Acta Crystallographica Section C

Crystal Structure Communications

Volume 59, Part 11 (November 2003)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The two-dimensional sheet of the (4,4)-network in poly[[dichlorocadmium(II)]-di-[mu]-1,1'-(1,4-butanediyl)diimidazole]. The Cl- anions have been omitted for clarity. See Ma, Yang & Liu [Acta Cryst. (2003), C59, m482-m483].

inorganic compounds


 

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Acta Cryst. (2003). C59, i107-i108  [ doi:10.1107/S0108270103020390 ]

A non-linear optical crystal, Cd3Zn3(BO3)4

T.-Q. Sun, F. Pan, R.-J. Wang, G.-Q. Shen, X.-Q. Wang and D.-Z. Shen

Synopsis: A single crystal, 3 × 1.5 × 1 mm, of Cd3Zn3(BO3)4 has been prepared by spontaneous nucleation and its strong second harmonic generation of Nd:YAG laser radiation ([lambda] 1064 nm) has been observed.

Formula: Cd3Zn3(BO3)4

Online 11 October 2003


 

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Acta Cryst. (2003). C59, i109-i111  [ doi:10.1107/S0108270103015877 ]

[Yb(H2O)8][Cd3Cl9(H2O)]·6H2O

S. Yahyaoui, R. Ben Hassen, B. Donnadieu, J.-C. Daran and A. Ben Salah

Synopsis: A new hydrated double salt, YbCd3Cl9·15H2O, has been synthesized, and its structure has been determined by single-crystal X-ray diffraction and compared with that of CeCd4Cl11·13H2O. The structure of the ytterbium compound contains a layered arrangement of Cd octahedra, with a decrease of the coordination number of the rare-earth cation from nine for Ce3+ to eight for Yb3+.

Formula: [Yb(H2O)8][Cd3Cl9(H2O)]·6H2O

Online 22 October 2003


 

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Acta Cryst. (2003). C59, i112-i114  [ doi:10.1107/S0108270103006243 ]

Cs6Mo27S31: a novel ternary reduced molybdenum sulfide containing Mo9 and Mo18 clusters

S. Picard, D. Salloum, P. Gougeon and M. Potel

Synopsis: Cs6Mo27S31 is the third member of the Cs2nMo9S11Mo6nS6n+2 series. The crystal structure consists of an equal mixture of Mo9S11S6 and Mo18S20S6 cluster units that are separated by Cs+ cations.

Formula: Cs6Mo27S31

Online 22 October 2003


 

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Acta Cryst. (2003). C59, i115-i116  [ doi:10.1107/S0108270103021152 ]

A new hydrated ammonium hydroxyborate, (NH4)2[B10O14(OH)4]·H2O

L.-Y. Li, G.-B. Li, M. Xiong, Y.-X. Wang and J.-H. Lin

Synopsis: In the title compound, the fundamental building blocks are connected to form infinite chains. These chains are linked via hydrogen bonds, thus forming sheets that are stacked along the [001] direction.

Formula: (NH4)2[B10O14(OH)4]·H2O

Online 22 October 2003


metal-organic compounds


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Acta Cryst. (2003). C59, m429-m431  [ doi:10.1107/S0108270103020249 ]

Diaquabis(1,10-phenanthroline-[kappa]2N,N')manganese(II) thiodiglycolate bis(1,10-phenanthroline-[kappa]2N,N')(thiodiglycolato-[kappa]2O,O')manganese(II) tridecahydrate

J. Marek, Z. Trávnícek and P. Kopel

Formula: [Mn(C12H8N2)2(H2O)2](C4H4O4S)·[Mn(C4H4O4S)(C12H8N2)2]·13H2O

Online 11 October 2003


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Acta Cryst. (2003). C59, m432-m434  [ doi:10.1107/S0108270103020225 ]

Hexafluorophosphates of chlorotris(dimethyl sulfide)platinum(II) and bromotris(dimethyl sulfide)platinum(II)

C. Hansson, V. Yu. Kukushkin, K. Lövqvist, S. Yong and Å. Oskarsson

Formula: [PtCl(C2H6S)3]PF6 and [PtBr(C2H6S)3]PF6

Online 11 October 2003


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Acta Cryst. (2003). C59, m435-m438  [ doi:10.1107/S0108270103020407 ]

Magnesium iodide-4,4'-bipyridine-water (1/3/4) and strontium iodide-4,4'-bipyridine-propan-1-ol (1/2.5/2)

B. W. Skelton, A. F. Waters, C. R. Whitaker and A. H. White

Formula: [Mg(C10H8N2)(H2O)4]I2·2C10H8N2 and [Sr2I4(C10H8N2)3(C3H8O)4]·2C10H8N2

Online 11 October 2003


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Acta Cryst. (2003). C59, m439-m441  [ doi:10.1107/S0108270103020432 ]

A trichloro-bridged binuclear ruthenium complex with 1,1,1-tris(diphenylphosphinomethyl)ethane

W. K. Seok, L. J. Zhang, K. Karaghiosoff, T. M. Klapötke and P. Mayer

Formula: [Ru2Cl3(C41H39P3)2]PF6·C2H6O

Online 11 October 2003


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Acta Cryst. (2003). C59, m442-m445  [ doi:10.1107/S0108270103020195 ]

Dichlorobis(imidazolidin-2-one-[kappa]O)zinc(II) at 150 K

L. R. Falvello, E. M. Miqueleiz, T. Soler and M. Tomás

Formula: [ZnCl2(C3H6N2O)2]

Online 11 October 2003


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Acta Cryst. (2003). C59, m446-m449  [ doi:10.1107/S0108270103020869 ]

[(1R,2R)-1,2-Diaminocyclohexane-[kappa]2N,N']([alpha]-diimine-[kappa]2N,N')platinum(II) bis(hexafluorophosphate), where [alpha]-diimine is 2,2'-bipyridine and 1,10-phenanthroline

T. Koshiyama and M. Kato

Formula: [Pt(C6H14N2)(C10H8N2)](PF6)2 and [Pt(C6H14N2)(C12H8N2)](PF6)2

Online 11 October 2003


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Acta Cryst. (2003). C59, m450-m451  [ doi:10.1107/S0108270103016901 ]

A barium perchlorate complex with a lateral macrobicycle derived from 4,13-diaza-18-crown-6 containing a pyridine Schiff base spacer

F. Avecilla, D. Esteban, C. Platas-Iglesias, S. Fernández-Martínez, A. De Blas and T. Rodríguez-Blas

Formula: [Ba(ClO4)(C33H41N5O4)](ClO4)

Online 11 October 2003


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Acta Cryst. (2003). C59, m452-m453  [ doi:10.1107/S0108270103017633 ]

A dimeric heteroleptic five-coordinate zinc(II) complex containing a non-motionally restricted N,N'-heterocyclic ligand

D. M. Hatch, W. F. Wacholtz and J. T. Mague

Formula: [Zn2(C6H4S2)2(C10H8N2)2]

Online 11 October 2003


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Acta Cryst. (2003). C59, m454-m455  [ doi:10.1107/S0108270103021097 ]

catena-Poly[[(1,10-phenanthroline-[kappa]2N,N')copper(II)]-[mu]-(dihydrogen benzene-1,2,4,5-tetracarboxylato)-[kappa]2O1:O4]

M.-L. Hu, H.-P. Xiao, S. Wang and X.-H. Li

Formula: [Cu(C10H4O8)(C12H8N2)]

Online 11 October 2003


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Acta Cryst. (2003). C59, m456-m458  [ doi:10.1107/S0108270103021425 ]

Polymeric dihydroxydiphthalatotricobalt(II)

S.-Y. Yang, L.-S. Long, R.-B. Huang, L.-S. Zheng and S. W. Ng

Formula: [Co3(C8H4O4)2(OH)2]

Online 22 October 2003


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Acta Cryst. (2003). C59, m459-m461  [ doi:10.1107/S0108270103021243 ]

Hemi(piperazinediium) hexaaquaaluminium(III) bis(sulfate) tetrahydrate: a new double aluminium sulfate salt

T. Bataille

Formula: (C4H12N2)0.5[Al(H2O)6](SO4)2·4H2O

Online 22 October 2003


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Acta Cryst. (2003). C59, m462-m464  [ doi:10.1107/S010827010302198X ]

Bis(2-chloro-5-methylpyridine-[kappa]N)bis(nitrato-[kappa]2O,O')copper(II)

R.-C. Xuan, M.-C. Li and Y.-H. Wan

Formula: [Cu(NO3)2(C6H6ClN)2]

Online 22 October 2003


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Acta Cryst. (2003). C59, m465-m466  [ doi:10.1107/S0108270103022078 ]

Bis(tetraphenylphosphonium) ([mu]-tetrathiotungstenio-[kappa]4S,S':S'':S''')bis[(cyano-[kappa]C)cuprate](2-) acetonitrile solvate monohydrate

S.-B. Qiao, C.-M. Jiao, Q.-F. Xu, Y. Zhang, B.-L. Li and J.-P. Lang

Online 22 October 2003


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Acta Cryst. (2003). C59, m467-m470  [ doi:10.1107/S0108270103021711 ]

Geometric isomers of chloro(6-methyl-1,4,8,11-tetraazacyclotetradecane-6-amine)cobalt(III) tetrachlorozincate(II)

P. V. Bernhardt and B. P. Macpherson

Formula: Two isomers of [CoCl(C11H27N5)][ZnCl4]

Online 22 October 2003


 

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Acta Cryst. (2003). C59, m471-m472  [ doi:10.1107/S0108270103021747 ]

(C4N2H12)[(GeO2)3(BO1.5F)2], a layered borogermanate containing three- and nine-membered rings

Y.-F. Li and X.-D. Zou

Synopsis: A new borogermanate, (C4H12N2)[(GeO2)3(BO1.5F)2], was solvo/hydrothermally synthesized. It has a layered structure containing three- and nine-membered rings built from GeO4 and BO3F tetrahedra. The layers are connected through hydrogen bonding via diprotonated piperazine cations located between the layers.

Formula: (C4H12N2)[(GeO2)3(BO1.5F)2]

Online 22 October 2003


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Acta Cryst. (2003). C59, m473-m474  [ doi:10.1107/S0108270103022285 ]

Chlorobis[N'-ethoxycarbonyl-N-(4-methylphenyl)thiourea-[kappa]S]copper(I)

Y.-M. Zhang, L. Xian and T.-B. Wei

Formula: [CuCl(C11H14N2O2S)2]

Online 22 October 2003


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Acta Cryst. (2003). C59, m475-m477  [ doi:10.1107/S0108270103022509 ]

Poly[sodium(I)-[mu]6-hydrogen benzene-1,4-dicarboxylato]

S. H. Dale and M. R. J. Elsegood

Formula: [Na(C8H5O4)]

Online 22 October 2003


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Acta Cryst. (2003). C59, m478-m481  [ doi:10.1107/S0108270103021978 ]

Influence of Cl/Br substitution on the stereochemical peculiarities of copper(I) [pi]-complexes with the 1-allyl-2-aminopyridinium cation

E. Goreshnik, D. Schollmeier and M. Mys'kiv

Formula: (C8H11N2)2[Cu2Cl4] and (C8H11N2)2[Cu2Br2.2Cl1.8]

Online 22 October 2003


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Acta Cryst. (2003). C59, m482-m483  [ doi:10.1107/S0108270103022443 ]

A novel CdII coordination polymer with 1,1'-(1,4-butanediyl)diimidazole

J.-F. Ma, J. Yang and J.-F. Liu

Formula: [CdCl2(C10H14N4)2]

Online 22 October 2003


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Acta Cryst. (2003). C59, m484-m486  [ doi:10.1107/S0108270103022650 ]

Tetraphenylarsonium iodide, a new determination

P. A. W. Dean, D. C. Craig, M. L. Scudder and I. G. Dance

Formula: [As(C6H5)4]I

Online 31 October 2003


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Acta Cryst. (2003). C59, m487-m490  [ doi:10.1107/S010827010302170X ]

{Bis[(S)-2-(4-tert-butyl-4,5-dihydrooxazol-2-yl)phenyl]phenylphoshine-[kappa]2N,P}(1,3-dimethyl-[pi]-allyl-[kappa]3C)palladium(II) hexafluorophosphate and (S)P-{bis[(S)-2-(4-tert-butyl-4,5-dihydrooxazol-2-yl)phenyl]phenylphosphine-[kappa]2N,P}dichloropalladium(II)

D. Masui, M. Ohnuki, M. Yamaguchi and T. Yamagishi

Formula: [Pd(C5H9)(C32H37N2O2P)]PF6 and [PdCl2(C32H37N2O2P)]

Online 31 October 2003


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Acta Cryst. (2003). C59, m491-m493  [ doi:10.1107/S0108270103023114 ]

A one-dimensional copper coordination polymer containing both dicyanamide and 1,10-phenanthroline ligands

A-Q. Wu, L.-Z. Cai, W.-T. Chen, G.-C. Guo and J.-S. Huang

Formula: [Cu(C2H3O2)(C2N3)(C12H8N2)]·3H2O

Online 31 October 2003


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Acta Cryst. (2003). C59, m494-m496  [ doi:10.1107/S0108270103022595 ]

A zirconium zwitterion containing a caged amine H atom

A. J. Nielson, C. Shen and J. M. Waters

Formula: [Zr(C27H31NO3)2]·2CHCl3

Online 31 October 2003


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Acta Cryst. (2003). C59, m497-m498  [ doi:10.1107/S010827010302064X ]

Bis([mu]-di-2-pyridylaminato 1-oxide)bis[(trifluoroacetato)copper(II)] acetonitrile disolvate

X.-R. Zeng, X.-N. Fang, S.-M. Peng and H.-M. Lin

Formula: [Cu2(C2F3O2)2(C10H8N3O)2]·2C2H3N

Online 31 October 2003


organic compounds


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Acta Cryst. (2003). C59, o605-o608  [ doi:10.1107/S0108270103020237 ]

3,5-Bis[4-(diethylamino)benzylidene]-1-methyl-4-piperidone and 3,5-bis[4-(diethylamino)cinnamylidene]-1-methyl-4-piperidone: prospective biophotonic materials

V. N. Nesterov, T. V. Timofeeva, S. S. Sarkisov, A. Leyderman, C.Y.-C. Lee and M. Yu. Antipin

Formula: C28H37N3O and C32H41N3O

Online 11 October 2003


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Acta Cryst. (2003). C59, o609-o610  [ doi:10.1107/S0108270103020420 ]

7-Methoxyanthra[1,9-de]-1,3,2-dioxathiine-8,11-dione 2,2-dioxide

B. W. Skelton and A. H. White

Formula: C15H8O7S

Online 11 October 2003


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Acta Cryst. (2003). C59, o611-o612  [ doi:10.1107/S0108270103021000 ]

2,3-Bis(2-methylphenylimino)-1,4-dithiacyclohexane

Y.-Z. Li, W.-W. Liu, Y.-J. Li, G.-J. Pan and H.-W. Hu

Formula: C18H18N2S2

Online 11 October 2003


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Acta Cryst. (2003). C59, o613-o615  [ doi:10.1107/S010827010302050X ]

4,4'-(Azinodimethylene)dipyridinium chloranilate dichloromethane disolvate

A. R. Kennedy and F. R. N. Waterson

Online 11 October 2003


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Acta Cryst. (2003). C59, o616-o619  [ doi:10.1107/S0108270103020997 ]

2-{[Tris(hydroxymethyl)methyl]aminomethylene}cyclohexa-3,5-dien-1(2H)-one and its 6-hydroxy and 6-methoxy derivatives

M. Odabasoglu, Ç. Albayrak, O. Büyükgüngör and P. Lönnecke

Formula: C11H15NO4, C11H15NO5 and C12H17NO5

Online 11 October 2003


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Acta Cryst. (2003). C59, o620-o621  [ doi:10.1107/S0108270103019577 ]

Herring-bone [pi]-[pi] interactions in trans-2,6-diphenyl-2,3,5,6-tetrahydrothiapyran-4-one

T. Narasimhamurthy, J. C. N. Benny, K. Pandiarajan and R. S. Rathore

Formula: C17H16OS

Online 11 October 2003


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Acta Cryst. (2003). C59, o622-o624  [ doi:10.1107/S0108270103019358 ]

4-(Piperidin-1-yl)pyridinium hexafluorophosphate at 150 K

B. D. James, S. Mutrofin, B. W. Skelton and A. H. White

Formula: C10H15N2+·PF6-

Online 11 October 2003


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Acta Cryst. (2003). C59, o625-o628  [ doi:10.1107/S0108270103020985 ]

N,N-Dimethyl-N'-[(1E,2E)-3-(4-nitrophenyl)prop-2-enylidene]benzene-1,4-diamine and N,N-dimethyl-4-[(1E,3E)-4-(4-nitrophenyl)buta-1,3-dienyl]-1-naphthylamine

V. V. Nesterov, A. Suina, M. Yu. Antipin, T. V. Timofeeva, S. Barlow and S. R. Marder

Formula: C17H17N3O2 and C22H20N2O2

Online 11 October 2003


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Acta Cryst. (2003). C59, o629-o633  [ doi:10.1107/S0108270103021401 ]

Four cytotoxic N4-substituted thiosemicarbazones derived from 2-hydroxynaphthalene-1-carboxaldehyde

P. V. Bernhardt, L. M. Caldwell, D. B. Lovejoy and D. R. Richardson

Formula: C13H13N3OS, C14H15N3OS, C18H15N3OS and C14H15N3OS·C2H6OS

Online 22 October 2003


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Acta Cryst. (2003). C59, o634-o635  [ doi:10.1107/S0108270103021413 ]

Two polymorphic forms of 2,5-bis(4-methoxycarbonylphenyl)-1,3,4-oxadiazole

G. Reck, I. Orgzall, B. Schulz and B. Dietzel

Formula: C18H14N2O5

Online 22 October 2003


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Acta Cryst. (2003). C59, o636-o637  [ doi:10.1107/S0108270103021164 ]

Bilayers in 4-iodo-N-(2-iodo-4-nitrophenyl)benzamide generated by a combination of an N-H...O=C hydrogen bond and two independent iodo-nitro interactions

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C13H8I2N2O3

Online 22 October 2003


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Acta Cryst. (2003). C59, o638-o640  [ doi:10.1107/S0108270103020638 ]

(±)-2-Oxocyclohexanepropionic acid: dual conformational selection and hydrogen bonding in a [delta]-keto acid, and a two-phase technique for crystallizing acids by contact with aqueous solutions of their salts

R. A. Lalancette and H. W. Thompson

Formula: C9H14O3

Online 22 October 2003


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Acta Cryst. (2003). C59, o641-o643  [ doi:10.1107/S0108270103021309 ]

1-(4-Chlorophenylsulfanyl)-2-nitro-4-(trifluoromethyl)benzene and 1-(4-chlorophenylsulfanyl)-4-nitro-2-(trifluoromethyl)benzene

D. E. Lynch and I. McClenaghan

Online 22 October 2003


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Acta Cryst. (2003). C59, o644-o646  [ doi:10.1107/S0108270103019814 ]

A new norkaurane-[gamma]-lactone from Parinari sprucei

C. A. Mattia, A. Braca, N. De Tommasi and R. Puliti

Formula: C20H28O6·0.5H2O

Online 22 October 2003


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Acta Cryst. (2003). C59, o647-o649  [ doi:10.1107/S0108270103022339 ]

(Z)-2-(3-Hydroxy-4-methoxybenzylidene)-1-azabicyclo[2.2.2]octan-3-one

V. N. Sonar, S. Parkin and P. A. Crooks

Formula: C15H17NO3

Online 22 October 2003


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Acta Cryst. (2003). C59, o650-o652  [ doi:10.1107/S0108270103022649 ]

Cephalexin: a channel hydrate

A. R. Kennedy, M. O. Okoth, D. B. Sheen, J. N. Sherwood, S. J. Teat and R. M. Vrcelj

Formula: C16H17N3O4S·1.9H2O

Online 22 October 2003


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Acta Cryst. (2003). C59, o653-o655  [ doi:10.1107/S0108270103022662 ]

4,5-Propylenedithio-1,3-dithiole-2-thione and 4,5-propylenedithio-1,3-dithiol-2-one

G. Xue, Q. Fang and W. Yu

Formula: C6H6S5 and C6H6OS4

Online 31 October 2003


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Acta Cryst. (2003). C59, o656-o658  [ doi:10.1107/S010827010302287X ]

Pseudosymmetry in ammonium [(carboxymethyl)sulfanyl]acetate

J. K. Maurin, M. Pawlowski and Z. Czarnocki

Formula: NH4+·C4H5O4S-

Online 31 October 2003


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