Acta Crystallographica Section C

Crystal Structure Communications

Volume 60, Part 9 (September 2004)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: A view of the unit cell of bis(tetraethylammonium) di-[mu]-chloro-bis[dichloropalladium(II)] at 292 K along the c axis. Displacement ellipsoids are drawn at the 50% probability level and H atoms are shown as small spheres of arbitrary radii. See Fábry, Dusek, Fejfarová, Krupková, Vanek & Nemec [Acta Cryst. (2004), C60, m426-m430].

inorganic compounds


 

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Acta Cryst. (2004). C60, i79-i83  [ doi:10.1107/S0108270104015938 ]

Alkali scandium arsenates. I. The framework structures of KSc(HAsO4)2 and RbScAs2O7

K. Schwendtner and U. Kolitsch

Synopsis: KSc(HAsO4)2 and RbScAs2O7 are both characterized by three-dimensional octahedral-tetrahedral frameworks, with intersecting tunnels hosting the alkali atoms. KSc(HAsO4)2 represents a new structure type, while RbScAs2O7 is the first reported diarsenate isotypic with KAlP2O7.

Formula: KSc(HAsO4)2 and RbScAs2O7

Online 11 August 2004


 

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Acta Cryst. (2004). C60, i84-i88  [ doi:10.1107/S010827010401594X ]

Alkali scandium arsenates. II. The framework structures of [alpha]- and [beta]-CsSc(HAsO4)2

K. Schwendtner and U. Kolitsch

Synopsis: The triclinic ([alpha]) and monoclinic ([beta]) modifications of CsSc(HAsO4)2 have three-dimensional octahedral-tetrahedral framework structures, with tunnels hosting the Cs atoms, and represent the first arsenate examples of their structure types. Strong to weak hydrogen bonds reinforce both frameworks.

Formula: Two modifications of CsSc(HAsO4)2

Online 11 August 2004


 

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Acta Cryst. (2004). C60, i89-i90  [ doi:10.1107/S0108270104017275 ]

A new chromate of tetravalent cerium: Ce2(CrO4)4·2H2O

U. Kolitsch and K. Schwendtner

Synopsis: The crystal structure of the new chromate Ce_{2}^{\rm IV}(CrO4)4·2H2O, prepared from an acidic aqueous solution at room temperature, is built from isolated CrO4 tetrahedra connected to isolated Ce(O,H2O)n (n = 8 and 9) polyhedra.

Formula: Ce2(CrO4)4·2H2O

Online 11 August 2004


 

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Acta Cryst. (2004). C60, i91-i93  [ doi:10.1107/S0108270104016105 ]

Powder neutron diffraction of SrNbO2N at room temperature and 1.5 K

S. G. Ebbinghaus, A. Weidenkaff, A. Rachel and A. Reller

Synopsis: The peroskite oxynitride SrNbO2N crystallizes in space group I4/mcm, both at room temperature and at 1.5 K. The Nb(O,N)6 octahedra are slightly rotated with respect to the tetragonal axis. A partially order of oxygen and nitrogen on the anionic sites was found.

Formula: SrNbO2N

Online 21 August 2004


 

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Acta Cryst. (2004). C60, i94-i96  [ doi:10.1107/S010827010401813X ]

Mg7(AsO4)2(HAsO4)4: a new magnesium arsenate with a very strong hydrogen bond

U. Kolitsch and P. Bartu

Synopsis: Hydrothermally synthesized Mg7(AsO4)2(HAsO4)4 has a framework structure built of edge- and corner-sharing MgO6, MgO4(OH)2, MgO5, AsO3(OH) and AsO4 polyhedra. The compound contains a very short hydrogen bond [O...O = 2.468 (3) Å].

Formula: Mg7(AsO4)2(HAsO4)4

Online 21 August 2004


metal-organic compounds


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Acta Cryst. (2004). C60, m421-m422  [ doi:10.1107/S0108270104016087 ]

Bis[1,3-bis(2-methyltetrazol-5-yl-[kappa]N4)triazenido-[kappa]N2]nickel(II)

A. S. Lyakhov, P. N. Gaponik, D. S. Pytleva, S. V. Voitekhovich and L. S. Ivashkevich

Formula: [Ni(C4H6N11)2]

Online 11 August 2004


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Acta Cryst. (2004). C60, m423-m425  [ doi:10.1107/S0108270104016889 ]

Bis([mu]-2-sulfonatobenzoato)bis[(1,10-phenanthroline)lead(II)] dihydrate

X.-H. Li and S.-Z. Yang

Formula: [Pb2(C7H4O5S)2(C12H8N2)2]·2H2O

Online 11 August 2004


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Acta Cryst. (2004). C60, m426-m430  [ doi:10.1107/S0108270104016725 ]

Two phases of bis(tetraethylammonium) di-[mu]-chloro-bis[dichloropalladium(II)]

J. Fábry, M. Dusek, K. Fejfarová, R. Krupková, P. Vanek and I. Nemec

Formula: (C8H20N)2[Pd2Cl6]

Online 11 August 2004


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Acta Cryst. (2004). C60, m431-m432  [ doi:10.1107/S0108270104016877 ]

An unexpected chelate conformation in trans-[(R)-N,N'-bis([alpha]-phenylsalicylidene)propane-1,2-diaminato(2-)]bis(1-methyl-1H-imidazole-[kappa]N3)cobalt(III) perchlorate

M. Hirotsu, M. Kojima, K. Nakajima, S. Kashino and Y. Yoshikawa

Formula: [Co(C29H24N2O2)(C4H6N2)2]ClO4

Online 11 August 2004


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Acta Cryst. (2004). C60, m433-m434  [ doi:10.1107/S0108270104017184 ]

Bis(4,4'-bipyridine-[kappa]N)bis(hydrogen phthalato)-[kappa]2O,O';[kappa]O-zinc(II)

E. Tang, Y.-M. Dai and S. Lin

Formula: [Zn(C8H5O4)2(C10H8N2)2]

Online 11 August 2004


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Acta Cryst. (2004). C60, m435-m436  [ doi:10.1107/S0108270104016816 ]

Bis([mu]-cystamine-[kappa]4N,S:S',N')bis[(2-aminoethanethiolato-[kappa]2N,S)iridium(III)] tetrabromide dihydrate

M. Fujita, Y. Miyashita, N. Amir, Y. Yamada, K. Fujisawa and K. Okamoto

Formula: [Ir2(C2H6NS)2(C4H12N2S2)2]Br4·2H2O

Online 11 August 2004


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Acta Cryst. (2004). C60, m437-m439  [ doi:10.1107/S0108270104016944 ]

catena-Poly[[[[mu]-pyridinium-3-carboxylato-bis[dioxomolybdenum(VI)]]-di-[mu]3-oxo] monohydrate]

S.-M. Chen, C.-Z. Lu, Y.-Q. Yu, Q.-Z. Zhang and X. He

Formula: [Mo2O6(C6H5NO2)]·H2O

Online 11 August 2004


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Acta Cryst. (2004). C60, m440-m442  [ doi:10.1107/S0108270104016099 ]

[mu]-Biphenyl-2,2'-dithiolato-[kappa]2S:S'-bis[(triphenylphosphine-[kappa]P)gold(I)]

S. A. Larkin, J. A. Krause Bauer, V. E. Konoplev, V. P. Dyadchenko, D. A. Lemenovskii, M. R. M. Bruce and A. E. Bruce

Formula: [Au2(C12H8S2)(C18H15P)2]

Online 11 August 2004


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Acta Cryst. (2004). C60, m443-m444  [ doi:10.1107/S0108270104017469 ]

A one-dimensional ladder-like coordination polymer derived from chains formed via hydrogen bonds: catena-poly[[aquadipyridinenickel(II)]-[mu]-2,2'-dithiodibenzoato-[kappa]3O,O':O'']

W.-N. Zhao, J.-W. Zou and Q.-S. Yu

Formula: [Ni(C14H8O4S2)(C5H5N)2(H2O)]

Online 11 August 2004


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Acta Cryst. (2004). C60, m445-m446  [ doi:10.1107/S0108270104017718 ]

Bis{[mu]-2-[3-(cyclohexylammonio)propyliminomethyl]phenolato}bis[dichlorocopper(II)]

Z.-L. You and H.-L. Zhu

Formula: [Cu2(C16H24N2O)2Cl4]

Online 11 August 2004


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Acta Cryst. (2004). C60, m447-m448  [ doi:10.1107/S010827010401772X ]

catena-Poly[1,4-diazoniabicyclo[2.2.2]octane [silver(I)-tri-[mu]-thiocyanato-[kappa]6S:S]]

Z.-D. Liu, Y. Zou, M.-Y. Tan and H.-L. Zhu

Formula: (C6H14N2)[Ag(NCS)3]

Online 11 August 2004


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Acta Cryst. (2004). C60, m449-m450  [ doi:10.1107/S0108270104016129 ]

[Pd(CH3COO)2]n from X-ray powder diffraction data

S. D. Kirik, R. F. Mulagaleev and A. I. Blokhin

Formula: [Pd(C2H3O2)2]

Online 21 August 2004


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Acta Cryst. (2004). C60, m451-m453  [ doi:10.1107/S0108270104018219 ]

Tetraaqua(3,4,7,8-tetramethyl-1,10-phenanthroline-[kappa]2N,N')zinc(II) thiosulfate

M. E. Díaz de Vivar, S. Baggio, A. Ibañez and R. Baggio

Formula: [Zn(C16H16N2)(H2O)4](S2O3)

Online 21 August 2004


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Acta Cryst. (2004). C60, m454-m456  [ doi:10.1107/S0108270104018165 ]

Aquabis(2-nitrobenzoato-[kappa]O)(1,10-phenanthroline-[kappa]2N,N')zinc(II)

K.-L. Zhang, J.-G. Lin, Y.-Q. Wang, W.-L. Xu and J.-T. Chen

Formula: [Zn(C7H4NO4)2(C12H8N2)(H2O)]

Online 21 August 2004


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Acta Cryst. (2004). C60, m457-m459  [ doi:10.1107/S0108270104017378 ]

Bis([mu]-ethyl pyridine-2,6-dicarboxylato)bis[diaquachlorocadmium(II)] dihydrate

E. Yang, Z.-J. Li, J. Zhang, Y.-B. Chen and Y.-G. Yao

Formula: [Cd2(C9H8NO4)2Cl2(H2O)4]·2H2O

Online 21 August 2004


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Acta Cryst. (2004). C60, m460-m464  [ doi:10.1107/S0108270104018645 ]

Poly[[bis[aqua(1,10-phenanthroline)lanthanum(III)]-[mu]-aqua-di-[mu]-5-sulfonatoisophthalato] monohydrate] and poly[[[triaqualanthanum(III)]-[mu]-5-sulfonatoisophthalato] monohydrate]

M.-L. Hu, Q. Miao, Q. Shi and M.-D. Ye

Formula: [La2(C8H3O7S)2(C12H8N2)2(H2O)3]·H2O and [La(C8H3O7S)(H2O)3]·H2O

Online 31 August 2004


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Acta Cryst. (2004). C60, m465-m466  [ doi:10.1107/S0108270104018840 ]

Amidobis[[eta]5-1,3-bis(trimethylsilyl)cyclopentadienyl]titanium(III)

C. D. Sofield, M. D. Walter and R. A. Andersen

Formula: [Ti(C11H21Si2)2(NH2)]

Online 31 August 2004


organic compounds


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Acta Cryst. (2004). C60, o623-o626  [ doi:10.1107/S0108270104014660 ]

Three 5H-indeno[1,2-c]pyridazin-5-one derivatives, potent type-B monoamine oxidase inhibitors

R. Frédérick, B. Norberg, F. Durant, F. Ooms and J. Wouters

Formula: C19H11F3N2O2, C19H11F3N2O2 and C16H13F3N2O2

Online 11 August 2004


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Acta Cryst. (2004). C60, o627-o629  [ doi:10.1107/S0108270104001428 ]

N-(3H-Thiazol-2-ylidene)nitramine and N-methyl-N-(thiazol-2-yl)nitramine

J. Zaleski, G. Spaleniak and J. B. Kyziol

Formula: C3H3N3O2S and C4H5N3O2S

Online 11 August 2004


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Acta Cryst. (2004). C60, o630-o632  [ doi:10.1107/S0108270104011989 ]

6[beta]-Azido-7[alpha]-hydroxy-17-oxo-5[alpha]-androstan-3[beta]-yl acetate

J. I. F. Paixão, J. A. R. Salvador, J. A. Paixão, A. Matos Beja, M. Ramos Silva and A. M. d'A. Rocha Gonsalves

Formula: C21H31N3O4

Online 11 August 2004


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Acta Cryst. (2004). C60, o633-o635  [ doi:10.1107/S0108270104015963 ]

The 1:1 adduct of hexamethylenetetramine (HMT) with racemic trans-1,2-cyclohexanedicarboxylic acid (CDA)

R. Venkatraman, P. C. Ray and F. R. Fronczek

Formula: C6H12N4·C8H12O4

Online 11 August 2004


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Acta Cryst. (2004). C60, o636-o638  [ doi:10.1107/S0108270104016014 ]

Two biologically active thiophene-3-carboxamide derivatives

Vasu, K. A. Nirmala, D. Chopra, S. Mohan and J. Saravanan

Formula: C24H24N2O2S and C24H24N2OS

Online 11 August 2004


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Acta Cryst. (2004). C60, o639-o641  [ doi:10.1107/S0108270104016518 ]

4',4',6',6'-Tetrachloro-3,4-dihydro-3-(6-methylpyridin-2-yl)spiro[1,3,2-benzoxazaphosphinine-2,2'-(2[lambda]5,4[lambda]5,6[lambda]5-cyclotriphosphazene)]

B. Tercan, T. Hökelek, H. Dal, Y. Süzen and Z. Kiliç

Formula: C13H12Cl4N5OP3

Online 11 August 2004


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Acta Cryst. (2004). C60, o642-o643  [ doi:10.1107/S0108270104016130 ]

Diethyl 3,8-dimethyl-4,7-diazadeca-2,8-dienedioate

Z.-M. Jin, L. Li, M.-C. Li, M.-L. Hu and L. Shen

Formula: C14H24N2O4

Online 11 August 2004


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Acta Cryst. (2004). C60, o644-o647  [ doi:10.1107/S0108270104016865 ]

Crystal engineering via C-H...F and C-H...[pi] interactions in two substituted indoles

A. R. Choudhury, K. Nagarajan and T. N. Guru Row

Formula: C20H18FN and C22H22FN

Online 11 August 2004


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Acta Cryst. (2004). C60, o648-o652  [ doi:10.1107/S0108270104016117 ]

1-[4-(Methylsulfonyl)phenyl]-5-phenyl-1H-pyrazole derivatives

C. Charlier, B. Norberg, L. Goossens, J.-P. Hénichart and F. Durant

Formula: C17H16N2O2S, C19H18N2O4S and C27H27N3O4S

Online 11 August 2004


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Acta Cryst. (2004). C60, o653-o655  [ doi:10.1107/S0108270104017007 ]

Secondary interactions in the isomorphous compounds 2,6-bis(chloromethyl)pyridinium chloride and 2,6-bis(bromomethyl)pyridinium bromide

V. Lozano and P. G. Jones

Formula: C7H8Cl2N+·Cl- and C7H8Br2N+·Br-

Online 11 August 2004


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Acta Cryst. (2004). C60, o656-o658  [ doi:10.1107/S0108270104015951 ]

Preference for the Diels-Alder addition of dienes syn to the O atom in cross-conjugated spirocyclic cyclohexadienones

J. C. Gallucci, Y. Tamura and L. A. Paquette

Formula: C27H20O3 and C28H22O3

Online 11 August 2004


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Acta Cryst. (2004). C60, o659-o661  [ doi:10.1107/S0108270104015847 ]

(Z)-2-(1-Phenylsulfonyl-1H-indol-3-ylmethylene)-1-azabicyclo[2.2.2]octan-3-one and (Z)-(S)-2-(1-phenylsulfonyl-1H-indol-3-ylmethylene)-1-azabicyclo[2.2.2]octan-3-ol

V. N. Sonar, S. Parkin and P. A. Crooks

Formula: C22H20N2O3S and C22H22N2O3S

Online 11 August 2004


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Acta Cryst. (2004). C60, o662-o664  [ doi:10.1107/S0108270104016749 ]

6-(4-Methoxybenzylamino)purin-3-ium chloride

Z. Trávnícek, I. Popa and K. Dolezal

Formula: C13H14N5O+·Cl-

Online 11 August 2004


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Acta Cryst. (2004). C60, o665-o667  [ doi:10.1107/S0108270104016737 ]

3,6-Bis(2-pyridyl)di-1,2,4-triazolo[3,4-a:4',3'-c]phthalazine

W.-F. Chang, Y.-S. Wen and L.-K. Liu

Formula: C20H12N8

Online 11 August 2004


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Acta Cryst. (2004). C60, o668-o670  [ doi:10.1107/S0108270104017792 ]

Desorption kinetics of a xanthenol-dioxane clathrate

A. Jacobs, L. R. Nassimbeni and B. Taljaard

Formula: C23H16O2·C4H8O2

Online 11 August 2004


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Acta Cryst. (2004). C60, o671-o673  [ doi:10.1107/S0108270104017457 ]

Structure-activity relationships in 4- and 5-androstene: 3[beta]-acetoxy-17-methyl-17-oxo-16,17-seco-5-androstene-16-carbonitrile and 17-methyl-3,17-dioxo-16,17-seco-4-androstene-16-carbonitrile

D. Lazar, O. Klisuric, S. Stankovic, K. Penov-Gasi, E. Djurendic and R. Kovacevic

Formula: C22H31NO3 and C20H27NO2

Online 11 August 2004


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Acta Cryst. (2004). C60, o674-o676  [ doi:10.1107/S0108270104018074 ]

1-Methyl-1-phenyl-3-[1-hydroxyimino-2-(succinimido)ethyl]cyclobutane

M. Dinçer, N. Özdemir, I Yilmaz, A. Çukurovali and O. Büyükgüngör

Formula: C17H20N2O3

Online 21 August 2004


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Acta Cryst. (2004). C60, o677-o679  [ doi:10.1107/S0108270104015604 ]

2-Amino-2-thiazoline and its 1:1 organic salt with 2-naphthoxyacetic acid

D. E. Lynch

Formula: C3H6N2S and C3H7N2S+·C12H9O3-

Online 21 August 2004


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Acta Cryst. (2004). C60, o680-o681  [ doi:10.1107/S0108270104015860 ]

Dimethyl 2-(4-bromophenyl)-10,11-dimethoxy-2,3,7,8-tetrahydrospiro[azepino[2,1-a]isoquinoline-3,9'-fluorene]-4,5-dicarboxylate

L. Feng, Z.-M. Li, Z.-X. Chen, Y.-S. Tan, L.-H. Weng and F.-G. Tao

Formula: C38H32BrNO6

Online 21 August 2004


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Acta Cryst. (2004). C60, o682-o685  [ doi:10.1107/S0108270104017342 ]

Orthorhombic and monoclinic polymorphs of 1,3,5-triphenylperhydro-1,3,5-triazine-2,4,6-trione at 120 K: chains and sheets formed by C-H...[pi](arene) hydrogen bonds

M. B. Mariyatra, K. Panchanatheswaran, J. N. Low and C. Glidewell

Formula: Two polymorphs of C21H15N3O3

Online 21 August 2004


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Acta Cryst. (2004). C60, o686-o689  [ doi:10.1107/S0108270104018323 ]

Hydrogen-bonded dimers in 2-nitrobenzaldehyde hydrazone and a three-dimensional hydrogen-bonded framework in 3-nitrobenzaldehyde hydrazone

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: Two isomers of C7H7N3O2

Online 21 August 2004


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Acta Cryst. (2004). C60, o690-o692  [ doi:10.1107/S0108270104018207 ]

1-Methylpiperazine-1,4-diium 4-nitrophthalate(2-) 4-nitrophthalic acid monohydrate

M.-L. Guo

Formula: C5H14N22+·C8H3NO62-·C8H5NO6·H2O

Online 21 August 2004


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Acta Cryst. (2004). C60, o693-o695  [ doi:10.1107/S0108270104017871 ]

C-H...[pi], [pi]-[pi] and C-H...Cl interactions in chloro-substituted Schiff bases and 4-chloro-N-[4-(dimethylamino)benzylidene]aniline

X.-L. You, C.-R. Lu, Y. Zhang and D.-C. Zhang

Formula: C15H15ClN2

Online 21 August 2004


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Acta Cryst. (2004). C60, o696-o698  [ doi:10.1107/S0108270104017883 ]

1-(4-Bromophenyl)-3-(4-methylphenyl)prop-2-en-1-one

L. Wang, Y. Zhang, C.-R. Lu and D.-C. Zhang

Formula: C16H13BrO

Online 21 August 2004


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Acta Cryst. (2004). C60, o699-o701  [ doi:10.1107/S0108270104018682 ]

Diethyl piperazine-1,4-diyldioxalate

F. J. Martínez-Martínez, R. E. Rojas-Pérez, E. V. García-Báez, H. Höpfl and I. I. Padilla-Martínez

Formula: C12H18N2O6

Online 31 August 2004


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Acta Cryst. (2004). C60, o702-o704  [ doi:10.1107/S0108270104017366 ]

N1-(4-tert-Butylphenyl)-N2-hydroxy-[alpha]-oxo-[alpha]-phenylacetamidine and N2-hydroxy-N1-(4-nitrophenyl)-[alpha]-oxo-[alpha]-phenylacetamidine hemihydrate

S. Soylu, M. Tas, H. Saraçoglu, H. Bati, N. Çaliskan and O. Büyükgüngör

Formula: C18H20N2O2 and C14H11N3O4·0.5H2O

Online 31 August 2004


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Acta Cryst. (2004). C60, o705-o708  [ doi:10.1107/S0108270104018736 ]

Two enamines derived from 1-n-alkyl-3-methylpyrazol-5-ones

J. Belmar, F. R. Pérez, Y. Moreno and R. Baggio

Formula: C19H27N3O and C30H52N6O2

Online 31 August 2004


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