# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' ' _shelx_refln_list_code 4 _shelx_F_calc_maximum 446.49 _exptl_crystal_F_000 1664.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.9439 _cell_length_b 14.0499 _cell_length_c 20.7267 _cell_angle_alpha 100.370 _cell_angle_beta 99.429 _cell_angle_gamma 95.899 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2418.76 2881.97 34.39 o 2 0 0 7672.74 8310.00 98.63 o 3 0 0 199349.08 225875.31 662.14 o 4 0 0 19587.46 22028.79 172.37 o 5 0 0 48354.10 53605.12 298.81 o 6 0 0 86.79 5.86 16.63 o 7 0 0 621.52 705.19 47.12 o 8 0 0 7003.86 8076.90 149.99 o 9 0 0 83.05 77.47 27.72 o 10 0 0 664.09 583.01 53.17 o 11 0 0 642.52 479.92 90.86 o 12 0 0 13.45 23.16 55.92 o 13 0 0 1060.81 1278.37 170.32 o 14 0 0 1291.79 1214.27 173.83 o 15 0 0 539.96 467.92 132.66 o 16 0 0 328.85 334.80 131.49 o -16 1 0 158.30 187.17 97.80 o -15 1 0 904.46 1014.23 171.49 o -14 1 0 367.93 438.91 131.25 o -13 1 0 9.91 -1.40 49.13 o -12 1 0 573.67 620.47 130.32 o -11 1 0 681.53 452.18 67.54 o -10 1 0 998.96 956.87 63.69 o -9 1 0 2525.88 2486.45 90.31 o -8 1 0 153.20 78.66 25.11 o -7 1 0 3085.54 2936.16 85.89 o -6 1 0 26244.94 27831.82 232.55 o -5 1 0 668.49 901.95 52.17 o -4 1 0 563.35 583.75 34.91 o -3 1 0 37402.86 41001.23 272.07 o -2 1 0 354.17 365.35 21.56 o -1 1 0 54004.18 61208.54 1106.21 o 0 1 0 3231.05 2536.63 537.06 o 1 1 0 3485.59 3768.14 60.32 o 2 1 0 8209.48 9068.86 152.20 o 3 1 0 42327.63 46417.19 523.27 o 4 1 0 6.52 21.51 15.18 o 5 1 0 6272.72 6559.33 109.75 o 6 1 0 2316.01 2183.32 72.19 o 7 1 0 203.64 282.67 35.79 o 8 1 0 190.67 270.29 38.91 o 9 1 0 1424.74 1156.73 66.46 o 10 1 0 850.59 853.06 63.90 o 11 1 0 526.14 497.74 99.95 o 12 1 0 1539.96 1585.80 178.28 o 13 1 0 26.63 59.89 65.51 o 14 1 0 90.81 61.30 73.00 o 15 1 0 1624.50 1960.37 226.24 o 16 1 0 134.37 184.60 101.07 o -16 2 0 691.71 1012.82 193.49 o -15 2 0 74.21 140.14 95.69 o -14 2 0 2.07 15.68 61.77 o -13 2 0 229.04 315.85 113.00 o -12 2 0 21.03 5.18 33.81 o -11 2 0 650.01 648.53 73.83 o -10 2 0 4464.45 4341.19 124.65 o -9 2 0 105.38 62.86 26.51 o -8 2 0 763.21 713.97 49.34 o -7 2 0 8935.90 9030.94 145.99 o -6 2 0 1040.13 1312.24 55.80 o -5 2 0 4758.42 5267.05 105.47 o -4 2 0 4865.73 5239.38 89.37 o -3 2 0 3658.82 4379.63 94.98 o -2 2 0 2774.01 2887.09 53.85 o -1 2 0 2589.74 3505.49 52.71 o 0 2 0 5528.54 6587.98 70.45 o 1 2 0 1190.95 1492.16 36.93 o 2 2 0 8619.06 9496.02 102.09 o 3 2 0 4398.74 4710.23 127.41 o 4 2 0 3843.66 3927.75 81.15 o 5 2 0 4292.50 4107.46 91.35 o 6 2 0 5902.69 6078.45 119.27 o 7 2 0 25.22 9.13 18.95 o 8 2 0 3206.31 3223.38 126.37 o 9 2 0 1382.88 1621.60 121.54 o 10 2 0 2.32 10.75 26.07 o 11 2 0 3042.06 3214.33 120.06 o 12 2 0 627.62 741.06 86.36 o 13 2 0 0.62 3.98 51.24 o 14 2 0 1974.72 2219.13 225.54 o 15 2 0 65.93 130.79 84.46 o 16 2 0 22.85 47.26 79.08 o -16 3 0 17.65 41.41 78.14 o -15 3 0 10.90 18.72 67.15 o -14 3 0 44.67 91.95 74.63 o -13 3 0 968.93 898.42 146.23 o -12 3 0 170.15 176.48 55.03 o -11 3 0 2797.83 2516.01 130.09 o -10 3 0 2195.89 2010.15 109.45 o -9 3 0 1011.18 944.82 59.36 o -8 3 0 6141.78 6689.47 146.42 o -7 3 0 6.92 31.38 20.10 o -6 3 0 894.55 965.40 50.63 o -5 3 0 5944.04 6893.74 120.10 o -4 3 0 9358.72 9866.53 148.55 o -3 3 0 6385.05 7061.24 177.13 o -2 3 0 42127.17 49109.73 249.08 o -1 3 0 94334.14 97811.73 3929.12 o 0 3 0 7080.49 8401.62 122.59 o 1 3 0 39075.87 43751.60 669.60 o 2 3 0 5240.56 5243.89 82.08 o 3 3 0 3535.42 3790.98 80.07 o 4 3 0 3671.11 3873.94 84.83 o 5 3 0 24465.24 24528.42 221.10 o 6 3 0 24.53 3.23 16.42 o 7 3 0 874.71 981.26 58.11 o 8 3 0 3263.45 3546.58 108.32 o 9 3 0 2960.22 2710.85 123.60 o 10 3 0 1889.25 1842.06 90.80 o 11 3 0 171.34 188.26 58.01 o 12 3 0 240.00 334.90 72.46 o 13 3 0 1232.21 1348.33 174.30 o 14 3 0 239.22 290.35 109.96 o 15 3 0 294.91 357.49 129.85 o -16 4 0 4.88 6.55 63.17 o -15 4 0 774.62 869.40 172.20 o -14 4 0 576.67 602.92 146.46 o -13 4 0 75.61 55.92 62.47 o -12 4 0 141.48 154.12 52.29 o -11 4 0 1235.47 1013.39 87.67 o -10 4 0 1130.47 1199.05 90.33 o -9 4 0 128.71 120.21 31.22 o -8 4 0 1803.22 1881.02 77.40 o -7 4 0 6202.05 6626.88 225.96 o -6 4 0 5246.22 5445.37 114.81 o -5 4 0 7081.39 7560.42 128.56 o -4 4 0 9072.86 10082.65 209.01 o -3 4 0 4143.56 5035.67 116.43 o -2 4 0 42652.50 45935.64 255.01 o -1 4 0 4109.44 3507.37 67.57 o 0 4 0 59.50 30.59 14.26 o 1 4 0 3171.11 2821.52 67.79 o 2 4 0 3097.77 3002.40 68.27 o 3 4 0 2371.57 2473.60 68.38 o 4 4 0 13665.80 13042.52 292.72 o 5 4 0 5193.34 5054.70 114.03 o 6 4 0 0.14 6.02 18.80 o 7 4 0 6833.05 6480.49 139.49 o 8 4 0 6868.90 7240.03 205.15 o 9 4 0 812.28 592.34 73.46 o 10 4 0 1663.10 1383.82 270.78 o 11 4 0 2115.35 2303.46 140.20 o 12 4 0 933.71 967.56 102.98 o 13 4 0 1030.93 1082.08 158.39 o 14 4 0 150.69 201.91 99.90 o 15 4 0 0.10 14.74 69.02 o -16 5 0 1.89 34.16 62.23 o -15 5 0 527.61 536.94 143.89 o -14 5 0 287.96 395.40 126.57 o -13 5 0 324.84 307.60 69.03 o -12 5 0 79.02 127.25 51.10 o -11 5 0 3436.43 3527.72 155.94 o -10 5 0 20.79 35.47 35.13 o -9 5 0 305.16 196.13 47.78 o -8 5 0 4944.95 4609.75 944.26 o -7 5 0 856.17 739.93 52.14 o -6 5 0 6294.82 6849.10 127.08 o -5 5 0 13721.86 14945.70 178.49 o -4 5 0 2847.47 3502.87 100.97 o -3 5 0 19859.40 21311.84 236.09 o -2 5 0 827.88 610.68 36.84 o -1 5 0 277.01 386.14 30.07 o 0 5 0 11961.04 12619.25 234.31 o 1 5 0 1691.34 1573.96 50.59 o 2 5 0 67.70 153.21 24.47 o 3 5 0 6541.86 6743.51 147.95 o 4 5 0 897.41 795.27 48.08 o 5 5 0 7991.99 8744.18 152.91 o 6 5 0 15.65 58.37 25.77 o 7 5 0 3682.16 3509.01 154.73 o 8 5 0 249.05 276.97 45.82 o 9 5 0 1167.35 1250.29 82.49 o 10 5 0 3245.41 3368.89 130.50 o 11 5 0 88.36 91.38 49.41 o 12 5 0 224.00 291.24 73.35 o 13 5 0 1184.62 1393.14 127.58 o -15 6 0 56.01 69.95 65.74 o -14 6 0 1974.70 2108.70 222.26 o -13 6 0 302.39 272.15 69.36 o -12 6 0 6330.77 6132.45 215.59 o -11 6 0 19.66 43.79 39.90 o -10 6 0 1902.44 1930.38 117.55 o -9 6 0 9809.37 9150.25 229.78 o -8 6 0 614.08 714.74 55.33 o -7 6 0 3030.92 3000.05 95.30 o -6 6 0 2347.30 1945.96 74.67 o -5 6 0 1070.60 991.89 53.44 o -4 6 0 2485.83 3136.87 85.97 o -3 6 0 1574.42 2036.93 67.30 o -2 6 0 37.68 94.24 22.43 o -1 6 0 19.67 39.38 17.95 o 0 6 0 169.60 199.60 27.10 o 1 6 0 334.85 252.31 28.06 o 2 6 0 1177.15 1315.00 53.28 o 3 6 0 1327.19 1444.16 60.07 o 4 6 0 17924.32 18017.42 398.38 o 5 6 0 625.60 639.37 49.66 o 6 6 0 2834.24 2345.68 375.00 o 7 6 0 2902.66 2532.13 100.85 o 8 6 0 73.16 108.40 36.26 o 9 6 0 1469.78 1477.79 87.97 o 10 6 0 477.08 506.71 78.21 o 11 6 0 236.09 283.07 70.02 o 12 6 0 1721.96 1902.82 204.02 o 13 6 0 134.77 219.69 104.35 o -15 7 0 1136.25 1325.87 189.51 o -14 7 0 216.72 263.68 103.41 o -13 7 0 90.18 138.51 56.73 o -12 7 0 1320.55 1337.86 204.83 o -11 7 0 1433.08 1321.07 106.17 o -10 7 0 1139.07 1092.71 94.03 o -9 7 0 670.93 508.74 105.40 o -8 7 0 93.30 61.52 39.10 o -7 7 0 1184.55 1100.03 158.72 o -6 7 0 2653.94 2673.53 89.65 o -5 7 0 54.25 91.30 27.24 o -4 7 0 0.49 9.34 17.68 o -3 7 0 179.75 264.96 32.93 o -2 7 0 2055.72 1806.41 65.60 o -1 7 0 85.55 76.01 21.62 o 0 7 0 707.50 542.30 38.73 o 1 7 0 8670.93 8841.20 128.50 o 2 7 0 544.23 555.27 40.16 o 3 7 0 5999.58 4827.34 106.90 o 4 7 0 1133.37 1116.68 60.92 o 5 7 0 56.46 43.95 25.61 o 6 7 0 1671.16 1619.38 79.81 o 7 7 0 3077.59 2813.94 108.30 o 8 7 0 101.85 89.76 34.50 o 9 7 0 1262.75 1369.12 110.11 o 10 7 0 13.14 -33.22 45.62 o 11 7 0 367.17 402.18 118.15 o 12 7 0 70.97 57.79 72.53 o 13 7 0 55.37 132.42 97.56 o -15 8 0 8.33 53.81 59.43 o -14 8 0 56.32 107.86 74.87 o -13 8 0 235.69 368.09 76.18 o -12 8 0 929.30 1064.22 104.22 o -11 8 0 67.27 98.77 47.13 o -10 8 0 716.79 722.14 82.55 o -9 8 0 2702.53 2616.44 139.75 o -8 8 0 516.89 525.71 83.76 o -7 8 0 1365.52 1329.95 73.43 o -6 8 0 4941.54 4984.55 158.04 o -5 8 0 823.96 1018.08 59.94 o -4 8 0 1145.18 1213.19 63.22 o -3 8 0 1058.51 965.71 55.18 o -2 8 0 237.38 351.40 38.33 o -1 8 0 2768.09 2579.03 79.30 o 0 8 0 7784.73 7469.66 133.16 o 1 8 0 863.84 1015.62 51.81 o 2 8 0 9620.15 9296.67 290.22 o 3 8 0 914.43 740.09 100.02 o 4 8 0 2377.69 2362.81 124.70 o 5 8 0 3527.22 3114.26 141.92 o 6 8 0 1884.29 1947.21 119.18 o 7 8 0 1168.08 1091.86 96.14 o 8 8 0 267.07 251.36 61.43 o 9 8 0 273.18 334.71 70.00 o 10 8 0 39.00 -3.74 53.58 o 11 8 0 225.99 304.39 116.05 o 12 8 0 65.01 73.00 80.95 o 13 8 0 445.04 542.33 144.12 o -15 9 0 203.35 351.41 123.77 o -14 9 0 128.98 165.04 61.80 o -13 9 0 396.83 472.05 88.21 o -12 9 0 3.89 4.47 35.17 o -11 9 0 518.26 566.66 85.20 o -10 9 0 674.86 728.43 84.85 o -9 9 0 445.76 517.11 77.56 o -8 9 0 436.51 404.04 66.38 o -7 9 0 3985.56 3172.56 684.24 o -6 9 0 2352.87 2474.06 94.89 o -5 9 0 514.74 491.27 55.47 o -4 9 0 3867.02 3893.01 113.39 o -3 9 0 1110.40 1093.26 106.72 o -2 9 0 2077.50 1812.52 108.91 o -1 9 0 10563.72 10278.71 253.99 o 0 9 0 66.92 71.14 24.58 o 1 9 0 1270.11 1203.53 89.96 o 2 9 0 2225.07 1873.30 108.69 o 3 9 0 2472.56 1797.57 252.80 o 4 9 0 1575.07 1542.04 144.24 o 5 9 0 235.80 185.08 52.20 o 6 9 0 140.65 114.53 47.97 o 7 9 0 1563.10 1507.60 113.19 o 8 9 0 1348.71 1379.29 110.38 o 9 9 0 278.19 353.75 112.54 o 10 9 0 110.89 129.85 83.76 o 11 9 0 372.64 544.43 134.53 o 12 9 0 172.38 166.11 96.16 o 13 9 0 77.96 98.97 92.42 o -14 10 0 347.17 446.67 90.66 o -13 10 0 342.51 462.16 88.65 o -12 10 0 332.67 345.12 76.68 o -11 10 0 945.05 923.23 98.64 o -10 10 0 412.04 471.47 80.23 o -9 10 0 808.48 817.78 89.63 o -8 10 0 407.39 334.07 63.58 o -7 10 0 1944.68 1908.67 116.51 o -6 10 0 675.95 617.19 57.50 o -5 10 0 516.76 452.40 48.93 o -4 10 0 292.21 311.70 41.91 o -3 10 0 261.44 284.46 40.66 o -2 10 0 4675.81 4559.51 161.08 o -1 10 0 4424.37 2818.40 1257.43 o 0 10 0 143.78 108.69 40.62 o 1 10 0 11.91 2.29 28.46 o 2 10 0 1907.10 1691.88 109.10 o 3 10 0 34.19 16.40 31.28 o 4 10 0 649.56 576.86 73.11 o 5 10 0 605.71 634.57 76.94 o 6 10 0 862.80 937.22 92.40 o 7 10 0 251.35 313.55 70.36 o 8 10 0 2509.18 2624.88 158.79 o 9 10 0 262.47 284.73 107.86 o 10 10 0 232.66 252.21 107.86 o 11 10 0 534.19 579.06 148.10 o 12 10 0 220.64 246.60 119.32 o -14 11 0 123.91 200.09 69.30 o -13 11 0 176.21 214.02 71.69 o -12 11 0 1415.06 1531.01 128.96 o -11 11 0 149.61 196.47 63.63 o -10 11 0 6.16 21.53 35.69 o -9 11 0 6.99 10.41 33.16 o -8 11 0 144.06 211.76 58.58 o -7 11 0 1977.36 1542.92 111.28 o -6 11 0 0.95 13.44 26.85 o -5 11 0 901.68 827.80 194.07 o -4 11 0 3037.52 2587.25 130.46 o -3 11 0 1163.87 1036.99 87.66 o -2 11 0 2982.52 2513.54 127.95 o -1 11 0 1583.43 1634.85 167.99 o 0 11 0 5.98 0.53 30.01 o 1 11 0 7668.67 6699.47 266.02 o 2 11 0 100.40 97.52 44.84 o 3 11 0 204.73 218.18 59.13 o 4 11 0 1325.53 1323.87 107.68 o 5 11 0 1133.49 1123.36 101.62 o 6 11 0 1207.78 1155.70 106.48 o 7 11 0 732.47 752.83 91.29 o 8 11 0 852.31 816.05 96.75 o 9 11 0 135.45 146.93 87.97 o 10 11 0 548.80 650.88 154.18 o 11 11 0 54.72 0.00 63.64 o -13 12 0 116.14 162.06 64.19 o -12 12 0 29.08 71.65 47.55 o -11 12 0 20.02 30.88 41.54 o -10 12 0 70.46 139.40 57.81 o -9 12 0 111.28 123.06 82.59 o -8 12 0 333.44 275.84 103.41 o -7 12 0 117.97 243.32 98.97 o -6 12 0 735.60 692.76 131.72 o -5 12 0 1393.83 1360.19 103.66 o -4 12 0 0.70 10.01 33.75 o -3 12 0 34.83 27.56 36.81 o -2 12 0 7841.06 7063.34 217.42 o -1 12 0 0.95 8.21 33.74 o 0 12 0 730.84 677.12 84.01 o 1 12 0 1015.95 951.56 93.46 o 2 12 0 1.22 12.94 34.74 o 3 12 0 2064.32 1943.38 130.61 o 4 12 0 41.19 49.35 40.31 o 5 12 0 195.47 199.08 62.81 o 6 12 0 543.85 530.55 88.34 o 7 12 0 5.22 27.67 38.84 o 8 12 0 1008.40 1032.71 168.92 o 9 12 0 5.67 -13.34 66.21 o 10 12 0 24.09 14.04 72.76 o -12 13 0 0.25 35.33 75.10 o -11 13 0 1221.85 1353.94 185.77 o -10 13 0 0.21 -11.46 63.17 o -9 13 0 371.46 506.29 128.91 o -8 13 0 793.31 856.07 140.14 o -7 13 0 65.78 51.24 65.28 o -6 13 0 789.99 861.45 142.25 o -5 13 0 644.87 693.60 87.13 o -4 13 0 451.89 409.31 73.58 o -3 13 0 3738.91 3518.13 170.32 o -2 13 0 33.57 33.60 39.36 o -1 13 0 0.24 29.49 35.67 o 0 13 0 982.73 959.15 96.37 o 1 13 0 18.85 18.76 38.46 o 2 13 0 108.94 110.17 52.03 o 3 13 0 219.39 234.74 66.07 o 4 13 0 177.74 192.71 63.43 o 5 13 0 86.50 117.56 56.01 o 6 13 0 2.41 10.21 40.07 o 7 13 0 1498.56 1558.91 134.84 o 8 13 0 25.58 43.52 70.42 o 9 13 0 1.78 -10.53 62.94 o -12 14 0 747.01 936.79 179.45 o -11 14 0 2.75 16.61 76.51 o -10 14 0 94.91 142.02 94.99 o -9 14 0 1255.92 1422.96 183.19 o -8 14 0 1372.22 1315.10 177.34 o -7 14 0 1843.78 1688.74 191.38 o -6 14 0 186.79 184.83 97.33 o -5 14 0 49.12 56.38 69.02 o -4 14 0 1583.27 1692.99 125.76 o -3 14 0 954.40 746.15 92.21 o -2 14 0 356.63 365.27 74.06 o -1 14 0 138.48 86.31 48.23 o 0 14 0 182.78 159.98 59.55 o 1 14 0 3.94 11.89 37.45 o 2 14 0 8.27 0.76 36.62 o 3 14 0 62.58 82.79 51.77 o 4 14 0 2390.51 2321.83 157.56 o 5 14 0 2.48 -5.69 38.69 o 6 14 0 1002.02 1154.23 119.04 o 7 14 0 96.80 122.13 99.67 o 8 14 0 61.21 26.67 86.10 o -10 15 0 1034.41 1239.30 189.74 o -9 15 0 275.16 210.80 107.15 o -8 15 0 2.53 25.97 73.70 o -7 15 0 846.65 940.53 167.99 o -6 15 0 1204.92 1137.76 171.96 o -5 15 0 1029.32 1060.08 160.26 o -4 15 0 407.18 396.50 83.79 o -3 15 0 692.65 683.43 93.55 o -2 15 0 68.05 60.65 45.71 o -1 15 0 176.09 159.94 58.74 o 0 15 0 155.20 194.18 61.63 o 1 15 0 66.32 91.33 51.28 o 2 15 0 293.98 276.52 75.09 o 3 15 0 1787.77 1747.30 139.48 o 4 15 0 32.42 50.30 47.81 o 5 15 0 1209.87 1251.01 128.20 o 6 15 0 325.07 418.87 92.18 o -8 16 0 255.39 384.40 133.59 o -7 16 0 503.36 611.11 150.20 o -6 16 0 138.11 113.71 92.65 o -5 16 0 36.46 76.74 83.99 o -4 16 0 778.09 892.10 149.97 o -3 16 0 39.07 99.58 53.46 o -2 16 0 5.41 18.65 40.63 o -1 16 0 217.03 268.19 72.81 o 0 16 0 312.37 375.03 82.28 o 1 16 0 175.72 258.55 73.64 o 2 16 0 651.17 659.66 103.75 o 3 16 0 6.85 6.14 44.77 o 4 16 0 17.31 41.73 51.05 o 5 16 0 548.40 646.91 148.33 o -6 17 0 89.96 127.98 94.99 o -5 17 0 37.31 69.02 77.91 o -4 17 0 240.54 356.79 127.04 o -3 17 0 157.97 179.07 65.08 o -2 17 0 110.39 227.08 73.19 o -1 17 0 249.77 353.46 85.92 o 0 17 0 54.55 47.25 47.38 o 1 17 0 735.78 942.08 117.19 o 2 17 0 7.57 28.44 48.32 o 3 17 0 305.77 276.78 112.54 o 1 -18 1 0.49 17.78 70.19 o -3 -17 1 739.32 660.92 107.53 o -2 -17 1 87.94 92.20 55.29 o -1 -17 1 8.60 66.95 50.26 o 0 -17 1 827.18 946.45 112.26 o 1 -17 1 38.10 50.83 47.39 o 2 -17 1 947.07 1008.84 114.72 o 3 -17 1 98.80 195.83 96.39 o 4 -17 1 3.45 37.20 65.74 o 5 -17 1 48.54 97.09 83.99 o 6 -17 1 4.93 25.50 70.66 o -5 -16 1 70.45 22.06 51.16 o -4 -16 1 1166.50 1291.11 135.46 o -3 -16 1 96.06 88.40 54.76 o -2 -16 1 7.46 26.91 45.16 o -1 -16 1 830.19 887.14 106.05 o 0 -16 1 83.54 139.12 56.49 o 1 -16 1 83.40 122.60 57.52 o 2 -16 1 790.32 741.83 101.83 o 3 -16 1 180.06 192.18 66.09 o 4 -16 1 7.15 56.85 65.74 o 5 -16 1 438.75 431.19 129.15 o 6 -16 1 611.06 562.21 142.72 o 7 -16 1 559.99 534.84 146.93 o 8 -16 1 43.90 6.32 71.59 o 9 -16 1 435.22 346.26 130.08 o -6 -15 1 449.87 448.27 143.89 o -5 -15 1 922.01 1121.99 120.61 o -4 -15 1 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