta Cryst. (2003). C59, o150-o152  [ doi:10.1107/S0108270103002580 ]

A perchlorate salt of an octaprotonated cryptand

V. McKee and G. G. Morgan

Formula: C₃₃H₅₉N₁₁⁸⁺·8ClO₄^-·5H₂O

Online 18 February 2003

 

Acta Cryst. (2003). C59, o153-o155  [ doi:10.1107/S0108270102022758 ]

2-Nitroso-1,3-diphenyl-1,2,3,4-tetrahydrobenzo[b][1,6]naphthyridine

B. Sivakumar, K. SethuSankar, U. P. Senthil Kumar, R. Jeyaraman and D. Velmurugan

Formula: C₂₄H₁₉N₃O

Online 18 February 2003

 

Acta Cryst. (2003). C59, o156-o158  [ doi:10.1107/S0108270103000878 ]

A cis-stilbene derivative

K. SethuSankar, S. Saravanan, D. Velmurugan and M. Parvez

Formula: C₁₅H₁₀N₄O₉

Online 18 February 2003

 

Acta Cryst. (2003). C59, o159-o161  [ doi:10.1107/S0108270103002567 ]

N-Carboxy-L-aspartic anhydride benzyl ester

H. Kanazawa and J. Magoshi

Formula: C₁₂H₁₁NO₅

Online 28 February 2003

 

Acta Cryst. (2003). C59, o162-o164  [ doi:10.1107/S0108270102023739 ]

An azonia derivative of hexahelicene

K. Sato, S. Arai, T. Yamagishi and T. Tanase

Formula: C₂₅H₁₆N⁺·PF₆^-

Online 28 February 2003

 

Acta Cryst. (2003). C59, o165-o166  [ doi:10.1107/S0108270103002610 ]

Methyl 2,6-dicarboxybenzoate

S. H. Dale and M. R. J. Elsegood

Formula: C₁₀H₈O₆

Online 28 February 2003

 

Acta Cryst. (2003). C59, o167-o170  [ doi:10.1107/S0108270103001495 ]

The epimeric 9-oxobicyclo[3.3.1]nonane-3-carboxylic acids: hydrogen-bonding patterns of the endo acid and the lactol of the exo acid

M. M. Papadakis, J. A. Pavon, R. A. Lalancette and H. W. Thompson

Formula: Two isomers of C₁₀H₁₄O₃

Online 28 February 2003

 

Acta Cryst. (2003). C59, o171-o173  [ doi:10.1107/S0108270103002865 ]

Methyl 3-O--L-fucopyranosyl -D-glucopyranoside trihydrate

M. Färnbäck, L. Eriksson and G. Widmalm

Formula: C₁₃H₂₄O₁₀·3H₂O

Online 28 February 2003

 

Acta Cryst. (2003). C59, o174-o176  [ doi:10.1107/S0108270103001355 ]

Taxiphyllin from Henriettella fascicularis

A. I. Calderón, C. Terreaux, M. P. Gupta, K. Hostettmann and K. J. Schenk

Formula: C₁₄H₁₇NO₇·2H₂O

Online 28 February 2003

 

Acta Cryst. (2003). C59, o177-o178  [ doi:10.1107/S0108270103000842 ]

5-Bromo-2,3-dihydro-4-methyl-3-nitrothiophene 1,1-dioxide

L. H. Strauss, V. V. Abzianidze, V. M. Berestovitskaya and I. E. Efremova

Formula: C₅H₆BrNO₄S

Online 28 February 2003

 

Acta Cryst. (2003). C59, e9  [ doi:10.1107/S0108270103004189 ]

A new polymorph of cis-transoid-cis-dicyclohexano-18-crown-6. Erratum

V. Ch. Kravtsov, M. S. Fonari, M. J. Zaworotko and J. Lipkowski

Synopsis: Erratum to Acta Cryst. (2002), C58, o683-o684.

Online 28 February 2003

 

Acta Cryst. (2003). C59, e10  [ doi:10.1107/S0108270102018085 ]

(1S,3R,8S,9S,10R)-2,2-Dichloro-9,10-epoxy-3,7,7,10-tetramethyltricyclo[6.4.0.0^1,3]dodecane and (1S,3R,8S,10R)-2,2-dichloro-3,7,7,10-tetramethyltricyclo[6.4.0.0^1,3]dodecan-9-one. Erratum

M. Dakir, A. Auhmani, H. El Jamili, M. Akssira, A. Benharref, A. Kenz and M. Pierrot

Synopsis: Erratum to Acta Cryst. (2002), C58, o518-o520.

Online 28 February 2003