Crystal Structure Communications

 

Acta Cryst. (2004). C60, i113-i116  [ doi:10.1107/S0108270104026368 ]

K₂[HCr₂AsO₁₀]: redetermination of phase II and the predicted structure of phase I

T. J. R. Weakley, E. R. Ylvisaker, R. J. Yager, P. Wu, P. Photinos and S. C. Abrahams

Synopsis: In the structure of K₂[HCr₂AsO₁₀], hydrogen bonds of 2.555  (5)  Å between terminal O atoms of shared AsO₃OH tetrahedra connect HCr₂AsO₁₀^2- ions. The displacement of the hydrogen-bonded O atoms by 0.586  Å in the predicted transition between phases II and I is larger than that of any other atom.

Formula: Two crystals phases of K₂[HCr₂AsO₁₀]

Online 11 November 2004

 

Acta Cryst. (2004). C60, i117-i119  [ doi:10.1107/S0108270104024205 ]

High-pressure synthesis of -DyBO₃

H. Emme and H. Huppertz

Synopsis: The title compound was obtained by the reaction of Dy₂O₃ and B₂O₃ under conditions of high temperature and pressure (3  GPa and 1323  K) using a Walker-type multi-anvil assembly. Its crystal structure has been determined by single-crystal X-ray diffraction.

Formula: DyBO₃

Online 23 November 2004

 

Acta Cryst. (2004). C60, i120-i122  [ doi:10.1107/S0108270104025144 ]

GdAlO₃ perovskite

D. du Boulay, N. Ishizawa and E. N. Maslen

Synopsis: A single-crystal synchrotron X-ray study of gadolinium aluminate, GdAlO₃, revealed a perovskite-type structure with a common orthorhombic Pnma distortion, which has been discussed in association with the characteristic short Gd-Al-Gd linkage.

Formula: GdAlO₃

Online 23 November 2004

 

Acta Cryst. (2004). C60, m601-m604  [ doi:10.1107/S0108270104018244 ]

Low-dimensional compounds containing cyano groups. X. (Dicyanamido-N¹)bis(1,10-phenanthroline-²N,N')copper(II) perchlorate

M. Burcák, I. Potocnák, P. Baran and L. Jäger

Formula: [Cu(C₂N₃)(C₁₂H₈N₂)₂]ClO₄

Online 11 November 2004

 

Acta Cryst. (2004). C60, m605-m608  [ doi:10.1107/S0108270104026502 ]

catena-Poly[[(di-2-pyridylamine)silver(I)]--nicotinato] and catena-poly[[(di-2-pyridylamine)silver(I)]--2,6-dihydroxybenzoato]

Y. Wang and N. Okabe

Formula: [Ag(C₆H₄NO₂)(C₁₀H₉N₃)] and [Ag(C₇H₅O₄)(C₁₀H₉N₃)]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m609-m611  [ doi:10.1107/S0108270104024783 ]

trans-Diaquabis(5-carboxy-1H-imidazole-4-carboxylato-²N³,O⁴)cobalt(II) 4,4'-bipyridine solvate

Y.-L. Wang, R. Cao and W.-H. Bi

Formula: [Co(C₅H₃N₂O₄)₂(H₂O)₂]·C₁₀H₈N₂

Online 11 November 2004

 

Acta Cryst. (2004). C60, m612-m614  [ doi:10.1107/S0108270104025648 ]

Bis(ethylenediammonium) decaaquadisodium decavanadate, (C₂H₁₀N₂)₂[Na₂(H₂O)₁₀][V₁₀O₂₈]

G.-B. Li, S.-H. Yang, M. Xiong and J.-H. Lin

Synopsis: In the title compound, the decavanadate anions are surrounded by [Na₂(H₂O)₁₀]²⁺ dications, forming layers, and diethylenediammonium cations are located between these layers.

Formula: (C₂H₁₀N₂)₂[Na₂(H₂O)₁₀][V₁₀O₂₈]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m615-m617  [ doi:10.1107/S0108270104025958 ]

(⁶-Biphenyl)tricarbonylchromium and -(⁶:⁶)-biphenyl-bis(tricarbonylchromium)

I. A. Guzei and C. J. Czerwinski

Formula: [Cr(C₁₂H₁₀)(CO)₃] and [Cr₂(C₁₂H₁₀)(CO)₆]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m618-m619  [ doi:10.1107/S0108270104026332 ]

4,4'-Thiodipyridinium tetrachlorocopper(II)

Y.-H. Wen, J.-K. Cheng, J. Zhang, Z.-J. Li and Y.-G. Yao

Formula: (C₁₀H₁₀N₂S)[CuCl₄]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m620-m622  [ doi:10.1107/S0108270104025089 ]

catena-Poly[[[-pyrazine-²N:N'-disilver(I)]-di--pyrazine-⁴N:N'] bis(trifluoromethanesulfonate) dihydrate]

Z.-L. You, H.-L. Zhu and W.-S. Liu

Formula: [Ag₂(C₄H₄N₂)₃](CF₃O₃S)₂·2H₂O

Online 11 November 2004

 

Acta Cryst. (2004). C60, m623-m624  [ doi:10.1107/S0108270104024424 ]

catena-Poly[[(benzoato-O)silver(I)]--2-aminopyrimidine-²N¹:N³]

Z.-L. You and H.-L. Zhu

Formula: [Ag(C₇H₅O₂)(C₄H₅N₃)]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m625-m627  [ doi:10.1107/S0108270104026344 ]

Dichlorobis(cumylcyclopentadienyl)titanium(IV)

R. Centore, Z. Csok and A. Tuzi

Formula: [Ti(C₁₄H₁₅)₂Cl₂]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m628-m630  [ doi:10.1107/S0108270104026459 ]

The copper(II) complexes di--bromo-bis{[2,6-bis(pyrazol-1-yl)pyridine]perchloratocopper(II)} and [2,6-bis(pyrazol-1-yl)pyridine]dibromocopper(II)

S. Chakrabarty, R. K. Poddar, R. D. Poulsen, A. L. Thompson and J. A. K. Howard

Formula: [Cu₂Br₂(ClO₄)₂(C₁₁H₉N₅)₂] and [CuBr₂(C₁₁H₉N₅)]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m631-m633  [ doi:10.1107/S0108270104025776 ]

Poly[methylammonium tris(₂-formato-²O:O')cobalt(II)]

M. Boca, I. Svoboda, F. Renz and H. Fuess

Formula: (CH₆N)[Co(CHO₂)₃]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m634-m636  [ doi:10.1107/S0108270104024862 ]

Butane-1,4-diamine zinc(II) hydrogen phosphite

L. K. Ritchie and W. T. A. Harrison

Formula: (C₄H₁₂N₂)_0.5[ZnHPO₃]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m637-m639  [ doi:10.1107/S0108270104027039 ]

-[H₂N(CH₂)₂NH₂]_0.5[ZnHPO₃], a second modification of ethylenediamine zinc hydrogen phosphite

L. E. Gordon and W. T. A. Harrison

Formula: [Zn₂(HPO₃)₂(C₂H₈N₂)]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m640-m642  [ doi:10.1107/S0108270104026575 ]

Bis[(R)-3,5-dichloro-N-(1-phenylethyl)salicylideneaminato-²N,O]copper(II) and bis[(R)-3-ethoxy-N-(1-phenylethyl)salicylideneaminato-²N,O]copper(II)

T. Akitsu and Y. Einaga

Formula: [Cu(C₁₅H₁₂Cl₂NO)₂] and [Cu(C₁₇H₁₈NO₂)₂]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m643-m644  [ doi:10.1107/S0108270104027040 ]

Bis(tetra-n-butylammonium) (-N,N'-diselenium dinitride)bis[tribromopalladate(II)]

S. M. Aucott, S. H. Dale, M. R. J. Elsegood, K. E. Holmes, S. L. M. James and P. F. Kelly

Formula: (C₁₆H₃₆N)₂[Pd₂Br₆(N₂Se₂)]

Online 11 November 2004

 

Acta Cryst. (2004). C60, m645-m647  [ doi:10.1107/S0108270104027052 ]

Sodium 1-carboxycyclopropane-1-carboxylate cyclopropane-1,1-dicarboxylic acid monohydrate

K. W. Muir, A. MacDonald and A. MacDonald

Formula: Na⁺·C₅H₅O₄^-·C₅H₆O₄·H₂O

Online 11 November 2004

 

Acta Cryst. (2004). C60, m648-m650  [ doi:10.1107/S0108270104027192 ]

Ethyltriphenylphosphonium perrhenate and (iodomethyl)triphenylphosphonium perrhenate

M. Holynska and T. Lis

Formula: (C₂₀H₂₀P)[ReO₄] and (C₁₉H₁₇IP)[ReO₄]

Online 23 November 2004

 

Acta Cryst. (2004). C60, m651-m653  [ doi:10.1107/S0108270104026757 ]

catena-Poly[[(pyridin-4-ol-N)silver(I)]--pyridin-4-olato-²N:O]

S. Gao, Z.-Z. Lu, L.-H. Huo and H. Zhao

Formula: [Ag(C₅H₄NO)(C₅H₅NO)]

Online 23 November 2004

 

Acta Cryst. (2004). C60, m654-m656  [ doi:10.1107/S0108270104027660 ]

Poly[[bis(pyridine-N)copper(II)]-₃-5-hydroxyisophthalato-³O:O':O'']

X.-Y. Cao, J. Zhang, Y. Kang, J.-K. Cheng and Y.-G. Yao

Formula: [Cu(C₈H₄O₅)(C₅H₅N)₂]

Online 23 November 2004

 

Acta Cryst. (2004). C60, m657-m658  [ doi:10.1107/S0108270104022280 ]

Poly[aquaneodymium(III)-₅-2-oxido-5-sulfonatobenzoato]

X.-Q. Wang, J. Zhang, Z.-J. Li, Y.-H. Wen, J.-K. Cheng and Y.-G. Yao

Formula: [Nd(C₇H₃O₆S)(H₂O)]

Online 23 November 2004

 

Acta Cryst. (2004). C60, m659-m660  [ doi:10.1107/S0108270104023832 ]

The first di--hydroxo-bridged binuclear copper complex containing a bis-guanidine ligand

S. Herres, U. Flörke and G. Henkel

Formula: [Cu₂(OH)₂(C₂₅H₄₆N₆)₂](PF₆)₂

Online 23 November 2004

 

Acta Cryst. (2004). C60, m661-m662  [ doi:10.1107/S0108270104028215 ]

Chlorobis[N-ethoxycarbonyl-N'-(p-methoxyphenyl)thiourea-S]copper(I)

B.-Q. Su, L. Xian, H.-B. Song and L. Sheng

Formula: [CuCl(C₁₁H₁₄N₂O₃S)₂]

Online 30 November 2004

 

Acta Cryst. (2004). C60, o843-o846  [ doi:10.1107/S0108270104024771 ]

Solvates of zafirlukast

D. Goldring, M. Botoshansky, R. L. Khalfin, B. Pertsikov, G. Nisnevitch, V. Ponomarev, I. Zaltzman, A. Gutman and M. Kaftory

Formula: C₃₁H₃₃N₃O₆S·H₂O, C₃₁H₃₃N₃O₆S·CH₄O and C₃₁H₃₃N₃O₆S·C₂H₆O

Online 11 November 2004

 

Acta Cryst. (2004). C60, o847-o849  [ doi:10.1107/S0108270104024709 ]

Butane-1,4-diyl bis(chloroacetate)

L. Urpí, M. Martínez-Palau, M. Font-Bardia and J. Puiggalí

Formula: C₈H₁₂Cl₂O₄

Online 11 November 2004

 

Acta Cryst. (2004). C60, o850-o852  [ doi:10.1107/S0108270104025077 ]

4,4'-Bis(N,N-diethylamino)-2,2'-bipyridine

P. Alborés, L. M. Baraldo, A. Ibañez and R. Baggio

Formula: C₁₈H₂₆N₄

Online 11 November 2004

 

Acta Cryst. (2004). C60, o853-o855  [ doi:10.1107/S0108270104024874 ]

Brucine and two solvates

A. Bialonska and Z. Ciunik

Formula: C₂₃H₂₆N₂O₄, C₂₃H₂₆N₂O₄·C₃H₆O and C₂₃H₂₆N₂O₄·C₃H₈O·2H₂O

Online 11 November 2004

 

Acta Cryst. (2004). C60, o856-o858  [ doi:10.1107/S0108270104025235 ]

Di-2-pyridyl ketone 4-methyl-4-phenylthiosemicarbazone

V. Philip, V. Suni and M. R. P. Kurup

Formula: C₁₉H₁₇N₅S

Online 11 November 2004

 

Acta Cryst. (2004). C60, o859-o861  [ doi:10.1107/S0108270104026356 ]

Self-inclusion in 5,11,17,23-tetra-tert-butyl-26,27,28-trihydroxy-25-(methoxycarbonylmethoxy)calix[4]arene chloroform trisolvate

A. Ben Othman, N. Cheriaa, R. Abidi, J. Vicens and P. Thuéry

Formula: C₄₇H₆₀O₆·3CHCl₃

Online 11 November 2004

 

Acta Cryst. (2004). C60, o862-o864  [ doi:10.1107/S0108270104026587 ]

The first bipodal thiocarbamic acid ester, O,O'-diethyl N,N'-(p-phenylenedicarbonyl)bis(thiocarbamate)

G. Blewett, C. Esterhuysen, M. W. Bredenkamp and K. R. Koch

Formula: C₁₄H₁₆N₂O₄S₂

Online 11 November 2004

 

Acta Cryst. (2004). C60, o865-o867  [ doi:10.1107/S0108270104025636 ]

Quinoline-2(1H)-thione, a structure with Z' = 8

P. Kus and P. G. Jones

Formula: C₉H₇NS

Online 11 November 2004

 

Acta Cryst. (2004). C60, o868-o871  [ doi:10.1107/S0108270104025223 ]

L-Methioninium chloride and L-selenomethioninium chloride at 103 K

M. Chruszcz, M. Cymborowski, A. Gawlicka-Chruszcz, S. Yasukawa, J. D. Ferrara and W. Minor

Formula: C₅H₁₂NO₂S⁺·Cl^- and C₅H₁₂NO₂Se⁺·Cl^-

Online 11 November 2004

 

Acta Cryst. (2004). C60, o872-o875  [ doi:10.1107/S0108270104026137 ]

Isomeric nitrophthalimides: sheets built from N-HO and C-HO hydrogen bonds

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: Two isomers of C₈H₄N₂O₄

Online 11 November 2004

 

Acta Cryst. (2004). C60, o876-o878  [ doi:10.1107/S0108270104024977 ]

Secondary interactions in 3-bromopyridinium tribromoacetate

P. G. Jones and V. Lozano

Formula: C₅H₅BrN⁺·C₂Br₃O₂^-

Online 11 November 2004

 

Acta Cryst. (2004). C60, o879-o883  [ doi:10.1107/S0108270104022231 ]

Four bromo-substituted pyrazoline and isoxazolinone spiro derivatives

G. Bruno, F. Nicoló, A. Rotondo, F. Foti, F. Risitano and G. Grassi

Formula: C₂₄H₁₈BrN₃O₂, C₂₄H₁₈BrN₃O₃, C₂₉H₂₀BrClN₄O and C₃₀H_22.89Br_1.11N₄O

Online 11 November 2004

 

Acta Cryst. (2004). C60, o884-o886  [ doi:10.1107/S0108270104023649 ]

6-Aza-2'-deoxy-2'-arabinofluorouridine, a 2'-deoxyribonucleoside with an N-sugar conformation in the solid state and in solution

F. Seela, P. Chittepu, J. He and H. Eickmeier

Formula: C₈H₁₀FN₃O₅

Online 11 November 2004

 

Acta Cryst. (2004). C60, o887-o889  [ doi:10.1107/S0108270104023789 ]

Imino Diels-Alder adducts. I. Two furo[3,2-c]quinoline diastereoisomers

K. Ravikumar, M. Mahesh and V. V. Narayana Reddy

Formula: Two diastereoisomers of C₁₇H₁₅ClFNO

Online 23 November 2004

 

Acta Cryst. (2004). C60, o890-o892  [ doi:10.1107/S0108270104026708 ]

11-Methyl-2,3-benzodipyrrin-1-one

R. Bonnett, M. Motevalli, F. J. Swanson and M. A. Vallés

Formula: C₁₄H₁₂N₂O

Online 23 November 2004

 

Acta Cryst. (2004). C60, o893-o896  [ doi:10.1107/S0108270104028355 ]

Swertisin dihydrate

S. Ohba, K. Yoshida and T. Kondo

Formula: C₂₂H₂₂O₁₀·2H₂O

Online 30 November 2004

 

Acta Cryst. (2004). C60, o897-o899  [ doi:10.1107/S0108270104027027 ]

X-ray investigations of bicyclic -methylene--valerolactones. II. (4aS,8aS)-4a-Methyl-3-methyleneperhydrochromen-2-one

H. Krawczyk, M. Sliwinski and W. M. Wolf

Formula: C₁₁H₁₆O₂

Online 30 November 2004

 

Acta Cryst. (2004). C60, o900-o902  [ doi:10.1107/S0108270104023777 ]

A pimpinellin monomer and dimer isolated from the roots of Esenbeckia grandiflora

P. E. S. de Oliveira, L. M. Conserva, C. A. De Simone, M. A. Pereira, V. R. S. Malta and D. O. Imbroisi

Formula: C₁₃H₁₀O₅ and C₂₆H₂₀O₁₀

Online 30 November 2004