Acta Crystallographica Section C

Crystal Structure Communications

Volume 61, Part 2 (February 2005)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The molecular structure of the cation in [mu]-acetato-acetonitriletris([mu]-N,N'-diphenylformamidinato)diruthenium tetrafluoroborate dichloromethane hemisolvate, with displacement ellipsoids shown at the 35% probability level. Only one orientation for the disordered phenyl group and the axially coordinated acetonitrile molecule is shown. H atoms have been omitted for clarity. See Angaridis, Cotton, Murillo & Wang [Acta Cryst. (2005), C61, m71-m73].

inorganic compounds


 

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Acta Cryst. (2005). C61, i9-i13  [ doi:10.1107/S0108270104030525 ]

Two new phosphate langbeinites, Rb2YbTi(PO4)3 and Rb2Yb0.32Ti1.68(PO4)3, investigated at 293 and 150 K

J. C. M. Gustafsson, S. T. Norberg, G. Svensson and J. Albertsson

Synopsis: The structures of Rb2YbTi(PO4)3 and Rb2Yb0.32Ti1.68(PO4)3 have been determined at both 293 and 150 K. Both compounds belong to the langbeinite structure type, with mixed Yb/Ti populations in the two crystallographically independent octahedral sites (of symmetry 3). Ytterbium favours one of these sites, where about two-thirds of the Yb atoms are found. The O-atom displacement parameters are large in both compounds at both temperatures.

Formula: Rb2YbTi(PO4)3 and Rb2Yb0.32Ti1.68(PO4)3

Online 15 January 2005


 

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Acta Cryst. (2005). C61, i14-i16  [ doi:10.1107/S010827010403166X ]

The bivalent metal hypophosphites Sr(H2PO2)2, Pb(H2PO2)2 and Ba(H2PO2)2

N. V. Kuratieva, M. I. Naumova, N. V. Podberezskaya and D. Yu. Naumov

Synopsis: The Sr(H2PO2)2, Pb(H2PO2)2 and Ba(H2PO2)2 structures consist of layers of cations bridged by hypophosphite anions. The cations exhibit square antiprismatic coordination by O atoms.

Formula: Sr(H2PO2)2, Pb(H2PO2)2 and Ba(H2PO2)2

Online 15 January 2005


 

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Acta Cryst. (2005). C61, i17-i19  [ doi:10.1107/S0108270104032482 ]

Two alkali metal chlorites, LiClO2 and KClO2

A. I. Smolentsev and D. Yu. Naumov

Synopsis: The lithium chlorite, LiClO2, and potassium chlorite, KClO2, structures consist of layers of alkali cations bridged by chlorite anions. The Li+ cations are tetrahedrally coordinated by oxygen. The coordination environment of the K+ cations involve eight O atoms, which form a distorted cube.

Formula: LiClO2 and KClO2

Online 15 January 2005


 

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Acta Cryst. (2005). C61, i20-i22  [ doi:10.1107/S0108270104033153 ]

A comparison of the clinopyroxene compounds CaZnSi2O6 and CaZnGe2O6

G. J. Redhammer and G. Roth

Synopsis: The synthetic compounds CaZnSi2O6 and CaZnGe2O6 belong to the clinopyroxene structure type. A detailed comparison is made between analogous silicate and germanate calcium pyroxenes.

Formula: CaZnSi2O6 and CaZnGe2O6

Online 15 January 2005


 

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Acta Cryst. (2005). C61, i23-i24  [ doi:10.1107/S0108270104033396 ]

High-pressure synthesis of the new rare-earth oxoborate [beta]-Gd2B4O9

H. Emme and H. Huppertz

Synopsis: The title compound was obtained by the reaction of Gd2O3 and B2O3 under high-pressure/high-temperature conditions of 3 GPa and 1223 K using a Walker-type multi-anvil assembly. The crystal structure has been determined by single-crystal X-ray diffraction.

Formula: Gd2B4O9

Online 22 January 2005


metal-organic compounds


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Acta Cryst. (2005). C61, m61-m63  [ doi:10.1107/S0108270104031397 ]

Poly[[diaquacobalt(II)]-[mu]-4,4'-bipyridine-[kappa]2N:N'-[mu]-p-phenylenebis(oxyacetato)-[kappa]2O:O']

Y.-M. Dai, E. Tang, Z.-J. Li and Y.-G. Yao

Formula: [Co(C10H8O6)(C10H8N2)(H2O)2]

Online 15 January 2005


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Acta Cryst. (2005). C61, m64-m66  [ doi:10.1107/S0108270104032986 ]

Tri-[mu]2-chloro-tetrachloro-[mu]3-oxo-hexakis(tetrahydrofuran-[kappa]O)dititanium(III)samarium(III): a novel trinuclear Sm-Ti mixed species

C. Villiers, P. Thuéry and M. Ephritikhine

Formula: [SmTi2Cl7O(C4H8O)6]

Online 15 January 2005


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Acta Cryst. (2005). C61, m67-m70  [ doi:10.1107/S010827010403197X ]

(Di-2-pyridylamine-[kappa]2N,N')(naphthalene-2,3-diolato-[kappa]2O,O')palladium(II) monohydrate and (di-2-pyridylamine-[kappa]2N,N')(3-oxidonaphthalene-2-carboxylato-[kappa]2O,O')palladium(II)

Y. Wang, Y. Mizubayashi, M. Odoko and N. Okabe

Formula: [Pd(C10H6O2)(C10H9N3)]·H2O and [Pd(C11H6O3)(C10H9N3)]

Online 15 January 2005


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Acta Cryst. (2005). C61, m71-m73  [ doi:10.1107/S0108270104032408 ]

A paramagnetic precursor for polymeric supramolecular assemblies based on multiply bonded dimetal units: [mu]-acetato-acetonitriletris([mu]-N,N'-diphenylformamidinato)diruthenium tetrafluoroborate dichloromethane hemisolvate

P. Angaridis, F. A. Cotton, C. A. Murillo and X.-P. Wang

Formula: [Ru2(C13H11N2)3(C2H3O2)(C2H3N)]BF4·0.5CH2Cl2

Online 15 January 2005


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Acta Cryst. (2005). C61, m74-m75  [ doi:10.1107/S0108270104032731 ]

trans-Di-[mu]-bromo-bis[bromo(triethylphosphine-[kappa]P)platinum(II)]

S. M. M. Cornet, K. B. Dillon, A. E. Goeta and A. L. Thompson

Formula: [Pt2Br4(C6H15P)2]

Online 15 January 2005


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Acta Cryst. (2005). C61, m76-m77  [ doi:10.1107/S0108270104032512 ]

Tris[(R)-lactamide-[kappa]2O,O']zinc(II) tetrabromozincate

A. Bekaert, P. Lemoine, J. D. Brion and B. Viossat

Formula: [Zn(C3H7NO2)3][ZnBr4]

Online 15 January 2005


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Acta Cryst. (2005). C61, m78-m80  [ doi:10.1107/S0108270104032615 ]

Di-[mu]-acetato-bis[bis(4-aminobenzoato)(2,2'-bipyridyl)manganese(II)]

Q.-Z. Zhang and C.-Z. Lu

Formula: [Mn2(C7H6NO2)2(C2H3O2)2(C10H8N2)2]

Online 15 January 2005


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Acta Cryst. (2005). C61, m81-m83  [ doi:10.1107/S0108270104032585 ]

Dimeric hexakis(4-methylbenzoato)bis(1,10-phenanthroline)didysprosium(III)

X. Li, Z.-Y. Zhang, D.-Y. Wang, H.-B. Song and Y.-Q. Zou

Formula: [Dy2(C8H7O2)6(C12H8N2)2]

Online 15 January 2005


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Acta Cryst. (2005). C61, m84-m86  [ doi:10.1107/S0108270104033256 ]

Bis[2,2'-(phenylphosphinediyl)dibenzenethiolato-[kappa]3S,P,S']germanium(IV)

M. Y. Chiang, J.-W. Lin and W.-F. Zeng

Formula: [Ge(C18H13PS2)2]

Online 15 January 2005


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Acta Cryst. (2005). C61, m87-m89  [ doi:10.1107/S0108270104031671 ]

A new layered zinc phosphate templated by protonated isonicotinate, [Zn2(C6H5NO2)2(HPO4)2]

G.-S. Guo, Y.-G. Wei, J. Li, Y. Wang and H.-Y. Guo

Formula: [Zn2(C6H5NO2)2(HPO4)2]

Online 15 January 2005


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Acta Cryst. (2005). C61, m90-m92  [ doi:10.1107/S0108270104033402 ]

Aurophilic interactions in [mu]-p-phenylenediethynyl-bis[(trimethyl phosphite)gold(I)] dichloromethane hemisolvate

D. Millar, L. N. Zakharov, A. L. Rheingold and L. H. Doerrer

Formula: [Au2(C10H4)(C3H9O3P)2]·0.5CH2Cl2

Online 15 January 2005


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Acta Cryst. (2005). C61, m93-m94  [ doi:10.1107/S0108270104033803 ]

[N-(2-Hydroxyethyl)ethylenediamine-[kappa]3N,N',O]-cis-bis(isothiocyanato-[kappa]N)copper(II)

H. Pasaoglu, A. Karadag, F. Tezcan and O. Büyükgüngör

Formula: [Cu(NCS)2(C4H12N2O)]

Online 22 January 2005


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Acta Cryst. (2005). C61, m95-m97  [ doi:10.1107/S0108270104029592 ]

fac-Bromotricarbonyl[2-(2-pyridylmethyl)-2,3-dihydro-1H-isoindol-1-one]rhenium(I) methanol solvate

L. Wei and J. Zubieta

Formula: [ReBr(C14H12N2O)(CO)3]·CH4O

Online 22 January 2005


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Acta Cryst. (2005). C61, m98-m100  [ doi:10.1107/S0108270104034158 ]

A three-dimensional supramolecular network built with the zigzag chain complex bis(5-carboxy-1H-imidazole-4-carboxylato)copper(II)

Y.-L. Bai, J. Tao, R.-B. Huang and L.-S. Zheng

Formula: [Cu(C5H3N2O4)2]

Online 22 January 2005


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Acta Cryst. (2005). C61, m101-m103  [ doi:10.1107/S0108270105000478 ]

A dinuclear complex of cobalt(II) with 2,2'-(1,4-butanediyl)dibenzimidazole

J. Yang, J.-F. Ma and Y.-Y. Liu

Formula: [Co2(NO3)2(C18H18N4)3](NO3)2·2C2H6O

Online 22 January 2005


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Acta Cryst. (2005). C61, m104-m106  [ doi:10.1107/S0108270104031695 ]

Chlorobis(dimethylamido)([eta]5-2,5-dimethylpyrrolyl)titanium(IV), [Ti(NMe2)2(DMP)Cl]

M. T. Duarte, A. Ferreira, A. R. Dias, M. M. Salema and J. F. Ferreira da Silva

Formula: [Ti(C2H6N)2(C6H8N)Cl]

Online 31 January 2005


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Acta Cryst. (2005). C61, m107-m108  [ doi:10.1107/S0108270104034134 ]

Diphenylmercury, redetermined at 120 K: sheets built from a single C-H...[pi](arene) hydrogen bond

C. Glidewell, J. N. Low and J. L. Wardell

Formula: [Hg(C6H5)2]

Online 31 January 2005


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Acta Cryst. (2005). C61, m109-m111  [ doi:10.1107/S0108270104032494 ]

Tetra-[mu]-acetato-[kappa]8O:O'-bis[(N1,N2-di-p-anisylformamidine-[kappa]N2)ruthenium(II)](Ru-Ru): an example of an axial bis-adduct of {Ru2}4+ tetracarboxylate with N-donor ligands

P. Angaridis, F. A. Cotton, C. A. Murillo and X.-P. Wang

Formula: [Ru2(C2H3O2)4(C15H16N2O2)2]

Online 31 January 2005


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Acta Cryst. (2005). C61, m112-m114  [ doi:10.1107/S0108270104030434 ]

[mu]-1,2-Bis(4-pyridyl)ethene-[kappa]2N:N'-bis(tetraaqua{4-[2-(4-pyridinio)ethenyl]pyridine-[kappa]N}cobalt(II)) hexaaquacobalt(II) tetrakis(sulfate) octahydrate

X.-H. Li, H.-P. Xiao and S.-Z. Yang

Formula: [Co2(C12H11N2)2(C12H10N2)(H2O)8][Co(H2O)6](SO4)4·8H2O

Online 31 January 2005


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Acta Cryst. (2005). C61, m115-m116  [ doi:10.1107/S010827010500034X ]

Di-[mu]-hydroxo-bis{(acetonitrile)dibenzyl(6-methyl-2-pyridylmethyl)amine-[kappa]2N,N]copper(II)} bis(perchlorate)

D. Rojas, A. M. García, J. Manzur and A. Vega

Formula: [Cu2(OH)2(C2H3N)2(C21H22N2)2](ClO4)2

Online 31 January 2005


organic compounds


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Acta Cryst. (2005). C61, o65-o66  [ doi:10.1107/S0108270104032743 ]

Tetra-n-butylammonium bromide-water (1/38)

W. Shimada, M. Shiro, H. Kondo, S. Takeya, H. Oyama, T. Ebinuma and H. Narita

Formula: C16H36N+·Br-·38H2O

Online 15 January 2005


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Acta Cryst. (2005). C61, o67-o69  [ doi:10.1107/S0108270104032123 ]

3-Bromo-1-(2-deoxy-[beta]-D-erythro-pentofuranosyl)-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine: a nucleoside which strongly enhances DNA duplex stability

F. Seela, V. R. Sirivolu, J. He and H. Eickmeier

Formula: C10H13BrN6O3

Online 15 January 2005


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Acta Cryst. (2005). C61, o70-o72  [ doi:10.1107/S0108270104031385 ]

The isomeric compounds nimbolide and isonimbolide

K. Anand Solomon, R. Malathi, S. S. Rajan, G. Anitha, J. Josepha Lourdu Raj, S. Narasimhan, G. Suresh and Geetha Gopalakrishnan

Formula: Two isomers of C27H30O7

Online 15 January 2005


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Acta Cryst. (2005). C61, o73-o74  [ doi:10.1107/S010827010403272X ]

Bis[4-(3-pyridylmethyleneamino)phenyl]methane

Q. Wang, X.-D. Pi and C.-Y. Su

Formula: C25H20N4

Online 15 January 2005


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Acta Cryst. (2005). C61, o75-o77  [ doi:10.1107/S0108270104033141 ]

Tris[4-(4-nitrophenyl)-3-aza-3-butenyl]amine: [pi]-stacked chains of hydrogen-bonded R_{\bf 2}^{\bf 2}(26) dimers

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

Formula: C27H27N7O6

Online 15 January 2005


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Acta Cryst. (2005). C61, o78-o80  [ doi:10.1107/S0108270104032925 ]

(Z)-3-(1H-Indol-3-yl)-2-(3-thienyl)acrylonitrile and (Z)-3-[1-(4-tert-butylbenzyl)-1H-indol-3-yl]-2-(3-thienyl)acrylonitrile

V. N. Sonar, S. Parkin and P. A. Crooks

Formula: C15H10N2S and C26H24N2S

Online 15 January 2005


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Acta Cryst. (2005). C61, o81-o84  [ doi:10.1107/S0108270104032573 ]

Fenofibric acid

N. P. Rath, W. Haq and G. K. Balendiran

Formula: C17H15ClO4

Online 15 January 2005


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Acta Cryst. (2005). C61, o85-o87  [ doi:10.1107/S0108270104025156 ]

9-(2-Chloroethylamino)acridine monohydrate and its precursor 9-phenoxyacridine

Y. Ebead, A. Sikorski, K. Krzyminski, T. Lis and J. Blazejowski

Formula: C15H13ClN2·H2O and C19H13NO

Online 15 January 2005


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Acta Cryst. (2005). C61, o88-o91  [ doi:10.1107/S0108270104031853 ]

Cyclic water pentamers in triclinic crystals of brucinium L-glycerate

A. Bialonska, Z. Ciunik, T. Popek and T. Lis

Formula: C23H27N2O4+·C3H5O4-·4.75H2O

Online 22 January 2005


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Acta Cryst. (2005). C61, o92-o94  [ doi:10.1107/S0108270104033657 ]

A Schiff base lateral macrobicycle derived from 4,13-diaza-18-crown-6 in its protonated form

F. Avecilla, D. Esteban, C. Platas-Iglesias, S. Fernández-Martínez, A. De Blas and T. Rodríguez-Blas

Formula: C33H43N5O42+·2ClO4-

Online 22 January 2005


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Acta Cryst. (2005). C61, o95-o97  [ doi:10.1107/S0108270104030975 ]

Hydrogen-bonding patterns in 2-amino-4,6-dimethylpyrimidinium hydrogen sulfate

M. Hemamalini, P. T. Muthiah, U. Rychlewska and A. Plutecka

Formula: C6H10N3+·HSO4-

Online 22 January 2005


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Acta Cryst. (2005). C61, o98-o100  [ doi:10.1107/S0108270104033281 ]

4-Amino-N-isopropylbenzamidinium chloride ethanol solvate

I. Jarak, G. Karminski-Zamola, G. Pavlovic and Z. Popovic

Formula: C10H16N{}_{3}^{\,+}·Cl-·C2H6O

Online 22 January 2005


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Acta Cryst. (2005). C61, o101-o104  [ doi:10.1107/S0108270104033931 ]

Three 1,2,4-triazole derivatives containing subtituted benzyl and benzylamino groups

V. T. Yilmaz, C. Kazak, E. Agar, B. Kahveci and K. Guven

Formula: C17H18N4O, C18H20N4O and C17H17ClN4O

Online 22 January 2005


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Acta Cryst. (2005). C61, o105-o109  [ doi:10.1107/S0108270104033451 ]

Hydrogen bonding in 1:1 proton-transfer compounds of 5-sulfosalicylic acid with 4-X-substituted anilines (X = F, Cl or Br)

G. Smith, U. D. Wermuth and J. M. White

Formula: C6H7FN+/C6H7ClN+/C6H7BrN+·C7H5O6S-·xH2O

Online 22 January 2005


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Acta Cryst. (2005). C61, o110-o111  [ doi:10.1107/S0108270104034079 ]

1,4-Diphenyl-1,4-di-4-pyridyl-2,3-diaza-1,3-butadiene: weak C-H...N and C-H...[pi] hydrogen bonds

E.-Q. Gao

Formula: C24H18N4

Online 22 January 2005


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Acta Cryst. (2005). C61, o112-o113  [ doi:10.1107/S0108270104033505 ]

N-(Diphenylselenio)diphenylsulfimidium tetraphenylborate

S. M. Aucott, S. H. Dale, M. R. J. Elsegood, L. M. Gilby, K. E. Holmes and P. F. Kelly

Formula: C24H20NSSe+·C24H20B-

Online 22 January 2005


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Acta Cryst. (2005). C61, o114-o117  [ doi:10.1107/S0108270104034146 ]

Two isomeric 2-[4-chloro-2-fluoro-5-(prop-2-ynyloxy)phenyl]hexahydroisoindole-1,3-dione compounds

B. Li, H.-B. Song, C.-T. Hsu, K.-L. Zhang, C. Wu and H.-Z. Yang

Formula: Two isomers of C17H13ClFNO3

Online 31 January 2005


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Acta Cryst. (2005). C61, o118-o121  [ doi:10.1107/S0108270104034055 ]

Piperazine-2,5-dione-oxalic acid-water (1/1/2) and a redetermination of piperazine-2,5-dione, both at 120 K: hydrogen-bonded sheets containing multiple ring types

T. R. Sarangarajan, K. Panchanatheswaran, J. N. Low and C. Glidewell

Formula: C4H6N2O2·C2H2O4·2H2O and C4H6N2O2

Online 31 January 2005


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Acta Cryst. (2005). C61, o122-o126  [ doi:10.1107/S0108270105000545 ]

Three trifluoromethyl-substituted protoporphyrinogen IX oxidase inhibitors

B. Li, Y.-M. Lan, C.-T. Hsu, Z.-L. Liu, H.-B. Song, C. Wu and H.-Z. Yang

Formula: C15H9ClF3NO5, C14H10ClF3N2O4 and C15H10ClF4NO3

Online 31 January 2005


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