Crystal Structure Communications

 

Acta Cryst. (2004). C60, i23-i24  [ doi:10.1107/S0108270103028671 ]

Europium(II) oxyiodide

W. Liao and R. Dronskowski

Synopsis: The structure of Eu₄OI₆, isotypic with Eu₄OCl₆ and Eu₄OBr₆, is characterized by O-centered tetrahedra of divalent europium cations and hexagonal channels parallel to [001] filled with iodide anions.

Formula: Eu₄OI₆

Online 10 February 2004

 

Acta Cryst. (2004). C60, i25-i26  [ doi:10.1107/S0108270103028312 ]

The Rb analogue of grimselite, Rb₆Na₂[(UO₂)(CO₃)₃]₂(H₂O)

K.-A. Hughes Kubatko and P. C. Burns

Synopsis: The Rb analogue of grimselite is based on isolated uranyl tricarbonate clusters, [(UO₂)(CO₃)₃], linked through corner sharing to RbO₁₀ and NaO₈ polyhedra. The title compound is isostructural with grimselite, with a reduced occupancy of the H₂O site (25% versus 50% in grimselite).

Formula: Rb₆Na₂[(UO₂)(CO₃)₃]₂(H₂O)

Online 10 February 2004

 

Acta Cryst. (2004). C60, i27-i29  [ doi:10.1107/S0108270104000599 ]

A new crystal phase of barium nitroprusside trihydrate studied by neutron diffraction at 20  K

G. Chevrier, J. M. Kiat, J. A. Güida and A. Navaza

Synopsis: The crystal structure of barium pentacyanonitrosylferrate trihydrate, in space group P1, is completely ordered. The study was performed to characterize the structural phase generated by the phase transition undergone by the crystals at 80  K, at which temperature the unit-cell volume doubles. The positional changes of the water molecules with respect to those of the compound at 105  K are presented.

Formula: Ba[Fe(CN)₅(NO)]·3H₂O

Online 10 February 2004

 

Acta Cryst. (2004). C60, i30-i32  [ doi:10.1107/S010827010400071X ]

A novel gallium arsenate organically templated by propane-1,3-diyldiammonium with a ULM-3-type open framework: [Ga₃(AsO₄)₃(OH)F](C₃H₁₂N₂)·H₂O

T. Loiseau and G. Ferey

Synopsis: The title oxyfluorinated gallium arsenate exhibits a three-dimensional framework, with ten-ring channels in which the diprotonated 1,3-diaminopropane and water molecules are encapsulated. This network is isostructural with that of phosphates with a ULM-3-type framework.

Formula: [Ga₃(AsO₄)₃(OH)F](C₃H₁₂N₂)·H₂O

Online 10 February 2004

 

Acta Cryst. (2004). C60, m101-m103  [ doi:10.1107/S0108270104001027 ]

Diaquatetrakis(pyridine-2,6-dicarboxylato-²O²,O⁶)tetrakis(-pyridine-3,5-dicarboxylic acid-²N:O)tetracopper(II): a copper complex with tetrameric molecular units

J. Chaigneau, J. Marrot and D. Riou

Formula: [Cu₄(C₇H₃NO₄)₄(C₇H₅NO₄)₄(H₂O)₂]

Online 10 February 2004

 

Acta Cryst. (2004). C60, m104-m106  [ doi:10.1107/S010827010400157X ]

A quadrupole-quadrupole stacking synthon in (2,3,5,6-tetrafluorobenzenethiolato-S)(triphenylphosphine-P)gold(I)

S. Watase, T. Kitamura, N. Kanehisa, M. Nakamoto, Y. Kai and S. Yanagida

Formula: [Au(C₆HF₄S)(C₁₈H₁₅P)]

Online 10 February 2004

 

Acta Cryst. (2004). C60, m107-m109  [ doi:10.1107/S0108270104000836 ]

[Benzylbis(dimethylamino)methylsilyl-²C,N](N,N,N',N'-tetramethylethylenediamine-²N,N)lithium(I)

H.-P. Shi, D.-S. Liu and S.-P. Huang

Formula: [Li(C₁₂H₂₁NSi)(C₆H₁₆N₂)]

Online 10 February 2004

 

Acta Cryst. (2004). C60, m110-m111  [ doi:10.1107/S0108270103029470 ]

Tetra--2-fluorobenzoato-bis[aqua(4,4'-bipyridine)(2-fluorobenzoato)lanthanum(III)]

X. Li, Y.-Q. Zou and H.-B. Song

Formula: [La(C₇H₄FO₂)₆(C₁₀H₈N₂)₂(H₂O)₂]

Online 10 February 2004

 

Acta Cryst. (2004). C60, m112-m113  [ doi:10.1107/S0108270103029445 ]

Polymeric aqua(₄-dihydrogen benzene-1,2,4,5-tetracarboxylato)(1,10-phenanthroline)cobalt(II)

M.-L. Hu, H.-P. Xiao and J.-X. Yuan

Formula: [Co(C₁₀H₄O₈)(C₁₂H₈N₂)(H₂O)]

Online 10 February 2004

 

Acta Cryst. (2004). C60, m114-m116  [ doi:10.1107/S0108270104000691 ]

Polymeric sodium 3,5-dicarboxybenzenesulfonate-urea-water (1/1/1)

E. Stos, T. Lis and V. Videnova-Adrabinska

Formula: [Na(C₈H₅O₇S)(CH₄N₂O)]·H₂O

Online 10 February 2004

 

Acta Cryst. (2004). C60, m117-m118  [ doi:10.1107/S0108270103028683 ]

catena-Poly[[silver(I)--ethane-1,2-diamine-²N:N'] 3-fluorobenzoate monohydrate]

Z.-L. You, L. Yang, Y. Zou, W.-J. Zeng, W.-S. Liu and H.-L. Zhu

Formula: [Ag(C₂H₈N₂)](C₇H₄FO₂)·H₂O

Online 10 February 2004

 

Acta Cryst. (2004). C60, m119-m122  [ doi:10.1107/S0108270104000848 ]

A polynuclear coordination glutarate of lanthanum(III) with an uncommon cage feature

B. Benmerad, A. Guehria-Laïdoudi, S. Dahaoui and C. Lecomte

Formula: [La₂(C₅H₆O₄)₃(H₂O)₃]·2H₂O

Online 10 February 2004

 

Acta Cryst. (2004). C60, m123-m125  [ doi:10.1107/S0108270104001556 ]

Bis[tetrakis(triphenylphosphine-P)silver(I)] di--trifluoroacetato-⁴O:O'-bis[bis(trifluoroacetato-O)stannate(IV)]

S.-Y. Yang, Z.-X. Xie and S. W. Ng

Formula: [Ag(C₁₈H₁₅P)₄]₂[Sn₂(CH₃)₄(C₂F₃O₂)₆]

Online 10 February 2004

 

Acta Cryst. (2004). C60, m126-m128  [ doi:10.1107/S0108270104001957 ]

Two new polymorphs of trans-bis(hinokitiolato)copper(II)

G. M. Arvanitis, M. E. Berardini and D. M. Ho

Formula: [Cu(C₁₀H₁₁O₂)₂]

Online 19 February 2004

 

Acta Cryst. (2004). C60, m129-m133  [ doi:10.1107/S0108270104001945 ]

RbCr^III(C₂O₄)₂·2H₂O, Cs₂Mg(C₂O₄)₂·4H₂O and Rb₂Cu^II(C₂O₄)₂·2H₂O: three new complex oxalate hydrates

U. Kolitsch

Synopsis: RbCr^III(C₂O₄)₂·2H₂O and Cs₂Mg(C₂O₄)₂·4H₂O represent two novel structure types among double-metal oxalate hydrates. Rb₂Cu^II(C₂O₄)₂·2H₂O is isotypic with K₂- and (NH₄)₂Cu^II(C₂O₄)₂·2H₂O. All three compounds have layered structures. The Cr, Mg and Cu atoms are six-, six- and (4 + 2)-coordinated, respectively.

Formula: [RbCr(C₂O₄)₂(H₂O)₂], [Cs₂Mg(C₂O₄)₂(H₂O)₄] and [Rb₂Cu(C₂O₄)₂(H₂O)₂]

Online 19 February 2004

 

Acta Cryst. (2004). C60, m134-m136  [ doi:10.1107/S0108270104001441 ]

Phenanthroline complexes of zinc and calcium carbamates

G. Reck and R. Becker

Formula: [Zn(C₉H₁₈NS₂)₂(C₁₂H₈N₂)]·0.5C₂H₆O and [Ca(C₁₃H₂₆NS₂)₂(C₁₂H₈N₂)₂]

Online 19 February 2004

 

Acta Cryst. (2004). C60, m137-m139  [ doi:10.1107/S0108270104002288 ]

Aqua(2,2'-diamino-4,4'-bi-1,3-thiazole-²N,N')(iminodiacetato-³O,N,O')chromium(III) chloride monohydrate

B.-X. Liu and D.-J. Xu

Formula: [Cr(C₄H₅NO₄)(C₆H₆N₄S₂)(H₂O)]Cl·H₂O

Online 19 February 2004

 

Acta Cryst. (2004). C60, m140-m142  [ doi:10.1107/S0108270104002380 ]

cis-Bis[1,3-bis(2-fluorophenyl)triazenido-²N¹,N³]bis(pyridine-N)cadmium(II)

M. Hörner, V. S. Carratu, J. Bordinhao, A. Silva and E. Niquet

Formula: [Cd(C₁₂H₈F₂N₃)₂(C₅H₅N)₂]

Online 28 February 2004

 

Acta Cryst. (2004). C60, m143-m146  [ doi:10.1107/S0108270104002264 ]

Heptaaquatetra-₃-hydroxy-hexa-₂-L-leucine-(L-leucine)tetraytterbium(III) tetrachlorozinc(II) trichlorohydroxyzinc(II) tetrachloride octahydrate

J.-P. Wang, C.-J. Niu and N.-H. Hu

Formula: [Yb₄(OH)₄(C₆H₁₃NO₂)₇(H₂O)₇][ZnCl₄][ZnCl₃(OH)]Cl₄·8H₂O

Online 28 February 2004

 

Acta Cryst. (2004). C60, o163-o165  [ doi:10.1107/S0108270103029111 ]

Diethyl 1-(4-fluorophenyl)-3-(2-furyl)-5-oxopyrrolidine-2,2-dicarboxylate and diethyl 1-(3,4-dichlorophenyl)-3-(2-furyl)-5-oxopyrrolidine-2,2-dicarboxylate

J. K. Ray, P. Haldar, M. Canle L., J. A. Santaballa and J. Mahía

Formula: C₂₀H₂₀FNO₆ and C₂₀H₁₉Cl₂NO₆

Online 10 February 2004

 

Acta Cryst. (2004). C60, o166-o168  [ doi:10.1107/S0108270103029639 ]

N-Benzyl-2,5-bis(2-thienyl)pyrrole

J. Palenzuela Conde, M. R. J. Elsegood and K. S. Ryder

Formula: C₁₉H₁₅NS₂

Online 10 February 2004

 

Acta Cryst. (2004). C60, o169-o172  [ doi:10.1107/S0108270104001404 ]

N,N'-Bis(2-methoxybenzylidene) adducts of ethane-1,2-diamine, propane-1,3-diamine and butane-1,4-diamine

J. Reglinski, M. K. Taylor and A. R. Kennedy

Formula: C₁₈H₂₀N₂O₂, C₁₉H₂₂N₂O₂ and C₂₀H₂₄N₂O₂

Online 10 February 2004

 

Acta Cryst. (2004). C60, o173-o175  [ doi:10.1107/S0108270104000666 ]

A 1,3,2-oxazaborolidine dimer derived from (S)-,-diphenylprolinol

M. Ortiz-Marciales, M. De Jesús, E. González, R. G. Raptis and P. Baran

Formula: C₃₄H₃₈B₂N₂O₂

Online 10 February 2004

 

Acta Cryst. (2004). C60, o176-o177  [ doi:10.1107/S0108270104000241 ]

Diethyl (Z,Z)-3,3'-(ethane-1,2-diyldiimino)dibut-2-enoate

Z.-F. Zhang, S. Jin, Z.-B. Shang, S.-P. Huang, B. Liu and J.-P. Guo

Formula: C₁₄H₂₄N₂O₄

Online 10 February 2004

 

Acta Cryst. (2004). C60, o178-o179  [ doi:10.1107/S0108270103025824 ]

Displaced - stacking and hydrogen bonds in 3-bromo-N-(2-hydroxy-1,1-dimethylethyl)benzamide

Y.-W. Wu, R.-J. Wang, Y.-Y. Jiang, H. Fu and Y.-F. Zhao

Formula: C₁₁H₁₄BrNO₂

Online 10 February 2004

 

Acta Cryst. (2004). C60, o180-o182  [ doi:10.1107/S010827010400112X ]

3,3,6,6-Tetramethyl-1,2,4,5-tetroxane: a twinned crystal structure

F. G. Gelalcha, B. Schulze and P. Lönnecke

Formula: C₆H₁₂O₄

Online 10 February 2004

 

Acta Cryst. (2004). C60, o183-o185  [ doi:10.1107/S0108270104000939 ]

rac-1-Phenylethylammonium carboxymethylphosphonate(1-): hydrogen-bonded anion sheets with pendent cations

D. E. Turkington, G. Ferguson, A. J. Lough and C. Glidewell

Formula: C₈H₁₂N⁺·C₂H₄O₅P^-

Online 10 February 2004

 

Acta Cryst. (2004). C60, o186-o190  [ doi:10.1107/S0108270104001489 ]

Racemic 5-(4-chlorophenyl)-2-methoxyindeno[1',2':2,3]pyrido[5,6-d]pyrimidine-4,6(3H,5H)-dione-dimethylformamide (1/1) and (5RS,5aSR,10bSR)-10b-hydroxy-2-methoxy-5-(4-methoxyphenyl)-5a,10b-dihydroindeno[1',2':2,3]pyrido[5,6-d]pyrimidine-4,6(3H,5H)-dione-dimethylformamide (1/1): chains of rings generated by N-HO and C-H(arene) hydrogen bonds

J. N. Low, J. Cobo, C. Cisneros, J. Quiroga and C. Glidewell

Formula: C₂₁H₁₄ClN₃O₃·C₃H₇NO and C₂₂H₁₉N₃O₅·C₃H₇NO

Online 10 February 2004

 

Acta Cryst. (2004). C60, o191-o193  [ doi:10.1107/S0108270104001118 ]

4-Amino-5-(2-hydroxy-4,4-dimethyl-6-oxocyclohexenylmethyl)-1-methyl-2-(methylsulfanyl)pyrimidin-6(1H)-one: hydrogen-bonded chains are -stacked in pairs

J. N. Low, J. Cobo, S. Cruz, J. Quiroga and C. Glidewell

Formula: C₁₅H₂₁N₃O₃S

Online 10 February 2004

 

Acta Cryst. (2004). C60, o194-o195  [ doi:10.1107/S0108270104000678 ]

5-Amino-3-tert-butyl-1-(4-nitrophenyl)-1H-pyrazole forms hydrogen-bonded sheets of alternating R(20) and R(32) rings

J. N. Low, J. Cobo, R. Abonia, J. Quiroga and C. Glidewell

Formula: C₁₃H₁₆N₄O₂

Online 10 February 2004

 

Acta Cryst. (2004). C60, o196-o197  [ doi:10.1107/S0108270104000332 ]

(1E)-2-(Diacetylamino)-1-methylprop-1-enyl acetate

B. Olesen and M. R. Bond

Formula: C₁₀H₁₅NO₄

Online 10 February 2004

 

Acta Cryst. (2004). C60, o198-o199  [ doi:10.1107/S0108270104000356 ]

Triethylammonium tetraphenylborate dichloromethane solvate

D. E. Janzen and K. R. Mann

Formula: C₆H₁₆N⁺·C₂₄H₂₀B^-·CH₂Cl₂

Online 10 February 2004

 

Acta Cryst. (2004). C60, o200-o203  [ doi:10.1107/S0108270103024053 ]

tert-Butyl (6S)-4-hydroxy-6-isobutyl-2-oxo-1,2,5,6-tetrahydropyridine-1-carboxylate and tert-butyl (4R,6S)-4-hydroxy-6-isobutyl-2-oxopiperidine-1-carboxylate

C. Didierjean, J. Marin, E. Wenger, J.-P. Briand, A. Aubry and G. Guichard

Formula: C₁₄H₂₃NO₄ and C₁₄H₂₅NO₄

Online 10 February 2004

 

Acta Cryst. (2004). C60, o204-o207  [ doi:10.1107/S0108270103024065 ]

(6S)-6-Isobutylpiperidine-2,4-dione and (4R,6S)/(4S,6S)-4-hydroxy-6-isobutylpiperidin-2-one

C. Didierjean, J. Marin, E. Wenger, J.-P. Briand, A. Aubry and G. Guichard

Formula: C₉H₁₇NO₂ and C₉H₁₅NO₂

Online 10 February 2004

 

Acta Cryst. (2004). C60, o208-o210  [ doi:10.1107/S0108270104001659 ]

A pair of epimeric 13-hydroxy-2,3,6,7-tetramethoxy-8b,11,12,12a,13,13a-hexahydro-9H-9a-azacyclopenta[b]triphenylene-10-ones

C. Nygren, T. Chen, S. Zhong, C. Kaczmarek, J. F. C. Turner and D. C. Baker

Formula: C₂₄H₂₇NO₆·C₃H₆O and C₂₄H₂₇NO₆

Online 19 February 2004

 

Acta Cryst. (2004). C60, o211-o214  [ doi:10.1107/S0108270104002227 ]

Melaminium maleate monohydrate

J. Janczak and G. J. Perpétuo

Formula: C₃H₇N₆⁺·C₄H₃O₄^-·H₂O

Online 19 February 2004

 

Acta Cryst. (2004). C60, o215-o216  [ doi:10.1107/S010827010400068X ]

N,N'-Bis(2-pyridyl)benzene-1,2-diamine

M. Gdaniec, I. Bensemann and T. Polonski

Formula: C₁₆H₁₄N₄

Online 19 February 2004

 

Acta Cryst. (2004). C60, o217-o218  [ doi:10.1107/S0108270104002550 ]

(Z)-3-(1-Methyl-1H-indol-3-yl)-2-(thiophen-3-yl)acrylonitrile

V. N. Sonar, S. Parkin and P. A. Crooks

Formula: C₁₆H₁₂N₂S

Online 19 February 2004

 

Acta Cryst. (2004). C60, o219-o222  [ doi:10.1107/S0108270104002707 ]

An analysis of C-HO and C-H interactions in three substituted 4-ketotetrahydroindoles

A. R. Choudhury, K. Nagarajan and T. N. Guru Row

Formula: C₂₂H₁₉ClFNO, C₂₃H₂₂FNO₂ and C₂₂H₂₁NO

Online 28 February 2004