Crystal Structure Communications

 

Acta Cryst. (2004). C60, i97-i100  [ doi:10.1107/S0108270104017986 ]

Calcium and strontium thiosulfate, CaS₂O₃·6H₂O and SrS₂O₃·5H₂O

P. Held and L. Bohatý

Synopsis: Triclinic CaS₂O₃·6H₂O is built up from [Ca(H₂O)₆(S₂O₃)] chains, parallel to [100], of alternating S₂O₃ and Ca(H₂O)₆O₂ groups sharing common O atoms. Monoclinic SrS₂O₃·5H₂O consists of [Sr(H₂O)₃O(S₂O₃)] layers of alternating S₂O₃ and Sr(H₂O)₄O₅ groups, parallel to (100), sharing O atoms and O-O edges.

Formula: CaS₂O₃·6H₂O and SrS₂O₃·5H₂O

Online 18 September 2004

 

Acta Cryst. (2004). C60, m467-m470  [ doi:10.1107/S0108270104017433 ]

Transition metal complexes with pyrazole-based ligands. XIX. Diaquabis(3,5-dimethyl-1H-pyrazole-1-carboxamidine-²N,N')metal(II) dinitrate, with metal = Co and Ni

Z. K. Jacimovic, V. Leovac, K. Mészáros Szécsényi, J. A. K. Howard and I. Radosavljevic Evans

Formula: [Co(C₆H₁₀N₄)₂(H₂O)₂](NO₃)₂ and [Ni(C₆H₁₀N₄)₂(H₂O)₂](NO₃)₂

Online 4 September 2004

 

Acta Cryst. (2004). C60, m471-m472  [ doi:10.1107/S0108270104019183 ]

catena-Poly[[(nitrato-²O,O')silver(I)]--2,2'-[1,4-phenylenebis(methylenethio)]bis(5-methyl-1,3,4-thiadiazole)-²N³:N^3']

Y. Zheng

Formula: [Ag(NO₃)(C₁₄H₁₄N₄S₄)]

Online 4 September 2004

 

Acta Cryst. (2004). C60, m473-m475  [ doi:10.1107/S0108270104019304 ]

Dicarbonyl(tropolonato)rhodium(I), a redetermination

G. Steyl, G. J. Kruger and A. Roodt

Formula: [Rh(C₇H₅O₂)(CO)₂]

Online 4 September 2004

 

Acta Cryst. (2004). C60, m476-m478  [ doi:10.1107/S0108270104019705 ]

1,4-Dimethylpyridinium hexakis(dimethylformamide-O)calcium(II) dodecamolybdophosphate

X.-J. Tan, S.-X. Sun, J.-P. Ma, L.-D. Liu, Y.-B. Dong, W.-T. Yu and D.-X. Xing

Formula: (C₇H₁₀N)[Ca(C₃H₇NO)₆][PMo₁₂O₄₀]

Online 4 September 2004

 

Acta Cryst. (2004). C60, m479-m481  [ doi:10.1107/S010827010401950X ]

Tetrakis(2,2'-bipyridine-²N,N')tetrakis(-salicylato-³O,O':O'')-quadro-tetrazinc(II) decahydrate

Y. Wang, M. Odoko and N. Okabe

Formula: [Zn₄(C₇H₄O₃)₄(C₁₀H₈N₂)₄]·10H₂O

Online 4 September 2004

 

Acta Cryst. (2004). C60, m482-m483  [ doi:10.1107/S010827010401933X ]

Dibromotetra-₃-methoxo-di-₂-methoxo-hexakis(tetrahydrofuran-d₈)tetramagnesium

B. Walfort, R. I. Yousef, T. Rüffer and D. Steinborn

Formula: [Mg₄Br₂(CH₃O)₆(C₄D₈O)₆]

Online 4 September 2004

 

Acta Cryst. (2004). C60, m484-m488  [ doi:10.1107/S0108270104019687 ]

Comparative study of two chemically isostructural polymers: [Cu₂(VO₂)(HPO₄)₂(NO₃)(bpy)₂]·2H₂O/H₃PO₄ (bpy is 2,2'-bipyridine)

Y. Moreno, A. Vega, E. Spodine, E. Ushak and R. Baggio

Formula: [Cu₂(VO₂)(HPO₄)₂(NO₃)(C₁₀H₈N₂)₂]·2H₂O/H₃PO₄

Online 4 September 2004

 

Acta Cryst. (2004). C60, m489-m491  [ doi:10.1107/S0108270104016956 ]

(2,2'-Bipyridyl-²N,N')bis(salicylato-²O,O')zinc(II)

P. Lemoine, K. Bendada and B. Viossat

Formula: [Zn(C₇H₅O₃)₂(C₁₀H₈N₂)]

Online 18 September 2004

 

Acta Cryst. (2004). C60, m492-m494  [ doi:10.1107/S0108270104019146 ]

The one-dimensional structure of Cu(dmen)₂Pd(CN)₄ (dmen is N,N-dimethylethylenediamine)

J. Kuchár, J. Cernák and K. A. Abboud

Formula: [CuPd(CN)₄(C₄H₁₂N₂)₂]

Online 18 September 2004

 

Acta Cryst. (2004). C60, m495-m497  [ doi:10.1107/S0108270104019638 ]

A new binding mode for thiosulfate in six-coordinate poly[[(1,10-phenanthroline-²N,N')cadmium(II)]--thiosulfato]

M. E. Díaz de Vivar, S. Baggio and R. Baggio

Formula: [Cd(S₂O₃)(C₁₂H₈N₂)]

Online 18 September 2004

 

Acta Cryst. (2004). C60, m498-m500  [ doi:10.1107/S0108270104019821 ]

Diaqua(sulfato-O)[2,4,6-tris(2-pyridyl)-1,3,5-triazine-³N¹,N²,N⁶]zinc(II) dihydrate

M. A. Harvey, S. Baggio and R. Baggio

Formula: [Zn(SO₄)(C₁₈H₁₂N₆)(H₂O)₂]·2H₂O

Online 18 September 2004

 

Acta Cryst. (2004). C60, m501-m503  [ doi:10.1107/S0108270104020050 ]

Poly[manganese(II)-₂-benzidine-²N:N'-₃-biphenyl-2,2'-dicarboxylato-⁴O:O',O'':O''']

M. Jiang, J. Li and F.-X. Zhang

Formula: [Mn(C₁₄H₈O₄)(C₁₂H₁₂N₂)]

Online 18 September 2004

 

Acta Cryst. (2004). C60, m504-m506  [ doi:10.1107/S0108270104020268 ]

Poly[diaqua-₄-oxalato-di-₆-phosphato-tetrazinc]

Y.-J. Zhong, Y.-Q. Sun and G.-Y. Yang

Formula: [Zn₄(C₂O₄)(PO₄)₂(H₂O)₂]

Online 18 September 2004

 

Acta Cryst. (2004). C60, m507-m508  [ doi:10.1107/S0108270104020293 ]

Bis[1,3-bis(trimethylsilyl)allyl]cobalt(II), a stable electron-deficient allyl complex

J. D. Smith, K. T. Quisenberry, T. P. Hanusa and W. W. Brennessel

Formula: [Co(C₉H₂₁Si₂)₂]

Online 18 September 2004

 

Acta Cryst. (2004). C60, m509-m511  [ doi:10.1107/S0108270104020426 ]

Poly[[copper(II)-di--5-aminoisophthalato(1-)-⁴N:O] monohydrate]

Q.-X. Liao, Z.-J. Li, J. Zhang, Y. Kang, Y.-M. Dai and Y.-G. Yao

Formula: [Cu(C₈H₆NO₄)₂]·H₂O

Online 25 September 2004

 

Acta Cryst. (2004). C60, m512-m514  [ doi:10.1107/S010827010402102X ]

[Cu(phen)₂(-IDA)Cu(phen)](ClO₄)₂·CH₃OH: tridentate and monodentate binding to two copper(II) species by a bridging ligand

Y.-B. Wei, C.-X. Yuan and P. Yang

Formula: [Cu₂(C₄H₅NO₄)(C₁₂H₈N₂)₃](ClO₄)₂·CH₄O

Online 25 September 2004

 

Acta Cryst. (2004). C60, m515-m516  [ doi:10.1107/S0108270104020839 ]

catena-Poly[[silver(I)--ethane-1,2-diamine-²N:N'] trifluoromethanesulfonate]

Z.-L. You and H.-L. Zhu

Formula: [Ag(C₂H₈N₂)](CF₃SO₃)

Online 25 September 2004

 

Acta Cryst. (2004). C60, m517-m519  [ doi:10.1107/S0108270104020785 ]

Bis(-2-aminopyridine)bis[(trifluoroacetato)silver(I)]

Z.-L. You and H.-L. Zhu

Formula: [Ag₂(C₂F₃O₂)₂(C₅H₆N₂)₂]

Online 25 September 2004

 

Acta Cryst. (2004). C60, m520-m522  [ doi:10.1107/S0108270104020657 ]

catena-Poly[[bis(quinoxaline-N)cobalt(II)]-di--dicyanamido-²N¹:N⁵] and catena-poly[[bis(quinoxaline-N)copper(II)]-di--dicyanamido-²N¹:N⁵]

J. Luo, B.-S. Liu, X.-G. Zhou, L.-H. Weng, Y.-R. Li and H.-X. Wu

Formula: [Co(C₂N₃)₂(C₈H₆N₂)₂] and [Cu(C₂N₃)₂(C₈H₆N₂)₂]

Online 25 September 2004

 

Acta Cryst. (2004). C60, m523-m525  [ doi:10.1107/S0108270104020840 ]

Aquadichloro(di-2-pyridyldiazene)copper(II) monohydrate

I. Uçar, F. Arslan, A. Bulut, H. Içbudak, H. Ölmez and O. Büyükgüngör

Formula: [CuCl₂(C₁₀H₈N₄)(H₂O)]·H₂O

Online 25 September 2004

 

Acta Cryst. (2004). C60, m526-m528  [ doi:10.1107/S0108270104020566 ]

Bis(1,10-phenanthroline-²N,N')(squarato-O)copper(II) trihydrate

A. Bulut, I. Uçar, O. Z. Yesilel, H. Içbudak, H. Ölmez and O. Büyükgüngör

Formula: [Cu(C₄O₄)(C₁₂H₈N₂)₂]·3H₂O

Online 25 September 2004

 

Acta Cryst. (2004). C60, m529-m531  [ doi:10.1107/S0108270104020499 ]

Polysulfonylamines. CLXXI. [Di(methanesulfonyl)amido-N]bis(2-picoline-N)copper(I)

P. G. Jones, E.-M. Zerbe and C. Wölper

Formula: [Cu(C₂H₆NO₄S₂)(C₆H₇N)₂]

Online 25 September 2004

 

Acta Cryst. (2004). C60, m532-m536  [ doi:10.1107/S0108270104020773 ]

(R,R)-Tricarbonyl{⁶-1-(diphenylphosphino)-2-[1-(diphenylphosphino)ethyl]benzene}chromium(0), (R,R)-tricarbonyl-1³C-{-1(⁶):2²P,P'-1-(diphenylphosphino)-2-[1-(diphenylphosphino)ethyl]benzene}[2(⁴)-norbornadiene]chromium(0)rhodium(I) tetrafluoroborate methanol 0.75-solvate and (R,R)-tricarbonyl-1³C-{-1(⁶):2²P,P'-1-(diphenylphosphino)-2-[1-(diphenylphosphino)ethyl]benzene}[2(⁴)-(Z,Z)-cycloocta-1,5-diene]chromium(0)rhodium(I) tetrafluoroborate methanol 1.5-solvate

W. Braun, B. Calmuschi, H.-J. Drexler, U. Englert, D. Heller and A. Salzer

Formula: [Cr(C₃₂H₂₈P₂)(CO)₃], [CrRh(C₇H₈)(C₃₂H₂₈P₂)(CO)₃]BF₄·0.75CH₄O and [CrRh(C₈H₁₂)(C₃₂H₂₈P₂)(CO)₃]BF₄·1.5CH₄O

Online 25 September 2004

 

Acta Cryst. (2004). C60, m537-m539  [ doi:10.1107/S0108270104021481 ]

A two-dimensional manganese(II) coordination polymer: poly[[diaquamanganese(II)]--4,4-bipyridine-²N:N'--(p-phenylenedioxydiacetato)-²O:O']

S. Gao, J.-W. Liu, L.-H. Huo, H. Zhao and J.-G. Zhao

Formula: [Mn(C₁₀H₈O₆)(C₁₀H₈N₂)(H₂O)₂]

Online 25 September 2004

 

Acta Cryst. (2004). C60, m540-m542  [ doi:10.1107/S0108270104021766 ]

Poly[[diaquacobalt(II)]-di--4-cyanobenzoato-⁴O:O']

H.-Y. He, J. Chen, X.-H. Wang and L.-G. Zhu

Formula: [Co(C₈H₄NO₂)₂(H₂O)₂]

Online 25 September 2004

 

Acta Cryst. (2004). C60, m543-m545  [ doi:10.1107/S0108270104021468 ]

Di--hydroxo-bis[aqua(1,10-phenanthroline-²N,N')copper(II)] trans-bis(2-{[(E)-5-formyl-2-oxido-O-benzylidene]amino-N}ethanesulfonato(2-))copper(II) hexahydrate

Y.-M. Jiang, J.-L. Zeng and K.-B. Yu

Formula: [Cu₂(OH)₂(C₁₂H₈N₂)₂(H₂O)₂][Cu(C₁₀H₉NO₅S)₂].6H₂O

Online 25 September 2004

 

Acta Cryst. (2004). C60, m546-m548  [ doi:10.1107/S0108270104021456 ]

A novel one-dimensional zigzag coordination polymer of copper(II) with dimethylglyoxime

B. Zhang, X. Liu, X. Wang, R. Wang, C. Xie, G. Shen and D. Shen

Formula: [Cu₄(C₂H₆N₂O₂)₂(C₂H₇N₂O₂)₂(C₂H₈N₂O₂)₂](ClO₄)₂·2H₂O

Online 30 September 2004

 

Acta Cryst. (2004). C60, o709-o710  [ doi:10.1107/S0108270104019067 ]

3,3-Bis(2-methoxyphenyl)-3H-benzo[f]chromene

H.-M. Huang, Y. Ding, P.-L. Chen and J.-B. Meng

Formula: C₂₇H₂₂O₃

Online 4 September 2004

 

Acta Cryst. (2004). C60, o711-o713  [ doi:10.1107/S0108270104019468 ]

Methyl 4-(2-chloro-5-nitrophenyl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

A. Linden, C. Safak and F. Aydin

Formula: C₂₀H₂₁ClN₂O₅

Online 4 September 2004

 

Acta Cryst. (2004). C60, o714-o717  [ doi:10.1107/S0108270104017706 ]

Hydantoin and hydrogen-bonding patterns in hydantoin derivatives

F.-L. Yu, C. H. Schwalbe and D. J. Watkin

Formula: C₃H₄N₂O₂

Online 4 September 2004

 

Acta Cryst. (2004). C60, o718-o722  [ doi:10.1107/S0108270104019201 ]

2-Pyridone-tartronic acid (1/1), 3-hydroxypyridinium hydrogen tartronate and 4-hydroxypyridinium hydrogen tartronate

T. Fukunaga, S. Kashino and H. Ishida

Formula: C₅H₅NO·C₃H₄O₅ and two isomers of C₅H₆NO⁺·C₃H₃O₅^-

Online 4 September 2004

 

Acta Cryst. (2004). C60, o723-o726  [ doi:10.1107/S0108270104017743 ]

The E and Z isomers of 3-(benzoxazol-2-yl)prop-2-enoic acid

J. G. Trujillo-Ferrara, I. I. Padilla-Martínez, F. J. Martínez-Martínez, H. Höpfl, N. Farfan-García and E. V. García-Báez

Formula: Two isomers of C₁₀H₇NO₃

Online 4 September 2004

 

Acta Cryst. (2004). C60, o727-o729  [ doi:10.1107/S010827010401947X ]

(+)-Camphoracetic acid: catemeric hydrogen bonding in a -keto acid

H. W. Thompson, M. L. Coté and R. A. Lalancette

Formula: C₁₂H₁₈O₃

Online 4 September 2004

 

Acta Cryst. (2004). C60, o730-o732  [ doi:10.1107/S0108270104019195 ]

1H-Imidazol-1-yl 1,2,3,4-tetrahydroisoquinolin-2-yl ketone

J. A. Grzyb, A. J. Lough and R. A. Batey

Formula: C₁₃H₁₃N₃O

Online 18 September 2004

 

Acta Cryst. (2004). C60, o733-o736  [ doi:10.1107/S0108270104020256 ]

Hydrogen-bonded chains in 5-methyl-2-trifluoromethyl-1,2,4-triazolo[1,5-a]pyrimidin-7(4H)-one and hydrogen-bonded chains of rings in 5-amino-3-trifluoromethyl-1H-1,2,4-triazole-5-methyl-2-trifluoromethyl-1,2,4-triazolo[1,5-a]pyrimidin-7(4H)-one (1/1), the co-crystal of a reaction product and one of its precursors

N. Boechat, K. D. B. Dutra, A. L. Valverde, S. M. S. V. Wardell, J. N. Low and C. Glidewell

Formula: C₇H₅F₃N₄O and C₃H₃F₃N₄·C₇H₅F₃N₄O

Online 18 September 2004

 

Acta Cryst. (2004). C60, o737-o739  [ doi:10.1107/S0108270104019730 ]

6-(3,4-Difluorobenzoyl)-3-[2-(4-pyridyl)ethyl]-1,3-benzothiazol-2(3H)-one

S. Özbey and N. Gökhan

Formula: C₂₁H₁₄F₂N₂O₂S

Online 18 September 2004

 

Acta Cryst. (2004). C60, o740-o743  [ doi:10.1107/S010827010401786X ]

Two N,N-dimethylbiguanidium salts displaying double hydrogen bonds to the counter-ions

L.-P. Lu, H.-M. Zhang, S.-S. Feng and M.-L. Zhu

Formula: C₄H₁₃N₅²⁺·C₂O₄^2-·H₂O and C₄H₁₃N₅²⁺·SO₄^2-·H₂O

Online 18 September 2004

 

Acta Cryst. (2004). C60, o744-o750  [ doi:10.1107/S0108270104020414 ]

Polarized molecular-electronic structures and supramolecular aggregation in 1-(6-amino-1,3-benzodioxol-5-yl)-3-arylprop-2-en-1-ones

J. N. Low, J. Cobo, M. Nogueras, P. Cuervo, R. Abonia and C. Glidewell

Formula: C₁₇H₁₅NO₃, two polymorphs of C₁₇H₁₅NO₄, and C₁₇H₁₂F₃NO₃

Online 18 September 2004

 

Acta Cryst. (2004). C60, o751-o753  [ doi:10.1107/S0108270104018190 ]

1-Chloro-1,3,3,5,5-pentaphenoxycyclotriphosphazene: a precursor of functionalized cyclophosphazene derivatives

J. Sopková-de Oliveira Santos, D. Bauchart, C. Besset and I. Dez

Formula: C₃₀H₂₅ClN₃O₅P₃

Online 25 September 2004

 

Acta Cryst. (2004). C60, o754-o756  [ doi:10.1107/S0108270104020141 ]

The twinned crystal structure of rac-(R,R)-N,N'-oxalyldivalinol

Z. Stefanic, A. Meden, M. Lutz, A. M. M. Schreurs and B. Kojic-Prodic

Formula: C₁₂H₂₄N₂O₄

Online 25 September 2004

 

Acta Cryst. (2004). C60, o757-o758  [ doi:10.1107/S0108270104018852 ]

2-[6-(3-Chlorophenyl)-2,4-dioxoperhydropyrimidin-3-yl]ethyl morpholine-4-carbodithioate

Y. Köysal, S. Isik, E. Septioglu and Ü. Çalis

Formula: C₁₇H₂₀ClN₃O₃S₂

Online 25 September 2004

 

Acta Cryst. (2004). C60, o759-o761  [ doi:10.1107/S0108270104020943 ]

Hydrogen-bonding patterns in cis-4-ammoniocyclohexanecarboxylate hemihydrate

E. E. Ávila, A. J. Mora, G. E. Delgado, B. M. Ramírez, A. Bahsas and S. Koteich

Formula: C₇H₁₃NO₂·0.5H₂O

Online 25 September 2004

 

Acta Cryst. (2004). C60, o762-o764  [ doi:10.1107/S0108270104020712 ]

(±)-(4-Oxo-4H-chromen-2-yl)(phenyl)methyl acetate

M. Malecka, W. Massa and E. Budzisz

Formula: C₁₈H₁₄O₄

Online 25 September 2004

 

Acta Cryst. (2004). C60, o765-o767  [ doi:10.1107/S0108270104021936 ]

The 1:1 adduct of 5-methylbenzene-1,3-diol (orcin) and 1,4-diazabicyclo[2.2.2]octane

Z.-M. Jin, C.-S. Lin, H.-B. Wang, M.-L. Hu, L. Shen and L.-R. Huang

Formula: C₆H₁₂N₂·C₇H₈O₂

Online 30 September 2004

 

Acta Cryst. (2004). C60, o768-o770  [ doi:10.1107/S0108270104021122 ]

4-Nitroanilinium nitrate

G. J. Perpétuo and J. Janczak

Formula: C₆H₇N₂O₂⁺·NO₃^-

Online 30 September 2004

 

Acta Cryst. (2004). C60, o771-o772  [ doi:10.1107/S0108270104021523 ]

L-Seryl-L-phenylalanine

I. H. Helle, C. V. Løkken, C. H. Görbitz and B. Dalhus

Formula: C₁₂H₁₆N₂O₄

Online 30 September 2004