Acta Crystallographica Section C

Crystal Structure Communications

Volume 60, Part 2 (February 2004)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The three independent residues of cyclohexanone oxime linked by hydrogen bonds into a trimeric structure. . See Lutz, Spek, Dabirian, van Walree & Jenneskens [Acta Cryst. (2004), C60, o127-o127].

inorganic compounds


 

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Acta Cryst. (2004). C60, i11-i13  [ doi:10.1107/S0108270103026623 ]

K4VP2S9

A. Gutzmann, C. Näther and W. Bensch

Synopsis: The crystal structure of the title compound, prepared by reacting a mixture of K2S3, VP, P4S3 and S, consists of discrete [VS(PS4)2]4- anions, which are stacked along the direction of the crystallographic b axis and separated by K+ cations. In the anion, the V atom is connected to five S atoms within a square pyramid. The VS5 group shares common edges with two bidentate [PS4] tetrahedra.

Formula: K4VP2S9

Online 17 January 2004


 

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Acta Cryst. (2004). C60, i14-i16  [ doi:10.1107/S0108270103029056 ]

In1.06Ho0.94Ge2O7: a thortveitite-type compound

E. A. Juarez-Arellano, I. Rosales, A. Oliver, J. L. Ruvalcaba, R. E. Carbonio, L. Bucio and E. Orozco

Synopsis: The crystal structure of a new indium holmium germanate, In1.06Ho0.94Ge2O7, belonging to the thortveitite structure type, is reported. The In3+ and Ho3+ cations occupy the same octahedral site, forming an hexagonal arrangement on the ab plane. In their turn, the hexagonal arrangements of (In/Ho)O6 octahedral layers are held together by sheets of isolated diortho groups comprised of double tetrahedra sharing a common vertex.

Formula: In1.06Ho0.94Ge2O7

Online 17 January 2004


 

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Acta Cryst. (2004). C60, i17-i19  [ doi:10.1107/S0108270103029068 ]

Cs2Cr4O13: a new structure type among alkali tetrachromates

U. Kolitsch

Synopsis: Cs2Cr4O13 contains a [Cr4O13]2- anion with a zigzag-like structure, built from four corner-linked CrO4 tetrahedra, and has a structure type previously unknown among alkali tetrachromates.

Formula: Cs2Cr4O13

Online 31 January 2004


 

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Acta Cryst. (2004). C60, i20-i22  [ doi:10.1107/S0108270103025666 ]

The high-temperature modification of zinc catena-polyphosphate, [beta]-Zn(PO3)2

M. Weil

Synopsis: Single crystals of the high-temperature modification of zinc catena-polyphosphate, [beta]-Zn(PO3)2, were grown from a melt and quenched from 1093 K to room temperature. The structure is built of corrugated (PO3)[infinity] polyphosphate chains linked by slightly distorted [ZnO4] tetrahedra into a three-dimensional network.

Formula: Zn(PO3)2

Online 31 January 2004


metal-organic compounds


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Acta Cryst. (2004). C60, m39-m41  [ doi:10.1107/S0108270103027847 ]

Poly[[bis(1H-benzimidazole-[kappa]N3)cadmium(II)]-[mu]-aqua-[mu]-succinato-[kappa]2O1:O4]

B.-X. Liu and D.-J. Xu

Formula: [Cd(C4H4O4)(C7H6N2)2(H2O)]

Online 10 January 2004


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Acta Cryst. (2004). C60, m42-m43  [ doi:10.1107/S0108270103027902 ]

An oxo-bridged centrosymmetric tetranuclear titanium compound

T. Kemmitt, G. J. Gainsford and N. I. Al-Salim

Formula: [Ti4(C5H11NO2)2(C4H9O)8O2]

Online 10 January 2004


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Acta Cryst. (2004). C60, m44-m46  [ doi:10.1107/S0108270103028014 ]

A new complex of HgBr2 and pyrimidine-2-thione: (pyrimidine-2-thionato-[kappa]S)(pyrimidinium-2-thionato-[kappa]S)mercury(II) tetrabromomercury(II)

D. Matkovic-Calogovic, D. Mrvos-Sermek, Z. Popovic and Z. Soldin

Formula: [Hg(C4H4N2S)(C4H3N2S)]2[HgBr4]

Online 10 January 2004


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Acta Cryst. (2004). C60, m47-m50  [ doi:10.1107/S0108270103028130 ]

(2,2'-Bipyridine-[kappa]2N,N')(1,1-cyclobutanedicarboxylato-[kappa]2O,O')palladium(II), (1,1-cyclobutanedicarboxylato-[kappa]2O,O')(1,10-phenanthroline-[kappa]2N,N')palladium(II) monohydrate and (1,1-cyclobutanedicarboxylato-[kappa]2O,O')(1,10-phenanthroline-[kappa]2N,N')palladium(II) dihydrate

Y. Muranishi and N. Okabe

Formula: [Pd(C6H6O4)(C10H8N2)], [Pd(C6H6O4)(C12H8N2)]·H2O and [Pd(C6H6O4)(C12H8N2)]·2H2O

Online 10 January 2004


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Acta Cryst. (2004). C60, m51-m54  [ doi:10.1107/S0108270103028385 ]

Bis[bis(pyrimidin-2-yl-[kappa]N)amine](dicyanamido-[kappa]N1)(trifluoromethanesulfonato-[kappa]O)copper(II) ethanol hemisolvate forms a hydrogen-bonded chain

H. Kooijman, A. L. Spek, G. A. van Albada, P. Gamez and J. Reedijk

Formula: [Cu(CF3SO3)(C2N3)(C8H7N5)2]·0.5C2H6O

Online 10 January 2004


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Acta Cryst. (2004). C60, m55-m56  [ doi:10.1107/S0108270103028270 ]

Bis(benzylammonium) hexachlorotin(IV)

M. Rademeyer

Formula: (C7H10N)2[SnCl6]

Online 10 January 2004


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Acta Cryst. (2004). C60, m57-m59  [ doi:10.1107/S0108270103028051 ]

[5,10,15,20-Tetrakis(pentafluorophenyl)porphyrinato]iron(II) benzene disolvate

Y. Oh, B.-C. Shin, D. Swenson, H. M. Goff and S. K. Kang

Formula: [Fe(C44H8F20N4)]·2C6H6

Online 10 January 2004


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Acta Cryst. (2004). C60, m60-m62  [ doi:10.1107/S0108270103028464 ]

Tetrameric dichloro(trimethylammonio-p-toluenesulfonamidate)mercury(II)

K. W. Muir, D. G. Morris and C. O. W. Chii

Formula: [Hg4Cl8(C10H16N2O2S)4]

Online 17 January 2004


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Acta Cryst. (2004). C60, m63-m64  [ doi:10.1107/S0108270103028907 ]

catena-Poly[bis[(2,2-bipyridine-[kappa]2N,N')copper(II)]-[mu]4-1,2,4,5-benzenetetracarboxylato-[kappa]4O1:O2:O3:O4]

H.-P. Xiao, X.-H. Li, J.-X. Yuan and M.-L. Hu

Formula: [Cu2(C10H2O8)(C10H8N2)2]

Online 17 January 2004


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Acta Cryst. (2004). C60, m65-m68  [ doi:10.1107/S0108270103028841 ]

Bis[tris(2,2'-bipyridine-[kappa]2N,N')ruthenium(II)] hexacyanoferrate(III) chloride octahydrate

K. Sakai, Y. Uchida, T. Kajiwara and T. Ito

Formula: [Ru(C10H8N2)3]2[Fe(CN)6]Cl·8H2O

Online 17 January 2004


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Acta Cryst. (2004). C60, m69-m72  [ doi:10.1107/S0108270103029500 ]

Bis(2,2'-bipyridine-[kappa]2N,N')(1,10-phenanthroline-[kappa]2N,N')ruthenium(II) tetracyanoplatinate(II)

K. Sakai and Y. Miyabe

Formula: [Ru(C10H8N2)2(C12H8N2)][Pt(CN)4]

Online 31 January 2004


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Acta Cryst. (2004). C60, m73-m75  [ doi:10.1107/S0108270104000216 ]

The Zn2+ salt of pamidronate: a role for water in the metal-cation binding properties of bisphosphonates

D. Fernández, G. Polla, D. Vega and J. A. Ellena

Formula: Zn2+·2C3H10NO7P2-·2H2O

Online 31 January 2004


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Acta Cryst. (2004). C60, m76-m78  [ doi:10.1107/S0108270103029573 ]

Poly[lead(II)-[mu]2-aqua-[mu]4-terephthalato]

S. H. Dale, M. R. J. Elsegood and S. Kainth

Formula: [Pb(C8H4O4)(H2O)]

Online 31 January 2004


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Acta Cryst. (2004). C60, m79-m81  [ doi:10.1107/S0108270104000186 ]

A novel five-coordinate cadmium phenanthroline thiosulfate

M. Harvey, S. Baggio, H. Pardo and R. Baggio

Formula: [Cd(S2O3)(C12H8N2)]

Online 31 January 2004


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Acta Cryst. (2004). C60, m82-m84  [ doi:10.1107/S0108270104000204 ]

Chloro{2,2'-[(1S,2S)-1,2-diphenyl-1,2-ethanediylbis(nitrilomethylidyne)]diphenolato-[kappa]4O,N,N',O'}(ethanol-[kappa]O)manganese(III)

I. V. Korendovych and E. V. Rybak-Akimova

Formula: [MnCl(C28H22N2O2)(C2H6O)]

Online 31 January 2004


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Acta Cryst. (2004). C60, m85-m87  [ doi:10.1107/S010827010302883X ]

Tetra-[mu]-benzoato-[kappa]8O:O'-bis({1-[(3,4-dimethoxyphenyl)methyl]-6,7-dimethoxyisoquinoline-[kappa]N}zinc(II)): the first crystal structure with papaverine as a ligand

V. Zelenák, M. Sabo, W. Massa and J. Cernák

Formula: [Zn2(C7H5O2)4(C20H21NO4)2]

Online 31 January 2004


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Acta Cryst. (2004). C60, m88-m90  [ doi:10.1107/S0108270104000344 ]

Diisopropylphosphitocobalamin-acetone-water (1/3.48/7.56)

S. M. Chemaly, H. M. Marques and C. B. Perry

Synopsis: The diisopropylphosphite ligand coordinates to the CoIII atom via its P atom. The crystal structure is isomorphous with that of other cobalamins that adopt packing type II, with a Co-P bond length [2.227 (1) Å] similar to that found in other phosphitocobalamins.

Formula: [Co(C68H102N13O17P2)]·3.48C3H6O·7.56H2O

Online 31 January 2004


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Acta Cryst. (2004). C60, m91-m93  [ doi:10.1107/S0108270104000411 ]

A polymeric ladder complex: catena-poly[[[[mu]-4,4'-bipyridyl-bis[aqua(p-aminobenzoato)copper(II)]]-di-[mu]-4,4'-bipyridyl] dinitrate tetrahydrate]

D.-H. Hu, W. Huang, K. Cui, Y.-Z. Li, S.-H. Gou and J.-L. Yan

Formula: [Cu2(C7H6NO2)2(C10H8N2)3(H2O)2](NO3)2·4H2O

Online 31 January 2004


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Acta Cryst. (2004). C60, m94-m96  [ doi:10.1107/S0108270104000605 ]

Tetrakis(tetrahydrofuran-[kappa]O)lithium mer-tris(carbazolyl-[kappa]N)-trans-dichloro(tetrahydrofuran-[kappa]O)zirconate

C. L. Nygren, M. E. T. Bragg and J. F. C. Turner

Formula: [Li(C4H8O)4][ZrCl2(C12H8N)3(C4H8O)]

Online 31 January 2004


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Acta Cryst. (2004). C60, m97-m100  [ doi:10.1107/S0108270104000198 ]

catena-Poly[[bis(hexafluoroacetylacetonato-[kappa]2O,O')zinc(II)]-[mu]-4,4'-bipyridine-[kappa]2N:N']

J. Granifo, M. T. Garland and R. Baggio

Formula: [Zn(C5HF6O2)2(C10H8N2)]

Online 31 January 2004


organic compounds


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Acta Cryst. (2004). C60, o103-o106  [ doi:10.1107/S0108270103027197 ]

2,4-Dinitrophenylhydrazones of 2,4-dihydroxybenzaldehyde, 2,4-dihydroxyacetophenone and 2,4-dihydroxybenzophenone

R. G. Baughman, K. L. Martin, R. K. Singh and J. O. Stoffer

Formula: C13H10N4O6·C3H7NO, C14H12N4O6·C3H7NO and C19H14N4O6·C4H9NO

Online 10 January 2004


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Acta Cryst. (2004). C60, o107-o109  [ doi:10.1107/S0108270103027859 ]

5,5'-Di-tert-butyl-2,2'-dihydroxy-3,3'-methylenedibenzaldehyde and 6,6'-di-tert-butyl-8,8'-methylenebis(spiro[4H-1,3-benzodioxin-2,1'-cyclohexane])

B. Masci, S. Levi Mortera, L. Seralessandri and P. Thuéry

Formula: C23H28O4 and C35H48O4

Online 10 January 2004


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Acta Cryst. (2004). C60, o110-o112  [ doi:10.1107/S0108270103028038 ]

16-(4-Isopropylbenzylidene)androst-4-ene-3,17-dione

S. Thamotharan, V. Parthasarathi, S. Dubey, D. P. Jindal and A. Linden

Formula: C29H36O2

Online 10 January 2004


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Acta Cryst. (2004). C60, o113-o114  [ doi:10.1107/S0108270103028282 ]

2,2'-Bipyridinium(1+) bromide monohydrate

R. J. Bowen, M. A. Fernandes, P. W. Gitari and M. Layh

Formula: C10H9N2+·Br-·H2O

Online 10 January 2004


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Acta Cryst. (2004). C60, o115-o117  [ doi:10.1107/S0108270103028178 ]

N1-(2,6-Dimethylphenyl)-N2-hydroxy-[alpha]-oxo-[alpha]-phenylacetamidine

S. Soylu, M. Tas, H. Saraçoglu, H. Bati, N. Çaliskan and O. Büyükgüngör

Formula: C16H16N2O2

Online 10 January 2004


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Acta Cryst. (2004). C60, o118-o119  [ doi:10.1107/S0108270103027835 ]

N-(2-Fluoroethyl)-3[beta]-(4-iodophenyl)-8-methyl-8-azabicyclo[3.2.1]octane-2[alpha]-carboxamide: a new cocaine derivative with equatorially attached ligands

B. Krebs and U. Flörke

Formula: C17H22FIN2O

Online 10 January 2004


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Acta Cryst. (2004). C60, o120-o124  [ doi:10.1107/S0108270103027914 ]

[pi]-Stacked hydrogen-bonded dimers in 2-(2-nitrophenylaminocarbonyl)benzoic acid, and hydrogen-bonded sheets in orthorhombic and monoclinic polymorphs of 2-(4-nitrophenylaminocarbonyl)benzoic acid

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: Isomers and polymorphs of C14H10N2O5

Online 10 January 2004


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Acta Cryst. (2004). C60, o125-o126  [ doi:10.1107/S0108270103029421 ]

4-Chloro-N-(trimethylammonio)benzamide chloride monohydrate

K. W. Muir, D. G. Morris and C. O. W. Chii

Formula: C10H14ClN2O+·Cl-·H2O

Online 17 January 2004


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Acta Cryst. (2004). C60, o127-o129  [ doi:10.1107/S0108270103029196 ]

Twinning by merohedry in cyclohexanone oxime: a revised structure

M. Lutz, A. L. Spek, R. Dabirian, C. A. van Walree and L. W. Jenneskens

Formula: Two refinements of C6H11NO

Online 17 January 2004


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Acta Cryst. (2004). C60, o130-o132  [ doi:10.1107/S010827010302866X ]

6-[3-Hydroxy-17-oxoestra-1,3,5(10)-trien-7[beta]-yl]hexanenitrile

C. Yamamoto, T. Matsumoto, M. Watanabe, E. M. S. Hitzer, S. Mataka and T. Thiemann

Formula: C24H31NO2

Online 17 January 2004


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Acta Cryst. (2004). C60, o133-o135  [ doi:10.1107/S010827010302941X ]

4-[(2-Chlorophenyl)diazenyl]-6-methoxy-2-{[tris(hydroxymethyl)methyl]aminomethylene}cyclohexa-3,5-dien-1(2H)-one

C. C. Ersanli, Ç. Albayrak, M. Odabasoglu, C. Thöne and A. Erdönmez

Formula: C18H20ClN3O5

Online 17 January 2004


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Acta Cryst. (2004). C60, o136-o139  [ doi:10.1107/S0108270103027586 ]

3-Oxa-6,8-diaza-1,2:4,5-dibenzocycloocta-1,4-dien-7-one: a three-dimensional network assembled by hydrogen-bonding, [pi]-[pi] and edge-to-face interactions

V. Böhmer, D. Meshcheryakov, I. Thondorf and M. Bolte

Formula: C13H10N2O2

Online 17 January 2004


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Acta Cryst. (2004). C60, o140-o142  [ doi:10.1107/S0108270103029329 ]

4-Oxocyclohexanecarboxylic acid: hydrogen bonding in the monohydrate of a [delta]-keto acid

A. Barcon, A. P. J. Brunskill, H. W. Thompson and R. A. Lalancette

Formula: C7H10O3·H2O

Online 31 January 2004


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Acta Cryst. (2004). C60, o143-o145  [ doi:10.1107/S0108270103029433 ]

3-Butyl-1-(5-nitrobenzo[c][1,2]thiazol-3-yl)-3-phenyltriazene

V. Kettmann, J. Lokaj, J. Kozísek, J. Prikryl and V. Machácek

Formula: C17H17N5O2S

Online 31 January 2004


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Acta Cryst. (2004). C60, o146-o148  [ doi:10.1107/S0108270103026775 ]

Monitoring structural transformations in crystals. 7. 1-Chloroanthracene and its photodimer

I. Turowska-Tyrk and K. Grzesniak

Formula: C14H9Cl and C28H18Cl2

Online 31 January 2004


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Acta Cryst. (2004). C60, o149-o151  [ doi:10.1107/S0108270103028154 ]

tert-Butyl 5-methoxy-3-pentylindole-1-carboxylate

J. F. Gallagher, C. M. Coleman and D. F. O'Shea

Formula: C19H27NO3

Online 31 January 2004


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Acta Cryst. (2004). C60, o152-o155  [ doi:10.1107/S010827010400023X ]

Two triclinic polymorphs of 2,3,5,6-tetrakis(naphthalen-2-ylsulfanylmethyl)pyrazine

J. Pacifico and H. Stoeckli-Evans

Formula: Two polymorphs of C48H36N2S4

Online 31 January 2004


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Acta Cryst. (2004). C60, o156-o157  [ doi:10.1107/S010827010400040X ]

sp-9-(o-Methylphenyl)fluorene

C. Y. Meyers, P. D. Robinson and A. W. McLean

Formula: C20H16

Online 31 January 2004


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Acta Cryst. (2004). C60, o158-o160  [ doi:10.1107/S0108270103029159 ]

An aza-steroidal [17,16-c]pyrazole derivative: 2'-(p-fluorophenyl)-17a-aza-2'H-pyrazolo[4',3':16,17]-D-homoandrost-4-en-3-one

S. Thamotharan, V. Parthasarathi, R. Gupta, D. P. Jindal and A. Linden

Formula: C26H30FN3O

Online 31 January 2004


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Acta Cryst. (2004). C60, o161-o162  [ doi:10.1107/S0108270103028452 ]

16-Cyano-13[alpha]-(5-methyl-1,3,4-oxadiazol-2-yl)-13,16-seco-17-norandrost-5-en-3[beta]-yl acetate

S. Thamotharan, V. Parthasarathi, R. Gupta, D. P. Jindal and A. Linden

Formula: C23H31N3O3

Online 31 January 2004


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