# GG1171 # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 0232 SHELXS97 TREF' _shelx_refln_list_code 4 _shelx_F_calc_maximum 122.13 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.7695 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.3625 _cell_length_b 9.5848 _cell_length_c 8.0433 _cell_angle_alpha 102.241 _cell_angle_beta 94.241 _cell_angle_gamma 97.773 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6283.46 5289.43 176.81 o 3 0 0 1965.16 1910.97 46.27 o 4 0 0 1826.42 1899.20 45.32 o 5 0 0 366.41 404.73 14.40 o 6 0 0 258.48 258.01 3.87 o 7 0 0 499.84 498.52 7.73 o 8 0 0 940.56 932.44 17.00 o 9 0 0 197.96 215.11 4.56 o 10 0 0 281.64 289.36 7.09 o 11 0 0 17.79 18.90 3.51 o 12 0 0 590.90 591.53 22.81 o 13 0 0 7.05 7.16 4.97 o 14 0 0 179.40 167.84 14.04 o -14 1 0 175.71 177.34 14.18 o -13 1 0 180.05 204.83 9.65 o -12 1 0 327.20 307.05 10.75 o -11 1 0 98.03 92.30 3.51 o -10 1 0 949.81 969.13 22.68 o -9 1 0 52.49 68.90 4.68 o -8 1 0 1292.96 1286.32 24.17 o -7 1 0 672.26 652.33 15.11 o -6 1 0 689.73 721.51 12.90 o -5 1 0 133.07 142.20 2.85 o -4 1 0 8866.93 8915.35 146.11 o -3 1 0 2039.69 2040.77 42.62 o -2 1 0 127.67 128.39 2.85 o 1 1 0 8108.55 0.89 87.94 o 2 1 0 180.44 189.21 4.68 o 3 1 0 217.86 267.10 3.72 o 4 1 0 3.32 10.50 1.39 o 5 1 0 188.67 216.56 4.75 o 6 1 0 47.39 51.09 2.56 o 7 1 0 520.22 566.20 16.52 o 8 1 0 3057.88 3186.43 57.90 o 9 1 0 159.11 155.09 9.43 o 10 1 0 281.24 304.08 7.87 o 11 1 0 370.27 359.36 11.26 o 12 1 0 17.99 20.47 6.58 o 13 1 0 485.47 461.12 26.90 o 14 1 0 3.67 -4.53 5.41 o -14 2 0 4.82 8.77 3.95 o -13 2 0 21.09 29.53 4.68 o -12 2 0 1007.07 1018.28 24.81 o -11 2 0 3.30 5.73 1.64 o -10 2 0 487.18 503.39 11.37 o -9 2 0 8.98 5.56 1.75 o -8 2 0 2004.98 1997.34 36.15 o -7 2 0 497.63 528.22 22.51 o -6 2 0 1202.86 1219.51 21.69 o -5 2 0 4182.19 4625.19 64.78 o -4 2 0 2092.60 2143.39 38.82 o -3 2 0 40.28 32.09 0.62 o -2 2 0 332.68 322.32 4.31 o -1 2 0 1554.56 1514.81 23.49 o 0 2 0 1451.53 1487.97 22.90 o 1 2 0 157.90 178.62 2.84 o 2 2 0 2931.75 2885.42 40.27 o 3 2 0 93.17 91.82 1.70 o 4 2 0 518.36 434.08 5.96 o 5 2 0 62.31 41.29 1.05 o 6 2 0 439.52 516.86 8.57 o 7 2 0 33.30 40.66 2.63 o 8 2 0 27.71 32.56 1.29 o 9 2 0 1551.61 1590.53 40.79 o 10 2 0 371.60 364.07 9.55 o 11 2 0 566.40 567.84 17.69 o 12 2 0 347.74 345.76 15.35 o 13 2 0 62.07 51.17 7.46 o -14 3 0 64.78 60.97 5.70 o -13 3 0 64.85 57.27 5.85 o -12 3 0 572.08 583.24 13.75 o -11 3 0 495.03 523.70 16.23 o -10 3 0 2.70 2.11 3.14 o -9 3 0 4078.32 4046.64 73.37 o -8 3 0 448.05 429.19 8.60 o -7 3 0 3591.71 3606.54 59.30 o -6 3 0 2049.08 2195.63 34.67 o -5 3 0 1403.29 1416.80 20.00 o -4 3 0 12386.06 12452.14 254.79 o -3 3 0 408.02 397.84 7.46 o -2 3 0 8.86 16.63 2.05 o -1 3 0 194.06 179.47 4.24 o 0 3 0 291.83 245.73 4.02 o 1 3 0 395.63 352.69 5.79 o 2 3 0 55.12 72.79 2.12 o 3 3 0 869.74 798.81 14.33 o 4 3 0 1.19 1.17 0.80 o 5 3 0 979.29 984.66 15.72 o 6 3 0 494.25 497.97 13.52 o 7 3 0 529.21 525.75 9.09 o 8 3 0 605.90 607.82 12.25 o 9 3 0 264.55 249.96 6.35 o 10 3 0 1323.77 1283.93 35.09 o 11 3 0 12.21 14.33 2.34 o 12 3 0 174.88 169.59 10.09 o 13 3 0 62.67 60.82 9.06 o -14 4 0 20.44 28.51 4.97 o -13 4 0 43.79 43.76 4.53 o -12 4 0 70.83 74.01 6.80 o -11 4 0 642.53 680.70 18.64 o -10 4 0 58.18 73.63 2.77 o -9 4 0 527.28 517.91 11.49 o -8 4 0 1539.59 1511.89 27.61 o -7 4 0 134.46 147.29 5.12 o -6 4 0 1536.79 1518.13 23.92 o -5 4 0 247.96 280.48 5.20 o -4 4 0 336.42 255.57 4.89 o -3 4 0 5.65 27.51 1.03 o -2 4 0 392.29 414.66 10.16 o -1 4 0 1185.97 1306.01 23.17 o 0 4 0 17.18 29.41 1.68 o 1 4 0 1379.53 1363.03 25.59 o 2 4 0 1502.48 1514.34 23.82 o 3 4 0 476.88 443.92 11.70 o 4 4 0 3269.74 3224.11 54.33 o 5 4 0 244.06 240.78 10.97 o 6 4 0 3971.37 3856.31 76.54 o 7 4 0 6.06 6.24 0.80 o 8 4 0 415.09 396.90 9.88 o 9 4 0 573.22 561.12 16.08 o 10 4 0 289.35 296.79 12.13 o 11 4 0 119.58 126.02 6.58 o 12 4 0 371.64 333.63 16.67 o -14 5 0 339.45 324.96 16.33 o -13 5 0 176.74 182.07 9.17 o -12 5 0 190.19 189.82 8.04 o -11 5 0 0.13 3.81 2.30 o -10 5 0 729.38 779.14 20.08 o -9 5 0 372.77 388.20 18.79 o -8 5 0 188.13 202.59 4.97 o -7 5 0 811.20 764.39 15.62 o -6 5 0 5.42 8.57 1.97 o -5 5 0 858.65 900.70 16.81 o -4 5 0 19.82 16.50 1.46 o -3 5 0 446.27 290.11 5.68 o -2 5 0 604.35 495.64 9.88 o -1 5 0 163.66 207.64 5.04 o 0 5 0 497.12 516.30 12.61 o 1 5 0 428.64 472.24 11.98 o 2 5 0 13374.83 13646.41 281.59 o 3 5 0 1963.66 1932.51 54.68 o 4 5 0 433.07 441.22 8.32 o 5 5 0 3017.29 2837.44 51.66 o 6 5 0 76.89 80.39 2.63 o 7 5 0 307.79 319.33 7.12 o 8 5 0 102.24 119.46 7.09 o 9 5 0 242.18 247.81 9.36 o 10 5 0 322.12 358.05 11.99 o 11 5 0 0.55 5.41 2.92 o 12 5 0 101.24 83.33 5.70 o -13 6 0 597.22 641.78 21.73 o -12 6 0 1.26 4.50 3.22 o -11 6 0 196.87 202.91 7.90 o -10 6 0 64.60 71.10 4.49 o -9 6 0 288.37 302.34 12.79 o -8 6 0 73.55 57.87 6.43 o -7 6 0 250.82 249.52 7.14 o -6 6 0 483.04 468.76 10.50 o -5 6 0 42.06 47.96 1.93 o -4 6 0 610.34 637.91 12.31 o -3 6 0 147.70 149.47 3.71 o -2 6 0 2633.28 2479.95 66.54 o -1 6 0 693.43 685.42 15.41 o 0 6 0 43.41 43.93 4.68 o 1 6 0 932.55 884.10 20.64 o 2 6 0 13.77 17.95 2.49 o 3 6 0 2403.91 2407.15 49.91 o 4 6 0 697.19 664.20 15.40 o 5 6 0 1240.50 1192.91 27.82 o 6 6 0 682.50 669.12 15.13 o 7 6 0 13.95 10.84 1.52 o 8 6 0 179.73 179.46 16.74 o 9 6 0 328.78 335.24 12.72 o 10 6 0 1416.93 1393.88 54.39 o 11 6 0 81.34 79.39 5.99 o -13 7 0 604.33 552.78 28.66 o -12 7 0 33.22 32.34 5.63 o -11 7 0 301.50 334.16 10.57 o -10 7 0 544.06 535.81 16.61 o -9 7 0 86.04 84.22 5.34 o -8 7 0 188.14 152.25 7.89 o -7 7 0 42.02 41.91 2.48 o -6 7 0 701.21 744.91 16.94 o -5 7 0 408.22 469.46 10.22 o -4 7 0 1.40 -0.24 1.12 o -3 7 0 4019.11 3940.22 73.13 o -2 7 0 69.97 72.40 5.26 o -1 7 0 961.12 886.81 21.80 o 0 7 0 771.07 777.08 20.63 o 1 7 0 996.13 970.30 23.06 o 2 7 0 1153.36 1112.72 25.68 o 3 7 0 26.47 33.52 3.66 o 4 7 0 278.43 276.12 16.74 o 5 7 0 135.78 122.07 5.11 o 6 7 0 219.74 224.47 9.80 o 7 7 0 62.57 73.88 12.13 o 8 7 0 1106.30 1151.79 31.00 o 9 7 0 87.93 65.06 5.56 o 10 7 0 99.40 92.69 7.02 o -12 8 0 4.48 8.28 7.16 o -11 8 0 185.02 204.43 19.15 o -10 8 0 139.86 148.20 6.27 o -9 8 0 255.43 276.05 8.14 o -8 8 0 149.87 149.90 4.99 o -7 8 0 1910.39 1718.10 43.98 o -6 8 0 582.39 552.09 14.33 o -5 8 0 624.40 674.19 25.37 o -4 8 0 1885.68 1917.21 37.01 o -3 8 0 63.84 70.55 6.51 o -2 8 0 7906.66 8146.37 168.62 o -1 8 0 2.81 7.98 4.39 o 0 8 0 378.63 379.00 10.18 o 1 8 0 93.34 102.05 4.24 o 2 8 0 43.72 45.98 2.94 o 3 8 0 35.28 44.28 5.92 o 4 8 0 75.62 69.61 6.80 o 5 8 0 109.77 109.86 7.53 o 6 8 0 16.45 14.28 3.07 o 7 8 0 276.60 311.16 24.78 o 8 8 0 120.66 145.03 8.33 o 9 8 0 78.45 64.62 6.43 o -11 9 0 76.82 56.71 5.09 o -10 9 0 57.83 53.06 12.87 o -9 9 0 446.98 447.70 13.54 o -8 9 0 186.23 197.39 5.73 o -7 9 0 211.55 197.16 6.60 o -6 9 0 1347.53 1348.34 34.64 o -5 9 0 126.80 123.95 10.16 o -4 9 0 273.87 320.23 10.75 o -3 9 0 140.63 142.26 4.80 o -2 9 0 34.78 37.41 3.36 o -1 9 0 1337.79 1378.11 32.98 o 0 9 0 96.86 102.72 4.65 o 1 9 0 841.00 874.01 22.82 o 2 9 0 1.57 4.64 2.27 o 3 9 0 89.98 89.26 4.37 o 4 9 0 278.87 273.70 23.47 o 5 9 0 103.86 98.86 9.21 o 6 9 0 1348.50 1427.94 58.24 o 7 9 0 91.65 85.76 10.31 o 8 9 0 494.22 465.50 23.25 o -10 10 0 96.25 84.94 9.65 o -9 10 0 30.04 23.62 2.77 o -8 10 0 143.59 137.88 5.69 o -7 10 0 644.87 671.95 34.50 o -6 10 0 153.05 152.66 9.14 o -5 10 0 457.53 464.69 15.76 o -4 10 0 76.83 70.70 5.48 o -3 10 0 266.42 289.52 13.45 o -2 10 0 17.63 15.26 2.56 o -1 10 0 7.01 7.71 3.22 o 0 10 0 42.24 38.39 4.97 o 1 10 0 82.00 82.35 5.92 o 2 10 0 18.56 20.33 3.23 o 3 10 0 48.36 53.22 4.21 o 4 10 0 3.51 5.61 3.15 o 5 10 0 82.80 92.85 6.59 o 6 10 0 8.27 4.18 12.87 o -8 11 0 30.89 28.80 4.24 o -7 11 0 244.71 251.06 10.60 o -6 11 0 147.53 177.14 21.49 o -5 11 0 465.49 485.67 17.36 o -4 11 0 61.25 51.68 4.32 o -3 11 0 1.89 6.25 4.53 o -2 11 0 31.45 36.01 5.34 o -1 11 0 254.19 248.93 9.92 o 0 11 0 120.39 124.48 6.65 o 1 11 0 473.66 480.59 17.17 o 2 11 0 35.86 37.69 3.81 o 3 11 0 1049.56 1099.13 38.52 o 4 11 0 9.40 10.43 5.37 o -4 12 0 248.50 267.42 24.12 o -3 12 0 570.83 550.56 22.08 o -2 12 0 133.24 130.12 8.21 o -1 12 0 555.94 541.25 21.41 o 0 12 0 78.91 75.93 6.43 o -1 -12 1 470.35 492.99 18.63 o 0 -12 1 287.57 301.50 12.46 o 1 -12 1 17.87 18.71 3.83 o 2 -12 1 422.33 430.96 34.65 o 3 -12 1 1.90 0.13 2.97 o 4 -12 1 566.46 570.63 19.56 o 5 -12 1 231.62 285.80 40.42 o -4 -11 1 552.89 523.73 22.38 o -3 -11 1 49.07 43.87 4.27 o -2 -11 1 381.33 400.70 14.05 o -1 -11 1 0.19 2.67 6.65 o 0 -11 1 115.70 95.65 5.40 o 1 -11 1 254.94 231.46 13.23 o 2 -11 1 23.91 25.65 3.75 o 3 -11 1 114.72 105.75 5.73 o 4 -11 1 58.13 69.75 4.36 o 5 -11 1 1964.12 2169.83 71.87 o 6 -11 1 96.46 103.51 5.78 o 7 -11 1 629.38 652.19 30.78 o 8 -11 1 24.01 12.58 3.30 o -6 -10 1 134.68 131.58 8.19 o -5 -10 1 258.42 267.82 14.37 o -4 -10 1 70.11 91.39 13.67 o -3 -10 1 201.93 203.69 7.84 o -2 -10 1 36.83 39.97 3.49 o -1 -10 1 544.68 550.20 21.71 o 0 -10 1 28.94 20.30 3.05 o 1 -10 1 584.47 614.40 28.51 o 2 -10 1 528.25 537.97 14.54 o 3 -10 1 663.90 700.53 20.07 o 4 -10 1 213.45 221.84 7.79 o 5 -10 1 64.27 70.11 4.00 o 6 -10 1 1053.43 1084.84 28.37 o 7 -10 1 91.30 114.34 8.77 o 8 -10 1 85.44 97.34 5.25 o 9 -10 1 201.79 193.89 10.26 o 10 -10 1 3.62 2.48 7.68 o -8 -9 1 136.17 131.87 12.87 o -7 -9 1 614.20 675.50 33.70 o -6 -9 1 235.95 259.57 11.38 o -5 -9 1 543.74 541.76 17.65 o -4 -9 1 55.77 57.01 5.04 o -3 -9 1 163.68 179.11 7.02 o -2 -9 1 242.02 259.06 16.30 o -1 -9 1 190.73 195.30 20.32 o 0 -9 1 272.35 262.77 8.24 o 1 -9 1 214.61 230.04 7.30 o 2 -9 1 252.34 282.66 8.48 o 3 -9 1 3.28 3.19 3.44 o 4 -9 1 47.01 47.89 4.46 o 5 -9 1 670.33 707.17 18.45 o 6 -9 1 4.88 2.95 4.02 o 7 -9 1 373.19 410.53 12.20 o 8 -9 1 2.56 4.34 1.39 o 9 -9 1 373.26 379.47 15.65 o 10 -9 1 117.05 109.98 6.58 o 11 -9 1 1.10 -2.00 5.26 o -9 -8 1 287.38 299.56 15.50 o -8 -8 1 126.63 102.68 7.99 o -7 -8 1 215.20 241.59 10.64 o -6 -8 1 430.42 459.87 18.15 o -5 -8 1 50.87 44.53 4.17 o -4 -8 1 244.25 227.94 7.13 o -3 -8 1 20.11 12.97 2.85 o -2 -8 1 862.91 847.54 33.41 o -1 -8 1 104.51 107.67 4.27 o 0 -8 1 998.77 946.79 21.61 o 1 -8 1 7228.01 7283.41 151.88 o 2 -8 1 17.37 32.80 2.77 o 3 -8 1 1413.07 1450.08 32.70 o 4 -8 1 82.21 70.50 7.24 o 5 -8 1 654.58 663.66 15.86 o 6 -8 1 855.84 809.16 20.57 o 7 -8 1 115.23 107.69 5.48 o 8 -8 1 1259.10 1278.13 33.03 o 9 -8 1 24.40 20.81 2.56 o 10 -8 1 366.25 381.73 18.64 o 11 -8 1 255.62 282.38 11.58 o 12 -8 1 229.25 207.96 9.48 o -10 -7 1 98.69 98.83 7.02 o -9 -7 1 822.48 791.68 31.58 o -8 -7 1 108.91 112.97 6.65 o -7 -7 1 107.38 106.51 4.65 o -6 -7 1 115.12 114.96 6.58 o -5 -7 1 457.10 470.21 11.24 o -4 -7 1 4.40 2.91 1.23 o -3 -7 1 1716.30 1652.36 58.77 o -2 -7 1 54.31 44.73 2.83 o -1 -7 1 1990.20 2046.39 44.08 o 0 -7 1 15.38 27.95 2.85 o 1 -7 1 746.85 691.91 18.19 o 2 -7 1 1982.92 1883.26 38.37 o 3 -7 1 47.08 41.49 2.38 o 4 -7 1 461.72 487.36 19.88 o 5 -7 1 46.82 50.47 8.41 o 6 -7 1 267.40 283.04 7.29 o 7 -7 1 917.78 924.06 23.33 o 8 -7 1 784.28 682.82 21.52 o 9 -7 1 2450.50 2416.06 54.04 o 10 -7 1 130.26 113.05 5.32 o 11 -7 1 516.08 537.04 18.49 o 12 -7 1 68.66 63.25 15.06 o 13 -7 1 46.96 39.63 8.33 o -11 -6 1 50.16 55.99 4.97 o -10 -6 1 26.90 26.61 3.51 o -9 -6 1 179.77 195.76 8.04 o -8 -6 1 413.18 406.69 10.96 o -7 -6 1 5.05 6.61 1.33 o -6 -6 1 34.14 36.24 2.05 o -5 -6 1 733.83 719.92 15.08 o -4 -6 1 630.65 602.68 11.89 o -3 -6 1 444.77 416.66 9.36 o -2 -6 1 404.40 340.49 15.94 o -1 -6 1 15.15 24.28 1.39 o 0 -6 1 832.98 774.66 15.68 o 1 -6 1 102.34 116.50 3.78 o 2 -6 1 558.71 486.84 11.82 o 3 -6 1 1509.16 1406.02 26.85 o 4 -6 1 72.20 82.46 7.82 o 5 -6 1 583.11 624.96 12.68 o 6 -6 1 8.01 14.09 1.90 o 7 -6 1 817.53 879.80 21.42 o 8 -6 1 447.23 453.40 21.93 o 9 -6 1 227.28 251.66 10.82 o 10 -6 1 1529.64 1479.46 31.78 o 11 -6 1 50.13 53.53 3.33 o 12 -6 1 346.98 352.80 14.84 o 13 -6 1 66.76 44.55 4.06 o -12 -5 1 1.51 -1.17 2.78 o -11 -5 1 415.30 391.38 18.28 o -10 -5 1 55.56 47.52 4.39 o -9 -5 1 621.83 608.34 17.98 o -8 -5 1 2557.82 2625.87 54.83 o -7 -5 1 101.38 93.47 7.97 o -6 -5 1 1561.43 1611.17 29.64 o -5 -5 1 622.27 574.90 11.34 o -4 -5 1 1998.37 2074.16 38.16 o -3 -5 1 3263.47 3423.06 80.04 o -2 -5 1 642.94 671.72 12.76 o -1 -5 1 4874.15 5102.13 106.07 o 0 -5 1 174.41 203.88 4.55 o 1 -5 1 2189.55 2242.61 42.90 o 2 -5 1 195.41 181.13 4.22 o 3 -5 1 2386.85 2194.25 38.13 o 4 -5 1 1848.67 1808.80 27.95 o 5 -5 1 406.79 443.13 10.45 o 6 -5 1 248.54 309.26 5.84 o 7 -5 1 1044.90 1045.77 20.55 o 8 -5 1 655.51 692.28 16.89 o 9 -5 1 208.25 223.47 11.11 o 10 -5 1 4.12 10.97 1.91 o 11 -5 1 1264.24 1305.97 28.80 o 12 -5 1 3.45 4.61 2.58 o 13 -5 1 14.29 20.46 2.73 o 14 -5 1 0.92 -3.22 3.80 o -13 -4 1 47.23 44.59 6.29 o -12 -4 1 39.21 42.40 4.09 o -11 -4 1 38.46 39.47 3.80 o -10 -4 1 769.90 793.28 24.56 o -9 -4 1 143.35 130.07 5.71 o -8 -4 1 1090.75 1141.78 23.27 o -7 -4 1 653.71 715.05 17.11 o -6 -4 1 548.15 534.09 9.82 o -5 -4 1 2008.53 1981.78 29.89 o -4 -4 1 94.08 71.47 2.27 o -3 -4 1 637.65 607.31 9.82 o -2 -4 1 99.85 87.83 2.10 o -1 -4 1 310.02 272.60 7.38 o 0 -4 1 2876.70 2910.33 36.62 o 1 -4 1 497.54 470.85 6.94 o 2 -4 1 626.51 501.16 7.26 o 3 -4 1 1825.23 1682.02 24.09 o 4 -4 1 215.32 176.58 3.07 o 5 -4 1 5.16 4.44 1.46 o 6 -4 1 21.03 15.73 1.61 o 7 -4 1 1347.61 1310.70 26.97 o 8 -4 1 1.51 5.86 1.23 o 9 -4 1 237.84 234.49 9.21 o 10 -4 1 39.15 38.23 2.12 o 11 -4 1 392.52 418.68 12.21 o 12 -4 1 451.81 484.90 11.38 o 13 -4 1 0.12 1.59 2.41 o 14 -4 1 23.35 15.94 3.95 o -13 -3 1 158.53 137.87 12.28 o -12 -3 1 320.54 295.18 12.13 o -11 -3 1 38.54 45.32 5.70 o -10 -3 1 168.07 157.22 5.73 o -9 -3 1 2854.73 2806.53 68.71 o -8 -3 1 442.46 432.32 9.34 o -7 -3 1 1577.57 1605.56 28.95 o -6 -3 1 870.31 931.84 31.07 o -5 -3 1 341.10 343.34 5.51 o -4 -3 1 1532.58 1510.90 21.29 o -3 -3 1 13.42 15.57 0.62 o -2 -3 1 141.37 176.97 2.78 o -1 -3 1 1292.32 1284.23 16.09 o 0 -3 1 867.50 935.39 12.69 o 1 -3 1 185.97 208.65 3.10 o 2 -3 1 252.00 275.60 3.95 o 4 -3 1 219.34 220.59 6.29 o 5 -3 1 1179.33 1162.40 18.13 o 6 -3 1 105.45 108.13 10.01 o 7 -3 1 20.89 21.10 2.27 o 8 -3 1 510.40 506.11 10.30 o 9 -3 1 275.82 277.93 6.94 o 10 -3 1 532.87 533.86 11.50 o 11 -3 1 977.66 977.27 21.08 o 12 -3 1 15.28 17.82 2.12 o 13 -3 1 479.35 460.57 21.77 o 14 -3 1 112.13 109.80 7.16 o -13 -2 1 540.12 484.80 28.36 o -12 -2 1 1007.42 1004.69 38.74 o -11 -2 1 57.69 59.67 3.37 o -10 -2 1 399.94 422.57 11.33 o -9 -2 1 16.98 17.22 1.19 o -8 -2 1 2903.68 2893.94 46.39 o -7 -2 1 147.64 191.11 3.48 o -6 -2 1 7.73 12.03 0.67 o -5 -2 1 941.68 1077.77 15.07 o -4 -2 1 650.35 638.54 8.62 o -3 -2 1 380.46 449.78 6.36 o -2 -2 1 216.63 205.67 3.20 o -1 -2 1 4727.41 4608.09 62.57 o 0 -2 1 1576.71 1542.53 20.06 o 1 -2 1 1856.67 1736.70 21.92 o 2 -2 1 934.93 885.72 19.23 o 3 -2 1 145.37 135.07 4.46 o 4 -2 1 5341.62 5601.77 215.06 o 5 -2 1 247.41 241.47 3.97 o 6 -2 1 1197.88 1183.81 21.94 o 7 -2 1 212.20 225.87 4.81 o 8 -2 1 235.39 242.86 5.70 o 9 -2 1 118.58 124.54 3.39 o 10 -2 1 962.79 1010.08 34.72 o 11 -2 1 4159.01 4223.36 88.50 o 12 -2 1 1.61 3.15 2.22 o 13 -2 1 494.58 501.76 21.78 o 14 -2 1 146.64 129.68 8.48 o -14 -1 1 379.63 352.05 22.66 o -13 -1 1 1.61 10.38 4.97 o -12 -1 1 720.92 723.69 32.60 o -11 -1 1 1.11 1.88 1.24 o -10 -1 1 92.56 89.79 8.77 o -9 -1 1 179.75 166.33 6.65 o -8 -1 1 407.78 403.42 6.70 o -7 -1 1 491.57 494.62 7.75 o -6 -1 1 1450.01 1551.91 21.88 o -5 -1 1 112.61 107.59 1.68 o -4 -1 1 153.00 166.08 2.46 o -3 -1 1 628.73 643.12 8.36 o -2 -1 1 490.48 470.51 7.59 o -1 -1 1 109.13 110.67 2.92 o 0 -1 1 146.82 0.03 0.73 o 1 -1 1 2.47 2.33 1.17 o 2 -1 1 352.20 397.37 12.13 o 3 -1 1 2342.63 2506.62 69.37 o 4 -1 1 844.30 863.70 40.35 o 5 -1 1 3418.58 3251.51 105.48 o 6 -1 1 112.91 106.19 2.00 o 7 -1 1 1525.18 1567.13 42.69 o 8 -1 1 457.08 452.93 9.09 o 9 -1 1 4.81 6.41 1.97 o 10 -1 1 46.66 51.23 2.66 o 11 -1 1 126.65 130.81 4.70 o 12 -1 1 2056.57 2078.15 51.86 o 13 -1 1 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350.10 14.67 o 4 1 9 67.83 50.47 6.80 o -7 2 9 6.13 4.48 3.75 o -6 2 9 348.26 360.59 17.15 o -5 2 9 306.19 298.50 14.47 o -4 2 9 159.80 172.97 7.20 o -3 2 9 259.29 279.88 11.33 o -2 2 9 63.47 60.14 6.07 o -1 2 9 124.45 112.13 11.84 o 0 2 9 725.33 687.65 24.02 o 1 2 9 66.40 66.24 19.08 o 2 2 9 404.57 404.79 22.08 o 3 2 9 0.22 1.20 4.36 o -5 3 9 306.82 281.36 17.84 o -4 3 9 382.95 379.75 28.29 o -3 3 9 23.24 23.73 2.99 o -2 3 9 39.06 44.59 6.83 o -1 3 9 197.88 163.23 8.06 o 0 3 9 175.88 158.66 8.60 o 1 3 9 3.32 4.27 7.97 o -1 -6 10 161.81 169.83 13.30 o 0 -6 10 117.21 112.75 8.26 o -3 -5 10 74.64 77.31 7.53 o -2 -5 10 5.91 -0.73 3.27 o -1 -5 10 4.63 10.38 5.12 o 0 -5 10 151.09 152.96 7.70 o 1 -5 10 492.31 504.71 16.69 o 2 -5 10 3.50 7.87 2.68 o -4 -4 10 88.04 91.05 6.08 o -3 -4 10 339.56 358.49 14.05 o -2 -4 10 3.55 8.12 3.50 o -1 -4 10 314.15 307.94 12.41 o 0 -4 10 4.49 5.73 4.46 o 1 -4 10 42.39 39.23 6.65 o 2 -4 10 277.59 269.22 12.01 o 3 -4 10 2.46 7.60 5.70 o -5 -3 10 107.57 95.86 5.97 o -4 -3 10 214.26 216.70 9.86 o -3 -3 10 54.78 53.81 5.10 o -2 -3 10 116.98 108.75 5.68 o -1 -3 10 254.60 269.14 36.40 o 0 -3 10 860.87 847.47 29.58 o 1 -3 10 67.21 66.38 8.26 o 2 -3 10 105.34 104.04 12.06 o 3 -3 10 369.03 317.84 15.20 o -5 -2 10 17.29 12.06 3.50 o -4 -2 10 729.53 764.87 27.67 o -3 -2 10 357.76 366.66 38.01 o -2 -2 10 57.54 60.05 10.09 o -1 -2 10 579.38 566.33 18.69 o 0 -2 10 313.70 299.56 11.47 o 1 -2 10 438.80 443.18 17.04 o 2 -2 10 155.62 144.93 7.70 o 3 -2 10 56.87 47.95 7.75 o -5 -1 10 398.81 397.89 15.64 o -4 -1 10 6.61 1.47 3.14 o -3 -1 10 112.53 114.58 6.82 o -2 -1 10 11.86 11.95 3.66 o -1 -1 10 371.78 357.29 24.63 o 0 -1 10 77.72 88.26 12.13 o 1 -1 10 54.43 50.59 13.08 o 2 -1 10 7.49 7.89 4.09 o -4 0 10 786.07 832.92 36.68 o -3 0 10 38.00 35.70 5.41 o -2 0 10 67.34 66.61 5.85 o -1 0 10 45.00 52.94 8.85 o 0 0 10 99.68 91.33 6.29 o 1 0 10 24.73 17.37 3.94 o