Crystal Structure Communications

 

Acta Cryst. (2004). C60, i53-i55  [ doi:10.1107/S0108270104002409 ]

The alkali hypophosphites KH₂PO₂, RbH₂PO₂ and CsH₂PO₂

M. I. Naumova, N. V. Kuratieva, N. V. Podberezskaya and D. Y. Naumov

Synopsis: The structures of the title compounds consist of layers of alkali cations and H₂PO₂^- hypophosphite anions, with the latter bridging four cations within the same layer. The hypophosphite anion has a distorted tetrahedral arrangement, with the P atom at the centre and two O and two H atoms at the vertices.

Formula: KH₂PO₂, RbH₂PO₂ and CsH₂PO₂

Online 9 April 2004

 

Acta Cryst. (2004). C60, i56-i58  [ doi:10.1107/S0108270104005384 ]

Sodium magnesium bis(vanadate) pyrovanadate: Na₆Mg₂(VO₄)₂(V₂O₇)

A. Mitiaev, A. Mironov, R. Shpanchenko and E. Antipov

Synopsis: The structure of Na₆Mg₂(VO₄)₂(V₂O₇) contains randomly oriented isolated pyrovanadate groups linked together by MgO₆ octahedra, thus forming a three-dimensional framework.

Formula: Na₆Mg₂(VO₄)₂(V₂O₇)

Online 9 April 2004

 

Acta Cryst. (2004). C60, i59-i60  [ doi:10.1107/S0108270104006134 ]

Oxygen-deficient strontium cobaltate, SrCoO_2.64

A. Nakatsuka, A. Yoshiasa, N. Nakayama, T. Mizota and H. Takei

Synopsis: SrCoO_2.64 crystallizes with a cubic perovskite-type structure. The displacement ellipsoids of the O atoms show large anisotropy in a direction perpendicular to that of the Co-O bonds.

Formula: SrCoO_2.64

Online 21 April 2004

 

Acta Cryst. (2004). C60, m197-m199  [ doi:10.1107/S0108270104006080 ]

catena-Poly[europium(III)-tri--2,3-dimethoxybenzoato]

X. Li, Y.-Q. Zou, B. Zheng and H.-M. Hu

Formula: [Eu(C₉H₉O₄)₃]

Online 9 April 2004

 

Acta Cryst. (2004). C60, m200-m202  [ doi:10.1107/S0108270104005797 ]

Rubidium bis(trifluoromethanesulfonyl)imidate dioxane disolvate

L.-X. Xue, C. W. Padgett, D. D. DesMarteau and W. T. Pennington

Formula: Rb⁺·C₂F₆NO₄S₂^-·2C₄H₈O₂

Online 9 April 2004

 

Acta Cryst. (2004). C60, m203-m204  [ doi:10.1107/S0108270104004007 ]

1,4-Diazabicyclo[2.2.2]octane-1,4-diium trichromate

C.-R. Ding, Z.-M. Jin, H.-B. Wang, M.-L. Hu and H. Lin

Formula: (C₆H₁₄N₂)[Cr₃O₁₀]

Online 21 April 2004

 

Acta Cryst. (2004). C60, m205-m207  [ doi:10.1107/S0108270104006560 ]

Chloro(histamine)(1,10-phenanthroline)copper(II) chloride monohydrate

E. Y. Bivián-Castro, S. Bernès, J. Escalante and G. Mendoza-Díaz

Formula: [CuCl(C₅H₉N₃)(C₁₂H₈N₂)]Cl·H₂O

Online 21 April 2004

 

Acta Cryst. (2004). C60, m208-m209  [ doi:10.1107/S0108270104006869 ]

A metal-mediated dimerization of the ligand bis(N,N-diethylamino)carbeniumdithiocarboxylate

S. R. Banerjee and J. Zubieta

Formula: (C₂₁H₄₂N₄S₄)[ReCl₅O]

Online 21 April 2004

 

Acta Cryst. (2004). C60, m210-m211  [ doi:10.1107/S0108270104005803 ]

Tris[N-(4-fluorophenyl)pyridine-2-carboxamidato-²N,N']cobalt(III) trihydrate: a novel meridional complex

J.-Y. Qi, Q.-Y. Yang, S.-S. Chan, Z.-Y. Zhou and A. S. C. Chan

Formula: [Co(C₁₂H₈FN₂O)₃]·3H₂O

Online 21 April 2004

 

Acta Cryst. (2004). C60, m212-m214  [ doi:10.1107/S0108270104007152 ]

A heterometallic polymeric complex: [Cu₂(N₃)₂(medpt)₂{Ni(CN)₄}]_n [medpt is bis(3-aminopropyl)methylamine]

D. Ghoshal, T. K. Maji, G. Rosair and G. Mostafa

Formula: [Cu₂Ni(CN)₄(N₃)₂(C₇H₁₉N₃)₂]

Online 30 April 2004

 

Acta Cryst. (2004). C60, m215-m218  [ doi:10.1107/S0108270104007450 ]

The catena-arsenite chain anion, [AsO₂]_n^n-: (H₃NCH₂CH₂NH₃)_0.5[AsO₂] and NaAsO₂ (revisited)

C. Lee and W. T. A. Harrison

Formula: (C₂H₁₀N₂)_0.5[AsO₂] and Na[AsO₂]

Online 30 April 2004

 

Acta Cryst. (2004). C60, m219-m220  [ doi:10.1107/S0108270104006729 ]

Bis[1,1-dimethylbiguanide(1-)-²N²,N⁵]copper(II) monohydrate

L.-P. Lu, P. Yang, S.-D. Qin and M.-L. Zhu

Formula: [Cu(C₄H₁₀N₅)₂]·H₂O

Online 30 April 2004

 

Acta Cryst. (2004). C60, m221-m223  [ doi:10.1107/S0108270104007668 ]

A novel bridged asymmetric binuclear manganese(II) complex with DTPB [DTPB is 1,1,4,7,7-pentakis(1H-benzimidazol-2-ylmethyl)-1,4,7-triazaheptane]

X.-X. Yan, L.-P. Lu and M.-L. Zhu

Formula: [Mn₂Cl₄(C₄₄H₄₃N₁₃)]·5CH₄O·4H₂O

Online 30 April 2004

 

Acta Cryst. (2004). C60, m224-m226  [ doi:10.1107/S0108270104007553 ]

Bis(pentane-1,5-diammonium) decaiodotriplumbate(II)

D. G. Billing and A. Lemmerer

Formula: (C₅H₁₆N₂)₂[Pb₃I₁₀]

Online 30 April 2004

 

Acta Cryst. (2004). C60, m227-m230  [ doi:10.1107/S0108270104007796 ]

Two furopyridine complexes of nickel(II) isothiocyanate

J. Miklovic, A. Krutosíková and P. Baran

Formula: [Ni(NCS)₂(C₇H₅NO)₄]·C₄H₈O and [Ni(NCS)₂(C₉H₉NO)₄]·6.6H₂O

Online 30 April 2004

 

Acta Cryst. (2004). C60, o303-o304  [ doi:10.1107/S0108270104004822 ]

3-(4-Acetylphenyl)-1-(4-nitrophenyl)triazene

M. Hörner, A. L. Brancher, A. Silva, J. Bordinhao and C. M. Mössmer

Formula: C₁₄H₁₂N₄O₃

Online 9 April 2004

 

Acta Cryst. (2004). C60, o305-o307  [ doi:10.1107/S0108270104005815 ]

3,3,4,4,5,5-Hexafluoro-1,2-bis(5-hydroxymethyl-2-methyl-3-thienyl)cyclopent-1-ene

S.-Z. Pu, F.-S. Zhang, R.-J. Wang and Q. Liang

Formula: C₁₇H₁₄F₆O₂S₂

Online 9 April 2004

 

Acta Cryst. (2004). C60, o308-o311  [ doi:10.1107/S0108270104006067 ]

{(E)- and {(Z)-2-[,-bis(methoxycarbonyl)vinyl]cyclopentadien-1-ylidene}triphenylphosphorane

L. J. Higham, P. G. Kelly, H. Müller-Bunz and D. G. Gilheany

Formula: Two isomers of C₂₉H₂₅O₄P

Online 9 April 2004

 

Acta Cryst. (2004). C60, o312-o314  [ doi:10.1107/S0108270104004287 ]

Methyl 2,6-di-O-benzyl-3,4-O-phenylphosphinediyl--D-galactopyranoside(P-B)borane with chirality on the P atom

M. J. Johansson, A. Bergh and K. Larsson

Formula: C₂₇H₃₂BO₆P

Online 9 April 2004

 

Acta Cryst. (2004). C60, o315-o317  [ doi:10.1107/S0108270104006110 ]

5,5-Dimethoxy-2-phenoxy-1,3,2-dioxaphosphorinane 2-oxide

K. Slepokura and T. Lis

Formula: C₁₁H₁₅O₆P

Online 9 April 2004

 

Acta Cryst. (2004). C60, o318-o320  [ doi:10.1107/S0108270104006122 ]

5-(2-Chlorophenyldiazenyl)salicylaldehyde and 4-(2-chlorophenyldiazenyl)-2-{[tris(hydroxymethyl)methyl]aminomethylene}cyclohexa-3,5-dien-1(2H)-one

Ç. Albayrak, M. Odabasoglu, O. Büyükgüngör and P. Lönnecke

Formula: C₁₃H₉ClN₂O₂ and C₁₇H₁₈ClN₃O₄

Online 9 April 2004

 

Acta Cryst. (2004). C60, o321-o324  [ doi:10.1107/S0108270104006687 ]

Two oxazane macrocycles

P. J. Cox and P. Lin

Formula: C₁₂H₃₂N₄O₄⁴⁺·4Cl^- and C₁₀H₂₈N₄O₄⁴⁺·4Cl^-

Online 9 April 2004

 

Acta Cryst. (2004). C60, o325-o327  [ doi:10.1107/S0108270104006109 ]

N,N'-Propylenedioxybis(2,4,6-trimethylbenzenesulfonamide): molecules of unexpected conformation form a molecular ladder built from two independent N-HO=S hydrogen bonds

S. M. S. V. Wardell, M. V. D. Rangel e Silva, P. F. Prado, J. N. Low and C. Glidewell

Formula: C₂₁H₃₀N₂O₆S₂

Online 9 April 2004

 

Acta Cryst. (2004). C60, o328-o330  [ doi:10.1107/S0108270104006092 ]

Hydrogen bonding in substituted nitroanilines: hydrogen-bonded sheets in 4-iodo-3-nitroaniline

S. J. Garden, J. L. Wardell, J. M. S. Skakle, J. N. Low and C. Glidewell

Formula: C₆H₅IN₂O₂

Online 9 April 2004

 

Acta Cryst. (2004). C60, o331-o333  [ doi:10.1107/S0108270104006146 ]

Triphenyl(3,4,5-triiodophenyl)methane

C. M. Reddy, A. Nangia, R. K. R. Jetti and R. Boese

Formula: C₂₅H₁₇I₃

Online 21 April 2004

 

Acta Cryst. (2004). C60, o334-o337  [ doi:10.1107/S0108270104006924 ]

2-Amino-4-(1-naphthyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile and 2-amino-7,7-dimethyl-4-(1-naphthyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile

V. N. Nesterov, D. J. Wiedenfeld, S. V. Nesterova and M. A. Minton

Formula: C₂₀H₁₆N₂O₂ and C₂₂H₂₀N₂O₂

Online 21 April 2004

 

Acta Cryst. (2004). C60, o338-o340  [ doi:10.1107/S0108270104006754 ]

A substituted EDOT precursor: diethyl 3,4-dihydroxythiophene-2,5-dicarboxylate

C. Faulmann and A. E. Pullen

Formula: C₁₀H₁₂O₆S

Online 21 April 2004

 

Acta Cryst. (2004). C60, o341-o343  [ doi:10.1107/S010827010400650X ]

1-(4-Bromophenyl)-2-methyl-4-nitro-1H-imidazole: bifurcated BrO halogen-nitro bonds

M. Kubicki

Formula: C₁₀H₈BrN₃O₂

Online 21 April 2004

 

Acta Cryst. (2004). C60, o344-o345  [ doi:10.1107/S0108270104006493 ]

3-Formylphenylboronic acid

B. Zarychta, J. Zaleski, A. Sporzynski, M. Dabrowski and J. Serwatowski

Formula: C₇H₇BO₃

Online 21 April 2004

 

Acta Cryst. (2004). C60, o346-o349  [ doi:10.1107/S0108270104006857 ]

(R)-2,3,4,5-Tetrahydro-2,2,4-trimethyl-1,5-benzothiazepine and rac-5-benzoyl-2,3,4,5-tetrahydro-2,2,4-trimethyl-1,5-benzothiazepine: chains built from N-HS and C-H(arene) hydrogen bonds

M. Muthukumar, K. Thanikasalam, E. M. Mohamed, J. N. Low and C. Glidewell

Formula: C₁₂H₁₇NS and C₁₉H₂₁NOS

Online 21 April 2004

 

Acta Cryst. (2004). C60, o350-o352  [ doi:10.1107/S0108270104006286 ]

2,3-Bis[(4-methylphenyl)sulfanyl]-4H-1-benzothiopyran-4-one 1,1-dioxide forms a framework built from C-HO, C-H(arene) and - interactions

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C₂₃H₁₈O₃S₃

Online 21 April 2004

 

Acta Cryst. (2004). C60, o353-o355  [ doi:10.1107/S0108270104006882 ]

1-Bromo-2,6-dihydroxybenzene containing R₄⁴(8) rings and C(2) helices

P. Kirsop, J. M. D. Storey and W. T. A. Harrison

Formula: C₆H₅BrO₂

Online 21 April 2004

 

Acta Cryst. (2004). C60, o356-o357  [ doi:10.1107/S010827010400410X ]

6-(2-Fluorobenzylidene)-2-[1-(2-fluoro-4-biphenyl)ethyl]thiazolo[3,2-b][1,2,4]triazol-5(6H)-one

Y. Köysal, S. Isik, E. Dogdas, B. Tozkoparan and M. Ertan

Formula: C₂₅H₁₇F₂N₃OS

Online 21 April 2004

 

Acta Cryst. (2004). C60, o358-o360  [ doi:10.1107/S0108270104007012 ]

N,N'-Bis(dipiperidin-1-ylmethylene)propane-1,3-diamine and N,N'-bis(1,3-dimethylperhydropyrimidin-2-ylidene)propane-1,3-diamine

S. Herres, U. Flörke and G. Henkel

Formula: C₂₅H₄₆N₆ and C₁₅H₃₀N₆

Online 30 April 2004

 

Acta Cryst. (2004). C60, o361-o363  [ doi:10.1107/S0108270104007036 ]

2-(4-Nitrophenoxy)benzoic acid: a three-dimensional hydrogen-bonded framework in a triclinic structure having Z' = 3

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C₁₃H₉NO₅

Online 30 April 2004

 

Acta Cryst. (2004). C60, o364-o367  [ doi:10.1107/S010827010400719X ]

Monoclinic pseudosymmetry in 2-phenoxybenzenesulfonamide, a triclinic structure having Z' = 4, and spontaneous resolution in monoclinic N-methyl-2-phenoxybenzenesulfonamide

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C₁₂H₁₁NO₃S and C₁₃H₁₃NO₃S

Online 30 April 2004

 

Acta Cryst. (2004). C60, o368-o370  [ doi:10.1107/S0108270104007103 ]

trans-4-Bromo-ONN-azoxybenzene at 100  K

K. Ejsmont, A. A. Domanski, J. B. Kyziol and J. Zaleski

Formula: C₁₂H₉BrN₂O

Online 30 April 2004

 

Acta Cryst. (2004). C60, o371-o373  [ doi:10.1107/S0108270104007255 ]

L-Isoleucyl-L-phenylalanine dihydrate

C. H. Görbitz

Formula: C₁₅H₂₂N₂O₃·2H₂O

Online 30 April 2004

 

Acta Cryst. (2004). C60, o374-o376  [ doi:10.1107/S0108270104006845 ]

Two stereoisomers of the rat toxicant norbormide

P. J. Steel, M. A. Brimble, B. Hopkins and D. Rennison

Formula: C₃₃H₂₅N₃O₃ and C₃₃H₂₅N₃O₃·0.5C₄H₈O₂

Online 30 April 2004

 

Acta Cryst. (2004). C60, o377-o380  [ doi:10.1107/S0108270104004342 ]

Vindoline and 16-demethoxyvindoline: two catharanthus-derived alkaloids

J. Ruszkowska, R. Chrobak, J. K. Maurin and Z. Czarnocki

Formula: C₂₅H₃₂N₂O₆ and C₂₄H₃₀N₂O₅

Online 30 April 2004