# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # #data_040513g data_I _shelx_title ' 040513G in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 421.34 _exptl_crystal_F_000 1492.00 _reflns_d_resolution_high 0.8406 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.7598 _cell_length_b 13.3458 _cell_length_c 19.7580 _cell_angle_alpha 91.619 _cell_angle_beta 97.925 _cell_angle_gamma 106.440 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 18841.66 -11.94 11.94 o 2 0 0 10260.58 10937.10 236.87 o 3 0 0 32444.41 35017.89 683.26 o 4 0 0 21514.27 23695.19 502.94 o 5 0 0 696.60 634.23 79.69 o 6 0 0 924.49 671.69 94.57 o 7 0 0 6103.00 6162.37 230.63 o 8 0 0 1603.27 1567.77 137.17 o 9 0 0 17627.09 17214.63 628.91 o 10 0 0 6134.35 6521.95 211.23 o 11 0 0 1029.31 867.22 249.91 o 12 0 0 3444.57 3521.24 183.71 o 13 0 0 531.22 557.29 201.25 o 14 0 0 19.12 219.06 201.62 o -14 1 0 20.09 59.37 160.13 o -13 1 0 1204.99 1150.76 204.92 o -12 1 0 6466.96 6613.28 233.61 o -11 1 0 458.60 435.37 137.17 o -10 1 0 9166.64 9885.13 355.68 o -9 1 0 28131.13 28028.67 679.77 o -8 1 0 1201.73 890.20 115.50 o -7 1 0 2509.87 2681.07 150.57 o -6 1 0 1399.42 1608.90 110.36 o -5 1 0 1067.89 1200.89 93.28 o -4 1 0 1231.21 1405.26 84.10 o -3 1 0 16409.59 18179.90 380.65 o -2 1 0 32493.94 36313.16 692.26 o 0 1 0 177531.55 -29.75 19.83 o 1 1 0 10888.11 10988.15 238.34 o 2 1 0 3707.43 4099.48 234.39 o 3 1 0 3310.01 3581.09 96.15 o 4 1 0 2766.57 3295.68 99.06 o 5 1 0 3294.06 3380.52 207.13 o 6 1 0 20129.97 22500.21 385.59 o 7 1 0 9080.94 9032.53 216.61 o 8 1 0 2118.30 1833.15 115.13 o 9 1 0 12205.03 12781.73 297.54 o 10 1 0 3561.95 3458.64 210.25 o 11 1 0 54.46 246.56 119.35 o 12 1 0 740.01 925.82 178.30 o 13 1 0 133.84 624.68 199.78 o 14 1 0 10.36 577.68 224.39 o -14 2 0 28.49 302.98 242.75 o -13 2 0 2314.67 3136.82 286.27 o -11 2 0 657.07 716.68 135.88 o -10 2 0 10142.87 10713.81 366.33 o -9 2 0 20348.54 21520.73 555.46 o -8 2 0 714.11 638.09 113.11 o -7 2 0 411.13 370.55 85.02 o -6 2 0 5192.59 5357.92 191.52 o -5 2 0 18.21 -7.34 67.76 o -4 2 0 2868.62 3269.21 135.51 o -3 2 0 16063.38 15192.18 346.13 o -2 2 0 16249.38 16576.14 358.98 o -1 2 0 20598.05 20884.66 435.19 o 0 2 0 61959.37 59840.07 2083.56 o 1 2 0 65.09 -21.17 37.92 o 2 2 0 4539.82 4927.16 184.82 o 3 2 0 1.26 35.47 71.34 o 4 2 0 2169.09 2324.18 126.24 o 5 2 0 1147.36 1222.04 82.61 o 6 2 0 39481.20 40705.70 1062.35 o 7 2 0 9983.38 10165.82 250.64 o 8 2 0 1296.65 1172.59 179.31 o 9 2 0 8281.72 8181.71 239.37 o 10 2 0 4359.92 4271.17 188.78 o 11 2 0 61.18 104.74 128.28 o 12 2 0 158.35 178.48 180.50 o 13 2 0 48.43 -24.79 187.48 o -14 3 0 36.50 297.65 217.78 o -13 3 0 1914.67 1713.93 232.47 o -12 3 0 9886.11 9940.76 421.60 o -11 3 0 1546.23 1436.66 186.19 o -10 3 0 5278.85 5459.64 276.17 o -9 3 0 10966.62 11594.28 389.65 o -8 3 0 363.62 449.51 119.17 o -7 3 0 721.14 607.42 109.99 o -6 3 0 3948.10 3831.46 178.85 o -5 3 0 133.44 131.47 76.02 o -4 3 0 9078.61 9319.94 265.33 o -3 3 0 68948.01 72265.88 1376.25 o -2 3 0 27358.42 27167.48 576.02 o -1 3 0 29865.64 28872.79 614.77 o 0 3 0 3222.54 3012.13 108.45 o 1 3 0 4559.70 5238.56 214.10 o 2 3 0 806.80 803.32 70.72 o 3 3 0 3122.30 3667.60 121.93 o 4 3 0 24410.84 28007.54 460.72 o 5 3 0 114.62 165.07 70.96 o 6 3 0 18916.25 18584.99 360.51 o 7 3 0 6727.30 6623.05 202.12 o 8 3 0 162.05 158.69 96.87 o 9 3 0 6892.27 7114.48 411.77 o 10 3 0 1359.58 1456.55 144.80 o 11 3 0 2.71 295.44 214.84 o 12 3 0 191.50 327.03 193.72 o 13 3 0 388.15 334.38 204.92 o -15 4 0 1056.62 1272.00 221.11 o -14 4 0 135.60 -72.53 210.80 o -13 4 0 2766.12 3186.40 278.37 o -11 4 0 167.80 -92.36 150.39 o -10 4 0 3609.77 3506.09 232.83 o -9 4 0 3239.10 3192.09 208.78 o -8 4 0 857.68 542.05 135.15 o -7 4 0 3629.18 3953.76 200.70 o -6 4 0 6862.86 6615.91 246.42 o -5 4 0 6618.93 6184.03 226.96 o -4 4 0 31131.74 31292.74 679.59 o -3 4 0 36139.79 34610.98 738.16 o -1 4 0 8567.26 7961.50 266.80 o 0 4 0 117.14 126.58 67.69 o 1 4 0 576.36 801.23 83.14 o 2 4 0 157.78 183.03 71.45 o 3 4 0 32550.89 36132.07 582.21 o 4 4 0 5363.40 5951.17 275.98 o 5 4 0 503.28 500.81 148.09 o 6 4 0 12614.94 12615.39 528.65 o 7 4 0 5134.13 6000.69 206.42 o 8 4 0 3138.85 2779.92 182.98 o 9 4 0 3264.05 3576.28 186.16 o 10 4 0 215.85 263.14 221.54 o 11 4 0 41.11 -39.69 141.09 o 12 4 0 415.81 814.73 225.67 o -15 5 0 1506.79 2291.42 311.24 o -14 5 0 514.68 199.23 211.90 o -13 5 0 4000.35 3850.38 307.20 o -12 5 0 6506.72 6494.72 349.43 o -11 5 0 160.83 5.14 164.16 o -10 5 0 1244.36 1091.45 165.44 o -9 5 0 249.27 -93.65 125.78 o -8 5 0 138.75 57.11 116.05 o -7 5 0 6614.87 6710.85 269.37 o -6 5 0 15491.27 14050.60 403.60 o -5 5 0 4313.72 4435.03 205.29 o -4 5 0 12205.44 10763.21 329.79 o -3 5 0 46661.43 45229.87 959.98 o -2 5 0 4370.85 4554.57 215.57 o -1 5 0 2015.34 2304.83 157.92 o 0 5 0 1944.70 1784.92 85.92 o 1 5 0 111.80 320.85 179.31 o 2 5 0 7367.65 8252.78 308.03 o 3 5 0 26217.06 26112.04 473.98 o 4 5 0 5423.75 5511.11 515.06 o 5 5 0 4483.25 4495.93 178.28 o 6 5 0 10946.60 10871.04 284.58 o 7 5 0 1969.33 1777.05 148.98 o 8 5 0 1205.21 1294.30 173.52 o 9 5 0 2096.94 1811.35 169.02 o 10 5 0 98.10 335.90 156.26 o 11 5 0 36.74 179.22 188.95 o 12 5 0 1184.12 938.13 234.85 o -14 6 0 219.51 -94.75 209.51 o -13 6 0 3247.74 2881.22 274.88 o -12 6 0 3783.25 3739.10 274.70 o -11 6 0 215.07 -19.28 165.99 o -10 6 0 1.70 33.05 137.17 o -9 6 0 90.78 158.47 133.86 o -8 6 0 302.08 375.32 130.92 o -7 6 0 6967.26 6166.77 271.21 o -6 6 0 28250.28 25334.01 636.07 o -5 6 0 4493.67 3874.62 208.23 o -4 6 0 7660.71 7251.06 284.61 o -3 6 0 32627.92 33094.27 781.68 o -2 6 0 4999.60 5431.18 257.07 o -1 6 0 27.24 23.96 74.58 o 0 6 0 3119.47 3181.74 187.66 o 1 6 0 655.26 687.80 184.54 o 2 6 0 12817.83 13340.41 327.49 o 3 6 0 23392.08 24518.32 912.33 o 4 6 0 2795.61 2782.87 157.47 o 5 6 0 5081.31 5096.78 202.99 o 6 6 0 10150.76 10193.67 293.40 o 7 6 0 742.18 1153.94 207.40 o 8 6 0 542.76 601.62 138.22 o 9 6 0 390.77 335.07 147.47 o 10 6 0 6.75 1.74 161.08 o 11 6 0 133.26 114.58 232.47 o -14 7 0 65.20 -17.99 215.57 o -13 7 0 2442.12 2047.76 266.99 o -12 7 0 1454.20 1183.81 209.15 o -11 7 0 527.88 391.48 164.71 o -10 7 0 3.74 -15.24 150.75 o -9 7 0 1842.34 1420.32 184.91 o -8 7 0 617.67 659.02 158.47 o -7 7 0 12811.93 12680.04 426.00 o -6 7 0 23769.28 21820.58 598.79 o -5 7 0 1612.12 2005.71 179.95 o -4 7 0 335.33 38.19 134.41 o -3 7 0 8088.68 7276.22 317.48 o -2 7 0 188.16 504.04 142.31 o -1 7 0 1211.57 1159.07 104.38 o 0 7 0 4056.16 4029.18 148.37 o 1 7 0 1215.75 1100.42 121.75 o 2 7 0 8641.85 8140.02 388.91 o 3 7 0 23332.08 21985.73 462.67 o 4 7 0 3287.97 3442.05 185.81 o 5 7 0 2581.20 2286.95 164.89 o 6 7 0 6968.65 7141.79 261.08 o 7 7 0 618.83 643.24 299.67 o 8 7 0 70.06 -0.20 137.71 o 9 7 0 299.54 233.92 159.01 o 10 7 0 163.71 450.32 176.25 o -14 8 0 252.44 -220.35 239.63 o -13 8 0 1353.88 1570.71 233.02 o -12 8 0 562.32 840.44 215.94 o -11 8 0 413.32 498.90 183.44 o -10 8 0 63.21 -73.82 168.57 o -9 8 0 2607.35 2855.88 240.55 o -8 8 0 34.04 107.24 150.02 o -7 8 0 10134.29 9804.88 390.56 o -6 8 0 15270.12 14778.11 491.56 o -5 8 0 2868.22 3136.64 239.63 o -4 8 0 1230.25 1032.69 178.85 o -3 8 0 6898.84 6413.56 319.50 o -2 8 0 32.01 -130.43 94.24 o -1 8 0 365.18 259.61 99.52 o 0 8 0 9508.86 9375.51 237.96 o 1 8 0 1714.07 1890.03 211.53 o 2 8 0 7010.32 6823.88 252.92 o 3 8 0 15259.96 14539.29 379.14 o 4 8 0 1985.14 1965.18 167.79 o 5 8 0 2066.39 1880.34 165.01 o 6 8 0 4919.36 4552.23 247.16 o 7 8 0 59.27 156.99 149.04 o 8 8 0 14.96 -171.73 209.70 o 9 8 0 963.99 735.31 219.80 o 10 8 0 464.97 328.68 238.34 o -14 9 0 272.78 266.99 235.40 o -13 9 0 3.43 54.17 206.02 o -12 9 0 1.98 242.57 188.76 o -11 9 0 236.08 429.31 196.11 o -10 9 0 4431.23 4452.48 293.61 o -9 9 0 8441.29 8798.27 395.52 o -8 9 0 124.84 67.94 164.53 o -7 9 0 12710.82 12487.61 471.73 o -6 9 0 19791.99 19853.62 625.79 o -5 9 0 326.30 116.23 172.79 o -4 9 0 1786.97 1984.22 227.32 o -3 9 0 1070.81 1070.28 130.23 o -2 9 0 794.82 613.21 133.03 o -1 9 0 818.96 630.93 196.29 o 0 9 0 15673.95 15672.91 548.11 o 1 9 0 4495.69 5203.68 309.04 o 2 9 0 2889.65 2873.00 189.01 o 3 9 0 8836.87 9276.89 699.23 o 4 9 0 751.63 799.03 234.76 o 5 9 0 1750.02 1727.53 183.40 o 6 9 0 579.76 353.87 155.03 o 7 9 0 113.82 119.60 174.72 o 8 9 0 185.24 453.83 190.38 o 9 9 0 1626.89 1377.73 218.61 o -13 10 0 3.74 247.71 221.63 o -12 10 0 354.43 -137.17 204.19 o -11 10 0 14.03 -46.64 199.23 o -10 10 0 3667.06 3126.35 284.43 o -9 10 0 10841.06 10355.57 458.87 o -8 10 0 1015.05 1105.04 214.65 o -7 10 0 3711.20 4151.52 309.95 o -6 10 0 3845.25 4480.75 315.83 o -5 10 0 205.89 196.14 134.17 o -4 10 0 1317.02 1250.66 266.90 o -3 10 0 259.69 328.42 119.08 o -2 10 0 273.36 238.53 168.93 o -1 10 0 1079.79 1137.72 221.26 o 0 10 0 12057.10 12346.03 505.88 o 1 10 0 2234.45 2317.50 238.34 o 2 10 0 4609.52 4235.07 296.92 o 3 10 0 9094.31 9305.89 328.29 o 4 10 0 1318.80 1350.57 182.60 o 5 10 0 141.69 197.53 161.91 o 6 10 0 0.73 -233.97 155.98 o 7 10 0 53.59 232.76 178.14 o 8 10 0 255.18 24.57 253.22 o -13 11 0 36.68 -36.28 242.75 o -12 11 0 574.69 860.23 239.54 o -11 11 0 15.40 22.40 237.97 o -10 11 0 2421.42 2457.05 275.07 o -9 11 0 8148.59 7810.19 421.05 o -8 11 0 1273.64 1280.95 244.03 o -7 11 0 3522.87 3373.96 219.25 o -6 11 0 2667.81 2731.90 224.48 o -5 11 0 356.71 459.67 153.52 o -4 11 0 613.77 493.15 138.31 o -3 11 0 1024.01 668.75 199.96 o -2 11 0 268.68 336.21 215.76 o -1 11 0 3045.98 3341.38 288.29 o 0 11 0 9425.93 10161.11 481.27 o 1 11 0 2111.22 2150.03 265.70 o 2 11 0 4230.02 4645.10 338.23 o 3 11 0 4242.32 4790.16 344.29 o 4 11 0 283.38 101.02 167.79 o 5 11 0 2.15 48.32 171.61 o 6 11 0 333.61 585.79 188.15 o 7 11 0 538.74 110.18 204.18 o -12 12 0 1119.24 1027.43 221.41 o -11 12 0 170.57 347.44 189.00 o -10 12 0 2680.55 3055.72 246.75 o -9 12 0 4566.39 4860.26 278.71 o -8 12 0 801.58 655.51 168.71 o -7 12 0 2701.78 2901.35 223.15 o -6 12 0 959.14 727.96 225.03 o -5 12 0 113.19 -183.98 151.73 o -4 12 0 1586.02 1676.11 288.47 o -3 12 0 4487.59 4740.95 363.21 o -2 12 0 2697.43 2816.58 310.14 o -1 12 0 1487.73 1687.31 267.35 o 0 12 0 9611.77 9432.31 479.62 o 1 12 0 804.25 878.27 240.55 o 2 12 0 877.53 592.18 226.41 o 3 12 0 2063.63 1967.88 270.29 o 4 12 0 9.39 218.51 241.46 o 5 12 0 33.82 -47.56 237.97 o 6 12 0 1037.63 856.05 257.99 o -11 13 0 20.70 259.13 288.29 o -10 13 0 2272.75 2723.61 254.84 o -9 13 0 3479.90 3708.13 266.07 o -8 13 0 237.18 -19.69 178.63 o -7 13 0 1207.23 1096.63 199.16 o -6 13 0 167.52 275.98 241.46 o -5 13 0 186.80 476.68 260.93 o -4 13 0 1171.83 887.63 278.19 o -3 13 0 7384.52 7656.32 464.01 o -2 13 0 350.05 415.35 253.22 o -1 13 0 4136.25 4223.13 360.27 o 0 13 0 4617.27 4496.18 366.14 o 1 13 0 746.26 1048.85 255.60 o 2 13 0 1152.65 1180.88 262.03 o 3 13 0 227.99 560.97 250.64 o 4 13 0 26.11 480.36 259.64 o -10 14 0 1372.92 960.76 240.80 o -9 14 0 2289.31 1811.42 258.72 o -8 14 0 53.69 68.07 326.57 o -7 14 0 231.14 211.53 270.66 o -6 14 0 2.21 -384.23 256.15 o -5 14 0 120.23 -22.40 264.23 o -4 14 0 705.31 1134.60 279.84 o -3 14 0 3638.04 4379.03 390.56 o -2 14 0 277.63 91.08 250.09 o -1 14 0 1507.08 1263.69 295.82 o 0 14 0 2927.89 2999.29 351.27 o 1 14 0 183.11 220.35 251.75 o 2 14 0 115.26 -129.45 248.81 o -8 15 0 61.12 -25.34 299.67 o -7 15 0 31.53 -265.89 301.69 o -6 15 0 277.59 690.97 311.24 o -5 15 0 140.91 280.02 284.98 o -4 15 0 451.14 370.73 296.73 o -3 15 0 3257.23 3820.81 394.97 o -2 15 0 597.06 836.95 287.37 o -1 15 0 1317.37 1355.50 319.87 o 0 15 0 1175.70 1151.31 296.18 o 0 -15 1 48.28 320.42 298.20 o 1 -15 1 103.78 148.92 244.59 o 2 -15 1 19.23 306.10 290.12 o 3 -15 1 595.44 1015.62 305.73 o 4 -15 1 274.38 415.54 288.84 o 5 -15 1 3144.15 3875.17 408.93 o 6 -15 1 586.87 249.18 298.75 o 7 -15 1 762.84 751.02 306.28 o 8 -15 1 2430.13 3088.71 392.58 o -3 -14 1 29.80 -44.80 261.66 o -2 -14 1 889.59 1226.96 287.74 o -1 -14 1 1535.95 1636.44 295.82 o 0 -14 1 38.29 292.51 256.34 o 1 -14 1 357.06 116.42 255.24 o 2 -14 1 1079.56 1361.01 304.81 o 3 -14 1 410.44 698.13 273.05 o 4 -14 1 2902.78 3143.43 359.17 o 5 -14 1 5149.29 5857.00 445.10 o 6 -14 1 888.89 822.81 291.04 o 7 -14 1 1114.30 926.56 299.49 o 8 -14 1 2434.29 1787.71 228.90 o 9 -14 1 469.80 1433.10 551.42 o 10 -14 1 30.35 -105.88 203.95 o -4 -13 1 1078.25 1277.83 282.96 o -3 -13 1 20.19 185.27 212.45 o -2 -13 1 588.55 1265.16 269.56 o -1 -13 1 280.93 318.03 208.78 o 0 -13 1 61.44 128.17 238.89 o 1 -13 1 73.21 287.74 232.83 o 2 -13 1 1878.43 1574.56 286.27 o 3 -13 1 684.67 344.29 245.32 o 4 -13 1 2977.65 3401.42 351.64 o 5 -13 1 6729.60 6788.70 449.32 o 6 -13 1 619.98 754.69 265.33 o 7 -13 1 1388.60 1388.22 198.16 o 8 -13 1 1288.78 1272.69 196.68 o 9 -13 1 107.02 45.08 182.72 o 10 -13 1 158.27 162.41 188.39 o 11 -13 1 540.59 814.33 233.48 o -6 -12 1 177.89 146.02 203.31 o -5 -12 1 2708.01 2642.55 349.71 o -4 -12 1 2139.86 2354.22 290.31 o -3 -12 1 60.44 -50.86 209.33 o -2 -12 1 572.17 678.67 236.14 o -1 -12 1 487.39 132.58 220.16 o 0 -12 1 30.63 444.55 227.32 o 1 -12 1 406.11 509.00 229.34 o 2 -12 1 1880.65 2072.18 284.43 o 3 -12 1 877.06 922.70 263.31 o 4 -12 1 3110.21 3159.22 312.16 o 5 -12 1 9173.71 9611.54 344.36 o 6 -12 1 22.96 -194.03 413.24 o 7 -12 1 2391.54 1957.05 279.11 o 8 -12 1 1085.81 908.75 253.03 o 9 -12 1 4.26 216.31 230.45 o 10 -12 1 331.86 286.27 231.36 o 11 -12 1 1037.55 1037.10 261.29 o 12 -12 1 747.44 869.08 264.78 o -7 -11 1 2962.94 3235.89 258.38 o -6 -11 1 92.17 189.26 493.76 o -5 -11 1 4304.81 3939.84 249.43 o -4 -11 1 2771.70 2902.09 239.99 o -3 -11 1 1.18 2.92 229.99 o -2 -11 1 216.03 280.21 212.08 o -1 -11 1 57.01 -0.18 194.46 o 0 -11 1 171.09 445.47 212.45 o 1 -11 1 2902.86 3200.72 305.36 o 2 -11 1 7793.72 7508.87 421.60 o 3 -11 1 389.33 429.31 230.45 o 4 -11 1 4425.73 4560.23 231.16 o 5 -11 1 11649.03 11775.89 519.65 o 6 -11 1 226.67 -304.63 203.09 o 7 -11 1 3339.84 3432.45 290.31 o 8 -11 1 7.20 -247.52 197.39 o 9 -11 1 224.36 58.76 206.58 o 10 -11 1 300.76 240.91 211.17 o 11 -11 1 3343.52 3969.36 336.40 o 12 -11 1 1477.77 1109.08 260.74 o 13 -11 1 580.44 -52.33 238.89 o -8 -10 1 1926.21 1961.59 231.02 o -7 -10 1 3388.52 3484.76 248.57 o -6 -10 1 32.00 -0.49 164.58 o -5 -10 1 4353.91 4320.63 250.59 o -4 -10 1 1967.42 1640.90 188.70 o -3 -10 1 107.46 238.96 147.34 o -2 -10 1 38.93 -210.98 140.65 o -1 -10 1 1119.60 976.69 215.76 o 0 -10 1 6.90 -110.72 155.16 o 1 -10 1 9452.39 9349.87 447.67 o 2 -10 1 15178.54 15026.92 565.37 o 3 -10 1 2361.70 2412.22 169.51 o 4 -10 1 11110.30 10949.22 465.85 o 5 -10 1 13199.63 13572.45 533.06 o 6 -10 1 3384.75 3436.86 292.33 o 7 -10 1 444.27 406.36 202.17 o 8 -10 1 81.69 329.60 189.87 o 9 -10 1 264.19 73.63 191.89 o 10 -10 1 2398.99 2247.72 255.60 o 11 -10 1 4221.93 4018.03 311.61 o 12 -10 1 327.32 270.11 206.21 o 13 -10 1 798.39 825.02 251.93 o -9 -9 1 35.49 81.57 289.30 o -8 -9 1 3537.16 3197.74 232.56 o -7 -9 1 4267.37 4441.06 492.48 o -6 -9 1 68.60 -126.47 157.36 o -5 -9 1 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