Acta Crystallographica Section C

Crystal Structure Communications

Volume 59, Part 6 (June 2003)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: Selectively labeled view of bis(4-methylpiperidine)(5,10,15,20-tetraphenylporphyrinato)iron(II), with ellipsoids at the 35% probability level. Only the H atoms attached to the piperidine N atoms are shown. See Munro & Ntshangase [Acta Cryst. (2003), C59, m224-m227].

inorganic compounds


 

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Acta Cryst. (2003). C59, i41-i44  [ doi:10.1107/S0108270103008552 ]

Cu3V10O28·24H2O and CuNa4V10O28·23H2O

A. Iida and T. Ozeki

Synopsis: Cu3V10O28·24H2O and CuNa4V10O28·23H2O exhibit catenary structures of [V10O28]6- anions linked by Cu2+ cations and by Na+ cations, respectively.

Formula: Cu3V10O28·24H2O and CuNa4V10O28·23H2O

Online 20 May 2003


 

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Acta Cryst. (2003). C59, i45-i46  [ doi:10.1107/S0108270103006486 ]

Raman spectroscopy of silver pertechnetate

M. J. Sarsfield, A. D. Sutton, F. R. Livens, I. May and R. J. Taylor

Synopsis: The title compound contains short Ag-O bonds supported by the reduction of the Raman stretching frequency of the Tc-O bonds.

Formula: AgTcO4

Online 20 May 2003


 

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Acta Cryst. (2003). C59, i47-i49  [ doi:10.1107/S0108270103009685 ]

A new polytype of orthoboric acid, H3BO3-3T

R. R. Shuvalov and P. C. Burns

Synopsis: The trigonal polytype of orthoboric acid consists of pseudo-hexagonal sheets of hydrogen-bonded B(OH)3 molecules, with van der Waals forces binding adjacent sheets and repetition after every third sheet.

Formula: H3BO3

Online 31 May 2003


 

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Acta Cryst. (2003). C59, i50-i52  [ doi:10.1107/S0108270103008047 ]

A new aquahydroxidocopper(II) oxovanadium(IV) vanadate, Cu(H2O)(OH)VO(VO4)

J.-C. Trombe, P. Rozier and J. Galy

Synopsis: Single crystals of a new aquahydroxidocopper(II) oxovanadium(IV) vanadate have been synthesized hydrothermally at 473 K. The three-dimensional structure presents layers of vanadate tetrahedra and distorted oxovanadium octahedra connected by Cu atoms.

Formula: Cu(H2O)(OH)VO(VO4)

Online 31 May 2003


 

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Acta Cryst. (2003). C59, i53-i54  [ doi:10.1107/S0108270103009715 ]

A synthetic zinc tellurium oxochloride, Zn2(TeO3)Cl2

M. Johnsson and K. W. Törnroos

Synopsis: Zn2(TeO3)Cl2 has a layered structure in which the Cl atoms and the 5s2 lone pairs of the TeIV atom protrude from the surfaces of each layer towards adjacent layers, which are only held together by dispersion forces. The compound is isostructural with the synthetic compound CuZn(TeO3)Cl2 and the mineral sophiite, Zn2(SeO3)Cl2.

Formula: Zn2(TeO3)Cl2

Online 31 May 2003


 

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Acta Cryst. (2003). C59, i55-i56  [ doi:10.1107/S0108270103009570 ]

A mixed-valent niobium oxysulfide, La2Nb3S2O8

L. Cario, H. Kabbour, C. Guillot-Deudon and A. Meerschaut

Synopsis: Dilanthanum triniobium disulfide octaoxide, La2Nb3S2O8, crystallizes in the orthorhombic space group Pnnm and is isostructural with the Ln2Ta3X2O8 (Ln = La, Ce, Pr and Nd, and X = S and Se) family of tantalum compounds.

Formula: La2Nb3S2O8

Online 31 May 2003


 

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Acta Cryst. (2003). C59, i57-i58  [ doi:10.1107/S0108270103010084 ]

KHCoP2O7·2H2O: a novel acidic pyrophosphate

M. Harcharras, K. Goubitz, A. Ennaciri, H. Assaaoudi and H. Schenk

Synopsis: The title compound is a new acidic pyrophosphate metallate. It consists of cobalt-pyrophosphate layers joined by K+ ions and H-atom bridges. The Co2+ ions are octahedrally surrounded by four pyrophosphate O atoms and two water molecules.

Formula: KHCoP2O7·2H2O

Online 31 May 2003


metal-organic compounds


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Acta Cryst. (2003). C59, m201-m203  [ doi:10.1107/S0108270103007613 ]

Bis{4-[N,N-bis(2-cyanoethyl)amino]pyridine-[kappa]N1}silver(I) perchlorate, with the perchlorate anion located in the cation cavity

J. Ni, Y.-Z. Li, Z. Xue, H.-L. Chen and Z.-L. Wang

Formula: [Ag(C11H12N4)2]ClO4

Online 10 May 2003


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Acta Cryst. (2003). C59, m204-m206  [ doi:10.1107/S0108270103008321 ]

The layered structure of poly[[di-[mu]-chloro-bis[chloro(2-ethyltetrazole-[kappa]N4)copper(II)]]-di-[mu]-2-ethyltetrazole-[kappa]2N1:N4]

A. S. Lyakhov, P. N. Gaponik, M. M. Degtyarik and L. S. Ivashkevich

Formula: [CuCl2(C3H6N4)2]

Online 10 May 2003


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Acta Cryst. (2003). C59, m207-m211  [ doi:10.1107/S0108270102023600 ]

Isostructural or not? Adducts of some aryltin halides with (E)-1,2-bis(4-pyridyl)ethene

S. A. Bajue, C. Lewis, K. Clarke, F. B. Bramwell, B. O. Patrick and C. P. Brock

Formula: Four [Sn2(aryl)6X2(C12H10N2)] structures

Online 10 May 2003


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Acta Cryst. (2003). C59, m212-m214  [ doi:10.1107/S0108270103008503 ]

Ferrocene compounds. XXXVIII. Dimethyl ferrocene-1,1'-dicarboxylate

M. Cetina, M. Jukic, V. Rapic and A. Golobic

Formula: [Fe(C7H7O2)2]

Online 20 May 2003


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Acta Cryst. (2003). C59, m215-m217  [ doi:10.1107/S0108270103007716 ]

trans-Bis[1,2-bis(diphenylphosphino)ethane-[kappa]2P,P']bis[4-(trimethylsilyl)buta-1,3-diynyl]ruthenium(II) and trans-bis[1,2-bis(diphenylphosphino)ethane-[kappa]2P,P']bis(buta-1,3-diynyl)ruthenium(II)

J. N. Anderson, N. J. Brookes, B. J. Coe, S. J. Coles, M. E. Light and M. B. Hursthouse

Formula: [Ru(C7H9Si)2(C26H24P2)2] and [Ru(C4H)2(C26H24P2)2]

Online 20 May 2003


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Acta Cryst. (2003). C59, m218-m220  [ doi:10.1107/S0108270103008916 ]

Bis(2-aminopyridine-[kappa]N1)(benzoato-[kappa]O)silver(I)

H.-L. Zhu, A. Usman, H.-K. Fun and X.-J. Wang

Formula: [Ag(C7H5O2)(C5H6N2)2]

Online 20 May 2003


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Acta Cryst. (2003). C59, m221-m223  [ doi:10.1107/S0108270103008977 ]

catena-Poly[[bis[[mu]-1,2-bis(1-methyltetrazol-5-yl)ethane-[kappa]2N4:N4']bis[chlorocopper(II)]]-di-[mu]-chloro]

D. O. Ivashkevich, A. S. Lyakhov, D. S. Pytleva, S. V. Voitekhovich and P. N. Gaponik

Formula: [Cu2Cl4(C6H10N8)2]

Online 20 May 2003


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Acta Cryst. (2003). C59, m224-m227  [ doi:10.1107/S0108270103008734 ]

[Fe(TPP)(4-MePip)2]: an axially compressed bis(secondary amine) complex of an iron(II) porphyrin

O. Q. Munro and M. M. Ntshangase

Formula: [Fe(C44H28N4)(C6H13N)2]

Online 20 May 2003


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Acta Cryst. (2003). C59, m228-m230  [ doi:10.1107/S0108270103008722 ]

Cobalt(II) and nickel(II) complexes of quinoline-2-carboxylate

N. Okabe and Y. Muranishi

Formula: [M(C10H6NO2)2(H2O)2]·2CH4O·2H2O (M = Co and Ni)

Online 20 May 2003


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Acta Cryst. (2003). C59, m231-m233  [ doi:10.1107/S0108270103009636 ]

An alkoxide cluster with 18 Li+ ions encapsulating two borate anions, [(tBuO)12Li18(BO3)2]

M. Tombul, R. J. Errington, R. A. Coxall and W. Clegg

Formula: [Li18(BO3)2(C4H9O)12]

Online 31 May 2003


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Acta Cryst. (2003). C59, m234-m236  [ doi:10.1107/S0108270103008904 ]

Bis[[mu]-1,2-bis(2-pyridyl)ethyne-[kappa]2N:N']bis[aquadinitratocadmium(II)]

M. B. Zaman, M. J. Davis, M. D. Smith and H.-C. zur Loye

Formula: [Cd2(NO3)4(C12H8N2)2(H2O)2]

Online 31 May 2003


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Acta Cryst. (2003). C59, m237-m240  [ doi:10.1107/S0108270103009417 ]

Two isomorphous complexes: dichloro[phthalocyaninato(2-)]tin(IV) and dichloro[phthalocyaninato(2-)]germanium(IV)

J. Janczak and R. Kubiak

Formula: [Sn(C32H16N8)Cl2] and [Ge(C32H16N8)Cl2]

Online 31 May 2003


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Acta Cryst. (2003). C59, m241-m242  [ doi:10.1107/S0108270103010035 ]

Bis[N,N'-diisopropyl-N-(trimethylsilyl)benzamidinium] di-[mu]-chloro-bis[tetrachlorozirconate(IV)] dichloromethane disolvate

R. Centore, A. Tuzi and D. Liguori

Formula: (C16H29N2Si)2[Zr2Cl10]·2CH2Cl2

Online 31 May 2003


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Acta Cryst. (2003). C59, m243-m245  [ doi:10.1107/S0108270103008357 ]

Bis(cyanoguanidine)silver(I) nitrate-cyanoguanidine (1/1)

R. Dronskowski and X.-H. Liu

Formula: [Ag(C2H4N4)2](NO3)·C2H4N4

Online 31 May 2003


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Acta Cryst. (2003). C59, m246-m248  [ doi:10.1107/S0108270103008382 ]

A bis(acetylacetonato)uranium(IV) complex of the Schiff base N,N'-bis(3-hydroxysalicylidene)-2-methyl-1,2-propanediamine

L. Salmon, P. Thuéry and M. Ephritikhine

Formula: [U(C18H18N2O4)(C5H7O2)2]·C4H8O

Online 31 May 2003


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Acta Cryst. (2003). C59, m249-m251  [ doi:10.1107/S0108270103010151 ]

Low-dimensional compounds containing cyano groups. VI. A unique two- and one-dimensional structure in amminebis(1,4-diaminobutane)tetrakis[dicyanoargentato(I)]dicopper(II) dihydrate

I. Potocnák, L. Triscíková and C. Wagner

Formula: [Ag4Cu2(CN)8(C4H12N2)2(NH3)]·2H2O

Online 31 May 2003


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Acta Cryst. (2003). C59, m252-m254  [ doi:10.1107/S0108270103010187 ]

Low-dimensional compounds containing cyano groups. VII. (Dicyanamido-[kappa]N1)bis(1,10-phenanthroline-[kappa]2N,N')copper(II) trifluoromethanesulfonate

I. Potocnák, M. Burcák, C. Wagner and L. Jäger

Formula: [Cu(C2N3)(C12H8N2)2](CF3SO3)

Online 31 May 2003


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Acta Cryst. (2003). C59, m255-m258  [ doi:10.1107/S0108270103009703 ]

Barium bis[6-amino-3-methyl-5-nitrosopyrimidine-2,4(1H,3H)-dionate] trihydrate: coordination polymer chains linked by hydrogen bonds

R. López Garzón, M. L. Godino Salido, J. N. Low and C. Glidewell

Formula: [Ba(C5H5N4O3)2(H2O)3]

Online 31 May 2003


organic compounds


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Acta Cryst. (2003). C59, o283-o285  [ doi:10.1107/S010827010300708X ]

(2RS)-5,6:7,8-Dibenzobicyclo[2.2.2]octan-2-ol

K. W. Muir, D. G. Morris and K. S. Ryder

Formula: C16H14O

Online 10 May 2003


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Acta Cryst. (2003). C59, o286-o288  [ doi:10.1107/S0108270103005286 ]

Hydrogen bonding in N,N'-bis[(1S)-2-azido-1-(2-methylpropyl)ethyl]oxalamide: twofold symmetry of R\bf{_2^2}(10) hydrogen-bonded dimers connected into an [alpha]-network

Z. Stefanic, B. Kojic-Prodic, Z. Dzolic, D. Katalenic, M. Zinic and A. Meden

Formula: C14H26N8O2

Online 10 May 2003


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Acta Cryst. (2003). C59, o289-o292  [ doi:10.1107/S0108270103007649 ]

Two members of the bisphosphonate class of drugs: a zwitterion and a molecular compound

D. Fernández, D. Vega and J. A. Ellena

Formula: C3H11NO6P2 and C5H13NO7P2·2H2O

Online 10 May 2003


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Acta Cryst. (2003). C59, o293-o297  [ doi:10.1107/S0108270103007686 ]

3,6-Dichloro-4-[2-(4-thiamorpholino)ethanesulfanyl]pyridazine and 3,6-bis(pyrazol-1-yl)-4-[2-(4-thiamorpholino)ethanesulfanyl]pyridazine

A. J. Blake, P. Hubberstey, A. D. Mackrell and C. Wilson

Formula: C10H13Cl2N3S2 and C16H19N7S2

Online 10 May 2003


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Acta Cryst. (2003). C59, o298-o301  [ doi:10.1107/S0108270103008345 ]

Derivatives of 4-(2-hydroxylphenyl)-2-phenyl-2,3-dihydro-1,5-benzothiazepine

M. Parvez, S. Umbreen and F. L. Ansari

Formula: C21H16ClNOS, C22H19NOS and C22H19NO2S

Online 10 May 2003


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Acta Cryst. (2003). C59, o302-o304  [ doi:10.1107/S0108270103008679 ]

1-(2-Hydroxy-4-methoxyphenyl)-3-(2,3,4-trimethoxyphenyl)prop-2-en-1-one

A. Subbiah Pandi, D. Velmurugan, S. Shanmuga Sundara Raj, H.-K. Fun and M. C. Bansal

Formula: C19H20O6

Online 10 May 2003


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Acta Cryst. (2003). C59, o305-o307  [ doi:10.1107/S0108270103008680 ]

1-Acetyl-4'-ethyl-2a'-phenyl-2',2a',5',5a'-tetrahydrospiro[1H-indole-3,2'-oxeto[5,4-b]oxazol]-2(3H)-one and 1-acetyl-4',5a'-diphenyl-2',2a',5',5a'-tetrahydrospiro[1H-indole-3,2'-oxeto[5,4-b]oxazol]-2(3H)-one

A. Usman, H.-K. Fun, L. Wang, Y. Zhang and J.-H. Xu

Formula: C21H18N2O4 and C25H18N2O4

Online 10 May 2003


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Acta Cryst. (2003). C59, o308-o310  [ doi:10.1107/S0108270103007625 ]

9,10-Diphenyl-9,10-epidioxyanthracene and 9,10-dihydro-10,10-dimethoxy-9-phenylanthracen-9-ol

A. Usman, H.-K. Fun, Y. Li and J.-H. Xu

Formula: C26H18O2 and C22H20O3

Online 10 May 2003


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Acta Cryst. (2003). C59, o311-o313  [ doi:10.1107/S0108270103008370 ]

(E,E,E)-1,6-Bis(2,4-dichlorophenyl)hexa-1,3,5-triene

Y. Sonoda, Y. Kawanishi and M. Goto

Formula: C18H12Cl4

Online 20 May 2003


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Acta Cryst. (2003). C59, o314-o316  [ doi:10.1107/S0108270103008369 ]

Dispiro[adamantane-2,2'-1',3',6',9',11',14'-hexathiacyclohexadecane-10',2''-adamantane]

A. Visnjevac, B. Kojic-Prodic, M. Vinkovic and K. Mlinaric-Majerski

Formula: C28H44S6

Online 20 May 2003


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Acta Cryst. (2003). C59, o317-o320  [ doi:10.1107/S0108270103008564 ]

(1R,3S,6S)-6-tert-Butyl-1-hydroxymethyl-5-methoxy-6-methyl-7-oxa-4-azaspiro[2.5]oct-4-en-8-one and dimethyl [(1S,1'R,3'S,6'S)-(6'-tert-butyl-5'-methoxy-6'-methyl-8'-oxo-7'-oxa-4'-azaspiro[2.5]oct-4'-en-1'-yl)hydroxymethyl]phosphonate

M. Malecka, K. T. Wanner and E. Budzisz

Formula: C13H21NO4 and C15H26NO7P

Online 20 May 2003


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Acta Cryst. (2003). C59, o321-o322  [ doi:10.1107/S0108270103008394 ]

6-(2-Hydroxybenzoyl)-5-(pyrrol-2-yl)-3H-pyrrolizine

S. P. Dey, D. K. Dey, A. K. Mallik and L. Dahlenburg

Formula: C18H14N2O2

Online 20 May 2003


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Acta Cryst. (2003). C59, o323-o325  [ doi:10.1107/S010827010300369X ]

cis,cis-Ceratospongamide N,N-dimethylacetamide hemisolvate in the presence of twinning

M. Doi, A. Asano and K. Yoza

Formula: C41H49N7O6S·0.5C4H9NO

Online 20 May 2003


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Acta Cryst. (2003). C59, o326-o328  [ doi:10.1107/S0108270103009181 ]

Ammonium N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl)glycinate monohydrate forms hydrogen-bonded bilayers

P. Arranz Mascarós, R. Cuesta Martos, C. Glidewell and J. N. Low

Formula: NH4+·C7H8N5O4-·H2O

Online 20 May 2003


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Acta Cryst. (2003). C59, o329-o331  [ doi:10.1107/S010827010300920X ]

meso-5,5,7,12,12,14-Hexamethyl-4,11-diaza-1,8-diazoniacyclotetradecane (S)-malate(2-) methanol disolvate: a chain of rings generated by two pairs of N-H...O hydrogen bonds

K. F. Bowes, G. Ferguson, A. J. Lough and C. Glidewell

Formula: C16H38N42+·C4H4O52-·2CH4O

Online 20 May 2003


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Acta Cryst. (2003). C59, o332-o334  [ doi:10.1107/S0108270103008333 ]

Two bis(ammonium) 1,5-naphthalenedisulfonate salts

S. Sakwa and K. A. Wheeler

Formula: 2NH4+·C10H6O6S22- and 2C7H15N4O+·C10H6O6S22-

Online 20 May 2003


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Acta Cryst. (2003). C59, o335-o337  [ doi:10.1107/S0108270103009223 ]

Hydrogen-bonded dimers of 1,8,10-trihydroxy-10-(prop-2-enyl)anthracen-9(10H)-one: S(6), R^{\bf 1}_{\bf 2}(10) and R^{\bf 2}_{\bf 2}(14) motifs

S. Thamotharan, V. Parthasarathi, S. Kumar, V. Kumar and A. Linden

Formula: C17H14O4

Online 20 May 2003


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Acta Cryst. (2003). C59, o338-o339  [ doi:10.1107/S0108270103007273 ]

2-Allenyl-2H-benzotriazole

H. Maeda, A. Osuka and H. Furuta

Formula: C9H7N3

Online 20 May 2003


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Acta Cryst. (2003). C59, o340-o342  [ doi:10.1107/S0108270103009302 ]

6-Amino-3-methyl-5-nitrosopyrimidine-2,4(1H,3H)-dione forms a three-dimensional hydrogen-bonded framework structure

M. L. Godino Salido, M. D. Gutiérrez Valero, J. N. Low and C. Glidewell

Formula: C5H6N4O3

Online 31 May 2003


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Acta Cryst. (2003). C59, o343-o345  [ doi:10.1107/S010827010300948X ]

1,4,7-Tris(2-cyanoethyl)-4,7-triaza-1-azoniacyclononane perchlorate

W.-B. Qi, Y.-Z. Li, J. Ni and Z.-L. Wang

Formula: C15H25N6+·ClO4-

Online 31 May 2003


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Acta Cryst. (2003). C59, o346-o348  [ doi:10.1107/S010827010300917X ]

t-3-Isopropyl-1-methyl-r-2,c-6-diphenylpiperidin-4-one thiosemicarbazone

N. Sampath, S. M. Malathy Sony, M. N. Ponnuswamy and M. Nethaji

Formula: C22H28N4S

Online 31 May 2003


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Acta Cryst. (2003). C59, o349-o352  [ doi:10.1107/S0108270103010047 ]

Bis(melaminium) DL-malate tetrahydrate

J. Janczak and G. J. Perpétuo

Formula: 2C3H7N6+·C4H4O52-·4H2O

Online 31 May 2003


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Acta Cryst. (2003). C59, o353-o356  [ doi:10.1107/S0108270103006656 ]

3-[2,6-Bis(diethylcarbamoyl)pyridin-4-yl]-N-(tert-butoxycarbonyl)alanine methyl ester: a chiral tridentate ligand that causes a diastereomeric excess of its lanthanide complexes in solution

G. Muller, B. Schmidt, J. Jiricek, J.-C.G. Bünzli and K. J. Schenk

Formula: C24H38N4O6

Online 31 May 2003


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